CN109925247B - Toning lotion with full-stage acne removing effect and preparation method thereof - Google Patents
Toning lotion with full-stage acne removing effect and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a toning lotion with a full-stage acne removing effect and a preparation method thereof. The toning lotion with the full-stage acne removing effect comprises the following components in percentage by mass: 5-15% of total-stage acne removing composition, wherein the composition comprises water, radix rehmanniae (REHMANNIA CHINENSIS) extract, hydroxyethyl piperazine ethanesulfonic acid, cortex Phellodendri (PHELLODENDRON AMURENSE) extract, butanediol, and herba Centellae (CENTELLA ASIATICA) leaf extract; 95-85% of cosmetic auxiliary material matrix. The invention is characterized in that aiming at the mechanism of the formation of the pox, the inhibition is carried out at each stage of the induction of the formation of the pox, and finally the safe and effective acne-removing effect is achieved.
Description
Technical Field
The invention relates to a skin care product, belongs to the technical field of daily chemicals, and particularly relates to toning lotion with a full-stage acne removing effect and a preparation method thereof.
Background
Acne, commonly known as whelk, is a chronic inflammation of the pilosebaceous glands caused by multiple factors. It is common among all kinds of people, especially among teenagers, both men and women. Acne, papule, pustule, nodule, cyst, etc. are formed mainly on the face and chest and back, which brings negative influence to the psychological and social interaction of patients.
The pathogenesis of acne is mainly as follows: under the influence of androgen, sebaceous gland is activated, sebum is excessively secreted, and open acne is formed; the follicular orifice is blocked due to disordered and excessive keratinization of the cutin, and closed acne is formed by open acne; inflammation is caused by overgrowth of acne bacteria; with the immune response, acne gradually worsens, forming chronic inflammation.
Acne is a common skin disease of people and has high morbidity. Probably because most people think that the acne is not caused by the common acne, the first choice is usually not to visit doctors at all but to prefer some acne-removing medicines or cosmetics to try to remove the acne in the face of the acne-removing needs, and if the acne-removing products are not selected properly, the acne-removing products can cause damage to the skin of the face of a patient, so that the acne is aggravated.
At present, acne removing products on the market are full of Linglan, and supervision departments are difficult to supervise in place. The food and drug administration in Shanghai has published a blacklist of health food and acne-removing cosmetics containing prohibited drug components, and the acne-removing cosmetics containing prohibited drugs are coated on the inspected products for a long time, and antibacterial drugs are illegally added. The substances can achieve the false image with good cosmetic effect in a short period, but consumers can easily generate contact dermatitis after long-term use, hormone faces are easily formed, serious people can cause drug resistance to antibiotics, and finally, the substances can cause health hidden troubles due to no drug.
Disclosure of Invention
In view of the problems in the prior art, a first object of the present invention is to provide a lotion with a full-stage acne removing effect, which can inhibit the activation of sebaceous glands for each stage of acne pathogenesis; accelerating cutin shedding to keep pores open; the acne bacteria are sterilized, and the number of the acne bacteria is reduced; has the effects of resisting oxidation, diminishing inflammation and reducing inflammation, and has the effect of removing acnes in all stages.
The second purpose of the invention is to provide a cosmetic lotion with the full-stage acne removing compound and the full-stage acne removing effect.
In order to achieve the two purposes, the invention adopts the following technical scheme:
the toning lotion with the full-stage acne removing effect comprises the following components in percentage by mass:
5-15% of a complete-stage acne removing compound, wherein the proportion of each component is as follows: 60-80% of water, 0.5-2% of rehmannia glutinosa (REHMANNIA CHINENSIS) root extract, 5-15% of hydroxyethylpiperazineethanesulfonic acid, 0.15-0.5% of cortex Phellodendri (PHELLODENDRON AMURENSE) bark extract, 10-20% of butanediol, 0.05-0.2% of centella asiatica (CENTELLA ASIATICA) leaf extract;
further, the full-stage acne removing compound is prepared from the following components in parts by weight:
70.66% water;
18% of butanediol;
1% of rehmannia glutinosa Libosch root extract;
10% of hydroxyethylpiperazine ethanesulfonic acid;
0.25% phellodendron amurense bark extract;
0.09% of centella asiatica leaf extract.
The components of the composition function roughly as follows:
rehmannia glutinosa (REHMANNIA CHINENSIS) root extract: inhibiting sebum activation and inhibiting excessive sebum secretion;
hydroxyethyl piperazine ethane sulfonic acid: accelerate cutin shedding and keep pores open;
cortex Phellodendri (PHELLODENDRON AMURENSE) bark extract: the acne bacteria are sterilized, and the number of the acne bacteria is reduced;
centella asiatica (CENTELLA ASIATICA) leaf extract: anti-oxidation, anti-inflammation and inflammation reduction; combining efficacy and ingredient considerations.
The humectant is selected from one or more of glycerin, butylene glycol, propylene glycol, 1, 3-propanediol, 1, 2-pentanediol, hexylene glycol, caprylyl glycol, ethylhexyl glycerin, polyethylene glycol-32, methyl gluceth-20, glyceryl acrylate/acrylic acid copolymer, glyceryl polyether-26, urea, allantoin, sodium PCA, PEG/PPG-17/6 copolymer, bis-PEG-18 methyl ether dimethylsilane, sorbitol, and combinations thereof;
said skin conditioning agent is selected from one or more of soluble proteoglycan, yeast extract, hydrolyzed rice protein, wild soybean (Glycine SOJA) protein, yeast/rice fermentation product filtrate, ALOE vera (Aloe Barbadensis) leaf juice powder, and combinations thereof;
the thickening agent is selected from one or more of sodium polyacrylate, acrylic acid (ester) copolymer sodium, carbomer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, acryloyl dimethyl taurate/VP copolymer, hydroxyethyl acrylate/acryloyl dimethyl taurate copolymer, xanthan gum, hydrolyzed SCLEROTIUM rolfsii (scleritum rolfsii) gum, hydroxyethyl acrylate/acryloyl dimethyl taurate copolymer and gellan gum;
the chelating agent is selected from one or more of disodium EDTA, tetrasodium EDTA and the combination thereof;
the solubilizer is one or more selected from PEG-60 hydrogenated castor oil, polysorbate-60 and polysorbate-20.
The selected preservative is selected from one or more of methylparaben, propylparaben, chlorphenesin, sodium dehydroacetate, and combinations thereof.
The pH regulator is one or more selected from citric acid, sodium citrate, sodium hydroxide, potassium hydroxide and their composition.
In order to achieve the second object, the invention adopts the following technical scheme:
the invention discloses a preparation method of a full-stage acne removing compound, which comprises the following process steps:
1) adding water and hydroxyethyl piperazine ethanesulfonic acid into a water phase pot, stirring and heating to 80-85 ℃, preserving heat and stirring for 20-25 minutes;
2) adding cooling water, stirring, cooling to 40-45 deg.C, adding butanediol, radix rehmanniae (REHMANNIA CHINENSIS) extract, cortex Phellodendri (Phellodendoron AMURENSE) extract, and herba Centellae (CENTELLA ASIATICA) leaf extract, and stirring for 15-20 min;
3) and continuously stirring and cooling until the temperature is lower than 38 ℃, stopping stirring, and discharging after the detection is qualified.
In addition, the invention also provides a preparation method of the toning lotion with the full-stage acne removing effect, which comprises the following steps:
1) adding water, humectant, thickener, chelating agent, and antiseptic (methyl hydroxybenzoate, propyl hydroxybenzoate) pH regulator into water phase pan, stirring and heating to 80-85 deg.C, maintaining the temperature, and stirring for 25-30 min;
2) cooling with boiled cooling water, stirring and cooling to 40-45 deg.C, adding the acne removing compound, skin conditioner, solubilizer, essence and antiseptic (including: chlorphenesin, phenoxyethanol, sodium dehydroacetate) into an emulsifying pot, and stirring for 20-25 minutes;
3) and continuously stirring and cooling until the temperature is lower than 38 ℃, stopping stirring, and discharging through a double-layer 800-mesh filter screen after the detection is qualified.
By the technical scheme, the invention has the following beneficial technical effects:
1) the cosmetic lotion with the full-stage acne removing effect acts on the pathogenesis of the acne formation at each stage of the acne formation. Inhibition of sebaceous gland activation; accelerating cutin shedding to keep pores open; the acne bacteria are sterilized, and the number of the acne bacteria is reduced; anti-oxidation, anti-inflammation and inflammation reduction; the safe and effective acne removing effect in the whole stage is achieved.
2) The acne-removing functional ingredients have a synergistic interaction effect, so that the safe and effective acne-removing effect is achieved.
Detailed Description
The present invention is illustrated by the following examples, which are provided for the purpose of further illustration only and are not intended to limit the scope of the present invention. Other insubstantial modifications and adaptations of the present invention can be made without departing from the scope of the present invention. Unless otherwise specified, the following percentages (%) are mass percentages.
The invention discloses a toning lotion with a full-stage acne removing effect and a preparation method thereof. The toning lotion mainly comprises a full-stage acne removing compound. The proportion of each component of the full-stage acne removing compound is as follows: 60-80% of water, 0.5-2% of radix rehmanniae (REHMANNIA CHINENSIS) extract, 5-15% of hydroxyethyl piperazine ethane sulfonic acid, 0.15-0.5% of cortex Phellodendri (PHELLODENDRON AMURENSE) extract, 10-20% of butanediol, and 0.05-0.2% of herba Centellae (CENTELLA ASIATICA) leaf extract.
The invention is characterized in that aiming at the mechanism of the formation of the pox, the inhibition is carried out at each stage of the induction of the formation of the pox, and finally the safe and effective acne-removing effect is achieved.
Examples 1 to 3
The following table 1 shows the proportion and content of the raw material components of the toning lotion with the full-stage acne removing effect.
TABLE 1 raw material component ratios (% by mass) of examples 1 to 3
The formula and the content of the raw material components of the full-stage acne removing compound A-C are shown in the following table 2.
TABLE 2 raw material component formula of full-stage acne removing compound A-C
The preparation process method of the full-stage acne removing compound A-C can be expressed as follows:
1) adding water and hydroxyethyl piperazine ethanesulfonic acid into a water phase pot, stirring and heating to 80-85 ℃, preserving heat and stirring for 20-25 minutes;
2) adding cooling water, stirring, cooling to 40-45 deg.C, adding butanediol, radix rehmanniae (REHMANNIA CHINENSIS) extract, cortex Phellodendri (Phellodendoron AMURENSE) extract, and herba Centellae (CENTELLA ASIATICA) leaf extract, and stirring for 15-20 min;
3) and continuously stirring and cooling until the temperature is lower than 38 ℃, stopping stirring, and discharging after the detection is qualified.
The preparation method of the full-stage acne-removing lotion of the above embodiments 1 to 3 can be expressed as follows:
1) adding water, allantoin, EDTA-disodium, citric acid, sodium citrate, glycerol, 1, 3-propylene glycol, polyethylene glycol-32, and methyl hydroxybenzoate into water phase pot, stirring and heating to 80-85 deg.C, maintaining the temperature and stirring for 20-25 min;
2) boiling cooling water, stirring, cooling to 40-45 deg.C, adding the acne removing compound A-C, solubilizer, essence, and phenoxyethanol, adding into emulsifying pot, and stirring for 15-20 min;
3) and continuously stirring and cooling until the temperature is lower than 38 ℃, stopping stirring, and discharging after the detection is qualified.
Test example for Effect verification
Acne removing Effect test example 1
1. The tester: 30 persons (20-45 years old), with acne on the face, divided into 3 groups of 10 persons each; one sample formulation was tried per group.
2. Testing parts: a good acne area;
3. the test method comprises the following steps: the GAGS scoring method is adopted.
The specific method comprises the following steps: the good acne part is divided into 6 areas: zone i, forehead, zone ii: right cheek, zone iii: left cheek, region iv: nose, chin zone v, zone vi: chest and upper back. The factor values of the I, II and III zones are 2, the factor values of the IV and V zones are 1, and the factor value of the VI zone is 3;
the skin damage score for each region is (the principle is that the most severe local skin damage determines the score for that region): 0 is no skin damage; 1 is more than or equal to 1 acne; 2 or more than 1 pimple; 3, more than or equal to 1 abscess; 4 is more than or equal to 1 node.
The total score of each subarea is factor score multiplied by skin damage score, and the sum of the total scores of different subareas is the comprehensive score.
4. Testing indexes are as follows: composite score
5. And (3) testing results: see Table 3
Table 3 acne removing effect test results
| Example sample | Before use | It is used for 7 days | It is used for 14 days | It is used for 21 days | It can be used for 28 days |
| Example 1 | 21.58 | 16.23 | 14.59 | 12.78 | 11.60 |
| Example 2 | 21.79 | 14.06 | 11.71 | 9.29 | 7.58 |
| Example 3 | 21.56 | 12.87 | 9.34 | 6.20 | 4.00 |
As can be seen from table 3, examples 1,2 and 3 showed very good acne removing effect. And the composite score reduction of example 3> the composite score reduction of example 2> the composite score reduction of example 1.
Safety test 2
1. The number of tested persons: 30 healthy people, 15 men and 15 women; the age range is 20-45 years.
2. The test method comprises the following steps: the patch test was performed for examples 1-3. Selecting a qualified spot tester, placing about 0.020-0.025 mL of a sample into the spot tester by using a closed spot test method, applying a medical adhesive tape to the back of a subject, removing the subject after 24h, observing skin reactions of 0.5h, 24h and 48h after the spot is removed, and recording results according to the skin reaction grading standard in technical Specification for cosmetic safety (2015 edition).
3. The evaluation criteria are as follows in table 3:
TABLE 3 grading Standard of adverse skin reactions
The results in table 3 show: the human skin closed patch test shows that 0 of 30 persons has positive reaction, and the test object does not cause adverse skin reaction to the batch of test objects according to the regulation in technical Specification for cosmetic safety (2015 edition).
Synergistic test example 3
The formula components of comparative examples 1-4 and examples 4-6 of the invention are proportioned
TABLE 4 raw material composition ratio (unit: mass%) for comparative examples
The manufacturing process of the above comparative examples 1 to 4 and examples 4 to 6 of the present invention can be expressed as follows:
1) adding water, allantoin, EDTA disodium, citric acid, sodium citrate, glycerol, butanediol, polyethylene glycol-32, methyl hydroxybenzoate and hydroxyethyl piperazine ethanesulfonic acid into a water phase pot, stirring and heating to 80-85 deg.C, and stirring for 20-25 min under heat preservation;
2) adding cooling water, stirring, cooling to 40-45 deg.C, adding radix rehmanniae (REHMANNIA CHINENSIS) extract, cortex Phellodendri (Phellodendoron AMURENSE) extract, herba Centellae (CENTELLA ASIATICA) leaf extract, solubilizer, essence, and phenoxyethanol, adding into emulsifying pot, and stirring for 15-20 min;
3) and continuously stirring and cooling until the temperature is lower than 38 ℃, stopping stirring, and discharging after the detection is qualified.
The formulas of comparative examples 1 to 4 and inventive examples 4 to 6 were subjected to the acne removing effect test, and the results are shown in table 5.
Table 5 acne removing effect test results
As can be seen from table 5, the acne removing effect is as follows: example 4> comparative example 3> comparative example 2> comparative example 1, it can be seen that the composition has a good acne removing effect through the synergistic effect among the components of the full-stage acne removing compound. Has more obvious acne removing effect than the combination of one, two or three components.
Wherein, the examples 4-6 are the collocation combinations selected by a large amount of experiments, and the experimental results also prove that the acne removing cream has better acne removing effect.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any simple modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention are within the scope of the technical solution of the present invention.
Claims (2)
1. The toning lotion with the full-stage acne removing effect is characterized by comprising the following components in percentage by weight:
5-15% of a complete-stage acne removing compound, wherein the proportion of each component of the complete-stage acne removing compound is as follows:
70.66% water;
18% of butanediol;
1% of rehmannia glutinosa Libosch root extract;
10% of hydroxyethylpiperazine ethanesulfonic acid;
0.25% phellodendron amurense bark extract;
0.09% of centella asiatica leaf extract;
the full-stage acne removing compound is prepared by the following steps:
1) adding water and hydroxyethyl piperazine ethanesulfonic acid into a water phase pot, stirring and heating to 80-85 ℃, preserving heat and stirring for 20-25 minutes;
2) adding cooling water, stirring, cooling to 40-45 deg.C, adding butanediol, radix et rhizoma Rhei extract, cortex Phellodendri extract, and herba Centellae extract, and stirring for 15-20 min;
3) continuously stirring and cooling to the temperature lower than 38 ℃, stopping stirring, and discharging after the detection is qualified;
95-85% of cosmetic auxiliary material matrix; the cosmetic auxiliary material matrix comprises the following components in percentage by mass:
2. the lotion with full-stage acne removing effect according to claim 1, characterized in that:
the humectant is selected from one or more of glycerin, butylene glycol, 1, 3-propylene glycol, 1, 2-pentanediol, hexylene glycol, caprylyl glycol, ethylhexyl glycerin, polyethylene glycol-32, methyl gluceth-20, glyceryl acrylate/acrylic acid copolymer, glyceryl polyether-26, urea, allantoin, sodium PCA, PEG/PPG-17/6 copolymer, bis-PEG-18 methyl ether dimethylsilane, sorbitol, and combinations thereof;
said skin conditioning agent is selected from one or more of soluble proteoglycan, yeast extract, hydrolyzed rice protein, wild soybean (Glycine SOJA) protein, yeast/rice fermentation product filtrate, ALOE vera (Aloe Barbadensis) leaf juice powder, and combinations thereof;
the thickening agent is selected from one or more of sodium polyacrylate, acrylic acid (ester) copolymer sodium, carbomer, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, acryloyl dimethyl taurate/VP copolymer, hydroxyethyl acrylate/acryloyl dimethyl taurate copolymer, xanthan gum, hydrolyzed SCLEROTIUM rolfsii (SCLEROTIUM rolfsii) gum, SCLEROTIUM rolfsii (SCLEROTIUM rolfsii) gum and gellan gum;
the chelating agent is selected from one or more of disodium EDTA, tetrasodium EDTA and the combination thereof;
the solubilizer is selected from one or more of PEG-60 hydrogenated castor oil, polysorbate-60 and polysorbate-20;
the preservative is selected from one or more of methylparaben, propylparaben, chlorphenesin and a combination thereof;
the pH regulator is one or more selected from citric acid, sodium citrate, sodium hydroxide, sodium potassium dehydroacetate and their composition.
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| CN110652486A (en) * | 2019-11-12 | 2020-01-07 | 江苏逸洁生物科技股份有限公司 | Medicinal acne-removing gel |
| CN110787099B (en) * | 2019-12-20 | 2022-02-18 | 广州伽能生物科技有限公司 | Composition for removing acne and preparation method thereof |
| CN111991293B (en) * | 2020-09-13 | 2021-04-16 | 广州丽彦妆生物科技有限公司 | Skin care essence lotion for treating and repairing sensitive acne skin and preparation method thereof |
| CN112107514A (en) * | 2020-09-22 | 2020-12-22 | 鲁南制药集团股份有限公司 | Anti-wrinkle skin care product composition and application thereof |
| CN112826754A (en) * | 2021-01-26 | 2021-05-25 | 广东丸美生物技术股份有限公司 | Concentrated lotion matrix and preparation method and application thereof |
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