DE1057588B - Verfahren zur Herstellung von Kaliumpersulfat - Google Patents
Verfahren zur Herstellung von KaliumpersulfatInfo
- Publication number
- DE1057588B DE1057588B DEF22012A DEF0022012A DE1057588B DE 1057588 B DE1057588 B DE 1057588B DE F22012 A DEF22012 A DE F22012A DE F0022012 A DEF0022012 A DE F0022012A DE 1057588 B DE1057588 B DE 1057588B
- Authority
- DE
- Germany
- Prior art keywords
- potassium
- solution
- ammonium
- column
- persulfate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 23
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 title claims description 17
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- 239000000243 solution Substances 0.000 claims description 42
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims description 35
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 24
- 238000000926 separation method Methods 0.000 claims description 23
- 238000006243 chemical reaction Methods 0.000 claims description 21
- 239000013078 crystal Substances 0.000 claims description 20
- 239000007787 solid Substances 0.000 claims description 17
- 229910001870 ammonium persulfate Inorganic materials 0.000 claims description 14
- 239000004160 Ammonium persulphate Substances 0.000 claims description 8
- 235000019395 ammonium persulphate Nutrition 0.000 claims description 8
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims description 8
- 229910052939 potassium sulfate Inorganic materials 0.000 claims description 8
- 235000011151 potassium sulphates Nutrition 0.000 claims description 8
- 239000000725 suspension Substances 0.000 claims description 8
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- JRKICGRDRMAZLK-UHFFFAOYSA-L peroxydisulfate Chemical compound [O-]S(=O)(=O)OOS([O-])(=O)=O JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 claims description 7
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 6
- 239000004159 Potassium persulphate Substances 0.000 claims description 6
- 150000002500 ions Chemical class 0.000 claims description 6
- 239000012452 mother liquor Substances 0.000 claims description 6
- 229910052700 potassium Inorganic materials 0.000 claims description 6
- 239000011591 potassium Substances 0.000 claims description 6
- 235000019394 potassium persulphate Nutrition 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 5
- 239000007790 solid phase Substances 0.000 claims description 5
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 4
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 4
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 4
- 238000004821 distillation Methods 0.000 claims description 4
- 239000012071 phase Substances 0.000 claims description 4
- 229910001414 potassium ion Inorganic materials 0.000 claims description 4
- 238000005868 electrolysis reaction Methods 0.000 claims description 3
- 239000001120 potassium sulphate Substances 0.000 claims description 3
- 230000015572 biosynthetic process Effects 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 238000012546 transfer Methods 0.000 claims description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 6
- -1 ammonium ions Chemical class 0.000 claims 2
- 230000003247 decreasing effect Effects 0.000 claims 2
- 150000002978 peroxides Chemical class 0.000 claims 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 1
- 238000009825 accumulation Methods 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- 230000001174 ascending effect Effects 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 238000009833 condensation Methods 0.000 claims 1
- 230000005494 condensation Effects 0.000 claims 1
- 230000006735 deficit Effects 0.000 claims 1
- 238000010790 dilution Methods 0.000 claims 1
- 239000012895 dilution Substances 0.000 claims 1
- 238000001914 filtration Methods 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 238000013508 migration Methods 0.000 claims 1
- 230000005012 migration Effects 0.000 claims 1
- 230000003647 oxidation Effects 0.000 claims 1
- 238000007254 oxidation reaction Methods 0.000 claims 1
- 238000012545 processing Methods 0.000 claims 1
- 239000002994 raw material Substances 0.000 claims 1
- 230000000630 rising effect Effects 0.000 claims 1
- 238000012795 verification Methods 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 239000002699 waste material Substances 0.000 claims 1
- 150000003839 salts Chemical class 0.000 description 7
- 239000002245 particle Substances 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 241000283986 Lepus Species 0.000 description 1
- NPYPAHLBTDXSSS-UHFFFAOYSA-N Potassium ion Chemical compound [K+] NPYPAHLBTDXSSS-UHFFFAOYSA-N 0.000 description 1
- 150000003863 ammonium salts Chemical class 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000008151 electrolyte solution Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 description 1
- CHKVPAROMQMJNQ-UHFFFAOYSA-M potassium bisulfate Chemical compound [K+].OS([O-])(=O)=O CHKVPAROMQMJNQ-UHFFFAOYSA-M 0.000 description 1
- 229910000343 potassium bisulfate Inorganic materials 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/055—Peroxyhydrates; Peroxyacids or salts thereof
- C01B15/06—Peroxyhydrates; Peroxyacids or salts thereof containing sulfur
- C01B15/08—Peroxysulfates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US816125XA | 1956-03-19 | 1956-03-19 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1057588B true DE1057588B (de) | 1959-05-21 |
Family
ID=22165244
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF22012A Pending DE1057588B (de) | 1956-03-19 | 1956-12-21 | Verfahren zur Herstellung von Kaliumpersulfat |
Country Status (3)
| Country | Link |
|---|---|
| BE (1) | BE553886A (enExample) |
| DE (1) | DE1057588B (enExample) |
| GB (1) | GB816125A (enExample) |
-
0
- BE BE553886D patent/BE553886A/xx unknown
-
1956
- 1956-12-04 GB GB36998/56A patent/GB816125A/en not_active Expired
- 1956-12-21 DE DEF22012A patent/DE1057588B/de active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| GB816125A (en) | 1959-07-08 |
| BE553886A (enExample) |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2635935A1 (de) | Verfahren zur reinigung von essigsaeure | |
| DE1642831A1 (de) | Verfahren und Vorrichtung zum Ausziehen eines Loesungsmittels aus einer Loesung | |
| DE2545658A1 (de) | Verfahren zur gewinnung von carbonsaeuren aus ihren waessrigen loesungen | |
| DE2442192A1 (de) | Verfahren zum reinigen von silicium | |
| DE566153C (de) | Verfahren und Vorrichtung zur Herstellung von Furfurol | |
| DE2605106A1 (de) | Verfahren und vorrichtung zur gewinnung von alkoholischen phosphorsaeureloesungen aus sauren phosphaten | |
| DE2800760C2 (de) | Verfahren zur Herstellung von Natriumpercarbonat aus einer Sodalösung bzw. -suspension | |
| DE3002359C2 (de) | Verfahren zum Entfernen von Verunreinigungen aus einer rohen Naßverfahrensphosphorsäure | |
| DE1057588B (de) | Verfahren zur Herstellung von Kaliumpersulfat | |
| DE649324C (de) | Verfahren zur Herstellung von Furfurol | |
| DE1492916C3 (de) | Verfahren für das Ausscheiden von Kalium aus industriellen Nebenprodukten | |
| EP0717028B1 (de) | Verfahren und Vorrichtung zur Gewinnung von Ameisensäure | |
| DE1618385B2 (de) | Verfahren und vorrichtungen zur gewinnung von azinen und/bzw. oder hydrazonen aus diese enthaltenden mischungen | |
| DE567602C (de) | Verfahren zur Gewinnung von Wasserstoffsuperoxyd | |
| DE656683C (de) | Verfahren zum Entwaessern von Hefe | |
| DE2432808B2 (de) | Verfahren zur Konzentrierung einer natriumchlorid- und natriumsulf athaltigen Ätznatronlauge | |
| DE690894C (de) | Verfahren zur Herstellung von Wasserstoffperoxyd | |
| DE1169456B (de) | Kontinuierliches Verfahren zur Gewinnung von Glutaminsaeure aus Zuckerruebenschlempe | |
| DE931588C (de) | Verfahren zur kontinuierlichen Herstellung von Salpetersaeure durch Umsetzung von Schwefelsaeure mit Salpeter | |
| DE1004154B (de) | Verfahren zur kontinuierlichen Gewinnung von Urantetrafluorid aus waessriger Loesung | |
| DE286973C (enExample) | ||
| DE1443538C (de) | Verfahren zur Herstellung von Weinsaure aus Weinstein | |
| DE344238C (de) | Verfahren zur Gewinnung der Leimstoffe aus Knochen, Fisch- und Lederabfaellen usw | |
| DE1120458C2 (de) | Verfahren zur abtrennung von aethylendiamin aus seinem rohrprodukt | |
| DE1618774C (de) | Verfahren zur kontinuierlichen Herstellung von Ameisensäure |