CN112266295A - Organic water-soluble fertilizer containing ox gall essence and preparation method thereof - Google Patents
Organic water-soluble fertilizer containing ox gall essence and preparation method thereof Download PDFInfo
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- CN112266295A CN112266295A CN202011172652.5A CN202011172652A CN112266295A CN 112266295 A CN112266295 A CN 112266295A CN 202011172652 A CN202011172652 A CN 202011172652A CN 112266295 A CN112266295 A CN 112266295A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
- C05F17/20—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation using specific microorganisms or substances, e.g. enzymes, for activating or stimulating the treatment
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F17/00—Preparation of fertilisers characterised by biological or biochemical treatment steps, e.g. composting or fermentation
- C05F17/40—Treatment of liquids or slurries
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
- C05G5/23—Solutions
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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Abstract
The invention discloses an organic water-soluble fertilizer containing ox gall, which comprises a substrate and a base solution, wherein the substrate comprises willow leaves, ox gall liquid, brown sugar, white spirit, strains, mineral fulvic acid raw powder, nitrogen phosphorus potassium, zinc, manganese and molybdenum and purified water; the base liquid is amino acid stock solution. The invention also discloses a preparation method of the organic water-soluble fertilizer. The invention can directly absorb the multiple vitamins, amino acids, peptides and minerals contained in the fertilizer by the root system of the crops, and provides more comprehensive nutrition, thereby leading the crops to achieve the effects of strongly rooting, improving the disease resistance, resisting premature senility and improving the yield and the quality.
Description
Technical Field
The invention relates to the technical field of organic fertilizers, and particularly relates to an organic water-soluble fertilizer containing ox gall and a preparation method thereof.
Background
In order to ensure the yield of crops, fertilizers are generally used in the crop planting process, and organic water-soluble fertilizers are used more at present. The organic water-soluble fertilizer is a multi-element compound fertilizer dissolved in water, has the characteristics of instant dissolution, high absorption rate, quick response, no residue, convenient application and the like, and is suitable for fertigation, foliar fertilization, soilless culture and the like. However, the traditional water-soluble fertilizer has unreasonable component proportion, incomplete nutrition, short duration and easy crop premature senility, and the crops after being fertilized have poor disease resistance, low yield and poor quality.
In addition, the existing organic water-soluble fertilizer is prepared by mixing compounds, so that the cost is high and the preparation process is complex. For example, in the patent of CN111533617A entitled "a nanocarbon organic fertilizer containing chitosan oligosaccharide and polyglutamic acid", the organic fertilizer comprises polyglutamic acid, mineral silicon titanium fine powder, amino acid stock solution, nanocarbon, biochar, a soil conditioner, trace elements and Chinese herbs, and the organic fertilizer has the effect of improving the nutrient content of soil, but is also prepared from various compounds, and has high cost and poor disease resistance.
Disclosure of Invention
In view of the above, the invention aims to provide the organic water soluble fertilizer containing the ox gall, which is low in cost, strong in environmental protection, strong in crop disease resistance and capable of promoting crop root growth and resisting premature senility, aiming at the defects of the prior art.
In order to achieve the purpose, the invention adopts the following technical scheme:
an organic water-soluble fertilizer containing ox gall comprises a substrate and a base solution, wherein the substrate comprises leaves, ox gall liquid, brown sugar, white spirit, strains, mineral fulvic acid raw powder, nitrogen phosphorus potassium, zinc manganese molybdenum and purified water; the base liquid is amino acid stock solution with the solution concentration of 80 percent.
Preferably, the leaves are fresh willow leaves.
Preferably, the addition amounts of the leaves, the purified water and the fel bovis seu Bubali solution are as follows by weight: 0.5-2 parts of leaves, 2-4 parts of purified water and 1-3 parts of ox gall essence liquid.
Preferably, the adding amount of the brown sugar is 2.5-4% of the total amount of the leaves.
Preferably, the white spirit is 60 degrees, and the addition amount of the white spirit is 0.05-0.15% of the total amount of the leaves.
Preferably, the addition amount of the strains is 0.15-0.25% of the total amount of the leaves; the strain is bacillus licheniformis or bacillus mucilaginosus.
Preferably, the addition amount of the mineral fulvic acid raw powder is 1-2% of the total amount of the leaves.
Preferably, the addition amount of the nitrogen, phosphorus and potassium is 4-6% of the total amount of the leaves; the addition amount of the zinc, manganese and molybdenum is 0.2-0.4% of the total amount of the leaves.
Preferably, the substrate and the base solution are added in a ratio of 1: 2.
A preparation method of an organic water-soluble fertilizer containing ox gall comprises the following steps:
(1) treatment of raw materials: washing fresh willow leaves, weighing according to the weight ratio, and crushing the weighed leaves by using a crusher to obtain crushed leaves for later use;
(2) fermentation treatment: placing crushed leaves in an autoclave, sterilizing at 260 ℃ for 70min, taking out, cooling to room temperature, then putting into a fermentation tank, simultaneously adding brown sugar, purified water, white spirit and strains into the fermentation tank, performing sealed and light-proof fermentation for 90 days, and performing deflation treatment when an air inflation condition occurs in the fermentation tank during fermentation to obtain a fermentation liquid;
(3) chelating treatment: adding weighed ox gall liquid, mineral source fulvic acid raw powder, nitrogen phosphorus potassium and zinc manganese molybdenum into fermentation liquor, uniformly stirring, and standing at normal temperature for 24 hours to obtain a water-soluble fertilizer primary liquid;
(4) preparation of the water-soluble fertilizer: and mixing the water-soluble fertilizer primary solution and the amino acid stock solution according to a ratio to obtain the organic water-soluble fertilizer.
The invention is further explained:
the willow leaves are used as basic raw materials, so that the resource is rich, the cost is low, the existing resources are reasonably utilized, and the fallen leaf garbage is further reduced; willow leaves contain abundant saccharides, amino acids, vitamins, flavones, triterpenes and lactones, can effectively improve the disease resistance and bacteriostatic ability of crops as water-soluble fertilizers, and are easy to absorb by the crops.
Brown sugar: the brown sugar contains various monosaccharide and polysaccharide energy substances such as glucose and fructose, and also contains partial substances such as vitamins, electrolytes, amino acids, cellulose, antioxidation and the like, and the substances can provide required nutrition for crops; meanwhile, brown sugar can effectively inhibit harmful bacteria from breeding in the ferment fermentation process, so that the ferment is prevented from deteriorating.
White spirit: the ferment is added with white spirit, so that the fermentation speed is accelerated, and various nutrient substances are fully fused.
Strain: the fertilizer can supplement beneficial microorganisms in soil, improve the disease resistance of crops, release fixed nutrient elements in the soil and activate the soil.
And (3) ox gall essence liquid: the plant growth regulator is rich in taurine, and has the effects of stimulating the development of reproductive organs of crops, improving the pollination and fruit-bearing capacity, promoting the transfer and absorption of plants to minerals such as calcium, iron, zinc and the like, regulating the ion balance of plant cells, and promoting the synthesis and storage of starch, sugar, protein and vitamins.
Mineral source fulvic acid raw powder: has the effects of degrading soil heavy metals, retaining water and fertilizer, promoting nutrient element conversion, supplementing organic matters and improving crop quality.
Nitrogen, phosphorus and potassium: provides a large amount of nitrogen, phosphorus and potassium elements for the growth of crops.
Zinc, manganese and molybdenum: provides the trace elements of zinc, manganese and molybdenum required by the growth of crops.
Amino acid stock solution: the amino acid can promote the growth of plant root systems, improve the germination of seeds, synthesize protein and provide nitrogen for the growth in a pressure period; promoting photosynthesis of plant leaves, enhancing disease and insect resistance of plants, increasing sugar content of crops, improving quality and increasing yield.
The invention has the beneficial effects that:
the invention can promote crops to take root, has obvious inhibiting effect on soil-borne diseases caused by pythium, rhizoctonia, fusarium oxysporum, verticillium wilt, fusarium and the like, and can directly absorb various vitamins, amino acids, peptides and minerals contained in the fermentation liquid by the root system of the crops to provide more comprehensive nutrition, thereby enabling the crops to achieve the effects of strongly taking root, improving disease resistance, resisting premature senility and improving yield and quality.
The bacillus licheniformis, the bacillus mucilaginosus and beneficial biological bacteria generated in the fermentation process have the function of promoting the decomposition of fixed nitrogen, phosphorus, potassium and other nutrient elements in the soil, the decomposed products can be absorbed by crops again, the functions of loosening the soil and balancing the pH value of the soil are achieved, and the soil growth environment is improved for the crops. The added organic ox gall essence liquid also has the functions of stimulating the development of crop reproductive organs, improving the pollination and fruit-bearing capacity, promoting the transport and absorption of plants to mineral substances such as calcium, iron, zinc and the like, regulating the ion balance of plant cells, and promoting the synthesis and storage of starch, sugar, protein and vitamin, thereby increasing the crop yield and improving the crop quality.
The preparation method is simple, the stability of the efficacy of the components of the water-soluble fertilizer is ensured, and the nutrient is more comprehensive, the fertility is more durable and the capability of inhibiting germs is stronger by adding the ox gall and the mineral source fulvic acid raw powder.
Detailed Description
The present invention will be further described with reference to the following examples.
Example 1
An organic water soluble fertilizer containing ox gall essence comprises a substrate and a base solution, wherein the substrate comprises fresh willow leaves, ox gall essence liquid, brown sugar, white spirit, strains, mineral fulvic acid raw powder, nitrogen phosphorus potassium, zinc manganese molybdenum and purified water; the base liquid is amino acid stock solution with the solution concentration of 80 percent.
Wherein the addition amounts of the leaves, the purified water and the fel bovis Seu Bubali extract are as follows by weight: 0.5 part of leaves, 2 parts of purified water and 1 part of ox gall essence liquid, wherein the addition amount of brown sugar is 2.5 percent of the total amount of the leaves; the Chinese liquor is 60% (v/v), and the addition amount is 0.05% of the total amount of leaves.
The addition amount of the strain is 0.15 percent of the total amount of the leaves; the strain is Bacillus mucilaginosus. The addition amount of the mineral source fulvic acid raw powder is 1 percent of the total amount of the leaves. The addition amount of the nitrogen, the phosphorus and the potassium is 4 percent of the total amount of the leaves; the addition amount of the zinc, manganese and molybdenum is 0.2 percent of the total amount of the leaves.
And mixing the substrate and the base solution in the ratio by weight of 1.
The preparation method of the organic water-soluble fertilizer containing the ox gall comprises the following steps:
(1) treatment of raw materials: washing fresh willow leaves, weighing according to the weight ratio, and crushing the weighed leaves by using a crusher to obtain crushed leaves for later use;
(2) fermentation treatment: placing crushed leaves in an autoclave, sterilizing at 260 ℃ for 70min, taking out, cooling to room temperature, then putting into a fermentation tank, simultaneously adding brown sugar, purified water, white spirit and strains into the fermentation tank, performing sealed and light-proof fermentation for 90 days, and performing deflation treatment when an air inflation condition occurs in the fermentation tank during fermentation to obtain a fermentation liquid;
(3) chelating treatment: adding weighed ox gall liquid, mineral source fulvic acid raw powder, nitrogen phosphorus potassium and zinc manganese molybdenum into the fermentation liquor, and uniformly stirring to obtain a water-soluble fertilizer primary liquid;
(4) preparation of the water-soluble fertilizer: and mixing the water-soluble fertilizer primary solution and the amino acid stock solution according to a ratio to obtain the organic water-soluble fertilizer.
Example 2
Compared with the embodiment 1, the difference of the embodiment is that the raw material proportion is different,
the addition amounts of the leaves, the purified water and the ox gall liquid in the organic water-soluble fertilizer are as follows according to parts by weight: 0.5-2 parts of leaves, 2-4 parts of purified water and 1-3 parts of ox gall extract, wherein the addition amount of brown sugar is 2.5-4% of the total amount of the leaves; the Chinese liquor is 60% (v/v), and the addition amount is 0.05-0.15% of the total amount of leaves.
The addition amount of the strain is 0.15-0.25% of the total amount of the leaves; the strain is Bacillus mucilaginosus. The addition amount of the mineral source fulvic acid raw powder is 1-2% of the total amount of the leaves. The addition amount of the nitrogen, the phosphorus and the potassium is 4-6% of the total amount of the leaves; the addition amount of the zinc, manganese and molybdenum is 0.2-0.4% of the total amount of the leaves.
And mixing the substrate and the base solution in the weight ratio of 1: 2.
The preparation method of the organic water-soluble fertilizer is consistent with the embodiment.
Example 3
Compared with the embodiment 1, the difference of the embodiment is that the raw material proportion is different,
the addition amounts of the leaves, the purified water and the ox gall liquid in the organic water-soluble fertilizer are as follows according to parts by weight: 1 part of leaves, 3 parts of purified water and 2 parts of ox gall essence liquid, wherein the addition amount of brown sugar is 3% of the total amount of the leaves; the Chinese liquor is 60% (v/v), and the addition amount is 0.1% of the total amount of leaves.
The addition amount of the strain is 0.2 percent of the total amount of the leaves; the strain is bacillus licheniformis and bacillus mucilaginosus which are mixed in equal amount. The addition amount of the mineral source fulvic acid raw powder is 1.5 percent of the total amount of the leaves. The addition amount of the nitrogen, the phosphorus and the potassium is 5% of the total amount of the leaves; the addition amount of the zinc, manganese and molybdenum is 0.3 percent of the total amount of the leaves.
And mixing the substrate and the base solution in the weight ratio of 1: 2.
The preparation method of the organic water-soluble fertilizer is consistent with the embodiment.
The organic water-soluble fertilizers prepared in examples 1-3 were used for corn planting: randomly selecting four mu fields as a No. 1-3 test field and a No. 4 control field respectively; and corn was planted, four acres of field were fertilized with equal amounts at the time of tassel of corn, the organic water-soluble fertilizer prepared in examples 1 to 3 was applied to each acre of test field, the compound fertilizer commonly used in the market was applied to the control field, and irrigation was carried out.
The four-ridge field corn is analyzed after the corn is ripe, and the results are as follows:
the corn in each mu of test field is more developed than the corn in the control field in root system, the corn cob is larger, the grains are more full, no diseases exist in the fruiting period, the insect pests on the corn are few, and the yield of each ridge of corn in the No. 1-3 test field is 400 jin more than that of the control field; in addition, the corn stalks in the test field are still emerald green when the corns are mature, so that the sufficient nutrient components of the corns are ensured.
The corn insect damage in the control field is serious, the corn has diseases, the corn stalks are dried and yellow when the corn is immature, the corn grains are shriveled, and the yield is low.
The soil of the test field and the soil of the control field are respectively analyzed, so that the pH value stability of the test field is high, the pH value of the soil of the control field is seriously unbalanced, the nutrient content of the soil of the test field is high, and the soil of the test field contains a large amount of amino acid, vitamin, mineral substances and the like which are easy to be absorbed by crops.
The results show that the organic water soluble fertilizer has the advantages of promoting the growth of crop roots, having strong disease resistance and anti-senilism capability, and effectively improving the yield and quality of crops.
Finally, the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting, and other modifications or equivalent substitutions made by the technical solutions of the present invention by those of ordinary skill in the art should be covered within the scope of the claims of the present invention as long as they do not depart from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. An organic water-soluble fertilizer containing ox gall is characterized by comprising a substrate and a base solution, wherein the substrate comprises leaves, ox gall solution, brown sugar, white spirit, strains, mineral fulvic acid raw powder, nitrogen phosphorus potassium, zinc, manganese and molybdenum and purified water; the base liquid is amino acid stock solution with the solution concentration of 80 percent.
2. The organic water-soluble fertilizer containing the bovine biliary substance of claim 1, wherein the leaves are fresh willow leaves.
3. The organic water-soluble fertilizer containing the ox gall extract as claimed in claim 2, wherein the addition amounts of the leaves, the purified water and the ox gall extract are as follows by weight: 0.5-2 parts of leaves, 2-4 parts of purified water and 1-3 parts of ox gall essence liquid.
4. The organic water-soluble fertilizer containing the bovine biliary extract as claimed in claim 3, wherein the brown sugar is added in an amount of 2.5-4% of the total amount of the willow leaves.
5. The organic water-soluble fertilizer containing the ox gall extract as claimed in claim 4, wherein the white spirit is 60 degrees, and the addition amount of the white spirit is 0.05-0.15% of the total amount of the leaves.
6. The organic water-soluble fertilizer containing the bovine biliary extract of claim 5, wherein the addition amount of the strain is 0.15-0.25% of the total amount of the leaves; the strain is bacillus licheniformis or bacillus mucilaginosus.
7. The organic water-soluble fertilizer containing the bovine biliary extract of claim 6, wherein the addition amount of the mineral original fulvic acid powder is 1-2% of the total amount of the leaves.
8. The organic water-soluble fertilizer containing the ox gall extract as claimed in claim 7, wherein the addition amount of the nitrogen, the phosphorus and the potassium is 4-6% of the total amount of the leaves; the addition amount of the zinc, manganese and molybdenum is 0.2-0.4% of the total amount of the leaves.
9. The organic water-soluble fertilizer containing the bovine biliary extract of claim 8, wherein the ratio of the substrate to the base solution is 1: 2.
10. A method for preparing the organic water-soluble fertilizer containing the bovine biliary extract as defined in any one of claims 1 to 9, which comprises the following steps:
(1) treatment of raw materials: washing fresh willow leaves, weighing according to the weight ratio, and crushing the weighed leaves by using a crusher to obtain crushed leaves for later use;
(2) fermentation treatment: placing crushed leaves in an autoclave, sterilizing at 260 ℃ for 70min, taking out, cooling to room temperature, then putting into a fermentation tank, simultaneously adding brown sugar, purified water, white spirit and strains into the fermentation tank, performing sealed and light-proof fermentation for 90 days, and performing deflation treatment when an air inflation condition occurs in the fermentation tank during fermentation to obtain a fermentation liquid;
(3) chelating treatment: adding weighed ox gall liquid, mineral source fulvic acid raw powder, nitrogen phosphorus potassium and zinc manganese molybdenum into fermentation liquor, uniformly stirring, and standing at normal temperature for 24 hours to obtain a water-soluble fertilizer primary liquid;
(4) preparation of the water-soluble fertilizer: and mixing the water-soluble fertilizer primary solution and the amino acid stock solution according to a ratio to obtain the organic water-soluble fertilizer.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114773131A (en) * | 2022-05-23 | 2022-07-22 | 郑州昕爵生物技术有限公司 | Special suspended alcohol water-soluble fertilizer for figs and preparation method thereof |
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