DE1112074B - Verfahren zur Herstellung von Thiophosphorsaeureestern - Google Patents
Verfahren zur Herstellung von ThiophosphorsaeureesternInfo
- Publication number
- DE1112074B DE1112074B DEF17526A DEF0017526A DE1112074B DE 1112074 B DE1112074 B DE 1112074B DE F17526 A DEF17526 A DE F17526A DE F0017526 A DEF0017526 A DE F0017526A DE 1112074 B DE1112074 B DE 1112074B
- Authority
- DE
- Germany
- Prior art keywords
- acid esters
- preparation
- thiophosphoric acid
- general formula
- german patent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 150000003580 thiophosphoric acid esters Chemical class 0.000 title claims description 6
- 238000000034 method Methods 0.000 title claims description 3
- 239000002253 acid Substances 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 5
- 125000004433 nitrogen atom Chemical group N* 0.000 claims description 5
- 230000002378 acidificating effect Effects 0.000 claims description 2
- 150000007513 acids Chemical class 0.000 claims description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O ammonium group Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims description 2
- 125000005843 halogen group Chemical group 0.000 claims description 2
- 229910052751 metal Inorganic materials 0.000 claims description 2
- 239000002184 metal Substances 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims 1
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 238000001816 cooling Methods 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 4
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 4
- -1 alkyl radicals Chemical class 0.000 description 4
- 229910052938 sodium sulfate Inorganic materials 0.000 description 4
- 235000011152 sodium sulphate Nutrition 0.000 description 4
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 3
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 description 3
- 239000012964 benzotriazole Substances 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- KZNICNPSHKQLFF-UHFFFAOYSA-N succinimide Chemical compound O=C1CCC(=O)N1 KZNICNPSHKQLFF-UHFFFAOYSA-N 0.000 description 3
- 241001465754 Metazoa Species 0.000 description 2
- 229910019142 PO4 Inorganic materials 0.000 description 2
- SWLVFNYSXGMGBS-UHFFFAOYSA-N ammonium bromide Chemical compound [NH4+].[Br-] SWLVFNYSXGMGBS-UHFFFAOYSA-N 0.000 description 2
- 150000003863 ammonium salts Chemical class 0.000 description 2
- 239000010452 phosphate Substances 0.000 description 2
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 2
- 229960002317 succinimide Drugs 0.000 description 2
- ISJWFCINBNWGQA-UHFFFAOYSA-N 3-(2-bromoethyl)pyrrolidine-2,5-dione Chemical compound BrCCC1C(=O)NC(C1)=O ISJWFCINBNWGQA-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 230000000895 acaricidal effect Effects 0.000 description 1
- 230000002824 aphicidal effect Effects 0.000 description 1
- 150000001735 carboxylic acids Chemical class 0.000 description 1
- 150000003841 chloride salts Chemical class 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- XKJCHHZQLQNZHY-UHFFFAOYSA-N phthalimide Chemical compound C1=CC=C2C(=O)NC(=O)C2=C1 XKJCHHZQLQNZHY-UHFFFAOYSA-N 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- CVHZOJJKTDOEJC-UHFFFAOYSA-N saccharin Chemical compound C1=CC=C2C(=O)NS(=O)(=O)C2=C1 CVHZOJJKTDOEJC-UHFFFAOYSA-N 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6515—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having three nitrogen atoms as the only ring hetero atoms
- C07F9/6518—Five-membered rings
- C07F9/65188—Five-membered rings condensed with carbocyclic rings or carbocyclic ring systems
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/16—Esters of thiophosphoric acids or thiophosphorous acids
- C07F9/165—Esters of thiophosphoric acids
- C07F9/1651—Esters of thiophosphoric acids with hydroxyalkyl compounds with further substituents on alkyl
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/553—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom
- C07F9/5537—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having one nitrogen atom as the only ring hetero atom the heteroring containing the structure -C(=O)-N-C(=O)- (both carbon atoms belong to the heteroring)
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE547771D BE547771A (US07368563-20080506-C00056.png) | 1955-05-13 | ||
| DEF17526A DE1112074B (de) | 1955-05-13 | 1955-05-13 | Verfahren zur Herstellung von Thiophosphorsaeureestern |
| CH347514D CH347514A (de) | 1955-05-13 | 1956-05-04 | Verfahren zur Herstellung von Thiophosphorsäureestern |
| GB14464/56A GB804761A (en) | 1955-05-13 | 1956-05-09 | Thiophosphoric acid esters |
| US583947A US2902493A (en) | 1955-05-13 | 1956-05-10 | Thiophosphoric acid esters and process for their production |
| FR1164532D FR1164532A (fr) | 1955-05-13 | 1956-05-12 | Esters d'acides thiophosphoriques et leur procédé de production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF17526A DE1112074B (de) | 1955-05-13 | 1955-05-13 | Verfahren zur Herstellung von Thiophosphorsaeureestern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1112074B true DE1112074B (de) | 1961-08-03 |
Family
ID=7088606
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF17526A Pending DE1112074B (de) | 1955-05-13 | 1955-05-13 | Verfahren zur Herstellung von Thiophosphorsaeureestern |
Country Status (6)
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE572314A (US07368563-20080506-C00056.png) * | 1957-10-25 | 1900-01-01 | ||
| US3242191A (en) * | 1963-01-26 | 1966-03-22 | Bayer Ag | Thiol_ or thionothiolphosphoric (-phosphonic, -phosphinic) acid esters of chloromethoxy benzotriazole compounds |
| US3316145A (en) * | 1965-01-11 | 1967-04-25 | Hercules Inc | O, o-dimethyl s-(1-succinimidoethyl) phos-phorodithioate and insecticidal compositions containing the same |
| DE2343147C2 (de) * | 1973-08-27 | 1982-06-09 | Henkel KGaA, 4000 Düsseldorf | Pyrrolidon-5,5-diphosphonsäuren, deren wasserlösliche Salze, und Verfahren zu ihrer Herstellung |
| CN109679723B (zh) * | 2017-10-18 | 2022-05-03 | 中国石油化工股份有限公司 | 汽轮机润滑油组合物及其制备方法 |
| CN109679711B (zh) * | 2017-10-18 | 2022-03-11 | 中国石油化工股份有限公司 | 生物柴油发动机润滑油组合物及其制备方法 |
| CN109679737B (zh) * | 2017-10-18 | 2022-05-03 | 中国石油化工股份有限公司 | 船用中速筒状活塞式发动机润滑油组合物及其制备方法 |
| CN109679753B (zh) * | 2017-10-18 | 2022-05-03 | 中国石油化工股份有限公司 | 膨润土润滑脂及其制备方法 |
| CN109679722B (zh) * | 2017-10-18 | 2022-05-03 | 中国石油化工股份有限公司 | 复合钙基润滑脂及其制备方法 |
| CN109679710B (zh) * | 2017-10-18 | 2022-03-11 | 中国石油化工股份有限公司 | 液压油组合物及其制备方法 |
| CN109679731B (zh) * | 2017-10-18 | 2022-05-03 | 中国石油化工股份有限公司 | 复合铝基润滑脂及其制备方法 |
| CN109679730B (zh) * | 2017-10-18 | 2022-05-03 | 中国石油化工股份有限公司 | 一种润滑脂及其制备方法 |
| CN109679743B (zh) * | 2017-10-18 | 2022-05-03 | 中国石油化工股份有限公司 | 全合成工业齿轮润滑油组合物及其制备方法 |
| CN109679721B (zh) * | 2017-10-18 | 2022-05-03 | 中国石油化工股份有限公司 | 工业润滑油组合物及其制备方法 |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE927092C (de) * | 1953-01-08 | 1955-04-28 | Bayer Ag | Verfahren zur Herstellung von Thiophosphorsaeureestern |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL86689C (US07368563-20080506-C00056.png) * | 1951-04-20 | 1900-01-01 | ||
| US2736726A (en) * | 1952-03-28 | 1956-02-28 | Geigy Ag J R | Basic phosphoric acid esters |
| DE930446C (de) * | 1953-02-09 | 1955-07-18 | Bayer Ag | Verfahren zur Herstellung von Thiophosphorsaeureestern |
| US2767194A (en) * | 1955-03-18 | 1956-10-16 | Stauffer Chemical Co | Compositions of matter |
-
0
- BE BE547771D patent/BE547771A/xx unknown
-
1955
- 1955-05-13 DE DEF17526A patent/DE1112074B/de active Pending
-
1956
- 1956-05-04 CH CH347514D patent/CH347514A/de unknown
- 1956-05-09 GB GB14464/56A patent/GB804761A/en not_active Expired
- 1956-05-10 US US583947A patent/US2902493A/en not_active Expired - Lifetime
- 1956-05-12 FR FR1164532D patent/FR1164532A/fr not_active Expired
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE927092C (de) * | 1953-01-08 | 1955-04-28 | Bayer Ag | Verfahren zur Herstellung von Thiophosphorsaeureestern |
Also Published As
| Publication number | Publication date |
|---|---|
| CH347514A (de) | 1960-07-15 |
| GB804761A (en) | 1958-11-19 |
| US2902493A (en) | 1959-09-01 |
| FR1164532A (fr) | 1958-10-10 |
| BE547771A (US07368563-20080506-C00056.png) |
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