CN1271468C - 卤化银彩色照相感光材料用漂白定影液浓缩组合物 - Google Patents
卤化银彩色照相感光材料用漂白定影液浓缩组合物 Download PDFInfo
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- CN1271468C CN1271468C CNB03146324XA CN03146324A CN1271468C CN 1271468 C CN1271468 C CN 1271468C CN B03146324X A CNB03146324X A CN B03146324XA CN 03146324 A CN03146324 A CN 03146324A CN 1271468 C CN1271468 C CN 1271468C
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- China
- Prior art keywords
- bleach
- silver halide
- concentrate composition
- bleaching agent
- silver
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- -1 silver halide Chemical class 0.000 title claims description 108
- 239000000463 material Substances 0.000 title claims description 103
- 229910052709 silver Inorganic materials 0.000 title claims description 86
- 239000004332 silver Substances 0.000 title claims description 86
- 238000004061 bleaching Methods 0.000 title description 3
- 239000007844 bleaching agent Substances 0.000 claims abstract description 71
- 150000003839 salts Chemical class 0.000 claims abstract description 37
- 238000012545 processing Methods 0.000 claims abstract description 34
- 239000002253 acid Substances 0.000 claims abstract description 19
- 239000007788 liquid Substances 0.000 claims description 111
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 31
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims description 30
- 238000002360 preparation method Methods 0.000 claims description 21
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 18
- 229910052760 oxygen Inorganic materials 0.000 claims description 18
- 239000001301 oxygen Substances 0.000 claims description 18
- 239000012141 concentrate Substances 0.000 claims description 17
- 235000014666 liquid concentrate Nutrition 0.000 claims description 17
- 235000008504 concentrate Nutrition 0.000 claims description 15
- 230000007115 recruitment Effects 0.000 claims description 15
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 13
- 230000005540 biological transmission Effects 0.000 claims description 8
- 230000000536 complexating effect Effects 0.000 claims description 7
- 229910052742 iron Inorganic materials 0.000 claims description 4
- DHCDFWKWKRSZHF-UHFFFAOYSA-L thiosulfate(2-) Chemical group [O-]S([S-])(=O)=O DHCDFWKWKRSZHF-UHFFFAOYSA-L 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 abstract description 83
- 238000000034 method Methods 0.000 abstract description 55
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 abstract description 24
- 230000008569 process Effects 0.000 abstract description 18
- 230000005484 gravity Effects 0.000 abstract 1
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- 229910021612 Silver iodide Inorganic materials 0.000 description 38
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- 239000002184 metal Substances 0.000 description 21
- 229940124543 ultraviolet light absorber Drugs 0.000 description 21
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 21
- XMBWDFGMSWQBCA-UHFFFAOYSA-M iodide Chemical compound [I-] XMBWDFGMSWQBCA-UHFFFAOYSA-M 0.000 description 20
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- 239000001384 succinic acid Substances 0.000 description 10
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- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- 239000005030 aluminium foil Substances 0.000 description 9
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 9
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- GZTPJDLYPMPRDF-UHFFFAOYSA-N pyrrolo[3,2-c]pyrazole Chemical class N1=NC2=CC=NC2=C1 GZTPJDLYPMPRDF-UHFFFAOYSA-N 0.000 description 9
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- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 9
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- 150000001412 amines Chemical class 0.000 description 8
- 229940006460 bromide ion Drugs 0.000 description 8
- 150000003842 bromide salts Chemical class 0.000 description 8
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- 229920003023 plastic Polymers 0.000 description 8
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- IOLCXVTUBQKXJR-UHFFFAOYSA-M potassium bromide Chemical compound [K+].[Br-] IOLCXVTUBQKXJR-UHFFFAOYSA-M 0.000 description 8
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- SQGYOTSLMSWVJD-UHFFFAOYSA-N silver(1+) nitrate Chemical compound [Ag+].[O-]N(=O)=O SQGYOTSLMSWVJD-UHFFFAOYSA-N 0.000 description 8
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- FZWLAAWBMGSTSO-UHFFFAOYSA-N Thiazole Chemical compound C1=CSC=N1 FZWLAAWBMGSTSO-UHFFFAOYSA-N 0.000 description 7
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- XYXNTHIYBIDHGM-UHFFFAOYSA-N ammonium thiosulfate Chemical compound [NH4+].[NH4+].[O-]S([O-])(=O)=S XYXNTHIYBIDHGM-UHFFFAOYSA-N 0.000 description 6
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- 150000007530 organic bases Chemical class 0.000 description 1
- 230000010355 oscillation Effects 0.000 description 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N oxalic acid Substances OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 150000002923 oximes Chemical class 0.000 description 1
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 1
- 150000004686 pentahydrates Chemical class 0.000 description 1
- JRKICGRDRMAZLK-UHFFFAOYSA-L peroxydisulfate Chemical compound [O-]S(=O)(=O)OOS([O-])(=O)=O JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000000825 pharmaceutical preparation Substances 0.000 description 1
- 229940127557 pharmaceutical product Drugs 0.000 description 1
- CMCWWLVWPDLCRM-UHFFFAOYSA-N phenidone Chemical compound N1C(=O)CCN1C1=CC=CC=C1 CMCWWLVWPDLCRM-UHFFFAOYSA-N 0.000 description 1
- 208000007578 phototoxic dermatitis Diseases 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229920000233 poly(alkylene oxides) Polymers 0.000 description 1
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 description 1
- 229920000768 polyamine Chemical class 0.000 description 1
- 229920001225 polyester resin Polymers 0.000 description 1
- 239000004645 polyester resin Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 239000004848 polyfunctional curative Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920000306 polymethylpentene Polymers 0.000 description 1
- 229920001955 polyphenylene ether Polymers 0.000 description 1
- 229920006380 polyphenylene oxide Polymers 0.000 description 1
- 229920002981 polyvinylidene fluoride Polymers 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 235000015497 potassium bicarbonate Nutrition 0.000 description 1
- 239000011736 potassium bicarbonate Substances 0.000 description 1
- 229910000028 potassium bicarbonate Inorganic materials 0.000 description 1
- DJEHXEMURTVAOE-UHFFFAOYSA-M potassium bisulfite Chemical compound [K+].OS([O-])=O DJEHXEMURTVAOE-UHFFFAOYSA-M 0.000 description 1
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- RWPGFSMJFRPDDP-UHFFFAOYSA-L potassium metabisulfite Chemical compound [K+].[K+].[O-]S(=O)S([O-])(=O)=O RWPGFSMJFRPDDP-UHFFFAOYSA-L 0.000 description 1
- 229940043349 potassium metabisulfite Drugs 0.000 description 1
- 235000010263 potassium metabisulphite Nutrition 0.000 description 1
- BHZRJJOHZFYXTO-UHFFFAOYSA-L potassium sulfite Chemical compound [K+].[K+].[O-]S([O-])=O BHZRJJOHZFYXTO-UHFFFAOYSA-L 0.000 description 1
- 235000019252 potassium sulphite Nutrition 0.000 description 1
- AYXYFBLDIAOCIP-UHFFFAOYSA-L potassium;sodium;bromide;chloride Chemical compound [Na+].[Cl-].[K+].[Br-] AYXYFBLDIAOCIP-UHFFFAOYSA-L 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 125000001500 prolyl group Chemical class [H]N1C([H])(C(=O)[*])C([H])([H])C([H])([H])C1([H])[H] 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 150000003233 pyrroles Chemical class 0.000 description 1
- MHOZZUICEDXVGD-UHFFFAOYSA-N pyrrolo[2,3-d]imidazole Chemical compound C1=NC2=CC=NC2=N1 MHOZZUICEDXVGD-UHFFFAOYSA-N 0.000 description 1
- QEIQICVPDMCDHG-UHFFFAOYSA-N pyrrolo[2,3-d]triazole Chemical compound N1=NC2=CC=NC2=N1 QEIQICVPDMCDHG-UHFFFAOYSA-N 0.000 description 1
- 238000011002 quantification Methods 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 229910001419 rubidium ion Inorganic materials 0.000 description 1
- 229920002379 silicone rubber Polymers 0.000 description 1
- HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 description 1
- APSBXTVYXVQYAB-UHFFFAOYSA-M sodium docusate Chemical group [Na+].CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC APSBXTVYXVQYAB-UHFFFAOYSA-M 0.000 description 1
- 235000010267 sodium hydrogen sulphite Nutrition 0.000 description 1
- 235000009518 sodium iodide Nutrition 0.000 description 1
- 229940001584 sodium metabisulfite Drugs 0.000 description 1
- 235000010262 sodium metabisulphite Nutrition 0.000 description 1
- 229960004025 sodium salicylate Drugs 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 235000010265 sodium sulphite Nutrition 0.000 description 1
- VGTPCRGMBIAPIM-UHFFFAOYSA-M sodium thiocyanate Chemical compound [Na+].[S-]C#N VGTPCRGMBIAPIM-UHFFFAOYSA-M 0.000 description 1
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- 239000007779 soft material Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- PJANXHGTPQOBST-UHFFFAOYSA-N stilbene Chemical compound C=1C=CC=CC=1C=CC1=CC=CC=C1 PJANXHGTPQOBST-UHFFFAOYSA-N 0.000 description 1
- 235000021286 stilbenes Nutrition 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 230000035882 stress Effects 0.000 description 1
- 125000000020 sulfo group Chemical group O=S(=O)([*])O[H] 0.000 description 1
- 239000002344 surface layer Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- RWRDLPDLKQPQOW-UHFFFAOYSA-N tetrahydropyrrole Substances C1CCNC1 RWRDLPDLKQPQOW-UHFFFAOYSA-N 0.000 description 1
- VXKWYPOMXBVZSJ-UHFFFAOYSA-N tetramethyltin Chemical compound C[Sn](C)(C)C VXKWYPOMXBVZSJ-UHFFFAOYSA-N 0.000 description 1
- PGAPATLGJSQQBU-UHFFFAOYSA-M thallium(i) bromide Chemical compound [Tl]Br PGAPATLGJSQQBU-UHFFFAOYSA-M 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 150000004764 thiosulfuric acid derivatives Chemical class 0.000 description 1
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 description 1
- 230000000699 topical effect Effects 0.000 description 1
- 229950004288 tosilate Drugs 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 150000003852 triazoles Chemical class 0.000 description 1
- WUUHFRRPHJEEKV-UHFFFAOYSA-N tripotassium borate Chemical compound [K+].[K+].[K+].[O-]B([O-])[O-] WUUHFRRPHJEEKV-UHFFFAOYSA-N 0.000 description 1
- 235000019798 tripotassium phosphate Nutrition 0.000 description 1
- 229910000404 tripotassium phosphate Inorganic materials 0.000 description 1
- BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 description 1
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 1
- 125000002987 valine group Chemical class [H]N([H])C([H])(C(*)=O)C([H])(C([H])([H])[H])C([H])([H])[H] 0.000 description 1
- 230000000007 visual effect Effects 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
- 235000020985 whole grains Nutrition 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C7/00—Multicolour photographic processes or agents therefor; Regeneration of such processing agents; Photosensitive materials for multicolour processes
- G03C7/30—Colour processes using colour-coupling substances; Materials therefor; Preparing or processing such materials
- G03C7/42—Bleach-fixing or agents therefor ; Desilvering processes
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C2200/00—Details
- G03C2200/44—Details pH value
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C2200/00—Details
- G03C2200/52—Rapid processing
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C5/00—Photographic processes or agents therefor; Regeneration of such processing agents
- G03C5/26—Processes using silver-salt-containing photosensitive materials or agents therefor
- G03C5/264—Supplying of photographic processing chemicals; Preparation or packaging thereof
- G03C5/266—Supplying of photographic processing chemicals; Preparation or packaging thereof of solutions or concentrates
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C5/00—Photographic processes or agents therefor; Regeneration of such processing agents
- G03C5/26—Processes using silver-salt-containing photosensitive materials or agents therefor
- G03C5/264—Supplying of photographic processing chemicals; Preparation or packaging thereof
- G03C5/267—Packaging; Storage
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C5/00—Photographic processes or agents therefor; Regeneration of such processing agents
- G03C5/26—Processes using silver-salt-containing photosensitive materials or agents therefor
- G03C5/395—Regeneration of photographic processing agents other than developers; Replenishers therefor
- G03C5/3958—Replenishment processes or compositions, i.e. addition of useful photographic processing agents
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C7/00—Multicolour photographic processes or agents therefor; Regeneration of such processing agents; Photosensitive materials for multicolour processes
- G03C7/30—Colour processes using colour-coupling substances; Materials therefor; Preparing or processing such materials
- G03C7/44—Regeneration; Replenishers
Landscapes
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Silver Salt Photography Or Processing Solution Therefor (AREA)
Abstract
Description
要素 | 特开平7-104448 | 特开平7-77775 | 特开平7-301895 |
反射型载体 | 7栏12行~12栏19行 | 35栏43行~44栏1行 | 5栏40行~9栏26行 |
卤化银乳剂 | 72栏29行~74栏18行 | 44栏36行~46栏29行 | 77栏48行~80栏28行 |
不同金属离子种类 | 74栏19行~同栏44行 | 46栏30行~47栏5行 | 80栏29行~81栏6行 |
储存稳定剂或灰雾防止剂 | 75栏9行~同栏18行 | 47栏20行~同栏29行 | 18栏11行~31栏37行(特别是巯基杂环化合物) |
化学增感法(化学增感剂) | 74栏45行~75栏6行 | 47栏7行~同栏17行 | 81栏9行~同栏17行 |
分光增感法(分光增感剂) | 75栏19行~76栏45行 | 47栏30行~49栏6行 | 81栏21行~82栏48行 |
蓝色成色剂 | 12栏20行~39栏49行 | 62栏50行~63栏16行 | 88栏49行~89栏16行 |
黄色成色剂 | 87栏40行~88栏3行 | 63栏17行~同栏30行 | 89栏17行~同栏30行 |
红色成色剂 | 88栏4行~同栏18行 | 63栏3行~64栏11行 | 31栏34行~77栏44行88栏32行~同栏46行 |
成色剂的乳化分散法 | 71栏3行~72栏11行 | 61栏36行~同栏49行 | 87栏35行~同栏48行 |
彩色图象储存性改良剂(防止粘污剂) | 39栏50行~70栏9行 | 61栏50行~62栏40行 | 87栏49行~88栏48行 |
褪色防止剂 | 70栏10行~71栏2行 | ||
染料(着色剂) | 77栏42行~78栏41行 | 7栏14行~19栏42行50栏3行~51栏14行 | 9栏27行~18栏10行 |
明胶品种 | 78栏42行~同栏48行 | 51栏15行~同栏20行 | 83栏13行~同栏19行 |
感光材料的层结构 | 39栏11行~同栏25行 | 44栏2行~同栏35行 | 31栏38行~32栏33行 |
感光材料被膜的pH值 | 72栏12行~同栏28行 | ||
扫描曝光 | 76栏6行~77栏41行 | 49栏7行~50栏2行 | 82栏49行~83栏12行 |
显影液中的抗氧剂 | 88栏19行~89栏22行 |
No | EDTAFe(III)浓度(mol/L) | EDTA浓度(mol/%) | pH | 比重 | -5℃经时析出性 | 50℃经时析出性 | 50℃经时Fe2+% | 备考 |
1 | 0.7 | 0 | 2.5 | 1.160 | ◎ | ×× | 3 | 比较例 |
2 | 0.7 | 0.1 | 2.5 | 1.160 | ◎ | ◎ | 3 | 本发明 |
3 | 0.7 | 0.3 | 2.5 | 1.160 | ◎ | ◎ | 3 | 本发明 |
4 | 0.7 | 3.0 | 2.5 | 1.160 | ○ | ◎ | 3 | 本发明 |
5 | 0.7 | 10.0 | 2.5 | 1.160 | ×× | ○ | 3 | 比较例 |
6 | 0.7 | 0.3 | 1.0 | 1.160 | ×× | × | 3 | 比较例 |
7 | 0.7 | 0.3 | 2.0 | 1.160 | ◎ | ◎ | 3 | 本发明 |
8 | 0.7 | 0.3 | 3.5 | 1.160 | ◎ | ◎ | 5 | 本发明 |
9 | 0.7 | 0.3 | 4.5 | 1.160 | × | ○ | 20 | 比较例 |
10 | 0.7 | 0.3 | 5.5 | 1.160 | × | ○ | 36 | 比较例 |
11 | 1.0 | 0.3 | 2.5 | 1.160 | ◎ | ◎ | 3 | 本发明 |
12 | 1.2 | 0.3 | 2.5 | 1.160 | × | × | 3 | 比较例 |
13 | 1.0 | 0.3 | 2.5 | 1.130 | ◎ | ◎ | 3 | 本发明 |
14 | 1.0 | 0.3 | 2.5 | 1.190 | ◎ | ◎ | 3 | 本发明 |
15 | 1.0 | 0.3 | 2.5 | 1.210 | × | ○ | 3 | 比较例 |
16 | 0.5 | 0 | 2.0 | 1.160 | ◎ | ×× | 3 | 比较例 |
17 | 0.5 | 0.3 | 2.0 | 1.160 | ◎ | ◎ | 3 | 本发明 |
18 | 0.5 | 10.0 | 2.0 | 1.160 | ×× | ○ | 3 | 比较例 |
19 | 0.5 | 0 | 5.0 | 1.160 | ○ | ×× | 30 | 比较例 |
20 | 0.5 | 0.3 | 5.0 | 1.160 | × | ◎ | 33 | 比较例 |
21 | 0.5 | 10.0 | 5.0 | 1.160 | ×× | ○ | 31 | 比较例 |
No | EDTA浓度(mol%) | 有机酸(mol/L) | pH | 容器的氧透过率(mL/24h) | -5℃经时析出性 | 50℃经时析出性 | 50℃经时Fe2+% | 备考 |
1 | 0 | - | 2.5 | 10 | ○ | ×× | 8 | 比较例 |
2 | 0.1 | - | 2.5 | 10 | ○ | ◎ | 8 | 本发明 |
3 | 0.3 | - | 2.5 | 10 | ○ | ◎ | 8 | 本发明 |
4 | 3.0 | - | 2.5 | 10 | ○ | ◎ | 8 | 本发明 |
5 | 10.0 | - | 2.5 | 10 | ×× | ○ | 1 | 比较例 |
6 | 0 | 琥珀酸(0.4) | 2.5 | 10 | ◎ | ×× | 1 | 比较例 |
7 | 0.1 | 琥珀酸(0.4) | 2.5 | 10 | ◎ | ◎ | 1 | 本发明 |
8 | 0.3 | 琥珀酸(0.4) | 2.5 | 10 | ◎ | ◎ | 1 | 本发明 |
9 | 3.0 | 琥珀酸(0.4) | 2.5 | 10 | ◎ | ◎ | 1 | 本发明 |
10 | 10.0 | 琥珀酸(0.4) | 2.5 | 10 | ×× | ○ | 1 | 比较例 |
11 | 0 | 醋酸(0.6) | 2.5 | 10 | ◎ | ×× | 1 | 比较例 |
12 | 0.1 | 醋酸(0.6) | 2.5 | 10 | ◎ | ◎ | 1 | 本发明 |
13 | 0.3 | 醋酸(0.6) | 2.5 | 10 | ◎ | ◎ | 1 | 本发明 |
14 | 3.0 | 醋酸(0.6) | 2.5 | 10 | ◎ | ◎ | 1 | 本发明 |
15 | 10.0 | 醋酸(0.6) | 2.5 | 10 | ×× | ○ | 1 | 比较例 |
16 | 0.1 | 醋酸(0.6) | 1.0 | 10 | ×× | ○ | 1 | 比较例 |
17 | 0.1 | 醋酸(0.6) | 4.5 | 10 | ×× | × | 18 | 比较例 |
18 | 0.1 | 醋酸(0.6) | 5.5 | 10 | ×× | × | 33 | 比较例 |
19 | 0.1 | 琥珀酸(0.4) | 2.5 | 0.5 | ◎ | ◎ | 12 | 本发明 |
20 | 0.1 | 琥珀酸(0.4) | 2.5 | 2 | ◎ | ◎ | 10 | 本发明 |
21 | 0.1 | 琥珀酸(0.4) | 2.5 | 4 | ◎ | ◎ | 3 | 本发明 |
22 | 0.1 | 琥珀酸(0.4) | 2.5 | 20 | ◎ | ◎ | 1 | 本发明 |
R1 | R2 | |
abcd | -CH3-CH3-H-H | -NHCH3-NH2-NH2-NHCH3 |
处理工序 | 温度(℃) | 时间(sec) | 补充量 |
彩色显影漂白定影漂洗(1)漂洗(2)漂洗(3)漂洗(4)干燥 | 45.040.040.040.040.040.080 | 2525744720 | 45mL/m2A剂17.5mL/m2B剂17.5mL/m2---175mL/m2 |
槽液 | 补充液 | |
阳离子交换水二甲基聚硅氧烷系表面活性剂(信越化学工业(株)制的聚硅氧烷KF351A)KOHNaOH乙二胺四乙酸钛试剂氯化钾溴化钠P-1(下述化合物)S-1(下述化合物)对甲苯磺酸钠亚硫酸钠m-羧基亚磺酸N,N-二(磺酸乙酯)羟基胺二钠盐N-乙基-N-(β-甲磺酰胺乙基)-3-甲基-4-氨基苯胺·3/2硫酸盐·1水盐 | 800mL0.05g4.0g2.0g4.0g0.5g19.0g0.036g1.5g3.5g15.0g0.2g2.0g5.0g6.7g | 800Ml0.05g9.0g6.0g4.0g0.5g--2.9g9.0g15.0g0.2g3.6g10.8g17.3g |
碳酸钾加水pH值(25℃,用氢氧化钾、硫酸调节) | 26.3g1000mL10.12 | 26.3g1000mL10.26 |
槽液 | 补充液A | 补充液B | |
水硫代硫酸铵(750g/L)重亚硫酸铵溶液(65%)亚硫酸铵乙二胺四乙酸(III)铵乙二胺四乙酸m-羧基磺酸硝酸琥珀酸咪唑氨水(27%)加水pH值(25℃,用氨、硝酸调节) | 650mL97.0mL13.0g21.0g37.0g1.6g3.0g5.2g6.7g1.3g3.4g1000mL5.9 | 300mL---184.0g0.4g14.0g25.0g33.0g--1000mL2.5 | 300mL376.0mL185.5mL--10.0g----36.0g1000mL5.75 |
处理工序 | 温度(℃) | 时间(sec) | 补充量 |
彩色显影漂白定影漂洗(1)漂洗(2)漂洗(3)漂洗(4)干燥 | 45.040.040.040.040.040.080 | 1616533516 | 45mL/m2A剂17.5mL/m2B剂17.5mL/m2---175mL/m2 |
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JP2002211187A JP3765486B2 (ja) | 2002-07-19 | 2002-07-19 | ハロゲン化銀カラー写真感光材料用漂白定着液濃縮組成物 |
JP211187/2002 | 2002-07-19 |
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CN1271468C true CN1271468C (zh) | 2006-08-23 |
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US (1) | US6927019B2 (zh) |
EP (1) | EP1383002B1 (zh) |
JP (1) | JP3765486B2 (zh) |
CN (1) | CN1271468C (zh) |
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EP1742106A4 (en) * | 2004-04-30 | 2007-07-25 | Fujifilm Corp | BLEACHING CONCENTRATE COMPOSITION FOR SILVER HALOGENIDE COLOR PHOTOGRAPHIC MATERIALS, ONE-PIECE CONCENTRATE COMPOSITION FOR RECYCLING COLOR DEVELOPERS AND DEVELOPMENT PROCESSES |
US7351522B2 (en) | 2004-08-20 | 2008-04-01 | Fujifilm Corporation | Concentrated processing composition for silver halide color paper and method of processing |
DE102004056397B4 (de) * | 2004-11-23 | 2008-01-17 | A&O Imaging Solutions Gmbh | Bleichfixierbadkonzentrat für fotografisches Material |
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JPH07122751B2 (ja) | 1988-04-28 | 1995-12-25 | 富士写真フイルム株式会社 | ハロゲン化銀カラー写真感光材料用漂白定着液濃縮組成物及び処理方法 |
JP3200465B2 (ja) * | 1992-04-24 | 2001-08-20 | 富士写真フイルム株式会社 | ハロゲン化銀写真感光材料用の処理組成物及びそれを用いた処理方法 |
JP3372994B2 (ja) * | 1993-06-11 | 2003-02-04 | 富士写真フイルム株式会社 | ハロゲン化銀カラー写真感光材料の処理方法 |
JP3515602B2 (ja) * | 1994-01-27 | 2004-04-05 | 富士写真フイルム株式会社 | ハロゲン化銀カラー写真感光材料及びカラー画像形成方法 |
JP3989082B2 (ja) | 1998-04-03 | 2007-10-10 | 富士フイルム株式会社 | 写真用処理剤組成物キット及びそれを用いる現像処理方法 |
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2002
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- 2003-07-18 EP EP03016322A patent/EP1383002B1/en not_active Expired - Lifetime
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DE60307744T2 (de) | 2006-12-21 |
EP1383002A1 (en) | 2004-01-21 |
US20040023167A1 (en) | 2004-02-05 |
JP2004053921A (ja) | 2004-02-19 |
JP3765486B2 (ja) | 2006-04-12 |
CN1470938A (zh) | 2004-01-28 |
EP1383002B1 (en) | 2006-08-23 |
DE60307744D1 (de) | 2006-10-05 |
US6927019B2 (en) | 2005-08-09 |
ATE337572T1 (de) | 2006-09-15 |
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