CZ2000593A3 - Způsob výroby glufosinátů a meziprodukty pro jejich výrobu - Google Patents

Způsob výroby glufosinátů a meziprodukty pro jejich výrobu Download PDF

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Publication number
CZ2000593A3
CZ2000593A3 CZ2000593A CZ2000593A CZ2000593A3 CZ 2000593 A3 CZ2000593 A3 CZ 2000593A3 CZ 2000593 A CZ2000593 A CZ 2000593A CZ 2000593 A CZ2000593 A CZ 2000593A CZ 2000593 A3 CZ2000593 A3 CZ 2000593A3
Authority
CZ
Czechia
Prior art keywords
formula
compounds
salts
optionally
ammonia
Prior art date
Application number
CZ2000593A
Other languages
Czech (cs)
English (en)
Inventor
Lothar Willms
Original Assignee
Hoechst Schering Agrevo Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst Schering Agrevo Gmbh filed Critical Hoechst Schering Agrevo Gmbh
Publication of CZ2000593A3 publication Critical patent/CZ2000593A3/cs

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Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
    • A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
    • A01N57/12—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing acyclic or cycloaliphatic radicals
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6571—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
    • C07F9/657163—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms the ring phosphorus atom being bound to at least one carbon atom
    • C07F9/657172—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms the ring phosphorus atom being bound to at least one carbon atom the ring phosphorus atom and one oxygen atom being part of a (thio)phosphinic acid ester: (X = O, S)
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/301—Acyclic saturated acids which can have further substituents on alkyl
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
    • C07F9/32—Esters thereof
    • C07F9/3205—Esters thereof the acid moiety containing a substituent or a structure which is considered as characteristic
    • C07F9/3211—Esters of acyclic saturated acids which can have further substituents on alkyl

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Plant Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CZ2000593A 1997-08-20 1998-08-08 Způsob výroby glufosinátů a meziprodukty pro jejich výrobu CZ2000593A3 (cs)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19736125A DE19736125A1 (de) 1997-08-20 1997-08-20 Verfahren zur Herstellung von Glufosinate und phosphorhaltige alpha-Aminonitrile als Zwischenprodukte

Publications (1)

Publication Number Publication Date
CZ2000593A3 true CZ2000593A3 (cs) 2000-06-14

Family

ID=7839559

Family Applications (1)

Application Number Title Priority Date Filing Date
CZ2000593A CZ2000593A3 (cs) 1997-08-20 1998-08-08 Způsob výroby glufosinátů a meziprodukty pro jejich výrobu

Country Status (27)

Country Link
US (1) US6359162B1 (cg-RX-API-DMAC7.html)
EP (1) EP1005475B1 (cg-RX-API-DMAC7.html)
JP (1) JP4519316B2 (cg-RX-API-DMAC7.html)
KR (1) KR100674326B1 (cg-RX-API-DMAC7.html)
CN (1) CN1261442C (cg-RX-API-DMAC7.html)
AR (1) AR015932A1 (cg-RX-API-DMAC7.html)
AT (1) ATE258180T1 (cg-RX-API-DMAC7.html)
AU (1) AU756471B2 (cg-RX-API-DMAC7.html)
BR (1) BR9811971B1 (cg-RX-API-DMAC7.html)
CA (1) CA2301181C (cg-RX-API-DMAC7.html)
CO (1) CO5031316A1 (cg-RX-API-DMAC7.html)
CZ (1) CZ2000593A3 (cg-RX-API-DMAC7.html)
DE (2) DE19736125A1 (cg-RX-API-DMAC7.html)
DK (1) DK1005475T3 (cg-RX-API-DMAC7.html)
ES (1) ES2214727T3 (cg-RX-API-DMAC7.html)
HU (1) HUP0003501A3 (cg-RX-API-DMAC7.html)
IL (1) IL134633A0 (cg-RX-API-DMAC7.html)
MY (1) MY132853A (cg-RX-API-DMAC7.html)
PH (1) PH11998002119A1 (cg-RX-API-DMAC7.html)
PL (1) PL191587B1 (cg-RX-API-DMAC7.html)
PT (1) PT1005475E (cg-RX-API-DMAC7.html)
RU (1) RU2275376C2 (cg-RX-API-DMAC7.html)
TR (1) TR200000456T2 (cg-RX-API-DMAC7.html)
TW (1) TW530063B (cg-RX-API-DMAC7.html)
UA (1) UA66806C2 (cg-RX-API-DMAC7.html)
WO (1) WO1999009039A1 (cg-RX-API-DMAC7.html)
ZA (1) ZA987465B (cg-RX-API-DMAC7.html)

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PL373673A1 (en) * 2002-03-21 2005-09-05 Schering Aktiengesellschaft Plasma carboxypeptidase b inhibitors
JP5336851B2 (ja) * 2006-09-20 2013-11-06 Ｍｅｉｊｉ Ｓｅｉｋａファルマ株式会社 リン含有α−アミノ酸の製造法およびその製造中間体
BR112012026205A2 (pt) 2010-04-14 2015-11-03 Strategic Enzyme Applic Inc processo para produção enzimática de um produto de fosfinotricina ou um precursor do mesmo
CN102372738B (zh) * 2010-08-14 2017-11-10 武汉工程大学 Lj反应在制备维蒂希试剂和草铵膦中的应用
AR088189A1 (es) 2011-09-30 2014-05-14 Meiji Seika Pharma Co Ltd Metodo para producir acido libre de glufosinato p
CN102372739B (zh) * 2011-12-05 2017-06-16 河北威远生化农药有限公司 一种草铵膦的合成方法
CN102399239A (zh) * 2011-12-27 2012-04-04 江苏优士化学有限公司 一种草铵膦及类似物的合成方法
CN102399240A (zh) * 2011-12-27 2012-04-04 江苏优士化学有限公司 一种改进的草铵膦及类似物的合成方法
CN103183707B (zh) * 2011-12-30 2016-06-15 中化蓝天集团有限公司 一种草胺膦的制备方法
CN102584893B (zh) * 2012-02-07 2015-03-04 浙江工业大学 一种草铵膦的制备方法
CN103374030B (zh) * 2012-04-13 2016-03-23 浙江新安化工集团股份有限公司 一种制备草铵膦的方法及其中间体的制备方法
CN103483379A (zh) * 2013-09-26 2014-01-01 江苏辉丰农化股份有限公司 一种草铵膦酸的制备方法
CN106459110A (zh) 2014-05-13 2017-02-22 拜耳作物科学股份公司 制备含磷羟腈的方法
CN104558033B (zh) * 2014-12-19 2016-05-18 浙江工业大学 一种l-草铵膦-n-羧酸酐及其制备和应用
US10334854B2 (en) 2015-04-27 2019-07-02 Bayer Cropscience Aktiengesellschaft Herbicide combinations comprising glufosinate and indaziflam
EP3344635B1 (de) 2015-09-02 2019-08-07 Basf Se Verfahren zur herstellung von phosphorhaltigen cyanhydrinestern
MX2018002726A (es) 2015-09-02 2018-04-13 Bayer Cropscience Ag Proceso para producir esteres de cianhidrina que contienen fosforo.
US10316048B2 (en) 2015-09-02 2019-06-11 Bayer Cropscience Aktiengesellschaft Process for producing phosphorus-containing cyanohydrin esters
MX2018002731A (es) 2015-09-02 2018-04-13 Bayer Cropscience Ag Proceso para la elaboracion de esteres de cianohidrina que contienen fosforo.
CN108137629B (zh) 2015-09-29 2020-09-01 拜耳作物科学股份公司 制备亚膦酸酯的方法
CN107236001A (zh) * 2016-04-06 2017-10-10 四川省乐山市福华通达农药科技有限公司 一种膦醛的合成方法
CN107417721B (zh) * 2016-05-24 2019-05-28 四川福思达生物技术开发有限责任公司 一种氢氰酸加成工艺
WO2018108794A1 (de) 2016-12-15 2018-06-21 Bayer Cropscience Aktiengesellschaft Verfahren zur herstellung von d-glufosinat oder dessen salzen unter verwendung von ephedrin
WO2018108797A1 (de) 2016-12-15 2018-06-21 Bayer Cropscience Aktiengesellschaft Verfahren zur herstellung von l-glufosinat oder dessen salzen unter verwendung von ephedrin
EP3392237B1 (de) 2017-04-21 2019-10-02 Evonik Degussa GmbH Verfahren zur herstellung von acroleincyanhydrinen
CA3070104C (en) * 2017-07-18 2023-08-08 Agrimetis, Llc Methods for the purification of l-glufosinate and crystalline l-glufosinate ammonium forms
JP7296936B2 (ja) 2017-07-21 2023-06-23 ビーエーエスエフ ソシエタス・ヨーロピア ｎ－ブチル（３－アミノ－３－シアノプロピル）メチルホスフィネート及び（３－アミノ－３－シアノプロピル）メチルホスフィン酸アンモニウム塩の混合物をもたらすための３－［ｎ－ブトキシ（メチル）ホスホリル］－１－シアノプロピルアセテートの反応による、グルホシネートの製造
CN111479816B (zh) 2017-12-19 2023-10-27 巴斯夫欧洲公司 制备含磷α-氨基腈的方法
CN109134534B (zh) * 2018-08-08 2020-09-08 江苏好收成韦恩农化股份有限公司 一种3,3-二烷氧基丙基甲基膦酸酯简易制备方法
KR102131687B1 (ko) * 2018-09-10 2020-07-08 주식회사 휴런 파킨슨 병 진단 장치 및 방법
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CN111662326B (zh) * 2019-03-05 2023-03-24 利尔化学股份有限公司 一种制备l-草铵膦的方法
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CN110003269B (zh) * 2019-04-29 2022-04-05 利尔化学股份有限公司 低能耗生产草铵膦的方法
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CN112898338A (zh) * 2019-12-04 2021-06-04 利尔化学股份有限公司 草铵膦中间体及草铵膦的制备方法
CN111659330B (zh) * 2020-04-23 2021-05-07 河北威远生物化工有限公司 一种连续化生产草铵膦的工艺与设备
CN112358499A (zh) * 2020-11-12 2021-02-12 江苏春江润田农化有限公司 一种草铵膦的合成方法
WO2022207543A1 (en) 2021-04-01 2022-10-06 Evonik Operations Gmbh Enzymatic method for producing l-glufosinate and its phosphoesters
EP4105335A1 (en) 2021-06-16 2022-12-21 Evonik Operations GmbH Enzymatic method for the production of l-glufosinate p-alkyl esters
JP7503214B2 (ja) * 2021-07-20 2024-06-19 リアー ケミカル カンパニー リミテッド グルホシネート又はその類似体を調製するための方法
EP4151643A1 (en) 2021-09-16 2023-03-22 Evonik Operations GmbH Improved process for production of phosphoesters of glufosinate precursors
CN114163472B (zh) * 2021-11-27 2024-08-09 永农生物科学有限公司 醇溶剂下合成α-氨基腈的方法及草铵膦的合成方法
MX2024011087A (es) 2022-03-14 2024-09-23 Evonik Operations Gmbh Metodo enzimatico para la produccion de p-esteres de l-glufosinato.
CN116789695B (zh) * 2022-11-17 2024-03-29 永农生物科学有限公司 一种草铵膦的制备方法
KR20250152064A (ko) 2023-02-23 2025-10-22 바스프 에스이 시안히드린 또는 시안히드린 유도체로부터 l-글루포시네이트의 제조 방법
AR132932A1 (es) 2023-06-13 2025-08-13 Basf Se Síntesis de glufosinato mediante un proceso basado en amidasa

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Also Published As

Publication number Publication date
IL134633A0 (en) 2001-04-30
AU756471B2 (en) 2003-01-16
CA2301181C (en) 2008-08-05
PT1005475E (pt) 2004-06-30
US6359162B1 (en) 2002-03-19
EP1005475A1 (de) 2000-06-07
UA66806C2 (uk) 2004-06-15
AR015932A1 (es) 2001-05-30
ES2214727T3 (es) 2004-09-16
KR20010023069A (ko) 2001-03-26
JP4519316B2 (ja) 2010-08-04
PL338855A1 (en) 2000-11-20
KR100674326B1 (ko) 2007-01-24
BR9811971A (pt) 2000-08-15
AU9259898A (en) 1999-03-08
TW530063B (en) 2003-05-01
ATE258180T1 (de) 2004-02-15
DE59810636D1 (de) 2004-02-26
WO1999009039A1 (de) 1999-02-25
PL191587B1 (pl) 2006-06-30
JP2001515084A (ja) 2001-09-18
CA2301181A1 (en) 1999-02-25
CO5031316A1 (es) 2001-04-27
TR200000456T2 (tr) 2000-07-21
PH11998002119A1 (en) 2003-10-10
ZA987465B (en) 1999-02-22
MY132853A (en) 2007-10-31
DE19736125A1 (de) 1999-02-25
HUP0003501A3 (en) 2002-01-28
BR9811971B1 (pt) 2010-12-28
RU2275376C2 (ru) 2006-04-27
DK1005475T3 (da) 2004-05-17
CN1267305A (zh) 2000-09-20
EP1005475B1 (de) 2004-01-21
HUP0003501A2 (en) 2001-03-28
CN1261442C (zh) 2006-06-28

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PD00 Pending as of 2000-06-30 in czech republic