DE112014005230B4 - Verfahren zur Auswertung der Konzentration eines Defekts in einem Silizium-Einkristall-Substrat - Google Patents

Verfahren zur Auswertung der Konzentration eines Defekts in einem Silizium-Einkristall-Substrat Download PDF

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Publication number
DE112014005230B4
DE112014005230B4 DE112014005230.2T DE112014005230T DE112014005230B4 DE 112014005230 B4 DE112014005230 B4 DE 112014005230B4 DE 112014005230 T DE112014005230 T DE 112014005230T DE 112014005230 B4 DE112014005230 B4 DE 112014005230B4
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concentration
crystal substrate
silicon single
defect
irradiation
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DE112014005230T5 (de
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Hiroyuki Kamada
Ryoji Hoshi
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Shin Etsu Handotai Co Ltd
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Shin Etsu Handotai Co Ltd
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    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L22/00—Testing or measuring during manufacture or treatment; Reliability measurements, i.e. testing of parts without further processing to modify the parts as such; Structural arrangements therefor
    • H01L22/10—Measuring as part of the manufacturing process
    • H01L22/12—Measuring as part of the manufacturing process for structural parameters, e.g. thickness, line width, refractive index, temperature, warp, bond strength, defects, optical inspection, electrical measurement of structural dimensions, metallurgic measurement of diffusions
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/06—Investigating concentration of particle suspensions
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/02—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance
    • G01N27/04—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating resistance
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/02—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance
    • G01N27/04—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating resistance
    • G01N27/041—Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating impedance by investigating resistance of a solid body
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/02104—Forming layers
    • H01L21/02365—Forming inorganic semiconducting materials on a substrate
    • H01L21/02367—Substrates
    • H01L21/0237—Materials
    • H01L21/02373—Group 14 semiconducting materials
    • H01L21/02381—Silicon, silicon germanium, germanium
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/02104—Forming layers
    • H01L21/02365—Forming inorganic semiconducting materials on a substrate
    • H01L21/02518—Deposited layers
    • H01L21/02587—Structure
    • H01L21/0259—Microstructure
    • H01L21/02598—Microstructure monocrystalline
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/04—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
    • H01L21/18—Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic Table or AIIIBV compounds with or without impurities, e.g. doping materials
    • H01L21/28—Manufacture of electrodes on semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/268
    • H01L21/28008—Making conductor-insulator-semiconductor electrodes
    • H01L21/28017—Making conductor-insulator-semiconductor electrodes the insulator being formed after the semiconductor body, the semiconductor being silicon
    • H01L21/28158—Making the insulator
    • H01L21/28167—Making the insulator on single crystalline silicon, e.g. using a liquid, i.e. chemical oxidation
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L22/00—Testing or measuring during manufacture or treatment; Reliability measurements, i.e. testing of parts without further processing to modify the parts as such; Structural arrangements therefor
    • H01L22/10—Measuring as part of the manufacturing process
    • H01L22/14—Measuring as part of the manufacturing process for electrical parameters, e.g. resistance, deep-levels, CV, diffusions by electrical means
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L22/00—Testing or measuring during manufacture or treatment; Reliability measurements, i.e. testing of parts without further processing to modify the parts as such; Structural arrangements therefor
    • H01L22/20—Sequence of activities consisting of a plurality of measurements, corrections, marking or sorting steps
    • H01L22/24—Optical enhancement of defects or not directly visible states, e.g. selective electrolytic deposition, bubbles in liquids, light emission, colour change
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10H—INORGANIC LIGHT-EMITTING SEMICONDUCTOR DEVICES HAVING POTENTIAL BARRIERS
    • H10H20/00—Individual inorganic light-emitting semiconductor devices having potential barriers, e.g. light-emitting diodes [LED]
    • H10H20/80—Constructional details
    • H10H20/81—Bodies
    • H10H20/8215—Bodies characterised by crystalline imperfections, e.g. dislocations; characterised by the distribution of dopants, e.g. delta-doping

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical & Material Sciences (AREA)
  • Power Engineering (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Computer Hardware Design (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Pathology (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Electrochemistry (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Testing Or Measuring Of Semiconductors Or The Like (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Investigating Or Analyzing Materials By The Use Of Electric Means (AREA)
DE112014005230.2T 2013-12-10 2014-11-12 Verfahren zur Auswertung der Konzentration eines Defekts in einem Silizium-Einkristall-Substrat Active DE112014005230B4 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2013255250A JP6036670B2 (ja) 2013-12-10 2013-12-10 シリコン単結晶基板の欠陥濃度評価方法
JP2013/255250 2013-12-10
PCT/JP2014/005680 WO2015087485A1 (ja) 2013-12-10 2014-11-12 シリコン単結晶基板の欠陥濃度評価方法

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DE112014005230T5 DE112014005230T5 (de) 2016-08-18
DE112014005230B4 true DE112014005230B4 (de) 2025-04-30

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Country Status (6)

Country Link
US (1) US9773710B2 (enExample)
JP (1) JP6036670B2 (enExample)
KR (1) KR102029647B1 (enExample)
CN (1) CN105814676B (enExample)
DE (1) DE112014005230B4 (enExample)
WO (1) WO2015087485A1 (enExample)

Families Citing this family (11)

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Publication number Priority date Publication date Assignee Title
JP6036670B2 (ja) * 2013-12-10 2016-11-30 信越半導体株式会社 シリコン単結晶基板の欠陥濃度評価方法
JP6406452B2 (ja) * 2015-06-30 2018-10-17 富士電機株式会社 半導体装置及びその製造方法
JP6531729B2 (ja) * 2016-07-19 2019-06-19 株式会社Sumco シリコン試料の炭素濃度評価方法、シリコンウェーハ製造工程の評価方法、シリコンウェーハの製造方法およびシリコン単結晶インゴットの製造方法
JP6805015B2 (ja) * 2017-02-10 2020-12-23 グローバルウェーハズ・ジャパン株式会社 検量線の作成方法、炭素濃度測定方法及びシリコンウェハの製造方法
JP6844561B2 (ja) * 2018-03-09 2021-03-17 信越半導体株式会社 酸素濃度評価方法
JP6852703B2 (ja) * 2018-03-16 2021-03-31 信越半導体株式会社 炭素濃度評価方法
JP7006517B2 (ja) * 2018-06-12 2022-01-24 信越半導体株式会社 シリコン単結晶基板中の欠陥密度の制御方法
JP7351266B2 (ja) * 2020-07-07 2023-09-27 信越半導体株式会社 半導体装置の製造方法
JP7322832B2 (ja) 2020-07-29 2023-08-08 信越半導体株式会社 量子コンピュータ用半導体装置の製造方法
CN112034008A (zh) * 2020-09-11 2020-12-04 电子科技大学 一种石墨烯晶体结构质量评价方法
CN119290973B (zh) * 2024-12-10 2025-05-30 江西联创光电超导应用有限公司 一种晶体缺陷检测分析方法及系统

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012199299A (ja) 2011-03-18 2012-10-18 Shin Etsu Handotai Co Ltd ライフタイム値の測定方法及びこれを用いたウエーハの選別方法

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JPH08102545A (ja) 1994-09-30 1996-04-16 Meidensha Corp 半導体素子のライフタイム制御方法
JPH0955415A (ja) * 1995-08-16 1997-02-25 Nippon Telegr & Teleph Corp <Ntt> 半導体中に発生した欠陥の評価方法
JP3984521B2 (ja) * 2002-09-20 2007-10-03 松下電器産業株式会社 透過型電子顕微鏡による観察方法
DE03756681T1 (de) * 2002-10-18 2005-12-29 Sumitomo Mitsubishi Silicon Corp. Verfahren zur bestimmung der punktdefektverteilung eines silicium-einkristallstabs
WO2006134662A1 (ja) * 2005-06-17 2006-12-21 Topcon Corporation 薄膜測定装置、薄膜測定方法および薄膜製造方法
US8037761B2 (en) * 2006-03-03 2011-10-18 Niigata University Quantitative evaluation device and method of atomic vacancy existing in silicon wafer
JP2008177296A (ja) * 2007-01-17 2008-07-31 Toyota Central R&D Labs Inc 半導体装置、ｐｎダイオード、ｉｇｂｔ、及びそれらの製造方法
JP4358889B1 (ja) * 2008-06-27 2009-11-04 日本エレクトロセンサリデバイス株式会社 ウエーハ欠陥検査装置
US8771415B2 (en) * 2008-10-27 2014-07-08 Sumco Corporation Method of manufacturing silicon single crystal, silicon single crystal ingot, and silicon wafer
JP5515406B2 (ja) * 2009-05-15 2014-06-11 株式会社Ｓｕｍｃｏ シリコンウェーハおよびその製造方法
US9187843B2 (en) * 2009-07-23 2015-11-17 Sumitomo Electric Industries, Ltd. Method and apparatus for producing semiconductor crystal, and semiconductor crystal
JP5519305B2 (ja) 2010-01-25 2014-06-11 トヨタ自動車株式会社 炭化珪素単結晶の欠陥検出方法
JP5678846B2 (ja) * 2011-09-08 2015-03-04 信越半導体株式会社 シリコン単結晶中窒素濃度算出方法および抵抗シフト量算出方法
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JP6036670B2 (ja) 2013-12-10 2016-11-30 信越半導体株式会社 シリコン単結晶基板の欠陥濃度評価方法
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Patent Citations (1)

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Publication number Priority date Publication date Assignee Title
JP2012199299A (ja) 2011-03-18 2012-10-18 Shin Etsu Handotai Co Ltd ライフタイム値の測定方法及びこれを用いたウエーハの選別方法

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SIEMIENIEC, R: Irradiation-Induced Deep Levels in Silicon for Power Device Tailoring. In: Journal of The Electrochemical Society, Vol. 153, 2006, No. 2, S. G108-G118 - DOI: 10.1149/1.2137649

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Publication number Publication date
KR102029647B1 (ko) 2019-10-08
JP6036670B2 (ja) 2016-11-30
JP2015115404A (ja) 2015-06-22
CN105814676B (zh) 2018-08-28
DE112014005230T5 (de) 2016-08-18
US9773710B2 (en) 2017-09-26
US20160300768A1 (en) 2016-10-13
CN105814676A (zh) 2016-07-27
KR20160097200A (ko) 2016-08-17
WO2015087485A1 (ja) 2015-06-18

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