CN110759721A - 一种宴会瓷及制备方法 - Google Patents

一种宴会瓷及制备方法 Download PDF

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CN110759721A
CN110759721A CN201911049727.8A CN201911049727A CN110759721A CN 110759721 A CN110759721 A CN 110759721A CN 201911049727 A CN201911049727 A CN 201911049727A CN 110759721 A CN110759721 A CN 110759721A
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banquet
porcelain
feldspar
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张建美
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Liling Zhenmei Art Porcelain Co Ltd
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Abstract

本发明公开了一种宴会瓷及制备方法,配方包括:粘土、长石、石英、碱土硅酸盐、碳酸盐、无水乙醇、氮化铝、金属氧化物、醋水和烧结助剂,各组分的质量百分含量分别是:15‑25%的粘土、20‑30%的长石、15‑25%的石英、10‑20%的碱土硅酸盐、2‑4%的碳酸盐、10‑20%的无水乙醇、1‑3%的氮化铝、5‑10%的金属氧化物、0.5‑1%的醋水和0.5‑1%的烧结助剂;制备方法包括以下步骤,步骤一,原料选取;步骤二,粉末制作;步骤三,制备陶胚;步骤四,干燥烧结;步骤五,宴会花纹烧制;步骤六,成品包装,该发明,安全可靠,采用粘土、长石与石英作为原料,先使用粉碎机进行粉碎,再利用化学进行固相法粉碎,粉碎更加彻底,有利于增加宴会瓷密度与硬度,同时避免宴会瓷煅烧开裂。

Description

一种宴会瓷及制备方法
技术领域
本发明涉及宴会瓷技术领域,具体为一种宴会瓷及制备方法。
背景技术
中国早在约公元前8000-2000年就发明了陶器,用陶土烧制的器皿叫陶器,用瓷土烧制的器皿叫瓷器,陶瓷则是陶器、炻器和瓷器的总称,古人称陶瓷为瓯,凡是用陶土和瓷土这两种不同性质的粘土为原料,经过配料、成型、干燥、焙烧等工艺流程制成的器物都可以叫陶瓷,通常纹上花纹在宴会上使用;传统宴会瓷原料直接采用粉碎机进行粉碎,粉碎不彻底,降低宴会瓷密度与硬度,煅烧时极易开裂,同时传统宴会瓷直接采用颜料涂抹,极其不耐磨,不利于用户使用,且传统宴会瓷原料昂贵,加工麻烦,不利于加工与生产,针对这些缺陷,设计一种宴会瓷及制备方法是很有必要的。
发明内容
本发明的目的在于提供一种宴会瓷及制备方法,以解决上述背景技术中提出的问题。
为了解决上述技术问题,本发明提供如下技术方案:一种宴会瓷,配方包括:粘土、长石、石英、碱土硅酸盐、碳酸盐、无水乙醇、氮化铝、金属氧化物、醋水和烧结助剂,各组分的质量百分含量分别是:15-25%的粘土、20-30%的长石、15-25%的石英、10-20%的碱土硅酸盐、2-4%的碳酸盐、10-20%的无水乙醇、1-3%的氮化铝、5-10%的金属氧化物、0.5-1%的醋水和0.5-1%的烧结助剂。
一种宴会瓷的制备方法,包括以下步骤,步骤一,原料选取;步骤二,粉末制作;步骤三,制备陶胚;步骤四,干燥烧结;步骤五,宴会花纹烧制;步骤六,成品包装;
其中上述步骤一中,按照各组分的质量百分含量分别是:15-25%的粘土、20-30%的长石、15-25%的石英、10-20%的碱土硅酸盐、2-4%的碳酸盐、10-20%的无水乙醇、1-3%的氮化铝、5-10%的金属氧化物、0.5-1%的醋水和0.5-1%的烧结助剂进行选取,并按照重量百分比之和为1进行称取;
其中上述步骤二中,粉末制作包括以下步骤:
1)将粘土、长石与石英倒入置料桶中,兑入一定量的水清洗搅拌;
2)将清洗后的粘土、长石与石英倒入粉碎机中,开启粉碎机进行打碎;
3)将打碎后的粉末混合物倒入反应釜,加入一定量的水,在兑入碳酸盐,升高温度至250-300℃,反应1-2h;
4)反应完成后,取出反应后的混合粉末,放置阴凉地静置冷却;
其中上述步骤三中,制备陶胚包括以下步骤:
1)人工将步骤二4)中混合粉末倒入搅拌釜中,兑入碱土硅酸盐,持续搅拌2-3h;
2)再兑入无水乙醇与氮化铝,升高料温至35-45℃,搅拌釜中通入惰性气体,反应1-2h;
3)将2)中混合物取出,放入压力容器中,采用压力容器直接静压成型;
其中上述步骤四中,干燥烧结包括以下步骤:
1)将步骤三中静压成型的陶胚放入醋水中进行清洗,再放入烧结助剂,浸泡1-2h;
2)再将浸泡完成的陶胚放入煅烧炉中,升温至200-300℃,加热30min进行干燥,随后将温度升高至800-950℃,煅烧1-2h;
3)将煅烧完成成型的陶胚放入保温箱中,逐步减少温度使其冷却;
其中上述步骤五中,宴会花纹烧制包括以下步骤:
1)将冷却好的陶胚浸水1-2h,再拿出使用刀具进行镌刻花纹;
2)将镌刻好的花纹涂抹上金属氧化物,涂抹完成后静置20min;
3)将涂抹完成的陶胚再次放入煅烧炉中进行煅烧,煅烧2-3h,即可得到宴会瓷;
其中上述步骤六中,将上述步骤五中所得的宴会瓷放在阴凉地静置冷却,冷却完成后装入泡沫箱中保存。
根据上述技术方案,所述组分的质量百分含量分别是:粘土16%、长石25%、石英20%、碱土硅酸盐10%、碳酸盐4%、无水乙醇10%、氮化铝3%、金属氧化物10%、醋水1%和烧结助剂1%。
根据上述技术方案,所述粘土为高岭石,长石为钠长石。
根据上述技术方案,所述金属氧化物为氧化钇。
根据上述技术方案,所述步骤三1)中兑入的水漫过粘土、长石与石英顶部。
根据上述技术方案,所述步骤五3)中煅烧炉温度在600-800℃。
与现有技术相比,本发明所达到的有益效果是:该发明,安全可靠,采用粘土、长石与石英作为原料,先使用粉碎机进行粉碎,再利用化学进行固相法粉碎,粉碎更加彻底,有利于增加宴会瓷密度与硬度,同时采用醋水浸泡,氮化铝、碱土硅酸盐与碳酸盐进行煅烧,避免宴会瓷煅烧开裂,增加宴会瓷的热导率,金属氧化物涂抹制作宴会瓷花纹,大大增加了耐磨性,有利于用户使用,该发明原料便宜成本低廉,加工方便,有利于加工与生产,该发明工艺简单严谨,能够代替其他较为昂贵的宴会瓷制备方法,效果显著,原料便宜成本低廉,加工方便,大大节约了生产成本,有利于加工与生产。
附图说明
附图用来提供对本发明的进一步理解,并且构成说明书的一部分,与本发明的实施例一起用于解释本发明,并不构成对本发明的限制。在附图中:
图1是本发明的工艺流程图。
具体实施方式
下面将结合本发明实施例中的附图,对本发明实施例中的技术方案进行清楚、完整地描述,显然,所描述的实施例仅仅是本发明一部分实施例,而不是全部的实施例。基于本发明中的实施例,本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例,都属于本发明保护的范围。
请参阅图1,本发明提供一种技术方案:一种宴会瓷及制备方法:
实施例1:
一种宴会瓷,配方包括:粘土、长石、石英、碱土硅酸盐、碳酸盐、无水乙醇、氮化铝、金属氧化物、醋水和烧结助剂,各组分的质量百分含量分别是:粘土16%、长石20%、石英25%、碱土硅酸盐10%、碳酸盐4%、无水乙醇10%、氮化铝3%、金属氧化物10%、醋水1%和烧结助剂1%。
一种宴会瓷的制备方法,包括以下步骤,步骤一,原料选取;步骤二,粉末制作;步骤三,制备陶胚;步骤四,干燥烧结;步骤五,宴会花纹烧制;步骤六,成品包装;
其中上述步骤一中,按照各组分的质量百分含量分别是:粘土16%、长石20%、石英25%、碱土硅酸盐10%、碳酸盐4%、无水乙醇10%、氮化铝3%、金属氧化物10%、醋水1%和烧结助剂1%进行选取,并按照重量百分比之和为1进行称取;
其中上述步骤二中,粉末制作包括以下步骤:
1)将粘土、长石与石英倒入置料桶中,兑入一定量的水清洗搅拌,兑入的水漫过粘土、长石与石英顶部;
2)将清洗后的粘土、长石与石英倒入粉碎机中,开启粉碎机进行打碎;
3)将打碎后的粉末混合物倒入反应釜,加入一定量的水,在兑入碳酸盐,升高温度至250-300℃,反应1-2h;
4)反应完成后,取出反应后的混合粉末,放置阴凉地静置冷却;
其中上述步骤三中,制备陶胚包括以下步骤:
1)人工将步骤二4)中混合粉末倒入搅拌釜中,兑入碱土硅酸盐,持续搅拌2-3h;
2)再兑入无水乙醇与氮化铝,升高料温至35-45℃,搅拌釜中通入惰性气体,反应1-2h;
3)将2)中混合物取出,放入压力容器中,采用压力容器直接静压成型;
其中上述步骤四中,干燥烧结包括以下步骤:
1)将步骤三中静压成型的陶胚放入醋水中进行清洗,再放入烧结助剂,浸泡1-2h;
2)再将浸泡完成的陶胚放入煅烧炉中,升温至200-300℃,加热30min进行干燥,随后将温度升高至800-950℃,煅烧1-2h;
3)将煅烧完成成型的陶胚放入保温箱中,逐步减少温度使其冷却;
其中上述步骤五中,宴会花纹烧制包括以下步骤:
1)将冷却好的陶胚浸水1-2h,再拿出使用刀具进行镌刻花纹;
2)将镌刻好的花纹涂抹上金属氧化物,涂抹完成后静置20min;
3)将涂抹完成的陶胚再次放入煅烧炉中进行煅烧,煅烧2-3h,即可得到宴会瓷,煅烧炉温度在600-800℃;
其中上述步骤六中,将上述步骤五中所得的宴会瓷放在阴凉地静置冷却,冷却完成后装入泡沫箱中保存。
其中,粘土为高岭石,长石为钠长石,金属氧化物为氧化钇。
实施例2:
一种宴会瓷,配方包括:粘土、长石、石英、碱土硅酸盐、碳酸盐、无水乙醇、氮化铝、金属氧化物、醋水和烧结助剂,各组分的质量百分含量分别是:粘土16%、长石25%、石英20%、碱土硅酸盐10%、碳酸盐4%、无水乙醇10%、氮化铝3%、金属氧化物10%、醋水1%和烧结助剂1%。
一种宴会瓷的制备方法,包括以下步骤,步骤一,原料选取;步骤二,粉末制作;步骤三,制备陶胚;步骤四,干燥烧结;步骤五,宴会花纹烧制;步骤六,成品包装;
其中上述步骤一中,按照各组分的质量百分含量分别是:粘土16%、长石25%、石英20%、碱土硅酸盐10%、碳酸盐4%、无水乙醇10%、氮化铝3%、金属氧化物10%、醋水1%和烧结助剂1%进行选取,并按照重量百分比之和为1进行称取;
其中上述步骤二中,粉末制作包括以下步骤:
1)将粘土、长石与石英倒入置料桶中,兑入一定量的水清洗搅拌,兑入的水漫过粘土、长石与石英顶部;
2)将清洗后的粘土、长石与石英倒入粉碎机中,开启粉碎机进行打碎;
3)将打碎后的粉末混合物倒入反应釜,加入一定量的水,在兑入碳酸盐,升高温度至250-300℃,反应1-2h;
4)反应完成后,取出反应后的混合粉末,放置阴凉地静置冷却;
其中上述步骤三中,制备陶胚包括以下步骤:
1)人工将步骤二4)中混合粉末倒入搅拌釜中,兑入碱土硅酸盐,持续搅拌2-3h;
2)再兑入无水乙醇与氮化铝,升高料温至35-45℃,搅拌釜中通入惰性气体,反应1-2h;
3)将2)中混合物取出,放入压力容器中,采用压力容器直接静压成型;
其中上述步骤四中,干燥烧结包括以下步骤:
1)将步骤三中静压成型的陶胚放入醋水中进行清洗,再放入烧结助剂,浸泡1-2h;
2)再将浸泡完成的陶胚放入煅烧炉中,升温至200-300℃,加热30min进行干燥,随后将温度升高至800-950℃,煅烧1-2h;
3)将煅烧完成成型的陶胚放入保温箱中,逐步减少温度使其冷却;
其中上述步骤五中,宴会花纹烧制包括以下步骤:
1)将冷却好的陶胚浸水1-2h,再拿出使用刀具进行镌刻花纹;
2)将镌刻好的花纹涂抹上金属氧化物,涂抹完成后静置20min;
3)将涂抹完成的陶胚再次放入煅烧炉中进行煅烧,煅烧2-3h,即可得到宴会瓷,煅烧炉温度在600-800℃;
其中上述步骤六中,将上述步骤五中所得的宴会瓷放在阴凉地静置冷却,冷却完成后装入泡沫箱中保存。
其中粘土为高岭石,长石为钠长石,金属氧化物为氧化钇。
实施例3:
一种宴会瓷,配方包括:粘土、长石、石英、碱土硅酸盐、碳酸盐、无水乙醇、氮化铝、金属氧化物、醋水和烧结助剂,各组分的质量百分含量分别是:粘土16%、长石30%、石英15%、碱土硅酸盐10%、碳酸盐4%、无水乙醇10%、氮化铝3%、金属氧化物10%、醋水1%和烧结助剂1%。
一种宴会瓷的制备方法,包括以下步骤,步骤一,原料选取;步骤二,粉末制作;步骤三,制备陶胚;步骤四,干燥烧结;步骤五,宴会花纹烧制;步骤六,成品包装;
其中上述步骤一中,按照各组分的质量百分含量分别是:粘土16%、长石30%、石英15%、碱土硅酸盐10%、碳酸盐4%、无水乙醇10%、氮化铝3%、金属氧化物10%、醋水1%和烧结助剂1%进行选取,并按照重量百分比之和为1进行称取;
其中上述步骤二中,粉末制作包括以下步骤:
1)将粘土、长石与石英倒入置料桶中,兑入一定量的水清洗搅拌,兑入的水漫过粘土、长石与石英顶部;
2)将清洗后的粘土、长石与石英倒入粉碎机中,开启粉碎机进行打碎;
3)将打碎后的粉末混合物倒入反应釜,加入一定量的水,在兑入碳酸盐,升高温度至250-300℃,反应1-2h;
4)反应完成后,取出反应后的混合粉末,放置阴凉地静置冷却;
其中上述步骤三中,制备陶胚包括以下步骤:
1)人工将步骤二4)中混合粉末倒入搅拌釜中,兑入碱土硅酸盐,持续搅拌2-3h;
2)再兑入无水乙醇与氮化铝,升高料温至35-45℃,搅拌釜中通入惰性气体,反应1-2h;
3)将2)中混合物取出,放入压力容器中,采用压力容器直接静压成型;
其中上述步骤四中,干燥烧结包括以下步骤:
1)将步骤三中静压成型的陶胚放入醋水中进行清洗,再放入烧结助剂,浸泡1-2h;
2)再将浸泡完成的陶胚放入煅烧炉中,升温至200-300℃,加热30min进行干燥,随后将温度升高至800-950℃,煅烧1-2h;
3)将煅烧完成成型的陶胚放入保温箱中,逐步减少温度使其冷却;
其中上述步骤五中,宴会花纹烧制包括以下步骤:
1)将冷却好的陶胚浸水1-2h,再拿出使用刀具进行镌刻花纹;
2)将镌刻好的花纹涂抹上金属氧化物,涂抹完成后静置20min;
3)将涂抹完成的陶胚再次放入煅烧炉中进行煅烧,煅烧2-3h,即可得到宴会瓷,煅烧炉温度在600-800℃;
其中上述步骤六中,将上述步骤五中所得的宴会瓷放在阴凉地静置冷却,冷却完成后装入泡沫箱中保存。
其中粘土为高岭石,长石为钠长石,金属氧化物为氧化钇。
各实施例性质对比如下表:
Figure DEST_PATH_IMAGE002
基于上述,本发明的优点在于,该发明,安全可靠,采用粘土、长石与石英作为原料,先使用粉碎机进行粉碎,再利用化学进行固相法粉碎,粉碎更加彻底,有利于增加宴会瓷密度与硬度,同时采用醋水浸泡,氮化铝、碱土硅酸盐与碳酸盐进行煅烧,避免宴会瓷煅烧开裂,增加宴会瓷的热导率,金属氧化物涂抹制作宴会瓷花纹,大大增加了耐磨性,有利于用户使用,该发明原料便宜成本低廉,加工方便,有利于加工与生产。
需要说明的是,在本文中,诸如第一和第二等之类的关系术语仅仅用来将一个实体或者操作与另一个实体或操作区分开来,而不一定要求或者暗示这些实体或操作之间存在任何这种实际的关系或者顺序。而且,术语“包括”、“包含”或者其任何其他变体意在涵盖非排他性的包含,从而使得包括一系列要素的过程、方法、物品或者设备不仅包括那些要素,而且还包括没有明确列出的其他要素,或者是还包括为这种过程、方法、物品或者设备所固有的要素。
最后应说明的是:以上所述仅为本发明的优选实施例而已,并不用于限制本发明,尽管参照前述实施例对本发明进行了详细的说明,对于本领域的技术人员来说,其依然可以对前述各实施例所记载的技术方案进行修改,或者对其中部分技术特征进行等同替换。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。

Claims (7)

1.一种宴会瓷,其特征在于:配方包括:粘土、长石、石英、碱土硅酸盐、碳酸盐、无水乙醇、氮化铝、金属氧化物、醋水和烧结助剂,各组分的质量百分含量分别是:15-25%的粘土、20-30%的长石、15-25%的石英、10-20%的碱土硅酸盐、2-4%的碳酸盐、10-20%的无水乙醇、1-3%的氮化铝、5-10%的金属氧化物、0.5-1%的醋水和0.5-1%的烧结助剂。
2.一种宴会瓷的制备方法,包括以下步骤,步骤一,原料选取;步骤二,粉末制作;步骤三,制备陶胚;步骤四,干燥烧结;步骤五,宴会花纹烧制;步骤六,成品包装;其特征在于:
其中上述步骤一中,按照各组分的质量百分含量分别是:15-25%的粘土、20-30%的长石、15-25%的石英、10-20%的碱土硅酸盐、2-4%的碳酸盐、10-20%的无水乙醇、1-3%的氮化铝、5-10%的金属氧化物、0.5-1%的醋水和0.5-1%的烧结助剂进行选取,并按照重量百分比之和为1进行称取;
其中上述步骤二中,粉末制作包括以下步骤:
1)将粘土、长石与石英倒入置料桶中,兑入一定量的水清洗搅拌;
2)将清洗后的粘土、长石与石英倒入粉碎机中,开启粉碎机进行打碎;
3)将打碎后的粉末混合物倒入反应釜,加入一定量的水,在兑入碳酸盐,升高温度至250-300℃,反应1-2h;
4)反应完成后,取出反应后的混合粉末,放置阴凉地静置冷却;
其中上述步骤三中,制备陶胚包括以下步骤:
1)人工将步骤二4)中混合粉末倒入搅拌釜中,兑入碱土硅酸盐,持续搅拌2-3h;
2)再兑入无水乙醇与氮化铝,升高料温至35-45℃,搅拌釜中通入惰性气体,反应1-2h;
3)将2)中混合物取出,放入压力容器中,采用压力容器直接静压成型;
其中上述步骤四中,干燥烧结包括以下步骤:
1)将步骤三中静压成型的陶胚放入醋水中进行清洗,再放入烧结助剂,浸泡1-2h;
2)再将浸泡完成的陶胚放入煅烧炉中,升温至200-300℃,加热30min进行干燥,随后将温度升高至800-950℃,煅烧1-2h;
3)将煅烧完成成型的陶胚放入保温箱中,逐步减少温度使其冷却;
其中上述步骤五中,宴会花纹烧制包括以下步骤:
将冷却好的陶胚浸水1-2h,再拿出使用刀具进行镌刻花纹;
将镌刻好的花纹涂抹上金属氧化物,涂抹完成后静置20min;
将涂抹完成的陶胚再次放入煅烧炉中进行煅烧,煅烧2-3h,即可得到宴会瓷;
其中上述步骤六中,将上述步骤五中所得的宴会瓷放在阴凉地静置冷却,冷却完成后装入泡沫箱中保存。
3.根据权利要求1所述的一种宴会瓷,其特征在于:所述组分的质量百分含量分别是:粘土16%、长石25%、石英20%、碱土硅酸盐10%、碳酸盐4%、无水乙醇10%、氮化铝3%、金属氧化物10%、醋水1%和烧结助剂1%。
4.根据权利要求1所述的一种宴会瓷,其特征在于:所述粘土为高岭石,长石为钠长石。
5.根据权利要求1所述的一种宴会瓷,其特征在于:所述金属氧化物为氧化钇。
6.根据权利要求2所述的一种宴会瓷的制备方法,其特征在于:所述步骤三1)中兑入的水漫过粘土、长石与石英顶部。
7.根据权利要求2所述的一种宴会瓷的制备方法,其特征在于:所述步骤五3)中煅烧炉温度在600-800℃。
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GB1310574A (en) * 1969-03-10 1973-03-21 Nippon Toki Kk White porcelain body
EP0080213A2 (en) * 1981-11-25 1983-06-01 Kabushiki Kaisha Toshiba Highly heat-conductive ceramic material
WO2001017925A1 (de) * 1999-09-03 2001-03-15 Siemens Aktiengesellschaft Verfahren zur herstellung eines porzellans, porzellan sowie keramischer isolator aus einem porzellan
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