DE102004027623A1 - Verfahren zur Herstellung von Peroxodisulfaten in wässriger Lösung - Google Patents

Verfahren zur Herstellung von Peroxodisulfaten in wässriger Lösung Download PDF

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Publication number
DE102004027623A1
DE102004027623A1 DE102004027623A DE102004027623A DE102004027623A1 DE 102004027623 A1 DE102004027623 A1 DE 102004027623A1 DE 102004027623 A DE102004027623 A DE 102004027623A DE 102004027623 A DE102004027623 A DE 102004027623A DE 102004027623 A1 DE102004027623 A1 DE 102004027623A1
Authority
DE
Germany
Prior art keywords
electrodes
bipolar
diamond
coated
electrolysis
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE102004027623A
Other languages
German (de)
English (en)
Inventor
Wolfgang Dr. Thiele
Hans-Jürgen KRAMER
Hans-Jürgen Dr. Förster
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
United Initiators GmbH and Co KG
United Initiators Inc
Original Assignee
United Initiators GmbH and Co KG
United Initiators Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by United Initiators GmbH and Co KG, United Initiators Inc filed Critical United Initiators GmbH and Co KG
Priority to DE102004027623A priority Critical patent/DE102004027623A1/de
Priority to AT05756088T priority patent/ATE373118T1/de
Priority to PCT/EP2005/006008 priority patent/WO2005121408A2/de
Priority to BRPI0511816-6A priority patent/BRPI0511816B1/pt
Priority to DE502005001500T priority patent/DE502005001500D1/de
Priority to EP05756088A priority patent/EP1753894B1/de
Priority to JP2007513875A priority patent/JP4852037B2/ja
Priority to KR1020077000239A priority patent/KR20070042141A/ko
Priority to ES05756088T priority patent/ES2290917T3/es
Priority to US11/569,464 priority patent/US20070187254A1/en
Priority to CN200580018399A priority patent/CN100591805C/zh
Publication of DE102004027623A1 publication Critical patent/DE102004027623A1/de
Priority to US13/027,672 priority patent/US20110132771A1/en
Priority to US15/062,836 priority patent/US9840783B2/en
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/28—Per-compounds
    • C25B1/30—Peroxides
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/22—Inorganic acids
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00—Electrolytic production of inorganic compounds or non-metals
    • C25B1/01—Products
    • C25B1/28—Per-compounds
    • C25B1/29—Persulfates
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/02—Electrodes; Manufacture thereof not otherwise provided for characterised by shape or form
    • C25B11/036—Bipolar electrodes
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
    • C25B11/052—Electrodes comprising one or more electrocatalytic coatings on a substrate
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
    • C25B11/055—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the substrate or carrier material
    • C25B11/057—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the substrate or carrier material consisting of a single element or compound
    • C25B11/059—Silicon
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00—Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04—Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/051—Electrodes formed of electrocatalysts on a substrate or carrier
    • C25B11/073—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material
    • C25B11/075—Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of a single catalytic element or catalytic compound
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/17—Cells comprising dimensionally-stable non-movable electrodes; Assemblies of constructional parts thereof
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/70—Assemblies comprising two or more cells
    • C25B9/73—Assemblies comprising two or more cells of the filter-press type
    • C—CHEMISTRY; METALLURGY
    • C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00—Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/70—Assemblies comprising two or more cells
    • C25B9/73—Assemblies comprising two or more cells of the filter-press type
    • C25B9/75—Assemblies comprising two or more cells of the filter-press type having bipolar electrodes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
  • Electrodes For Compound Or Non-Metal Manufacture (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE102004027623A 2004-06-05 2004-06-05 Verfahren zur Herstellung von Peroxodisulfaten in wässriger Lösung Withdrawn DE102004027623A1 (de)

Priority Applications (13)

Application Number Priority Date Filing Date Title
DE102004027623A DE102004027623A1 (de) 2004-06-05 2004-06-05 Verfahren zur Herstellung von Peroxodisulfaten in wässriger Lösung
KR1020077000239A KR20070042141A (ko) 2004-06-05 2005-06-03 수용액에서 퍼옥소이황산염의 제조방법
ES05756088T ES2290917T3 (es) 2004-06-05 2005-06-03 Procedimiento para la preparacion de peroxodisulfatos en solucion acuosa.
BRPI0511816-6A BRPI0511816B1 (pt) 2004-06-05 2005-06-03 Processo para a produção de peroxodissulfatos em solução aquosa , e célula eletrolítica bipolar.
DE502005001500T DE502005001500D1 (de) 2004-06-05 2005-06-03 Verfahren zur herstellung von peroxodisulfaten in wässriger lösung
EP05756088A EP1753894B1 (de) 2004-06-05 2005-06-03 Verfahren zur herstellung von peroxodisulfaten in wässriger lösung
JP2007513875A JP4852037B2 (ja) 2004-06-05 2005-06-03 水溶液中でのペルオキソ二硫酸塩の製造方法
AT05756088T ATE373118T1 (de) 2004-06-05 2005-06-03 Verfahren zur herstellung von peroxodisulfaten in wässriger lösung
PCT/EP2005/006008 WO2005121408A2 (de) 2004-06-05 2005-06-03 Verfahren zur herstellung von peroxodisulfaten in wässriger lösung
US11/569,464 US20070187254A1 (en) 2004-06-05 2005-06-03 Method for producing peroxodisulfates in aqueous solution
CN200580018399A CN100591805C (zh) 2004-06-05 2005-06-03 在水溶液中制备过氧二硫酸盐的方法
US13/027,672 US20110132771A1 (en) 2004-06-05 2011-02-15 Method for producing peroxodisulfates in aqueous solution
US15/062,836 US9840783B2 (en) 2004-06-05 2016-03-07 Method for producing peroxodisulfates in aqueous solution

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102004027623A DE102004027623A1 (de) 2004-06-05 2004-06-05 Verfahren zur Herstellung von Peroxodisulfaten in wässriger Lösung

Publications (1)

Publication Number Publication Date
DE102004027623A1 true DE102004027623A1 (de) 2005-12-22

Family

ID=35429257

Family Applications (2)

Application Number Title Priority Date Filing Date
DE102004027623A Withdrawn DE102004027623A1 (de) 2004-06-05 2004-06-05 Verfahren zur Herstellung von Peroxodisulfaten in wässriger Lösung
DE502005001500T Expired - Lifetime DE502005001500D1 (de) 2004-06-05 2005-06-03 Verfahren zur herstellung von peroxodisulfaten in wässriger lösung

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE502005001500T Expired - Lifetime DE502005001500D1 (de) 2004-06-05 2005-06-03 Verfahren zur herstellung von peroxodisulfaten in wässriger lösung

Country Status (10)

Country Link
US (3) US20070187254A1 (https=)
EP (1) EP1753894B1 (https=)
JP (1) JP4852037B2 (https=)
KR (1) KR20070042141A (https=)
CN (1) CN100591805C (https=)
AT (1) ATE373118T1 (https=)
BR (1) BRPI0511816B1 (https=)
DE (2) DE102004027623A1 (https=)
ES (1) ES2290917T3 (https=)
WO (1) WO2005121408A2 (https=)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009004155A1 (de) * 2009-01-09 2010-07-15 Eilenburger Elektrolyse- Und Umwelttechnik Gmbh Verfahren und Vorrichtung zum Regenerieren von Peroxodisulfat-Beizlösungen
DE102021115850A1 (de) 2021-06-18 2022-12-22 Technische Universität Bergakademie Freiberg, Körperschaft des öffentlichen Rechts Verfahren zur Laugung metallhaltiger Erze mittels elektrochemisch hergestellter Laugungslösung

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5106523B2 (ja) * 2009-12-16 2012-12-26 株式会社東芝 エッチング処理方法、微細構造体の製造方法、およびエッチング処理装置
JP5751884B2 (ja) * 2011-03-29 2015-07-22 森永乳業株式会社 複極式電解槽
EP2697730A4 (en) * 2011-04-15 2015-04-15 Advanced Diamond Technologies Inc ELECTROCHEMICAL SYSTEM AND METHOD FOR PROPORTION OF OXIDIZERS AT HIGH CURRENT DENSITY
EP2546389A1 (de) 2011-07-14 2013-01-16 United Initiators GmbH & Co. KG Verfahren zur Herstellung eines Ammonium- oder Akalimetallperosodisulfats im ungeteilten Elektrolyseraum
PL2872673T3 (pl) 2012-07-13 2020-12-28 United Initiators Gmbh Niepodzielone ogniwo elektrolityczne i jego zastosowanie
TW201406998A (zh) * 2012-07-13 2014-02-16 United Initiators Gmbh & Co Kg 無分隔電解槽及其用途
CN104487615B (zh) * 2012-07-13 2017-08-25 联合引发剂有限责任两合公司 不分离的电解槽及其应用
EP4630590A1 (en) * 2022-11-29 2025-10-15 Ecox Global Pte Ltd Method and process for electrochemical oxidation

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE20005681U1 (de) * 2000-03-27 2000-06-21 Eilenburger Elektrolyse- und Umwelttechnik GmbH, 04838 Eilenburg Elektrolysezelle zur Desinfektion von Wässern
FR2790268B1 (fr) * 1999-02-25 2001-05-11 Suisse Electronique Microtech Cellule d'electrolyse a electrode bipolaire comportant du diamant
DE19948184C2 (de) * 1999-10-06 2001-08-09 Fraunhofer Ges Forschung Elektrochemische Herstellung von Peroxo-dischwefelsäure unter Einsatz von diamantbeschichteten Elektroden
DE10019683A1 (de) * 2000-04-20 2001-10-25 Degussa Verfahren zur Herstellung von Alkalimetall- und Ammoniumperoxodisulfat
EP1229149A1 (fr) * 2001-01-31 2002-08-07 CSEM Centre Suisse d'Electronique et de Microtechnique SA Electrode de grandes dimensions
EP1254972A1 (fr) * 2001-05-01 2002-11-06 CSEM Centre Suisse d'Electronique et de Microtechnique SA Cellule electrochimique modulaire

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3926770A (en) * 1972-06-08 1975-12-16 Ppg Industries Inc Electrolytic cell having silicon bipolar electrodes
TW364024B (en) * 1995-08-17 1999-07-11 Eilenburger Elektrolyse & Umwelttechnik Gmbh Process for the combined electrochemical preparation of sodium peroxodisulfate and sodium hydroxide solution
US5681445A (en) * 1995-12-21 1997-10-28 Hydro-Quebec Modified surface bipolar electrode
JP3554630B2 (ja) * 1996-04-11 2004-08-18 ペルメレック電極株式会社 耐久性を有する電解用電極
JPH1161472A (ja) * 1997-08-08 1999-03-05 Shinko Pantec Co Ltd 水素酸素発生装置の電解セルおよびその電極板
DE19911746A1 (de) * 1999-03-16 2000-09-21 Basf Ag Diamantelektroden
DE10015209A1 (de) * 2000-03-27 2001-10-11 Eilenburger Elektrolyse & Umwelttechnik Gmbh Verfahren und Vorrichtung zur elektrochemischen Desinfektion von Wässern
JP2004099914A (ja) * 2002-09-04 2004-04-02 Permelec Electrode Ltd ペルオキソ二硫酸塩の製造方法

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2790268B1 (fr) * 1999-02-25 2001-05-11 Suisse Electronique Microtech Cellule d'electrolyse a electrode bipolaire comportant du diamant
DE19948184C2 (de) * 1999-10-06 2001-08-09 Fraunhofer Ges Forschung Elektrochemische Herstellung von Peroxo-dischwefelsäure unter Einsatz von diamantbeschichteten Elektroden
DE20005681U1 (de) * 2000-03-27 2000-06-21 Eilenburger Elektrolyse- und Umwelttechnik GmbH, 04838 Eilenburg Elektrolysezelle zur Desinfektion von Wässern
DE10019683A1 (de) * 2000-04-20 2001-10-25 Degussa Verfahren zur Herstellung von Alkalimetall- und Ammoniumperoxodisulfat
EP1229149A1 (fr) * 2001-01-31 2002-08-07 CSEM Centre Suisse d'Electronique et de Microtechnique SA Electrode de grandes dimensions
EP1254972A1 (fr) * 2001-05-01 2002-11-06 CSEM Centre Suisse d'Electronique et de Microtechnique SA Cellule electrochimique modulaire

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009004155A1 (de) * 2009-01-09 2010-07-15 Eilenburger Elektrolyse- Und Umwelttechnik Gmbh Verfahren und Vorrichtung zum Regenerieren von Peroxodisulfat-Beizlösungen
DE102021115850A1 (de) 2021-06-18 2022-12-22 Technische Universität Bergakademie Freiberg, Körperschaft des öffentlichen Rechts Verfahren zur Laugung metallhaltiger Erze mittels elektrochemisch hergestellter Laugungslösung
DE102021115850B4 (de) 2021-06-18 2022-12-29 Technische Universität Bergakademie Freiberg, Körperschaft des öffentlichen Rechts Verfahren zur Laugung metallhaltiger Erze mittels elektrochemisch hergestellter Laugungslösung

Also Published As

Publication number Publication date
WO2005121408A2 (de) 2005-12-22
US20110132771A1 (en) 2011-06-09
CN100591805C (zh) 2010-02-24
WO2005121408A3 (de) 2006-06-08
KR20070042141A (ko) 2007-04-20
CN1965107A (zh) 2007-05-16
US20070187254A1 (en) 2007-08-16
ES2290917T3 (es) 2008-02-16
US9840783B2 (en) 2017-12-12
EP1753894B1 (de) 2007-09-12
BRPI0511816A (pt) 2007-12-26
JP2008501856A (ja) 2008-01-24
BRPI0511816B1 (pt) 2015-07-28
EP1753894A2 (de) 2007-02-21
ATE373118T1 (de) 2007-09-15
JP4852037B2 (ja) 2012-01-11
DE502005001500D1 (de) 2007-10-25
US20160186338A1 (en) 2016-06-30

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