DE112004000141B4 - Verfahren zur Bestimmung einer Qualität eines Gasdiffusionsmediums - Google Patents
Verfahren zur Bestimmung einer Qualität eines Gasdiffusionsmediums Download PDFInfo
- Publication number
- DE112004000141B4 DE112004000141B4 DE112004000141.2T DE112004000141T DE112004000141B4 DE 112004000141 B4 DE112004000141 B4 DE 112004000141B4 DE 112004000141 T DE112004000141 T DE 112004000141T DE 112004000141 B4 DE112004000141 B4 DE 112004000141B4
- Authority
- DE
- Germany
- Prior art keywords
- contact angle
- sample
- liquid
- diffusion
- pores
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000009792 diffusion process Methods 0.000 title claims abstract description 154
- 238000000034 method Methods 0.000 title claims abstract description 48
- 239000007788 liquid Substances 0.000 claims abstract description 129
- 238000009736 wetting Methods 0.000 claims abstract description 77
- 239000000446 fuel Substances 0.000 claims abstract description 40
- 230000008859 change Effects 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 239000011148 porous material Substances 0.000 description 137
- 239000000463 material Substances 0.000 description 65
- 238000012360 testing method Methods 0.000 description 64
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 42
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 34
- 239000004810 polytetrafluoroethylene Substances 0.000 description 34
- 238000001179 sorption measurement Methods 0.000 description 32
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 28
- 230000004584 weight gain Effects 0.000 description 28
- 235000019786 weight gain Nutrition 0.000 description 28
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 21
- 238000000576 coating method Methods 0.000 description 20
- 239000012528 membrane Substances 0.000 description 15
- 239000007787 solid Substances 0.000 description 15
- 239000011248 coating agent Substances 0.000 description 14
- 239000007789 gas Substances 0.000 description 9
- 239000000376 reactant Substances 0.000 description 9
- 230000000977 initiatory effect Effects 0.000 description 8
- 238000012545 processing Methods 0.000 description 8
- 230000014509 gene expression Effects 0.000 description 7
- 229920006395 saturated elastomer Polymers 0.000 description 7
- 238000004519 manufacturing process Methods 0.000 description 6
- 230000003197 catalytic effect Effects 0.000 description 5
- 239000012530 fluid Substances 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000002245 particle Substances 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 4
- 230000003993 interaction Effects 0.000 description 4
- 230000005499 meniscus Effects 0.000 description 4
- 238000003908 quality control method Methods 0.000 description 4
- 238000010998 test method Methods 0.000 description 4
- 230000001133 acceleration Effects 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 3
- 239000007800 oxidant agent Substances 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 0 CC1**(C)=CC1 Chemical compound CC1**(C)=CC1 0.000 description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229910052731 fluorine Inorganic materials 0.000 description 2
- 239000011737 fluorine Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 238000013507 mapping Methods 0.000 description 2
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 239000005518 polymer electrolyte Substances 0.000 description 2
- 230000007704 transition Effects 0.000 description 2
- 238000012935 Averaging Methods 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000000712 assembly Effects 0.000 description 1
- 238000000429 assembly Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000013480 data collection Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000000105 evaporative light scattering detection Methods 0.000 description 1
- 230000000763 evoking effect Effects 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 239000002737 fuel gas Substances 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 229920000554 ionomer Polymers 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- -1 polytetrafluoroethylene Polymers 0.000 description 1
- 239000010970 precious metal Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000000275 quality assurance Methods 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 238000011179 visual inspection Methods 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N13/00—Investigating surface or boundary effects, e.g. wetting power; Investigating diffusion effects; Analysing materials by determining surface, boundary, or diffusion effects
- G01N13/04—Investigating osmotic effects
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
- G01N15/088—Investigating volume, surface area, size or distribution of pores; Porosimetry
- G01N15/0893—Investigating volume, surface area, size or distribution of pores; Porosimetry by measuring weight or volume of sorbed fluid, e.g. B.E.T. method
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Inert Electrodes (AREA)
- Fuel Cell (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/342,976 | 2003-01-15 | ||
| US10/342,976 US6928893B2 (en) | 2003-01-15 | 2003-01-15 | Method of making a gas diffusion media and quality controls for same |
| PCT/US2004/000794 WO2004066416A2 (en) | 2003-01-15 | 2004-01-13 | Method of making a gas diffusion media and quality controls for same |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE112004000141T5 DE112004000141T5 (de) | 2006-04-27 |
| DE112004000141B4 true DE112004000141B4 (de) | 2019-03-28 |
Family
ID=32711846
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE112004000141.2T Expired - Lifetime DE112004000141B4 (de) | 2003-01-15 | 2004-01-13 | Verfahren zur Bestimmung einer Qualität eines Gasdiffusionsmediums |
Country Status (5)
| Country | Link |
|---|---|
| US (2) | US6928893B2 (enExample) |
| JP (1) | JP4976693B2 (enExample) |
| CN (1) | CN1784597B (enExample) |
| DE (1) | DE112004000141B4 (enExample) |
| WO (1) | WO2004066416A2 (enExample) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7107864B2 (en) * | 2003-01-15 | 2006-09-19 | General Motors Corporation | Quality control methods for gas diffusion media |
| US20060240312A1 (en) * | 2005-04-25 | 2006-10-26 | Tao Xie | Diffusion media, fuel cells, and fuel cell powered systems |
| US20070059580A1 (en) * | 2005-09-15 | 2007-03-15 | Budinski Michael K | Design strategies for corrosion mitigation |
| US7722979B2 (en) * | 2005-10-14 | 2010-05-25 | Gm Global Technology Operations, Inc. | Fuel cells with hydrophobic diffusion medium |
| US20100028744A1 (en) * | 2008-08-04 | 2010-02-04 | Gm Global Technology Operations, Inc. | Gas diffusion layer with lower gas diffusivity |
| US20100028750A1 (en) * | 2008-08-04 | 2010-02-04 | Gm Global Technology Operations, Inc. | Gas diffusion layer with lower gas diffusivity |
| CA2842462C (en) | 2011-07-20 | 2020-01-28 | Brigham Young University | Hydrogel materials incorporating eluting ceragenin compound |
| US9234843B2 (en) | 2011-08-25 | 2016-01-12 | Alliance For Sustainable Energy, Llc | On-line, continuous monitoring in solar cell and fuel cell manufacturing using spectral reflectance imaging |
| BR112015023747B1 (pt) | 2013-03-15 | 2023-04-18 | Brigham Young University | Uso de um composto antimicrobiano catiônico esteroide (csa) para a preparação de uma composição para tratar, reduzir, ou prevenir inflamação aguda ou crônica e/ou dor aguda ou crônica associada com uma doença ou um sintoma de doença |
| US11524015B2 (en) | 2013-03-15 | 2022-12-13 | Brigham Young University | Methods for treating inflammation, autoimmune disorders and pain |
| US11690855B2 (en) | 2013-10-17 | 2023-07-04 | Brigham Young University | Methods for treating lung infections and inflammation |
| US20150203527A1 (en) | 2014-01-23 | 2015-07-23 | Brigham Young University | Cationic steroidal antimicrobials |
| US10370403B2 (en) | 2015-04-22 | 2019-08-06 | Brigham Young University | Methods for the synthesis of ceragenins |
| US10226550B2 (en) | 2016-03-11 | 2019-03-12 | Brigham Young University | Cationic steroidal antimicrobial compositions for the treatment of dermal tissue |
| US10480935B2 (en) | 2016-12-02 | 2019-11-19 | Alliance For Sustainable Energy, Llc | Thickness mapping using multispectral imaging |
| US10959433B2 (en) | 2017-03-21 | 2021-03-30 | Brigham Young University | Use of cationic steroidal antimicrobials for sporicidal activity |
| US12186328B2 (en) | 2019-05-23 | 2025-01-07 | Brigham Young University | Use of CSA compounds to stimulate stem cells and hair growth |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4412405A1 (de) | 1994-04-11 | 1995-10-12 | Michael Dipl Ing Breitwieser | Vorrichtung und Verfahren zur Messung von Kräften und Ermittlung von Stoffeigenschaften |
| EP0731520A1 (en) | 1995-03-09 | 1996-09-11 | Johnson Matthey Public Limited Company | Materials for use in catalytic electrode manufacture |
| WO1997050143A1 (en) | 1996-06-25 | 1997-12-31 | The Dais Corporation | Gas diffusion electrode |
| US5763113A (en) | 1996-08-26 | 1998-06-09 | General Motors Corporation | PEM fuel cell monitoring system |
| DE10048182A1 (de) * | 1999-10-25 | 2001-05-17 | Gen Motors Corp | Verbundananordnung zur Gasverteilung bei Brennstoffzellen |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4050822A (en) * | 1976-03-10 | 1977-09-27 | Rame-Hart, Inc. | Drop measuring apparatus, and a method of evaluating materials wettability |
| US4676807A (en) * | 1985-07-05 | 1987-06-30 | Pall Corporation | Process for removal of liquid aerosols from gaseous streams |
| KR940003440Y1 (ko) * | 1989-06-21 | 1994-05-25 | 대우전자 주식회사 | 오디오(Audio)용 회전헤드(Head)의 조작판 출몰장치 |
| JPH05144444A (ja) * | 1991-11-25 | 1993-06-11 | Toshiba Corp | 燃料電池およびそれに用いる電極の製造方法 |
| JP3245929B2 (ja) * | 1992-03-09 | 2002-01-15 | 株式会社日立製作所 | 燃料電池及びその応用装置 |
| US5583285A (en) * | 1994-11-29 | 1996-12-10 | Lucent Technologies Inc. | Method for detecting a coating material on a substrate |
| US6329094B1 (en) * | 1997-05-14 | 2001-12-11 | Sanyo Electric Co., Ltd. | Polymer electrolyte fuel cell showing stable and outstanding electric-power generating characteristics |
| US5910378A (en) * | 1997-10-10 | 1999-06-08 | Minnesota Mining And Manufacturing Company | Membrane electrode assemblies |
| US6103077A (en) * | 1998-01-02 | 2000-08-15 | De Nora S.P.A. | Structures and methods of manufacture for gas diffusion electrodes and electrode components |
| US7098163B2 (en) * | 1998-08-27 | 2006-08-29 | Cabot Corporation | Method of producing membrane electrode assemblies for use in proton exchange membrane and direct methanol fuel cells |
| US6150049A (en) * | 1999-09-17 | 2000-11-21 | Plug Power Inc. | Fluid flow plate for distribution of hydration fluid in a fuel cell |
| JP4470271B2 (ja) * | 2000-03-31 | 2010-06-02 | 株式会社エクォス・リサーチ | 燃料電池および燃料電池装置 |
| JP2002025578A (ja) * | 2000-07-12 | 2002-01-25 | Toyota Motor Corp | 燃料電池用の電極・電解質膜接合体の製造方法およびそれに用いられる基材 |
| JP2002313359A (ja) * | 2001-04-17 | 2002-10-25 | Mitsubishi Heavy Ind Ltd | 固体高分子型燃料電池 |
| US6821661B2 (en) * | 2001-08-31 | 2004-11-23 | Plug Power, Inc. | Hydrophilic anode gas diffusion layer |
| US6684685B2 (en) * | 2002-06-21 | 2004-02-03 | Porous Materials, Inc. | Liquid extrusion porosimeter and method |
| US7024921B2 (en) * | 2002-11-06 | 2006-04-11 | Sutton Stephen P | Capillary devices for determination of surface characteristics and contact angles and methods for using same |
-
2003
- 2003-01-15 US US10/342,976 patent/US6928893B2/en not_active Expired - Lifetime
-
2004
- 2004-01-13 CN CN2004800070808A patent/CN1784597B/zh not_active Expired - Lifetime
- 2004-01-13 DE DE112004000141.2T patent/DE112004000141B4/de not_active Expired - Lifetime
- 2004-01-13 WO PCT/US2004/000794 patent/WO2004066416A2/en not_active Ceased
- 2004-01-13 JP JP2005518801A patent/JP4976693B2/ja not_active Expired - Fee Related
-
2005
- 2005-05-12 US US11/127,376 patent/US7284411B2/en not_active Expired - Lifetime
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4412405A1 (de) | 1994-04-11 | 1995-10-12 | Michael Dipl Ing Breitwieser | Vorrichtung und Verfahren zur Messung von Kräften und Ermittlung von Stoffeigenschaften |
| EP0731520A1 (en) | 1995-03-09 | 1996-09-11 | Johnson Matthey Public Limited Company | Materials for use in catalytic electrode manufacture |
| WO1997050143A1 (en) | 1996-06-25 | 1997-12-31 | The Dais Corporation | Gas diffusion electrode |
| US5763113A (en) | 1996-08-26 | 1998-06-09 | General Motors Corporation | PEM fuel cell monitoring system |
| DE10048182A1 (de) * | 1999-10-25 | 2001-05-17 | Gen Motors Corp | Verbundananordnung zur Gasverteilung bei Brennstoffzellen |
| US6350539B1 (en) | 1999-10-25 | 2002-02-26 | General Motors Corporation | Composite gas distribution structure for fuel cell |
Also Published As
| Publication number | Publication date |
|---|---|
| US20050199079A1 (en) | 2005-09-15 |
| US20040134292A1 (en) | 2004-07-15 |
| US7284411B2 (en) | 2007-10-23 |
| DE112004000141T5 (de) | 2006-04-27 |
| US6928893B2 (en) | 2005-08-16 |
| JP2006516353A (ja) | 2006-06-29 |
| WO2004066416A3 (en) | 2005-12-15 |
| CN1784597A (zh) | 2006-06-07 |
| CN1784597B (zh) | 2010-12-01 |
| WO2004066416A2 (en) | 2004-08-05 |
| JP4976693B2 (ja) | 2012-07-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| 8180 | Miscellaneous part 1 | ||
| 8127 | New person/name/address of the applicant | ||
| R081 | Change of applicant/patentee | ||
| R016 | Response to examination communication | ||
| R018 | Grant decision by examination section/examining division | ||
| R020 | Patent grant now final | ||
| R071 | Expiry of right |