CN1220716C - 聚酯前体纯化方法 - Google Patents

聚酯前体纯化方法 Download PDF

Info

Publication number
CN1220716C
CN1220716C CNB018148727A CN01814872A CN1220716C CN 1220716 C CN1220716 C CN 1220716C CN B018148727 A CNB018148727 A CN B018148727A CN 01814872 A CN01814872 A CN 01814872A CN 1220716 C CN1220716 C CN 1220716C
Authority
CN
China
Prior art keywords
catalyst
oligomer
hydrogen
terephthalic acid
hydrogenation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNB018148727A
Other languages
English (en)
Chinese (zh)
Other versions
CN1449419A (zh
Inventor
小C·E·苏姆纳
R·B·舍帕德
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Eastman Chemical Co
Original Assignee
Eastman Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Eastman Chemical Co filed Critical Eastman Chemical Co
Publication of CN1449419A publication Critical patent/CN1449419A/zh
Application granted granted Critical
Publication of CN1220716C publication Critical patent/CN1220716C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78Preparation processes
    • C08G63/82Preparation processes characterised by the catalyst used
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/48Separation; Purification; Stabilisation; Use of additives
    • C07C67/60Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B9/00Making granules
    • B29B9/12Making granules characterised by structure or composition
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B9/00Making granules
    • B29B9/16Auxiliary treatment of granules
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B9/00Making granules
    • B29B9/16Auxiliary treatment of granules
    • B29B2009/165Crystallizing granules

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CNB018148727A 2000-08-29 2001-08-24 聚酯前体纯化方法 Expired - Fee Related CN1220716C (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US22869500P 2000-08-29 2000-08-29
US60/228,695 2000-08-29
US09/812,581 US6380352B1 (en) 2000-08-29 2001-03-20 Polyester precursor purification process
US09/812,581 2001-03-20

Publications (2)

Publication Number Publication Date
CN1449419A CN1449419A (zh) 2003-10-15
CN1220716C true CN1220716C (zh) 2005-09-28

Family

ID=26922575

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB018148727A Expired - Fee Related CN1220716C (zh) 2000-08-29 2001-08-24 聚酯前体纯化方法

Country Status (14)

Country Link
US (1) US6380352B1 (enExample)
EP (1) EP1313788B1 (enExample)
JP (1) JP2004507560A (enExample)
KR (1) KR100779294B1 (enExample)
CN (1) CN1220716C (enExample)
AR (1) AR033388A1 (enExample)
AT (1) ATE342296T1 (enExample)
BR (1) BR0113498A (enExample)
CA (1) CA2419422C (enExample)
DE (1) DE60123810T2 (enExample)
ES (1) ES2269445T3 (enExample)
MX (1) MXPA03001617A (enExample)
TW (1) TW527373B (enExample)
WO (1) WO2002018471A2 (enExample)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2146172C1 (ru) * 1999-07-29 2000-03-10 Институт катализа им.Г.К.Борескова СО РАН Каталитическая композиция, способ ее приготовления и способ очистки терефталевой кислоты
US6762276B2 (en) * 2002-02-27 2004-07-13 Eastman Chemical Company Hydrogenation of polyester oligomers containing terephthalic acid residues
TW200418901A (en) 2003-02-25 2004-10-01 Du Pont Process for the manufacture of polyester via hydrogenation treatment of recycled diol
DE10339366A1 (de) * 2003-08-27 2005-03-24 Dr. Johannes Heidenhain Gmbh Verfahren und Vorrichtung zur Regelung einer Lichtquelle eines Positionsmessgerätes
US7129316B2 (en) 2004-01-07 2006-10-31 Invista North America S.A R.L. Process for the manufacture of polyester via hydrogenation treatment of recycled diol
CN101072808B (zh) * 2004-12-21 2010-08-11 日立化成工业株式会社 酸酐类环氧树脂固化剂的制造方法、酸酐类环氧树脂固化剂、环氧树脂组合物、其固化物和光半导体装置
US7067615B1 (en) 2005-06-13 2006-06-27 Eastman Chemical Company Hydrotreating polyester precursors
US7390869B2 (en) * 2005-06-13 2008-06-24 Eastman Chemical Company Process for removing metal species in the presence of hydrogen and a porous material and polyester polymer containing reduced amounts of metal species
KR101101930B1 (ko) * 2011-04-19 2012-01-02 김용남 프리캐스트 콘크리트 경량 판상 마감재
US9550713B1 (en) 2015-07-09 2017-01-24 Loop Industries, Inc. Polyethylene terephthalate depolymerization
US10252976B1 (en) 2017-09-15 2019-04-09 9449710 Canada Inc. Terephthalic acid esters formation
US12071519B2 (en) 2017-09-15 2024-08-27 9449710 Canada Inc. Terephthalic acid esters formation
PE20210858A1 (es) 2018-06-25 2021-05-18 9449710 Canada Inc Formacion de esteres de acido tereftalico
US11248103B2 (en) 2019-03-20 2022-02-15 9449710 Canada Inc. Process for the depolymerization of polyethylene terephthalate (PET)
CN114375313A (zh) * 2019-07-19 2022-04-19 帝人株式会社 热塑性树脂和包含该热塑性树脂的光学构件
IT201900025039A1 (it) * 2019-12-20 2021-06-20 Garbo S R L Processo per purificare il bis(2-idrossietil)tereftalato.
WO2021245578A1 (en) 2020-06-05 2021-12-09 Koch Technology Solutions, Llc A method for manufacturing an oligomeric polyethylene terephthalate (pet) substrate
CN115698123A (zh) * 2020-06-05 2023-02-03 科氏技术英国有限公司 用于制造低聚聚对苯二甲酸乙二酯(pet)底物的方法
WO2025160816A1 (zh) * 2024-01-31 2025-08-07 江苏集萃先进纤维材料研究所有限公司 基于分步反应逐步结晶的回收纯化bhet的方法

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1134949A (en) 1965-05-14 1968-11-27 Sumitomo Chemical Co Method for treating crude bis--ß-hydroxyethyl terephthalate
US3501420A (en) 1967-10-20 1970-03-17 Eastman Kodak Co High purity polyester depolymerization products from polyester scrap by polish hydrogenation
JPS4836141A (enExample) * 1971-09-14 1973-05-28
JPS5828255B2 (ja) 1974-05-04 1983-06-15 東洋紡績株式会社 1,4 シクロヘキサンジメタノ−ル ノ セイゾウホウ
DE2504156A1 (de) * 1975-02-01 1976-08-05 Dynamit Nobel Ag Niedermolekulare terephthalsaeure- aethylenglykolester, ihre herstellung und verwendung
JPH0672922A (ja) * 1992-08-26 1994-03-15 Toyobo Co Ltd 廃ポリエチレンテレフタレートから高純度の原料モノマーを回収する方法
US5597891A (en) 1995-08-01 1997-01-28 Eastman Chemical Company Process for producing polyester articles having low acetaldehyde content
US5648032A (en) 1995-08-01 1997-07-15 Eastman Chemical Company Process for producing polyester articles having low acetaldehyde content
JP3891454B2 (ja) * 1996-12-19 2007-03-14 三井化学株式会社 芳香族ジカルボン酸エステルの精製方法

Also Published As

Publication number Publication date
TW527373B (en) 2003-04-11
DE60123810T2 (de) 2007-03-01
US6380352B1 (en) 2002-04-30
KR100779294B1 (ko) 2007-11-27
CA2419422C (en) 2007-07-17
DE60123810D1 (de) 2006-11-23
EP1313788B1 (en) 2006-10-11
ATE342296T1 (de) 2006-11-15
JP2004507560A (ja) 2004-03-11
BR0113498A (pt) 2003-07-29
EP1313788A2 (en) 2003-05-28
WO2002018471A2 (en) 2002-03-07
AR033388A1 (es) 2003-12-17
MXPA03001617A (es) 2003-06-04
CA2419422A1 (en) 2002-03-07
ES2269445T3 (es) 2007-04-01
WO2002018471A3 (en) 2002-05-30
CN1449419A (zh) 2003-10-15
KR20030045787A (ko) 2003-06-11

Similar Documents

Publication Publication Date Title
CN1220716C (zh) 聚酯前体纯化方法
CN1138025A (zh) 制备对苯二甲酸的方法
KR101288685B1 (ko) 폴리에스터 제조용으로 적당한 카복실산/다이올 혼합물의 제조방법
CN1171847C (zh) 制备乳酸酯组合物的方法和其作为溶剂的应用
KR100685194B1 (ko) 나프탈렌 디카르복실산의 저온 정제
CN101861349A (zh) 用于改性pet的简化间苯二甲酸方法
CN100393773C (zh) 含有对苯二甲酸残基的聚酯低聚物的氢化作用
JP3820045B2 (ja) ヒドロキシカルボン酸エステルの製造方法
CN1301956C (zh) 粗混合酸的纯化
KR101304600B1 (ko) 폴리에스터 전구체의 수소처리
HK1050910B (en) Low temperature purification of naphthalene dicarboxylic acids

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
C56 Change in the name or address of the patentee

Owner name: EASTMAN CHEMICAL COMPANY

Free format text: FORMER NAME OR ADDRESS: YISIMAN CHEMICAL COMPANY

CP01 Change in the name or title of a patent holder

Address after: Tennessee

Patentee after: EASTMAN CHEMICAL Co.

Address before: Tennessee

Patentee before: EASTMAN CHEMICAL Co.

C17 Cessation of patent right
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20050928

Termination date: 20100824