CN1147147A - Method for forming fine patterns of semiconductor device - Google Patents

Method for forming fine patterns of semiconductor device Download PDF

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Publication number
CN1147147A
CN1147147A CN96107007A CN96107007A CN1147147A CN 1147147 A CN1147147 A CN 1147147A CN 96107007 A CN96107007 A CN 96107007A CN 96107007 A CN96107007 A CN 96107007A CN 1147147 A CN1147147 A CN 1147147A
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China
Prior art keywords
wafer
photoresist
oxygen plasma
oxygen
oxidation
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Granted
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CN96107007A
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Chinese (zh)
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CN1080929C (en
Inventor
卜喆圭
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SK Hynix Inc
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Hyundai Electronics Industries Co Ltd
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Publication of CN1147147A publication Critical patent/CN1147147A/en
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Publication of CN1080929C publication Critical patent/CN1080929C/en
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    • GPHYSICS
    • G03PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03FPHOTOMECHANICAL PRODUCTION OF TEXTURED OR PATTERNED SURFACES, e.g. FOR PRINTING, FOR PROCESSING OF SEMICONDUCTOR DEVICES; MATERIALS THEREFOR; ORIGINALS THEREFOR; APPARATUS SPECIALLY ADAPTED THEREFOR
    • G03F7/00Photomechanical, e.g. photolithographic, production of textured or patterned surfaces, e.g. printing surfaces; Materials therefor, e.g. comprising photoresists; Apparatus specially adapted therefor
    • G03F7/16Coating processes; Apparatus therefor
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/027Making masks on semiconductor bodies for further photolithographic processing not provided for in group H01L21/18 or H01L21/34
    • H01L21/033Making masks on semiconductor bodies for further photolithographic processing not provided for in group H01L21/18 or H01L21/34 comprising inorganic layers
    • H01L21/0334Making masks on semiconductor bodies for further photolithographic processing not provided for in group H01L21/18 or H01L21/34 comprising inorganic layers characterised by their size, orientation, disposition, behaviour, shape, in horizontal or vertical plane
    • H01L21/0338Process specially adapted to improve the resolution of the mask
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/027Making masks on semiconductor bodies for further photolithographic processing not provided for in group H01L21/18 or H01L21/34
    • H01L21/0271Making masks on semiconductor bodies for further photolithographic processing not provided for in group H01L21/18 or H01L21/34 comprising organic layers
    • H01L21/0273Making masks on semiconductor bodies for further photolithographic processing not provided for in group H01L21/18 or H01L21/34 comprising organic layers characterised by the treatment of photoresist layers
    • H01L21/0274Photolithographic processes
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/027Making masks on semiconductor bodies for further photolithographic processing not provided for in group H01L21/18 or H01L21/34
    • H01L21/033Making masks on semiconductor bodies for further photolithographic processing not provided for in group H01L21/18 or H01L21/34 comprising inorganic layers
    • H01L21/0334Making masks on semiconductor bodies for further photolithographic processing not provided for in group H01L21/18 or H01L21/34 comprising inorganic layers characterised by their size, orientation, disposition, behaviour, shape, in horizontal or vertical plane
    • H01L21/0337Making masks on semiconductor bodies for further photolithographic processing not provided for in group H01L21/18 or H01L21/34 comprising inorganic layers characterised by their size, orientation, disposition, behaviour, shape, in horizontal or vertical plane characterised by the process involved to create the mask, e.g. lift-off masks, sidewalls, or to modify the mask, e.g. pre-treatment, post-treatment

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  • Engineering & Computer Science (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Computer Hardware Design (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Power Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Photosensitive Polymer And Photoresist Processing (AREA)
  • Exposure Of Semiconductors, Excluding Electron Or Ion Beam Exposure (AREA)
  • Exposure And Positioning Against Photoresist Photosensitive Materials (AREA)
  • Weting (AREA)

Abstract

A method for forming fine patterns in a semiconductor device comprises prepareing a wafer, oxidizing the upper surface of the wafer to form an oxide film, and then coating a photoresist onto the oxidized wafer. The photoresist is then exposed and developed to form photoresist patterns. The method prevents foot or uncut occurring at the lower part of the patterns, thus allowing the width of the patterns to be easily controlled. The method is therefore useful for the high integration of semiconductor devices in addition to being high in production yield.

Description

Form the method for fine pattern of semiconductor device
The present invention relates generally to a kind of method that forms fine pattern of semiconductor device.This method is applicable to highly intergrated semiconductor device, is particularly suited for preventing to produce the defective patterns that has counterdie and undercutting, thereby controls graphic width easily.
Carry out photoetching process when on wafer, forming the photoresist figure, be coated in the pollution that photoresist on the wafer is subjected to amine in the air possibly.This pollution cause photoresist figure both sides residual have uncorroded bottom photoresist figure stay the film phenomenon or because of the undercutting phenomenon of corrosion in the undercutting of photoresist figure bottom takes place, so can not form accurate fine pattern.
To this, the photoresist figure bottom counterdie that caused by amine or the generation of undercutting are described below with reference to accompanying drawings.
At first, illustrate that the conventional chemical that is used to form the photoresist figure strengthens the light reaction mechanism of photoresist.
Figure 1A represents that typical two component positivity chemistry strengthens the light reaction of photoresist, and figure B represents that typical three component negative chemicals strengthen the light reaction of photoresist.
Shown in Figure 1A, the positivity chemistry strengthens photoresist generally by forming with the resin and the photic sour initator 3 of dissolution inhibitor 2 bondings.Resin 1 by dissolution inhibitor 2 constraints is insoluble to alkaline solution, and is not subjected to the resin energy of dissolution inhibitor 2 constraints molten.
Therefore, utilize this species diversity of solubility to form the formation that negative chemical strengthens the photoresist figure, more particularly, unexposed photoresist does not dissolve naturally, and after its exposure, because from the photic sour initator proton (H that is a kind of strong acid +) resin 1 is broken away from from dissolution inhibitor 2, so its dissolving.Because luminous energy produces and heat energy activates, proton plays catalyst, and dissolution inhibitor 2 and resin 1 are broken away from.
It is to make resin, make dissolution inhibitor and make photic sour initator with three fluosulfonic acid triphenylsulfonium with tert-butoxycarbonyl with polyhydroxy styrene that this pair of representative component chemistry strengthens photoresist.
Negative chemical enhancing photoresist generally is three components shown in Figure 1B, i.e. resin 1, photic sour initator 3 and crosslinking agent 4.
Opposite with positivity chemistry enhancing photoresist, negative chemical strengthens photoresist can be dissolved in alkaline solution when unexposed., after negative chemical strengthened the photoresist exposure, owing to making soluble resin 1 change into soluble resin with crosslinking agent 2 bondings, thus, the difference of this solubility can form the photoresist figure.
More particularly, be the proton (H that a kind of strong acid produces by light from photic sour initator +) activatable crosslinking agent 4, make it and resin 1 bonding, polymerization can take place then, thus, the negative photoresist that unexposed portion can be molten is owing to a kind of solubility variation is experienced in illumination.
Shown in Figure 1A, promote the crosslinking agent 4 and the proton of resin 1 bonding to produce, and activate by heat energy by luminous energy.
It is to make resin, make crosslinking agent, make photic sour initator with phenthazine with melamine with polyvinyl phenol that representative this three components chemistry strengthens photoresist.
But polyvinyl phenol has high solubility in alkaline solution.Specifically, after two component positivity chemistry strengthened the photoresist exposure, tert-butoxycarbonyl broke away from from the polyhydroxy styrene as resin, and changes into polyvinyl phenol.
As mentioned above, form figure,, all need produce proton by strong acid no matter photoresist is positivity or negativity in order to strengthen photoresist with chemistry.In other words, to positive photoresist, have only the part of exposure in strong acid, to dissolve, and to negative photoresist, the part of exposure still keep its figure in strong acid.Therefore, in both cases, the existence of strong acid is necessary.Do not producing or do not having the proton place, the negative photoresist dissolving, and positive photoresist does not dissolve.
Below with reference to Fig. 2 and 3 this counterdie of explanation or undercuttings.
Fig. 2 A to 2C represents a conventional embodiment that forms the photoresist figure with negative chemical enhancing photoresist on wafer.
At first, Fig. 2 A is the profile behind coating positive photoresist 12 on the wafer 11.
Fig. 2 B makes profile after positive photoresist 12 exposure with photomask.
Fig. 2 C is the positive photoresist 12 that exposed 15 the profile with the photoresist figure that is formed with counterdie 16 on wafer 11 that develops.Discovery is to be caused by the pollution of amine (not shown) to positive photoresist at these counterdies that the bottom of figure 15 forms.
Referring to Fig. 3, its expression is another kind of to strengthen photoresist forms the order of photoresist figure on wafer conventional embodiment with negative chemical.
As shown in Figure 3A, at first, coating negative photoresist 22 on wafer 21.
Shown in Fig. 3 B, subsequently, make negative photoresist 22 exposures with photomask.
Shown in Fig. 3 C, then, development negative photoresist 22 is to be formed with the photoresist figure 25 of undercutting 26 on wafer 21.Find that this undercutting photoresist figure also is to be caused by the reason identical with the photoresist figure that causes having counterdie.
The photoresist that is caused by amine is discussed below to be polluted and is how to cause such as the such defective of counterdie or undercutting.
Usually, the film that is used for producing the semiconductor devices comprises oxide, nitride, polysilicon, titanium nitride and boron-phosphorosilicate glass (BPSG) or the like.Wherein titanium nitride and boron-phosphorosilicate glass are easy to pollute by being present in airborne amine, so the surperficial amine concentration height of film.Because amine, the derivative that is ammonia is alkaline, during so it can come by the strong acid that consumption is present in film surface and strong acid, thereby consumption strong acid, cause the positive photoresist of positive photoresist figure two bottom sides not dissolve, and cause the negative photoresist dissolving of these figure two bottom sides.That is,,, and produce as shown in Figure 3A counterdie 16 just it does not dissolve if positive photoresist is polluted by amine.If negative photoresist is polluted by amine, just polymerization does not take place in it, and the undercutting of generation shown in Fig. 3 B.
As mentioned above, because produce counterdie or undercutting because amine pollutes, so be difficult to produce accurate Micropicture by prior art, the rate that manufactures a finished product of semiconductor device is not high.
Especially in the integrated 256M DRAM device of height, the width that needs figure is that 0.25 μ m and admissible error are 10%.If have counterdie or undercutting to produce, satisfy width conditions is that 0.225 to 0.275 μ m is practically impossible.Therefore, common process is unsuitable for highly intergrated semiconductor device.
Therefore,, an object of the present invention is to provide a kind of method that forms fine pattern of semiconductor device, thereby form the fine pattern that does not have undercutting or counterdie for overcoming the problem in the above-mentioned prior art.So just, can easily control graphic width.
Another object of the present invention provides a kind of method that forms fine pattern of semiconductor device, thereby can improve the semiconductor device rate that manufactures a finished product.
Another purpose of the present invention provides a kind of method that forms fine pattern of semiconductor device, and this method is suitable for making highly intergrated semiconductor device.
The present invention be based on to counterdie and undercutting be by amine the pollution of wafer is caused with the result of study that can prevent their generation by the oxidation wafer.
Therefore, in order to realize above-mentioned purpose of the present invention, provide a kind of method that forms fine pattern of semiconductor device here, this method comprises the following steps: to be ready to wafer for forming figure; The upper surface of oxidation wafer forms oxide-film; On already oxidised wafer, apply photoresist; And make this photoresist exposure and develop formation photoresist figure.
According to a scheme of the present invention, a kind of method that forms fine pattern in semiconductor device comprises the following steps: to be ready to wafer for forming figure; Utilize oxygen plasma oxidation upper wafer surface, form oxide-film; Already oxidised wafer is made bottom layer treatment; On the wafer of having handled, apply photoresist; And make this photoresist exposure and develop formation photoresist figure.
According to another aspect of the present invention, a kind of method that forms fine pattern in semiconductor device comprises the following steps: to be ready to wafer for forming figure; With the upper surface of strong acid oxidation wafer, form oxide-film; Already oxidised wafer is made bottom layer treatment; On the wafer of having handled, apply photoresist; And make this photoresist exposure and develop formation photoresist figure.
Can obviously find out other purpose of the present invention and scheme from the explanation to embodiment with reference to the accompanying drawings, wherein:
Figure 1A is the sketch that the conventional two component positivity chemistry of expression strengthen the photoresist light reaction;
Figure 1B is the sketch that the conventional three component negative chemicals of expression strengthen the photoresist light reaction;
Fig. 2 A to 2C represents a kind of profile that forms the conventional method of fine pattern with positive photoresist in semiconductor device;
Fig. 3 A to 3C is the another kind of profile that forms the conventional method of fine pattern with negative photoresist in semiconductor device of expression;
Fig. 4 A to 4D is expression forms the method for fine pattern in semiconductor device according to the first embodiment of the present invention a profile; And
Fig. 5 A to 5C is a profile of representing to form according to a second embodiment of the present invention the method for fine pattern in semiconductor device.
Can understand the effect of the preferred embodiment of the present invention better with reference to accompanying drawing, similar Reference numeral is represented similar parts respectively.
Referring to Fig. 4, its expression forms the method for fine pattern in semiconductor device according to the first embodiment of the present invention.
Shown in Fig. 4 A, at first, the surface of oxidation wafer 31 forms the thin oxide film 32 that helps prevent amine and wafer reaction.The thickness of oxide-film 32 is preferably less than 1000 dusts.This oxidation technology is carried out in plasma reactor, in this reactor, under predetermined pressure, makes oxygen stand electric field action, to produce oxygen plasma.Specifically, oxygen plasma is under 10 to the 100mTorr pressure, under about electric field of 10 to 100W, produced by the mixture of pure oxygen or oxygen and argon or nitrogen with about speed of 10 to 1000cm3/min.The bottom that oxide on the wafer 31 does not allow airborne amine to pollute formed figure in subsequent technique is to prevent the undercutting in the prior art or the generation of counterdie.
Available in addition chemical vapor deposition (CVD) technology generations forms oxide-film for this oxygen plasma technology on wafer 31.
Then, carry out a kind of bottom layer treatment technology, to strengthen the adhesiveness of the photoresist that in subsequent technique, on wafer, forms.
Shown in Fig. 4 B, subsequently, coating positive photoresist 33 on the oxide-film on the wafer 31 32.Also can apply negative photoresist in addition and replace positive photoresist 33.
Shown in Fig. 4 C, after this, utilize light 35 to make positive photoresist 33 exposures with photomask 34.
Shown in Fig. 4 D, last, the positive photoresist that develops and exposed forms photoresist figure 36 on the oxide-film on the wafer 31 32.
Referring to Fig. 5, its expression forms the method for fine pattern according to a second embodiment of the present invention in semiconductor device.
Shown in Fig. 5 A, at first, the surface of oxidation wafer 41, growth helps prevent the thin oxide film 42 of amine and wafer 41 reactions.This oxidation technology is used in the strong acid and is polluted the amine on wafer 41 surfaces.This strong acid is optional from sulfuric acid, phosphoric acid, nitric acid and hydrochloric acid.Then, carry out a kind of bottom layer treatment technology, to strengthen the adhesiveness of the photoresist that in subsequent technique, on wafer 41, forms.
Shown in Fig. 5 B, subsequently, coating negative photoresist 43 on the oxide-film on the wafer 41 42.Can replace negative photoresist 43 to apply by positive photoresist in addition.
Shown in Fig. 5 C, after this, make negative photoresist 43 exposures by light 45 with photomask 44.
Shown in Fig. 5 D, last, this negative photoresist 43 that develops forms photoresist figure 46 on the oxide-film on the wafer 41 42.
As mentioned above, the method according to this invention prevents that with the oxidation of wafer surface amine from polluting wafer, thereby forms the accurate fine pattern that does not have counterdie or undercutting.Therefore, method of the present invention can easily be controlled the width of figure.Since these advantages, the method according to this invention, and the rate of finished products of semiconductor production increases.Simultaneously, the method according to this invention needing to be very beneficial for the manufacturing of the highly intergrated semiconductor device of fine pattern.
Though the invention has been described with example above, should be understood that used term is to be used for illustrating essence of the present invention, rather than limitation of the present invention here.
According to above-mentioned indication, can make various corrections and modification to the present invention, so should be understood that, within the scope of the appended claims, can utilize the present invention in every way, and be not limited to those descriptions.

Claims (20)

1. method that forms fine pattern of semiconductor device, this method may further comprise the steps:
Be ready to wafer for forming figure;
The upper surface of the said wafer of oxidation forms oxide-film;
On already oxidised said wafer, apply photoresist; And
Make said photoresist exposure and develop formation photoresist figure.
2. according to the method for claim 1, it is characterized in that: carry out said oxidation step by oxygen plasma treatment.
3. according to the method for claim 2, it is characterized in that: utilization is carried out said oxygen plasma treatment by the plasma reactor of the said upper wafer surface of oxygen plasma oxidation therein.
4. according to the method for claim 3, it is characterized in that: the gas flow rate under 10 to the 100mTorr pressure, in about 10 to 100 watts electric field, with 10 to 1000cm3/min produces said oxygen plasma.
5. according to the method for claim 4, it is characterized in that: said oxygen plasma utilizes pure oxygen to produce.
6. according to the method for claim 4, it is characterized in that: said oxygen plasma is to utilize the mixture of oxygen and argon to produce.
7. according to the method for claim 4, it is characterized in that: said oxygen plasma is to utilize the mixture of oxygen and nitrogen to produce.
8. according to the method for claim 1, it is characterized in that: carry out said oxidation step by chemical vapor deposition.
9. according to the method for claim 1, it is characterized in that: carry out said oxidation step by strong acid.
10. according to the method for claim 9, it is characterized in that: said strong acid is selected from sulfuric acid, phosphoric acid, nitric acid and hydrochloric acid.
11. the method according to claim 1 is characterized in that: said oxide thickness is about 1000 dusts or littler.
12., before said applying step, also comprise the step of said upper wafer surface being made bottom layer treatment according to the method for claim 1.
13. a method that forms fine pattern of semiconductor device, this method may further comprise the steps:
Be ready to wafer for forming figure;
With the upper surface of the said wafer of oxygen plasma oxidation, form oxide-film;
Said already oxidised wafer is made bottom layer treatment;
On the said wafer of having handled, apply photoresist; And
Make said photoresist exposure and develop formation photoresist figure.
14. the method according to claim 13 is characterized in that: utilization is carried out said oxidation step by the plasma reactor of the said upper wafer surface of oxygen plasma oxidation therein.
15. the method according to claim 14 is characterized in that: be the gas flow rate under 10 to the 100mTorr pressure, under about 10 to 100 watts electric field, with 10 to 1000cm3/min, produce said oxygen plasma.
16. the method according to claim 15 is characterized in that: said oxygen plasma utilizes pure oxygen to produce.
17. the method according to claim 15 is characterized in that: said oxygen plasma is to utilize the mixture of oxygen and argon to produce.
18. the method according to claim 15 is characterized in that: said oxygen plasma is to utilize the mixture of oxygen and nitrogen to produce.
19. a method that forms fine pattern of semiconductor device, this method may further comprise the steps:
Be ready to wafer for forming figure;
With the upper surface of the said wafer of strong acid oxidation, form oxide-film;
Said already oxidised wafer is made bottom layer treatment;
On the said wafer of having handled, apply photoresist; And
Make said photoresist exposure and develop formation photoresist figure.
20. the method according to claim 19 is characterized in that: said strong acid is selected from sulfuric acid, phosphoric acid, nitric acid and hydrochloric acid.
CN96107007A 1995-06-26 1996-06-26 Method for forming fine patterns of semiconductor device Expired - Fee Related CN1080929C (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1019950017482A KR0172237B1 (en) 1995-06-26 1995-06-26 Method of manufacturing micropattern of semiconductor device
KR17482/95 1995-07-15

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CN1147147A true CN1147147A (en) 1997-04-09
CN1080929C CN1080929C (en) 2002-03-13

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JP (1) JPH09120942A (en)
KR (1) KR0172237B1 (en)
CN (1) CN1080929C (en)
DE (1) DE19625595B4 (en)
GB (1) GB2302759B (en)
TW (1) TW384514B (en)

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CN101713914B (en) * 2008-10-01 2013-06-12 台湾积体电路制造股份有限公司 Photomask and method of fabricating a photomask
CN104124205A (en) * 2014-07-18 2014-10-29 华进半导体封装先导技术研发中心有限公司 RDL preparation method
CN105789475A (en) * 2014-12-24 2016-07-20 固安翌光科技有限公司 Organic light-emitting device and preparation method thereof

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US6656643B2 (en) 2001-02-20 2003-12-02 Chartered Semiconductor Manufacturing Ltd. Method of extreme ultraviolet mask engineering
US6582861B2 (en) 2001-03-16 2003-06-24 Applied Materials, Inc. Method of reshaping a patterned organic photoresist surface
KR100704838B1 (en) * 2001-06-14 2007-04-09 삼성광주전자 주식회사 Brush and brush manufacturing method for a motor
KR100391001B1 (en) * 2001-06-28 2003-07-12 주식회사 하이닉스반도체 Method for forming a metal line
JP4822239B2 (en) * 2001-09-28 2011-11-24 Hoya株式会社 Mask blank, method for manufacturing the same, and method for manufacturing the mask
KR20030043724A (en) * 2001-11-27 2003-06-02 엔이씨 일렉트로닉스 코포레이션 Method of manufacturing semiconductor device
KR100437614B1 (en) * 2001-12-22 2004-06-30 주식회사 하이닉스반도체 Method for forming metal interconnection line of semiconductor device

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Publication number Priority date Publication date Assignee Title
CN101713914B (en) * 2008-10-01 2013-06-12 台湾积体电路制造股份有限公司 Photomask and method of fabricating a photomask
CN104124205A (en) * 2014-07-18 2014-10-29 华进半导体封装先导技术研发中心有限公司 RDL preparation method
CN105789475A (en) * 2014-12-24 2016-07-20 固安翌光科技有限公司 Organic light-emitting device and preparation method thereof

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Publication number Publication date
CN1080929C (en) 2002-03-13
TW384514B (en) 2000-03-11
GB9613344D0 (en) 1996-08-28
KR0172237B1 (en) 1999-03-30
GB2302759A (en) 1997-01-29
DE19625595B4 (en) 2005-10-20
JPH09120942A (en) 1997-05-06
DE19625595A1 (en) 1997-01-02
KR970003413A (en) 1997-01-28
GB2302759B (en) 2000-07-19

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