DE1105176B - Verfahren zur Isolierung von festen chlorierten oder sulfochlorierten Homo- oder Mischpolymerisaten von Olefinen aus ihren Loesungen - Google Patents
Verfahren zur Isolierung von festen chlorierten oder sulfochlorierten Homo- oder Mischpolymerisaten von Olefinen aus ihren LoesungenInfo
- Publication number
- DE1105176B DE1105176B DEF25730A DEF0025730A DE1105176B DE 1105176 B DE1105176 B DE 1105176B DE F25730 A DEF25730 A DE F25730A DE F0025730 A DEF0025730 A DE F0025730A DE 1105176 B DE1105176 B DE 1105176B
- Authority
- DE
- Germany
- Prior art keywords
- sulfochlorinated
- solutions
- chlorinated
- copolymers
- homopolymers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 18
- 229920001577 copolymer Polymers 0.000 title claims description 9
- 239000007787 solid Substances 0.000 title claims description 7
- 150000001336 alkenes Chemical class 0.000 title claims description 4
- 229920001519 homopolymer Polymers 0.000 title claims description 4
- 238000002955 isolation Methods 0.000 title description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 238000001556 precipitation Methods 0.000 claims description 11
- 239000002904 solvent Substances 0.000 claims description 10
- 229920000098 polyolefin Polymers 0.000 claims description 7
- 229910052751 metal Inorganic materials 0.000 claims description 6
- 239000002184 metal Substances 0.000 claims description 6
- 150000002739 metals Chemical class 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 3
- 239000002270 dispersing agent Substances 0.000 claims description 3
- 230000000737 periodic effect Effects 0.000 claims description 3
- 239000004065 semiconductor Substances 0.000 claims description 3
- 150000002484 inorganic compounds Chemical class 0.000 claims description 2
- 229910010272 inorganic material Inorganic materials 0.000 claims description 2
- 150000002894 organic compounds Chemical class 0.000 claims 1
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 24
- -1 Polyethylenes Polymers 0.000 description 23
- 239000000243 solution Substances 0.000 description 17
- 239000004698 Polyethylene Substances 0.000 description 16
- 229920000573 polyethylene Polymers 0.000 description 16
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 15
- 239000002245 particle Substances 0.000 description 7
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 6
- 239000004743 Polypropylene Substances 0.000 description 6
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 6
- 239000000440 bentonite Substances 0.000 description 6
- 229910000278 bentonite Inorganic materials 0.000 description 6
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 6
- 229910052801 chlorine Inorganic materials 0.000 description 6
- 239000000460 chlorine Substances 0.000 description 6
- 229920001155 polypropylene Polymers 0.000 description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- 229910052717 sulfur Inorganic materials 0.000 description 5
- 239000011593 sulfur Substances 0.000 description 5
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 4
- 239000005018 casein Substances 0.000 description 4
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 4
- 235000021240 caseins Nutrition 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- 238000010626 work up procedure Methods 0.000 description 3
- YXIWHUQXZSMYRE-UHFFFAOYSA-N 1,3-benzothiazole-2-thiol Chemical compound C1=CC=C2SC(S)=NC2=C1 YXIWHUQXZSMYRE-UHFFFAOYSA-N 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 2
- 239000005977 Ethylene Substances 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 239000007900 aqueous suspension Substances 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical group OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 2
- 239000003995 emulsifying agent Substances 0.000 description 2
- 229920000159 gelatin Polymers 0.000 description 2
- 235000019322 gelatine Nutrition 0.000 description 2
- 229920001083 polybutene Polymers 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
- 238000001256 steam distillation Methods 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 description 1
- STMRWVUTGPZZER-UHFFFAOYSA-N 2,3-bis(2-methylpropyl)phenol Chemical class CC(C)CC1=CC=CC(O)=C1CC(C)C STMRWVUTGPZZER-UHFFFAOYSA-N 0.000 description 1
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical class [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- NJVJNPLRNCIAQO-UHFFFAOYSA-N C(OC)(OC)=O.[Ba] Chemical compound C(OC)(OC)=O.[Ba] NJVJNPLRNCIAQO-UHFFFAOYSA-N 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 239000001828 Gelatine Substances 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 241000947853 Vibrionales Species 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical class [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- 229910000410 antimony oxide Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000011324 bead Substances 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 229910052736 halogen Inorganic materials 0.000 description 1
- 150000002367 halogens Chemical class 0.000 description 1
- 231100000171 higher toxicity Toxicity 0.000 description 1
- 150000004679 hydroxides Chemical class 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 229910003480 inorganic solid Inorganic materials 0.000 description 1
- 229910000464 lead oxide Inorganic materials 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical class [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000001095 magnesium carbonate Substances 0.000 description 1
- 235000011160 magnesium carbonates Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- OFGGZGXWRWYORO-UHFFFAOYSA-N methanol;tetrachloromethane Chemical compound OC.ClC(Cl)(Cl)Cl OFGGZGXWRWYORO-UHFFFAOYSA-N 0.000 description 1
- APVPOHHVBBYQAV-UHFFFAOYSA-N n-(4-aminophenyl)sulfonyloctadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(=O)NS(=O)(=O)C1=CC=C(N)C=C1 APVPOHHVBBYQAV-UHFFFAOYSA-N 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- VTRUBDSFZJNXHI-UHFFFAOYSA-N oxoantimony Chemical class [Sb]=O VTRUBDSFZJNXHI-UHFFFAOYSA-N 0.000 description 1
- YEXPOXQUZXUXJW-UHFFFAOYSA-N oxolead Chemical compound [Pb]=O YEXPOXQUZXUXJW-UHFFFAOYSA-N 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 150000004760 silicates Chemical class 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000011877 solvent mixture Substances 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical compound C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/34—Introducing sulfur atoms or sulfur-containing groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/06—Treatment of polymer solutions
- C08F6/12—Separation of polymers from solutions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/18—Introducing halogen atoms or halogen-containing groups
- C08F8/20—Halogenation
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE578595D BE578595A (en:Method) | 1958-05-10 | ||
| NL238917D NL238917A (en:Method) | 1958-05-10 | ||
| DEF25730A DE1105176B (de) | 1958-05-10 | 1958-05-10 | Verfahren zur Isolierung von festen chlorierten oder sulfochlorierten Homo- oder Mischpolymerisaten von Olefinen aus ihren Loesungen |
| US811005A US3168499A (en) | 1958-05-10 | 1959-05-05 | Process for isolating chlorinated or sulfochlorinated polyolefins |
| FR794301A FR1223893A (fr) | 1958-05-10 | 1959-05-11 | Procédé d'isolement de polyoléfines chlorées ou sulfochlorées |
| GB16144/59A GB911641A (en) | 1958-05-10 | 1959-05-11 | Process for the isolation of chlorinated or sulphochlorinated polyolefines |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF25730A DE1105176B (de) | 1958-05-10 | 1958-05-10 | Verfahren zur Isolierung von festen chlorierten oder sulfochlorierten Homo- oder Mischpolymerisaten von Olefinen aus ihren Loesungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1105176B true DE1105176B (de) | 1961-04-20 |
Family
ID=7091742
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF25730A Pending DE1105176B (de) | 1958-05-10 | 1958-05-10 | Verfahren zur Isolierung von festen chlorierten oder sulfochlorierten Homo- oder Mischpolymerisaten von Olefinen aus ihren Loesungen |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3168499A (en:Method) |
| BE (1) | BE578595A (en:Method) |
| DE (1) | DE1105176B (en:Method) |
| FR (1) | FR1223893A (en:Method) |
| GB (1) | GB911641A (en:Method) |
| NL (1) | NL238917A (en:Method) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1215371B (de) * | 1963-08-26 | 1966-04-28 | Buna Chem Werke Veb | Verfahren zur Aufarbeitung von bei der Chlorierung von Polymeren anfallenden Chlorier-loesungen |
| DE1258096B (de) | 1960-03-31 | 1968-01-04 | Phillips Petroleum Co | Verfahren zur Gewinnung eines kautschukartigen Kohlenwasserstoffhomopolymerisats oder -mischpolymerisats aus Loesungen |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE633818A (en:Method) * | 1962-06-21 | |||
| DE2262536A1 (de) * | 1972-12-21 | 1974-06-27 | Hoechst Ag | Verfahren zur herstellung hellgefaerbter, thermostabiler chlorierungsprodukte von poly-alpha-olefinen |
| DE2262535A1 (de) * | 1972-12-21 | 1974-06-27 | Hoechst Ag | Verfahren zur herstellung hellgefaerbter, thermostabiler chlorierungsprodukte von poly-alpha-olefinen |
| DE3105404A1 (de) * | 1981-02-14 | 1982-09-02 | Hoechst Ag, 6000 Frankfurt | Verfahren zur herstellung eines feinkoernigen nichtagglomerierenden chlorpolyethylens |
| US4680380A (en) * | 1983-01-19 | 1987-07-14 | The B. F. Goodrich Company | Odor-free chlorosulfonated polyolefins |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2398803A (en) * | 1941-06-27 | 1946-04-23 | Ici Ltd | Halogenated polymers of ethylene and process of preparation |
| US2592814A (en) * | 1947-12-20 | 1952-04-15 | Du Pont | Isolation of chlorosulfonated polymers of ethylene from solution |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA530791A (en) * | 1956-09-25 | Leroy Ludlow John | Isolation of chlorosulfonated polymers of ethylene from solution | |
| US2523289A (en) * | 1945-08-14 | 1950-09-26 | Jasco Inc | Modifying agents for use in lowtemperature polymerization reactions |
| US2640048A (en) * | 1949-01-12 | 1953-05-26 | Du Pont | Chlorosulfonation of polythene using azo catalysts |
| US2809950A (en) * | 1955-06-10 | 1957-10-15 | Du Pont | Curable dispersions of chlorosulfonated ethylene polymers and process of coating with same |
| US3005812A (en) * | 1958-02-06 | 1961-10-24 | Allied Chem | Process for removing solvents from chlorinated polyethylene resins |
-
0
- NL NL238917D patent/NL238917A/xx unknown
- BE BE578595D patent/BE578595A/xx unknown
-
1958
- 1958-05-10 DE DEF25730A patent/DE1105176B/de active Pending
-
1959
- 1959-05-05 US US811005A patent/US3168499A/en not_active Expired - Lifetime
- 1959-05-11 FR FR794301A patent/FR1223893A/fr not_active Expired
- 1959-05-11 GB GB16144/59A patent/GB911641A/en not_active Expired
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2398803A (en) * | 1941-06-27 | 1946-04-23 | Ici Ltd | Halogenated polymers of ethylene and process of preparation |
| US2592814A (en) * | 1947-12-20 | 1952-04-15 | Du Pont | Isolation of chlorosulfonated polymers of ethylene from solution |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1258096B (de) | 1960-03-31 | 1968-01-04 | Phillips Petroleum Co | Verfahren zur Gewinnung eines kautschukartigen Kohlenwasserstoffhomopolymerisats oder -mischpolymerisats aus Loesungen |
| DE1215371B (de) * | 1963-08-26 | 1966-04-28 | Buna Chem Werke Veb | Verfahren zur Aufarbeitung von bei der Chlorierung von Polymeren anfallenden Chlorier-loesungen |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1223893A (fr) | 1960-06-21 |
| GB911641A (en) | 1962-11-28 |
| US3168499A (en) | 1965-02-02 |
| BE578595A (en:Method) | |
| NL238917A (en:Method) |
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