CS240956B2 - Preparation method of pearl-lustrous pigments - Google Patents
Preparation method of pearl-lustrous pigments Download PDFInfo
- Publication number
- CS240956B2 CS240956B2 CS832038A CS203883A CS240956B2 CS 240956 B2 CS240956 B2 CS 240956B2 CS 832038 A CS832038 A CS 832038A CS 203883 A CS203883 A CS 203883A CS 240956 B2 CS240956 B2 CS 240956B2
- Authority
- CS
- Czechoslovakia
- Prior art keywords
- pigment
- titanium
- calcined
- dried
- washed
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
- C09C1/0021—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings comprising a core coated with only one layer having a high or low refractive index
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/0015—Pigments exhibiting interference colours, e.g. transparent platelets of appropriate thinness or flaky substrates, e.g. mica, bearing appropriate thin transparent coatings
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
- C09C2200/10—Interference pigments characterized by the core material
- C09C2200/102—Interference pigments characterized by the core material the core consisting of glass or silicate material like mica or clays, e.g. kaolin
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C2200/00—Compositional and structural details of pigments exhibiting interference colours
- C09C2200/30—Interference pigments characterised by the thickness of the core or layers thereon or by the total thickness of the final pigment particle
- C09C2200/301—Thickness of the core
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C2220/00—Methods of preparing the interference pigments
- C09C2220/10—Wet methods, e.g. co-precipitation
- C09C2220/103—Wet methods, e.g. co-precipitation comprising a drying or calcination step after applying each layer
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S106/00—Compositions: coating or plastic
- Y10S106/03—Mica
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Cosmetics (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19823211602 DE3211602A1 (de) | 1982-03-30 | 1982-03-30 | Verfahren zur herstellung von perlglanzpigmenten mit verbesserten glanzeigenschaften |
Publications (2)
Publication Number | Publication Date |
---|---|
CS203883A2 CS203883A2 (en) | 1985-06-13 |
CS240956B2 true CS240956B2 (en) | 1986-03-13 |
Family
ID=6159642
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CS832038A CS240956B2 (en) | 1982-03-30 | 1983-03-24 | Preparation method of pearl-lustrous pigments |
Country Status (6)
Country | Link |
---|---|
US (1) | US4537636A (fr) |
EP (1) | EP0090260B1 (fr) |
JP (1) | JPS58180561A (fr) |
BR (1) | BR8301636A (fr) |
CS (1) | CS240956B2 (fr) |
DE (2) | DE3211602A1 (fr) |
Families Citing this family (88)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4623396A (en) * | 1983-09-14 | 1986-11-18 | Shiseido Company Ltd. | Titanium-mica composite material |
JPS61166501A (ja) * | 1985-01-18 | 1986-07-28 | Yoshio Morita | 水溶液反応による二酸化チタン光学薄膜の形成方法 |
US5116664A (en) * | 1988-02-09 | 1992-05-26 | Shiseido Company Ltd. | Titanium-mica composite material |
JP2813060B2 (ja) * | 1990-11-28 | 1998-10-22 | 株式会社曙ブレーキ中央技術研究所 | ノンアスベスト摩擦材 |
DE4120921A1 (de) | 1991-06-25 | 1993-01-07 | Merck Patent Gmbh | Oberflaechenmodifizierte plaettchenfoermige substrate mit verbessertem absetz- und aufruehrverhalten |
JPH0543816A (ja) * | 1991-08-19 | 1993-02-23 | Dainichiseika Color & Chem Mfg Co Ltd | 雲母チタン顔料の製造方法 |
JP3073836B2 (ja) * | 1992-07-02 | 2000-08-07 | メルク・ジヤパン株式会社 | 耐変色性を有する真珠光沢顔料およびその製造方法 |
AU7726494A (en) * | 1993-09-14 | 1995-04-03 | Heatshield Technologies, Inc. | Photon-diffusive materials as heat resistant coatings |
US5376698A (en) * | 1993-09-21 | 1994-12-27 | The Mearl Corporation | Polyolefin compositions containing coated mica particles to prevent yellowing and methods therefore |
JP3542388B2 (ja) * | 1994-10-11 | 2004-07-14 | 株式会社資生堂 | 低次酸化チタン含有顔料及びその製造方法 |
DE4443048A1 (de) | 1994-12-05 | 1996-06-13 | Merck Patent Gmbh | Effektpulverlacke |
US5693134A (en) | 1994-12-29 | 1997-12-02 | Merck Patent Gesellschaft Mit Beschrankter Haftung | Gray interference pigment and process for producing the same |
DE19522397A1 (de) * | 1995-06-23 | 1997-01-02 | Merck Patent Gmbh | Lasermarkierbare Kunststoffe |
US6290766B1 (en) * | 1999-02-24 | 2001-09-18 | Engelhard Corporation | Lustrous interference pigments with black absorption color |
DE10046152A1 (de) | 2000-09-15 | 2002-03-28 | Merck Patent Gmbh | Pigmentpräparation in Granulatform |
DE19951869A1 (de) | 1999-10-28 | 2001-05-03 | Merck Patent Gmbh | Farbstarke Interferenzpigmente |
DE19951871A1 (de) | 1999-10-28 | 2001-05-03 | Merck Patent Gmbh | Farbstarke Interferenzpigmente |
US6451102B1 (en) | 2000-05-04 | 2002-09-17 | Merck Patent Gmbh | Pigment modification improving handling characteristics |
DE10034972A1 (de) | 2000-07-19 | 2002-01-31 | Merck Patent Gmbh | Verfahren zur Herstellung eines Pulverlacks, ein Pulverlack sowie die Verwendung von Effektpigmenten |
DE10137831A1 (de) | 2001-08-02 | 2003-02-13 | Merck Patent Gmbh | Mehrschichtige Interferenzpigmente |
CA2494077C (fr) * | 2002-07-31 | 2011-04-12 | Power Medical Interventions, Inc. | Dispositif introducteur pour orifices |
BR0313832A (pt) | 2002-08-30 | 2005-07-05 | Ciba Sc Holding Ag | Pigmentos de brilho coloridos tendo pelo menos um revestimento de siox, com x=0,03 a 0,95, para uso em formulações cosméticas e de cuidado pessoal |
AU2003292216A1 (en) | 2002-12-17 | 2004-07-09 | Merck Patent Gmbh | Silvery white interference pigments having a high luster and based on transparent substrate laminae |
DE10310736A1 (de) | 2003-03-10 | 2004-09-23 | Merck Patent Gmbh | Interferenzpigmente mit Körperfarbe |
DE102004035769A1 (de) | 2004-07-27 | 2006-03-23 | Merck Patent Gmbh | Mehrschichtige Interferenzpigmente |
US7943194B2 (en) | 2004-08-23 | 2011-05-17 | Basf Se | Process for preparing flake-form pigments based on aluminum and on Sioz(Z=0.7-2.0) comprising forming a layer of separating agent |
DE102004057918A1 (de) | 2004-11-30 | 2006-06-01 | Merck Patent Gmbh | Laserkennzeichnung von Wertdokumenten |
DE102005002124A1 (de) | 2005-01-17 | 2006-07-27 | Merck Patent Gmbh | Farbstarke rote Effektpigmente |
DE102005001997A1 (de) | 2005-01-17 | 2006-07-20 | Merck Patent Gmbh | Effektpigmente mit starkem Farbtop |
DE102006027025A1 (de) | 2006-06-08 | 2007-12-13 | Merck Patent Gmbh | Silberweiße-Effektpigmente |
KR20090079194A (ko) * | 2006-09-05 | 2009-07-21 | 후지필름 헌트 케미칼스 유.에스.에이., 아이엔씨. | 유기 흡수 촉진 첨가제를 함유하는 레이저-마킹용 코팅 및 레이저-마킹용 물질 형성용 조성물 |
JP5535425B2 (ja) * | 2006-12-22 | 2014-07-02 | メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフツング | フィラー、その製造方法、および化粧料 |
AU2007337324B2 (en) * | 2006-12-22 | 2013-03-14 | Asahi Glass Company, Limited | Fluororesin film and method for producing the same |
DE102007010986A1 (de) | 2007-03-05 | 2008-09-11 | Merck Patent Gmbh | Übergangsmetallhaltige Effektpigmente |
ATE459328T1 (de) | 2007-04-05 | 2010-03-15 | Eckart Gmbh | Kosmetische zusammensetzungen enthaltend perlglanzpigmente |
ATE432964T1 (de) | 2007-04-05 | 2009-06-15 | Eckart Gmbh | Effektpigmente mit einem substrat aus glasplättchen |
CN101688067B (zh) | 2007-07-12 | 2013-12-11 | 巴斯夫欧洲公司 | 基于珍珠岩薄片的干扰颜料 |
DE102007058601A1 (de) | 2007-12-04 | 2009-06-10 | Merck Patent Gmbh | Sicherheitspigment |
ATE503806T1 (de) | 2007-12-17 | 2011-04-15 | Merck Patent Gmbh | Füllstoffpigmente |
KR20100114029A (ko) | 2007-12-19 | 2010-10-22 | 메르크 파텐트 게엠베하 | 전기전도성 코어를 갖는, 강렬한 색채를 갖고/갖거나 광변성인 안료 |
KR101634405B1 (ko) | 2007-12-19 | 2016-06-28 | 메르크 파텐트 게엠베하 | 높은 전기전도성의 광변성 안료 |
DE102008025277A1 (de) | 2008-05-27 | 2009-12-03 | Merck Patent Gmbh | Glaszusammensetzung |
DE102008050924A1 (de) | 2008-10-10 | 2010-04-15 | Merck Patent Gmbh | Pigmente |
DE102009020208A1 (de) | 2009-05-07 | 2010-11-11 | Merck Patent Gmbh | Verfahren zum Codieren von Produkten |
DE102009023157A1 (de) | 2009-05-29 | 2010-12-02 | Merck Patent Gmbh | Beschichtete Partikel |
DE102009023158A1 (de) | 2009-05-29 | 2010-12-02 | Merck Patent Gmbh | Beschichtete Partikel und deren Verwendung |
US8936799B2 (en) | 2009-10-28 | 2015-01-20 | Basf Se | Pigments with improved sparkling effect |
DE102009051171A1 (de) | 2009-10-29 | 2011-05-05 | Merck Patent Gmbh | Pigmente |
KR101859238B1 (ko) | 2010-02-04 | 2018-05-17 | 메르크 파텐트 게엠베하 | 효과 안료 |
WO2011095447A2 (fr) | 2010-02-04 | 2011-08-11 | Basf Se | Compositions de pigment possédant un effet luisant amélioré |
DE102010049375A1 (de) | 2010-10-26 | 2012-04-26 | Merck Patent Gmbh | Pigmente |
KR101906619B1 (ko) | 2010-12-09 | 2018-10-10 | 메르크 파텐트 게엠베하 | 자성 안료 |
WO2012076110A1 (fr) | 2010-12-09 | 2012-06-14 | Merck Patent Gmbh | Pigments noirs brillants |
DE102011103425A1 (de) | 2011-06-07 | 2012-12-13 | Merck Patent Gmbh | Wellenlängenselektiv reflektierende Beschichtung |
EP2607432A1 (fr) | 2011-12-21 | 2013-06-26 | Merck Patent GmbH | Pigments à effets basés sur des substrats avec un facteur de forme circulaire de 1.2-2 |
DE102011121804A1 (de) | 2011-12-21 | 2013-06-27 | Merck Patent Gmbh | Effektpigmente |
DE102012000887A1 (de) | 2012-01-19 | 2013-07-25 | Merck Patent Gmbh | Effektpigmente |
US8876965B2 (en) | 2012-05-09 | 2014-11-04 | J.M. Huber Corporation | Blended opacifier for coatings and polymeric matrices |
DE102012017608A1 (de) | 2012-09-06 | 2014-05-08 | Merck Patent Gmbh | Goldpigment |
DE102012020392A1 (de) | 2012-10-18 | 2014-04-24 | Merck Patent Gmbh | Pigmente |
US8585818B1 (en) * | 2013-03-14 | 2013-11-19 | Basf Se | Coated perlite flakes |
EP2799398B1 (fr) | 2013-04-30 | 2018-05-23 | Merck Patent GmbH | Flocons d'alumine alpha |
EP3395763B1 (fr) | 2013-04-30 | 2020-06-17 | Merck Patent GmbH | Utilisations de flocons d'alumine |
WO2014202180A1 (fr) | 2013-06-17 | 2014-12-24 | Merck Patent Gmbh | Pigments d'interférence optiquement variables et transparents, aux propriétés électriquement semi-conductrices |
JP6608813B2 (ja) | 2013-06-17 | 2019-11-20 | メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフツング | 高い色濃度を有する透明な電気的半導体性干渉顔料 |
DE102013012023A1 (de) | 2013-07-19 | 2015-01-22 | Merck Patent Gmbh | Pigmentgemisch |
DE102014003975A1 (de) | 2014-03-20 | 2015-10-08 | Merck Patent Gmbh | Effektpigmente |
DE102014018275A1 (de) | 2014-12-12 | 2016-06-16 | Merck Patent Gmbh | Nichtmetallische Pigmente mit metallischen Eigenschaften |
DE102014018276A1 (de) | 2014-12-12 | 2016-06-16 | Merck Patent Gmbh | Elektrisch leitfähige, farbige Interferenzpigmente |
EP3081601A1 (fr) * | 2015-04-15 | 2016-10-19 | Schlenk Metallic Pigments GmbH | Pigments nacrés comprenannt des substrats monolithiques |
DE102015013400A1 (de) | 2015-10-19 | 2017-04-20 | Merck Patent Gmbh | Pigment/Fritten-Gemisch |
DE102016000054A1 (de) | 2016-01-05 | 2017-07-06 | Merck Patent Gmbh | Oberflächenfärbung von Lebensmitteln |
KR20170099369A (ko) | 2016-02-23 | 2017-08-31 | 메르크 파텐트 게엠베하 | 효과 안료 |
DE102016004164A1 (de) | 2016-04-11 | 2017-10-12 | Merck Patent Gmbh | Pigmentgemisch |
DE102017002554A1 (de) | 2017-03-17 | 2018-09-20 | Merck Patent Gmbh | Effektpigmente |
DE102017011800A1 (de) | 2017-12-20 | 2019-06-27 | Merck Patent Gmbh | Effektpigmente |
EP3517579B1 (fr) | 2018-01-23 | 2022-10-26 | Merck Patent GmbH | Mélange de pigments interférentiels rouge, bleu et vert |
JP2021519846A (ja) | 2018-04-04 | 2021-08-12 | アルタナ アーゲー | 着色されたヘクトライトを基礎とするエフェクト顔料および被覆された着色されたヘクトライトならびにそれらの製造 |
EP3564200A1 (fr) | 2018-05-04 | 2019-11-06 | Merck Patent GmbH | Couleurs céramiques |
EP3564197A1 (fr) | 2018-05-04 | 2019-11-06 | Merck Patent GmbH | Couleurs céramiques |
EP3564202A1 (fr) | 2018-05-04 | 2019-11-06 | Merck Patent GmbH | Couleurs céramiques |
DE102019003072A1 (de) | 2019-04-30 | 2020-11-05 | Merck Patent Gmbh | Effektpigmente |
DE102019003073A1 (de) | 2019-04-30 | 2020-11-05 | Merck Patent Gmbh | Pigment/Fritten-Gemisch |
TW202124596A (zh) | 2019-09-20 | 2021-07-01 | 德商麥克專利有限公司 | 顏料 |
DE102019006869A1 (de) | 2019-10-02 | 2021-04-08 | Merck Patent Gmbh | Interferenzpigmente |
EP3967491A1 (fr) | 2020-09-15 | 2022-03-16 | Röhm GmbH | Feuilles réfléchissant la chaleur présentant de meilleures propriétés mécaniques et une haute résistance aux intempéries |
EP3974395A1 (fr) | 2020-09-25 | 2022-03-30 | Merck Patent GmbH | Mélange de pigment et de frittes |
EP4389828A1 (fr) | 2022-12-19 | 2024-06-26 | Merck Patent GmbH | Pigments à effet avec au moins une couche de tio2, dans laquelle le tio2 est dopé avec du ti(3+) et du fluorure |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3087828A (en) * | 1961-06-28 | 1963-04-30 | Du Pont | Nacreous pigment compositions |
US3087829A (en) * | 1961-06-28 | 1963-04-30 | Du Pont | Micaceous pigment composition |
US3342617A (en) * | 1965-08-12 | 1967-09-19 | Du Pont | Nacreous pigment compositions |
FR1496353A (fr) * | 1966-10-10 | 1967-09-29 | Du Pont | Réglage de la couleur du mica et de pigments nacrés préparés à partir de celui-ci |
BE759469A (fr) * | 1969-11-29 | 1971-05-26 | Merck Patent Gmbh | Pigment a brillant nacre et leurs procedes de |
US3650790A (en) * | 1970-02-13 | 1972-03-21 | Du Pont | Nacreous mica pigment compositions |
DE2009566C2 (de) * | 1970-02-28 | 1972-06-15 | Merck Patent Gmbh | Verfahren zur Herstellung von Titandioxid- bzw. Titandioxidaquatüberzügen |
JPS5632842B2 (fr) * | 1972-09-18 | 1981-07-30 | ||
DE2313331C2 (de) * | 1973-03-17 | 1986-11-13 | Merck Patent Gmbh, 6100 Darmstadt | Eisenoxidhaltige Glimmerschuppenpigmente |
US3833208A (en) * | 1973-05-04 | 1974-09-03 | Allegheny Ludlum Ind Inc | Muffle furnace |
US4134776A (en) * | 1977-12-27 | 1979-01-16 | The Mearl Corporation | Exterior grade titanium dioxide coated mica |
-
1982
- 1982-03-30 DE DE19823211602 patent/DE3211602A1/de not_active Withdrawn
-
1983
- 1983-03-16 EP EP83102593A patent/EP0090260B1/fr not_active Expired
- 1983-03-16 DE DE8383102593T patent/DE3360915D1/de not_active Expired
- 1983-03-24 CS CS832038A patent/CS240956B2/cs unknown
- 1983-03-29 BR BR8301636A patent/BR8301636A/pt not_active IP Right Cessation
- 1983-03-30 JP JP58052852A patent/JPS58180561A/ja active Granted
- 1983-03-30 US US06/480,200 patent/US4537636A/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
US4537636A (en) | 1985-08-27 |
JPS58180561A (ja) | 1983-10-22 |
JPH0536463B2 (fr) | 1993-05-31 |
EP0090260A1 (fr) | 1983-10-05 |
EP0090260B1 (fr) | 1985-10-02 |
DE3211602A1 (de) | 1983-10-13 |
DE3360915D1 (en) | 1985-11-07 |
BR8301636A (pt) | 1983-12-13 |
CS203883A2 (en) | 1985-06-13 |
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