DE1039049B - Verfahren zur Herstellung von Salpetersaeureestern und organischen Nitroverbindungen - Google Patents

Verfahren zur Herstellung von Salpetersaeureestern und organischen Nitroverbindungen

Info

Publication number
DE1039049B
DE1039049B DEN6308A DEN0006308A DE1039049B DE 1039049 B DE1039049 B DE 1039049B DE N6308 A DEN6308 A DE N6308A DE N0006308 A DEN0006308 A DE N0006308A DE 1039049 B DE1039049 B DE 1039049B
Authority
DE
Germany
Prior art keywords
reaction
injector
acid
separator
nitration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
DEN6308A
Other languages
German (de)
English (en)
Inventor
Dipl-Ing Nils Agne Per Nilsson
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nitroglycerin AB
Original Assignee
Nitroglycerin AB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nitroglycerin AB filed Critical Nitroglycerin AB
Publication of DE1039049B publication Critical patent/DE1039049B/de
Pending legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B43/00—Formation or introduction of functional groups containing nitrogen
    • C07B43/02—Formation or introduction of functional groups containing nitrogen of nitro or nitroso groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/02—Preparation of esters of nitric acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DEN6308A 1951-11-06 1952-11-04 Verfahren zur Herstellung von Salpetersaeureestern und organischen Nitroverbindungen Pending DE1039049B (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SE735888X 1951-11-06

Publications (1)

Publication Number Publication Date
DE1039049B true DE1039049B (de) 1958-09-18

Family

ID=20319690

Family Applications (1)

Application Number Title Priority Date Filing Date
DEN6308A Pending DE1039049B (de) 1951-11-06 1952-11-04 Verfahren zur Herstellung von Salpetersaeureestern und organischen Nitroverbindungen

Country Status (6)

Country Link
US (1) US2737522A (en:Method)
BE (1) BE515328A (en:Method)
CH (1) CH308265A (en:Method)
DE (1) DE1039049B (en:Method)
FR (1) FR1065893A (en:Method)
GB (1) GB735888A (en:Method)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1094172B (de) 1957-02-08 1960-12-01 J Meissner Fa Verfahren und Vorrichtung zur Herstellung von Sprengstoffen durch Nitrierung von fluessigen oder festen organischen Stoffen mittels Salpeter- oder Mischsaeure
EP0489211A1 (en) * 1988-08-15 1992-06-10 Nrm International Technologies C.V. Jet impingement reactor
WO2015022110A1 (de) 2013-08-15 2015-02-19 Josef Meissner Gmbh & Co. Kg Verfahren und vorrichtung zur entfernung von bei der herstellung von aliphatischen nitratestern anfallenden verunreinigungen

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3086042A (en) * 1955-12-23 1963-04-16 Ici Ltd Continuous production of liquid explosive nitric esters
US2951866A (en) * 1956-09-28 1960-09-06 Hercules Powder Co Ltd Apparatus and method for continuous nitration
US3111538A (en) * 1957-02-07 1963-11-19 Hercules Powder Co Ltd Continuous manufacture of explosive liquid nitric acid esters
US2951877A (en) * 1957-02-25 1960-09-06 Hercules Powder Co Ltd Process for the preparation of trinitrotoluene
US3053908A (en) * 1957-02-25 1962-09-11 Hercules Powder Co Ltd Preparation of nitrated toluene
BE573258A (en:Method) * 1957-11-29
US3009944A (en) * 1958-01-03 1961-11-21 Nitroglycerin Ab Manufacture of nitric acid esters of aliphatic alcohols
US3221494A (en) * 1961-02-13 1965-12-07 North American Aviation Inc Compositions, processes, and apparatus for the improvement of bi-propellant fuels
FR2244734B1 (en:Method) * 1973-09-20 1976-11-19 Aquitaine Petrole
DE2723247C2 (de) * 1977-05-24 1982-09-16 Hoechst Ag, 6000 Frankfurt Verfahren zur kontinuierlichen Herstellung von 3-Nitro-4-acetylaminotoluol
US4329523A (en) * 1980-09-02 1982-05-11 International Minerals & Chemical Corp. Process for the nitration of methane
US4973770A (en) * 1988-12-15 1990-11-27 C-I-L, Inc. Manufacture of organic nitro compounds
EP0436443B1 (en) * 1990-01-04 1996-04-17 Nrm International Technologies C.V. Nitration process
DE19539205A1 (de) * 1995-10-22 1997-04-24 Meissner Gmbh & Co Kg Josef Verfahren zur Aromatennitrierung
RU2188817C2 (ru) * 2000-12-04 2002-09-10 Федеральный научно-производственный центр "Алтай" Способ получения жидких нитроэфиров и установка для его осуществления
DE102004007706A1 (de) * 2004-02-16 2005-08-25 Dynamit Nobel Gmbh Explosivstoff- Und Systemtechnik Verfahren zur Herstellung von flüssigen Nitratestern
ES2310953B1 (es) * 2006-04-28 2009-11-19 Baños 10, S.L. Dispositivo mezclador de un gas y un liquido o fluido.

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE183183C (en:Method) *

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US449687A (en) * 1891-04-07 maxim
US2254352A (en) * 1937-12-08 1941-09-02 Standard Oil Dev Co Process for the manufacture of alkyl nitrates
US2363834A (en) * 1942-06-30 1944-11-28 Hercules Powder Co Ltd Nitration apparatus

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE183183C (en:Method) *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1094172B (de) 1957-02-08 1960-12-01 J Meissner Fa Verfahren und Vorrichtung zur Herstellung von Sprengstoffen durch Nitrierung von fluessigen oder festen organischen Stoffen mittels Salpeter- oder Mischsaeure
EP0489211A1 (en) * 1988-08-15 1992-06-10 Nrm International Technologies C.V. Jet impingement reactor
WO2015022110A1 (de) 2013-08-15 2015-02-19 Josef Meissner Gmbh & Co. Kg Verfahren und vorrichtung zur entfernung von bei der herstellung von aliphatischen nitratestern anfallenden verunreinigungen
DE102013110952A1 (de) 2013-08-15 2015-02-19 Josef Meissner Gmbh & Co. Kg Verfahren und Vorrichtung zur Entfernung von bei der Herstellung von aliphatischen Nitratestern anfallenden Verunreinigungen
EA027521B1 (ru) * 2013-08-15 2017-08-31 Йозеф Майсснер Гмбх Унд Ко. Кг Способ и аппарат для удаления загрязняющих примесей, возникающих в процессе производства сложных алифатических азотно-кислых эфиров
US10513486B1 (en) 2013-08-15 2019-12-24 Josef Meissner Gmbh & Co. Kg Method and device for removing contaminants arising during the production of aliphatic nitrate esters

Also Published As

Publication number Publication date
CH308265A (fr) 1955-07-15
BE515328A (en:Method) 1900-01-01
GB735888A (en) 1955-08-31
FR1065893A (fr) 1954-05-31
US2737522A (en) 1956-03-06

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