CN115671005A - Oil-control capillary pore-collecting composition, oil-control capillary pore-collecting essence and preparation method thereof - Google Patents
Oil-control capillary pore-collecting composition, oil-control capillary pore-collecting essence and preparation method thereof Download PDFInfo
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Abstract
The application discloses an oil-control and capillary-pore-collecting composition, oil-control and capillary-pore-collecting essence and a preparation method thereof. The oil-control capillary pore-collecting composition comprises the following components in parts by weight: 1 part of cinnamon bark extract; 0.002-100 parts of sanguisorba root extract; 0.002-2000 parts of crowtoe seed extract blocks a plurality of passages secreted by grease, has quick response and far better effect than that of a single plant extract, simultaneously solves the problems of compatibility and ionicity of other oil control cosmetics, and can be used in the formula of any dosage form; the oil-control capillary pore-collecting composition is safer and has no stimulation by replacing chemical synthesis or non-natural components in the traditional makeup product.
Description
Technical Field
The application belongs to the technical field of daily cosmetics, and particularly relates to an oil-controlled capillary pore collecting composition, oil-controlled capillary pore collecting essence and a preparation method thereof.
Background
With the improvement of living standard of people, skin problems are more and more emphasized, and a plurality of skins are accompanied by a series of facial skin problems such as glossy complexion, large pores, dark yellow skin, rough skin texture, seborrheic dermatitis and the like at the present stage, so that normal life and work of people are seriously influenced.
However, the existing oil control cosmetics have poor oil control effect, complex formula, large irritation and high sensitization risk.
Disclosure of Invention
In view of the above, the present application provides an oil-controlling pore-narrowing composition, an oil-controlling pore-narrowing essence and a preparation method thereof, and aims to provide an oil-controlling pore-narrowing composition for cosmetics.
In a first aspect, the embodiments of the present application provide an oil-control capillary composition, which comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract.
According to an embodiment of one aspect of the present application, the oil control pore composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.2-10 parts of sanguisorba root extract;
0.2-20 parts of crowtoe seed extract.
According to an embodiment of one aspect of the present application, the oil control pore composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract.
0.02-1000 parts of zostera marina extract.
According to an embodiment of one aspect of the present application, the oil control composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract.
0.02-1000 parts of zostera marina extract;
0.002-1000 parts of red clover flower extract.
According to an embodiment of one aspect of the present application, the oil control pore composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba officinalis root extract;
0.002-2000 parts of crowtoe seed extract.
0.02-1000 parts of zostera marina extract;
0.002-1000 parts of red clover flower extract;
0.002-200 parts of rosewood seed extract.
In a second aspect, the application provides an oil-control capillary Kong Jinghua liquid, which comprises the following components in percentage by mass:
0.01 to 5 percent of cinnamon bark extract;
0.01 to 10 percent of sanguisorba root extract;
0.01-20% of crowtoe seed extract;
0-10% of zostera marina extract;
0-10% of red clover flower extract;
0-2% of rosewood seed extract;
0-2% of polyquaternium-51, lecithin, hydrogenated lecithin, phosphatidylcholine or a combination thereof;
0-8% of humectant;
0-8% of preservative;
0.1-8% of thickening agent;
0-5% of pH regulator;
6 to 99.85 percent of water.
According to an embodiment of one aspect of the application, the oil-control capillary pore essence comprises the following components in percentage by mass:
1% -5% of cinnamon bark extract;
1-10% of sanguisorba root extract;
1-20% of crowtoe seed extract;
1% -5% of zostera marina extract;
1-10% of red clover flower extract;
1% -2% of rosewood seed extract;
0.1% -2% of polyquaternium-51, lecithin, hydrogenated lecithin, phosphatidylcholine or a combination thereof;
0.1 to 5 percent of humectant;
0.1-5% of preservative;
0.1-5% of thickening agent;
0.1-3% of pH regulator;
30 to 93.7 percent of water.
According to an embodiment of one aspect of the application, the humectant is selected from the group consisting of glycerin, butylene glycol, 1,3-propanediol, 1,2-pentanediol, caprylyl glycol, and sodium hyaluronate, or a combination thereof.
According to an embodiment of one aspect of the application, the preservative is selected from phenoxyethanol, p-hydroxyacetophenone, 1,2-pentanediol, 1,2-hexanediol, caprylyl glycol, ethylhexylglycerin, benzoic acid, sodium benzoate, caprylhydroxamic acid, or combinations thereof.
According to an embodiment of one aspect of the application, the thickener is selected from carbomers, acrylic polymers cross-linked with C10-C30 alkanol acrylates, xanthan gum or combinations thereof.
According to an embodiment of one aspect of the present application, the pH adjusting agent is selected from arginine, tromethamine, sodium hydroxide aqueous emulsion or a combination thereof; and 5% of sodium hydroxide water emulsion can be selected.
In a third aspect, the application provides a method for preparing the oil-controlling fine wool Kong Jinghua liquid of the second aspect, comprising:
preparing an aqueous phase solution: mixing humectant, antiseptic, thickener and water;
mixing the aqueous phase solution, cinnamon bark extract, sanguisorba officinalis root extract, crowtoe seed extract, zostera marina extract, red clover flower extract and rosewood seed extract, homogenizing and emulsifying, and adding a pH regulator to obtain the oil-controlling and capillary pore-collecting essence.
In a fourth aspect, the present application provides an oil-controlling cosmetic or pharmaceutical composition comprising: the oil control pore composition of the first aspect and a cosmetically acceptable adjuvant.
Compared with the prior art, the application has at least the following beneficial effects:
the oil-controlling capillary pore-harvesting compositions provided by the present application are all derived from plant extracts of all-natural sources; 1 part of cinnamon bark extract, 0.002-100 parts of sanguisorba officinalis root extract and 0.002-2000 parts of crowtoe seed extract are compounded, so that the synergistic effect and the combined action are realized, the blockage is realized on a plurality of paths secreted by grease, the effect is fast, the effect is far better than that of a single plant extract, the problems of compatibility and ionic property of other oil control cosmetics are solved, and the oil control cosmetic can be used in the formula of any dosage form; the oil-control capillary pore-collecting composition is safer and has no stimulation by replacing chemical synthesis or non-natural components in the traditional makeup product.
Secondly, when the oil-control pore-narrowing composition is added with the efficient polyquaternium-51, the lecithin or the combination thereof, the extract can be effectively promoted to penetrate into the skin, the absorption of the skin to the extract can be improved to the greatest extent, the effect is enhanced, and the effects of controlling oil and refining pores are improved.
Drawings
FIG. 1 shows a graph of skin condition before and after the use of the oil control harvested fine hair Kong Jinghua liquid of example 1;
figure 2 shows a graph of skin condition before and after using the oil control fluff Kong Jinghua liquid of comparative example 1.
Detailed Description
In order to make the application purpose, technical solution and beneficial technical effects of the present application clearer, the present application is further described in detail with reference to the following embodiments. It should be understood that the embodiments described in this specification are only for the purpose of explaining the present application and are not intended to limit the present application.
For the sake of brevity, only some numerical ranges are explicitly disclosed herein. However, any lower limit may be combined with any upper limit to form ranges not explicitly recited; and any lower limit may be combined with any other lower limit to form a range not explicitly recited, and similarly any upper limit may be combined with any other upper limit to form a range not explicitly recited. Also, although not explicitly recited, each point or individual value between endpoints of a range is encompassed within the range. Thus, each point or individual value may, as its lower or upper limit, be combined with any other point or individual value or with other lower or upper limits to form ranges not explicitly recited.
In the description of the present application, it is to be noted that, unless otherwise specified, "above" and "below" are inclusive of the present number, and "plural" of "one or more" means two or more.
The above summary of the present application is not intended to describe each disclosed embodiment or every implementation of the present application. The following description more particularly exemplifies illustrative embodiments. At various points throughout this application, guidance is provided through a list of embodiments that can be used in various combinations. In each instance, the list is provided only as a representative group and should not be construed as exhaustive.
The skin problems of people are more and more emphasized, and the skin of many people is accompanied by a series of facial skin problems such as full gloss, large pores, dark yellow skin, rough skin texture, seborrheic dermatitis and the like, so that the normal life and work are seriously influenced. However, the existing oil control cosmetics have unsatisfactory oil control effect and durability, and most of the existing oil control cosmetics have complex formula, large irritation and high sensitization risk.
In related products, zinc gluconate or zinc PCA and other raw materials with zinc ions are mostly used for controlling oil, so that the effect is not obvious enough on the whole, the onset period is long, and the requirement of consumers for quickly controlling oil cannot be met.
In addition, the existence of zinc ions has great limitation on the use of a cosmetic formula, the zinc ions have great destructiveness on carbomer and an acrylic thickener, the viscosity of a system can be greatly reduced, and meanwhile, the zinc ions have poor compatibility on raw materials with chelating and adsorbing properties, and the formula can be precipitated.
Through the research of the inventor, the invention provides a compound oil-fat-secretion blocking agent which takes plant extracts as main materials, combines a plurality of plant extracts, blocks each passage of oil secretion, has quick response and has better effect than single plant extracts, zinc gluconate and zinc PCA; meanwhile, the problems of compatibility and ionic property are solved, the composition can be used in the formula of any dosage form, and the compatibility with raw materials is not limited.
Based on this, the inventors have conducted a great deal of research and have provided an oil-controlling pore-forming composition comprising specific plant extracts, which can control oil rapidly and effectively while blocking various pathways for oil secretion, zinc gluconate, zinc PCA; meanwhile, the problems of compatibility and ionic property are solved, and the composition can be used in the formula of any dosage form.
Oil control pore composition
In a first aspect, the embodiments of the present application provide an oil-control capillary composition, which comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract. According to the embodiment of the application, the cinnamon extract mainly exists in the form of volatile oil, contains cinnamaldehyde, eugenol and the like, and the oil-controlling and capillary-harvesting composition used for the application has mild stimulation effect and avoids excessive secretion of oil through stimulation; also has effects of promoting blood circulation, removing blood stasis, and relieving fever.
According to the embodiment of the application, the elm root extract has better antiallergic and antioxidant effects and stronger oxygen radical scavenging effect. Can achieve the effect of refining pores by scavenging oxygen free radicals.
According to the embodiment of the application, the crowtoe seed extract is a natural extraction product, and the oil-control capillary pore-collecting composition used for the application is safe, can relieve and resist allergy, enables oil to be naturally secreted, avoids excessive secretion of oil through stimulation, can effectively moisten skin, relieves and repairs the skin, and avoids dryness of the skin. The extract of Lotus japonicus is suitable for 8 types of skin such as non-pigmented skin, tolerant skin, tight skin, wrinkled skin, pigmented skin, sensitive skin, dry skin, and oily skin. In addition, the crowtoe also has the effects of tonifying deficiency and clearing heat, and can reduce the secretion of grease.
According to the embodiment of the application, the cinnamon bark extract, the sanguisorba officinalis root extract and the crowtoe seed extract in parts by weight can act together to effectively control oil secretion and shrink pores.
In some embodiments, the oil control pore composition further comprises 5-200 parts of polyquaternium-51, lecithin, hydrogenated lecithin, phosphatidylcholine, or a combination thereof. The red-removing composition can be better wrapped, and the absorption of the active substances by the skin can be promoted, so that the active substances can more effectively act on the deep layer of the skin, and the red-removing effect is achieved.
In some embodiments, the oil control pore composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.2-10 parts of sanguisorba root extract;
0.2-20 parts of crowtoe seed extract.
According to the embodiment of the application, the cinnamon bark extract, the sanguisorba officinalis root extract and the crowtoe seed extract in parts by weight can act together to further effectively control the secretion of grease and gather pores.
In some embodiments, the oil control composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract.
0.02-1000 parts of zostera marina extract.
According to the embodiment of the application, the oil-control fine pore-harvesting composition containing the zostera marina extract can avoid excessive metabolism of vegetable oil and fat, avoid acne on acne faces and the like, promote skin pores to be cleaner, further adjust water-oil balance of skin and enable the skin to be smoother, smoother and finer; the skin moisturizing and water locking cream also has the functions of moisturizing, moisturizing and locking water, is beneficial to tightly locking deep moisture of the skin, and can also supplement the lacking moisture to the dry skin.
In some embodiments, the oil control pore composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract.
0.02-1000 parts of zostera marina extract;
0.002-1000 parts of red clover flower extract.
According to the present embodiment, the red clover extract contains flavonoids, proteins, amino acids, saccharides, vitamins, and the like. Wherein the isoflavone has strong antioxidant, free radical injury protecting and free radical scavenging effects. The composition for controlling oil and collecting fine pores, which is prepared from the red clover extract, has the effects of whitening, resisting aging and astringing pores. The red clover flower extract is suitable for 7 types of skin, such as non-pigmented skin, firming skin, pigmented skin, dry skin, oily skin, sensitive skin, and wrinkled skin.
In some embodiments, the oil control composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract.
0.02-1000 parts of zostera marina extract;
0.002-1000 parts of red clover flower extract;
0.002-200 parts of rosewood seed extract.
According to the embodiment of the application, the oil-controlled pore-narrowing composition containing the rosewood seed extract can reduce pore blockage and avoid pore enlargement. The rosewood seed extract can also help sebocyte to transfer to other central parts in sebaceous glands, so that sebum synthesis is reduced, excessive oil secretion is reduced, and the problem of oil secretion is radically solved.
In some embodiments, the oil control pore composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
2-10 parts of sanguisorba officinalis root extract;
2-20 parts of crowtoe seed extract;
2-10 parts of zostera marina extract;
2-10 parts of red clover flower extract;
0.2-10 parts of rosewood seed extract.
According to the embodiment of the application, the cinnamon bark extract, the sanguisorba officinalis root extract, the Lotus japonicus seed extract, the zostera marina extract, the red clover flower extract and the rosewood seed extract in parts by weight act together, so that pores can be further effectively narrowed, and grease can be further effectively controlled.
Oil-control fine wool Kong Jinghua liquid
In a second aspect, the application provides an oil-control capillary Kong Jinghua liquid, which comprises the following components in percentage by mass:
0.01 to 5 percent of cinnamon bark extract;
0.01 to 10 percent of sanguisorba root extract;
0.01-20% of crowtoe seed extract;
0-10% of zostera marina extract;
0-10% of red clover flower extract;
0-2% of rosewood seed extract;
0-2% of polyquaternium-51, lecithin, hydrogenated lecithin, phosphatidylcholine or a combination thereof;
0-8% of humectant;
0-8% of preservative;
0.1-8% of thickening agent;
0-5% of pH regulator;
6 to 99.85 percent of water.
The oil-controlling and fine-hair-harvesting Kong Jinghua liquid provided by the application is all from plant extracts of all natural sources; the cinnamon bark extract, the sanguisorba officinalis root extract, the Lotus japonicus seed extract, the zostera marina extract, the red clover flower extract and the rosewood seed extract are compounded, and under the combined action, a plurality of passages secreted by grease are blocked, so that the effect is fast, the effect is far better than that of a single plant extract, the better effect of controlling oil and reducing pores can be achieved, and the safety and the no stimulation are added. Secondly, the extract can be effectively promoted to penetrate into the skin by adding efficient polyquaternium-51, lecithin or a combination of the polyquaternium-51 and the lecithin, so that the absorption of the skin on the extract can be improved to the greatest extent, the effect is enhanced, and the effects of controlling oil and refining pores are improved.
In some embodiments, the oil-controlling harvested nap Kong Jinghua liquid has a viscosity of 10 to 25pa.s, optionally 15 to 22pa.s. The above viscosity was measured using a rotational viscometer. The oil-controlling and fine-hair-harvesting Kong Jinghua liquid with the viscosity has good skin feel and also has the effects of moisturizing and protecting the skin.
In some embodiments, the oil-control pore-forming essence comprises the following components in percentage by mass:
0.01 to 5 percent of cinnamon bark extract;
0.01 to 10 percent of sanguisorba root extract;
0.01-20% of crowtoe seed extract;
0.1-10% of zostera marina extract;
0.01 to 10 percent of red clover flower extract;
0.01 to 2 percent of rosewood seed extract;
0.1% -2% of polyquaternium-51, lecithin, hydrogenated lecithin, phosphatidylcholine or a combination thereof;
0-8% of humectant;
0-8% of preservative;
0-8% of thickening agent;
0-5% of pH regulator;
6 to 99.85 percent of water.
In some embodiments, the oil-control pore-forming essence comprises the following components in percentage by mass:
1% -5% of cinnamon bark extract;
1-10% of sanguisorba root extract;
1-20% of crowtoe seed extract;
1-5% of zostera marina extract;
1-10% of red clover flower extract;
1% -2% of rosewood seed extract;
0.1% -2% of polyquaternium-51, lecithin, hydrogenated lecithin, phosphatidylcholine or a combination thereof;
0.1-5% of humectant;
0.1-5% of preservative;
0.1-5% of thickening agent;
0.1-3% of pH regulator;
30 to 93.7 percent of water.
According to the embodiment of the application, the components with the mass fractions act together, so that the effects of controlling oil and shrinking pores can be improved.
In some embodiments, the humectant is selected from glycerin, butylene glycol, 1,3-propanediol, 1,2-pentanediol, caprylyl glycol, and sodium hyaluronate, or a combination thereof. The humectant can further improve the moisture retention of deep skin and realize long-acting moisture retention.
In some embodiments, the preservative is selected from phenoxyethanol, p-hydroxyacetophenone, 1,2-pentanediol, 1,2-hexanediol, caprylyl glycol, ethylhexyl glycerol, benzoic acid, sodium benzoate, caprylhydroxamic acid, or combinations thereof. The preservative can be well compatible with other substances, and the red-removing service life and shelf life can be prolonged by adding the preservative.
In some embodiments, the thickening agent is selected from carbomers, acrylic polymers crosslinked with C10-C30 alkanol acrylate, xanthan gum, or combinations thereof.
According to the embodiment of the application, the thickening agent has an important effect on thickening, stability and rheological property of the anti-reddening cream for skin; by using the thickener in the above weight ratio, a cream for skin can have good consistency, and excellent spreadability and spreadability.
In some embodiments, the pH adjusting agent is selected from arginine, tromethamine, sodium hydroxide aqueous emulsion, or combinations thereof; and 5% of sodium hydroxide water emulsion can be selected. The pH regulator can regulate the pH of the oil-controlling and fine hair Kong Jinghua liquid, so that the liquid can better act on skin and avoid stimulation. In addition, arginine is an alkaline nutrient substance, acts on skin, and is beneficial to healing and repairing damaged tissues.
Preparation method of oil-control fine wool Kong Jinghua liquid
In a third aspect, the application provides a method for preparing the oil-controlling harvested fine hair Kong Jinghua liquid of the second aspect, comprising:
s100, preparing an aqueous phase solution: mixing humectant, antiseptic, thickener and water;
s200, mixing the aqueous phase solution, the cinnamon bark extract, the sanguisorba officinalis root extract, the Lotus japonicus seed extract, the zostera marina extract, the red clover flower extract and the rosewood seed extract, homogenizing and emulsifying, and adding a pH regulator to obtain the oil-controlling and capillary pore-collecting essence.
The preparation method of the all-natural oil-control capillary pore essence can be used for preparing the oil-control capillary pore Kong Jinghua, is simple in process, short in time consumption, low in equipment requirement, stable in prepared essence system, free of harm to body health of a user, and extremely high in large-scale application potential.
In some embodiments, step S100 comprises: preparing an aqueous phase solution: mixing humectant, antiseptic, thickener and water, heating to 82 + -2 deg.C, maintaining the temperature, stirring and dissolving.
In some embodiments, step S200 comprises: mixing the aqueous phase solution, the cinnamon bark extract, the sanguisorba officinalis root extract, the Lotus japonicus seed extract, the zostera marina extract, the red clover flower extract and the rosewood seed extract, and then cooling to 40-45 ℃.
In some embodiments, step S200 comprises: homogenizing and emulsifying by high-pressure micro-jet equipment.
According to the embodiment of the application, the raw materials are uniformly mixed by a high-pressure micro-jet device. The high-pressure micro-jet equipment is used for promoting the polyquaternium-51, lecithin or the combination thereof to wrap the active components, and simultaneously, the oil-controlling and capillary essence liquid is more uniform and uniform, so that the particle size of the essence liquid can be controlled to be less than 100nm, the absorption of skin is promoted, and the effective action rate is improved.
In a fourth aspect, the present application provides an oil-controlling cosmetic or pharmaceutical composition comprising:
the oil control pore composition of the first aspect and a cosmetically acceptable adjuvant.
The cosmetic or pharmaceutical composition of the present application may be added with various desired cosmetic or pharmaceutically acceptable excipients according to various formulation forms of the composition. For example, when the composition of the present application is prepared as a liquid, the excipient may be selected from water, physiological saline, and the like; when the composition of the present invention is prepared into a gel, the excipient may be selected from cellulose derivatives, starch, gelatin, agar, polysaccharides, and the like; when the composition of the present application is prepared as a cream, the excipient may be selected from glycerin, vaseline, paraffin, etc.; when the composition of the present application is prepared as a foam, the excipient may be selected from hydroxypropyl methylcellulose, sodium lauryl sulfate polyethylene glycol, sodium fatty alcohol-polyoxyethylene ether sulfonate, and the like; when the compositions of the present application are prepared as a patch, the excipient may be selected from cellulose derivatives, starch, gelatin, agar, polysaccharides, and the like.
According to the embodiment of the application, the cosmetic or pharmaceutical composition is suitable for cleaning, washing and protecting skin products such as aqua products, emulsified products, oil products and the like, and can also be used in beauty products such as essences, facial masks and the like, such as ointments, foundation make-up and the like.
Examples
The present disclosure is more particularly described in the following examples that are intended as illustrative only, since various modifications and changes within the scope of the present disclosure will be apparent to those skilled in the art. Unless otherwise indicated, all parts, percentages, and ratios reported in the following examples are on a weight basis, and all reagents used in the examples are commercially available or synthesized according to conventional methods and can be used directly without further treatment, and the equipment used in the examples is commercially available.
Examples 1 to 10
The embodiment of the application provides an oil-control capillary Kong Jinghua liquid, which comprises the following components in percentage by mass:
0.01 to 5 percent of cinnamon bark extract;
0.01 to 10 percent of sanguisorba root extract;
0.01 to 20 percent of crowtoe seed extract;
0-10% of zostera marina extract;
0-10% of red clover flower extract;
0-2% of rosewood seed extract;
0-2% of polyquaternium-51, lecithin, hydrogenated lecithin, phosphatidylcholine or a combination thereof;
0-8% of humectant;
0-8% of preservative;
0.1-8% of thickening agent;
0-5% of pH regulator;
6 to 99.85 percent of water.
The preparation method of the oil-control fine hair Kong Jinghua liquid comprises the following steps:
s100, preparing an aqueous phase solution: mixing humectant, antiseptic, thickener and water;
s200, mixing the aqueous phase solution, the cinnamon bark extract, the sanguisorba officinalis root extract, the Lotus japonicus seed extract, the zostera marina extract, the red clover flower extract and the rosewood seed extract, homogenizing and emulsifying through high-pressure micro-jet treatment, adding a pH regulator to the particle size micro-nano level, and thus obtaining the oil-control oil-collecting capillary essence.
The specific components and amounts of the examples are shown in table 1.
TABLE 1
Comparative examples 1 to 4
The comparative examples of the present application are different from the examples in that: the oil-controlling and fine-wool Kong Jinghua liquid has different components and contents.
Test section
1. Physical and chemical tests the oil control essence is subjected to physical and chemical tests according to methods of visual inspection, a pH tester, standing at different temperatures for different times and the like, and the results are as follows:
1. appearance: a translucent yellowish viscous liquid;
2, pH value: 5.5.0-7.5, viscosity 15-25Pa.s;
3. the heat resistance stability is inspected (48 ℃ multiplied by 48 h) and is qualified;
4. and (6) the cold resistance stability is tested (-15 ℃ multiplied by 48 h) and the product is qualified.
2. To demonstrate the safety and efficacy of the product, the following tests were performed:
1) And safety testing:
the experimental steps are as follows: 30 volunteers, 6 of each volunteer were divided into two groups, the oil control essence samples of examples 1-5 were tested, each tester performed a spot-sticking control experiment on the inner sides of the left and right arms, 1.0g of the product of the present invention was applied to the inner side of the left hand twice a day, and the skin reaction phenomena after 24h, 48h, and 72h were recorded, wherein the inner sides of the right hand and the left hand were coated with 1.0g of blank base material twice a day.
The experimental results are as follows: after the oil control essence samples of examples 1-10 were painted for 24h, 48h and 72h, no allergic phenomena such as skin redness or erythema appeared, which indicates that the oil control essence of the oil control essence samples of examples 1-5 is safe and has no adverse reaction.
2) In vitro efficacy evaluation test:
pore shrinkage test
1. Test objects: selecting 5 forehead grease with the weight of more than 100 mu g/cm 2 The subject is used as an experimental object to evaluate the oil control effect and pore refining effect of the oil control pore refining essence.
2. Detection indexes are as follows:
oil content (μ g/cm) 2 ) Use of a Sebumeter-SM-815 from CK, germany
Total pore volume (mm) 3 ) Using skin tester Antera 3D of Ireland Miravex scientific
Total pore area (mm) 2 )——Antera 3D
3. Experimental method
3.1 test screening: the grease content of the forehead of the subject is tested by a Sebumeter probe, and the grease content of the forehead is more than 100 mu g/cm 2 The groups are entered.
3.2 base value test: the testee cleans the face by using an amino acid cleansing face uniformly provided by a laboratory, and after waiting for 30min in the laboratory environment, the left and right faces of the testee are shot by an Antera 3D image acquisition device, and the grease content at the forehead of the testee is tested.
3.3 test of revisit: the subject uses the product all the face in the morning and evening every day, returns to the laboratory after 12 days, and the subject uses the amino acid face cleaning that the laboratory provided in unison again to clean the face to wait 30min in the laboratory environment after, the laboratory staff shoots the subject's left and right face with an Antera 3D image acquisition device. And the oil content at the forehead was measured with a German CK oil tester, the results are shown in Table 3.
TABLE 3
The experimental results are as follows: and (3) effect comparison: example 10>Example 9>Example 8>Example 7>Example 6>Example 5>Example 4>Example 3>Example 2>>Example 1>Comparative example>Placebo after comparing the sample of example 1 with the placebo, the fat secreted from the forehead was measured to decrease by 76. Mu.g/cm after 8h 2 After comparing the sample of example 2 with the blank, the person tested that the fat secreted from his forehead decreased 81. Mu.g/cm after 8 hours 2 After comparing the sample of example 3 with the blank, the person detected a reduction of 91. Mu.g/cm in the fat secreted by his forehead after 8h 2 After comparing the sample of example 4 with the blank, the person tested that the fat secreted from his forehead had decreased 86. Mu.g/cm after 8 hours 2 After comparing the sample of example 5 with the blank, the person tested that the fat secreted from his forehead decreased 84. Mu.g/cm after 8 hours 2 Examples 5-10 showed more reduction and better oil control. After comparing the sample of comparative example 1 with the blank, the person detected that the fat secreted from the forehead decreased by 71. Mu.g/cm after 8 hours 2 People in contrast toAfter using the sample of comparative example 2 and the blank, the fat secreted by the forehead was measured to decrease by 76. Mu.g/cm after 8h 2 . In conclusion, the oil control effect of the embodiment 10 is the best.
To sum up, the oil control essence that contains oil control cosmetic composition of this application is safe, low amazing, and the essence that often uses oil control cosmetic composition moreover can the effectual grease secretion that restraines facial skin, improves the greasy phenomenon of skin, great improvement people's travelling comfort.
3) Number of pores and pore diameter and volume reduction effect test
Volunteers of oily skin or mixed skin (between 18 and 55 years of age) were divided into 9 groups of 10 persons (5 males, 5 females) per group, volunteers were applied 2 times a day for 30 days using examples 1-3, 6, 7, comparative examples 4-6 and market contestants, and evaluated by image analysis to measure the number of prominent pores (> 0.25 mm) around the cheeks and nose (ratio meter). The results of the test using the reduction in number of pores, diameter of pores and volume after 30 days were compared with the test results of 0 day, and the test results are shown in tables 5 and 6.
Table 4 pore number test results (human) using 7 days
Table 5 test results of pore diameter and volume reduction using 7 days (human)
FIG. 1 is a diagram of the skin condition before and after the application of the oil-controlling pore-forming essence Kong Jinghua of example 1, the left diagram showing the skin condition in the initial state, and the right diagram showing the skin condition after the application of the oil-controlling pore-forming essence of example 1 for 7 days; fig. 2 shows a skin condition before and after the use of the oil-controlling pore-forming essence Kong Jinghua of comparative example 1, the left is the initial skin condition, and the right is the 7-day after the use of the oil-controlling pore-forming essence of comparative example 1.
From the results in tables 4 and 5, it can be seen that the essence solutions of examples 1 to 3, 6 and 7, when used in an amount of 2ml per day, have a greater reduction in the number of pores, pore diameter and volume after 7 days, and have a better pore-forming effect, especially the best pore-forming effect of example 10, compared with the comparative example.
The above description is only for the specific embodiments of the present application, but the scope of the present application is not limited thereto, and any person skilled in the art can easily think of various equivalent modifications or substitutions within the technical scope of the present application, and these modifications or substitutions should be covered within the scope of the present application. Therefore, the protection scope of the present application shall be subject to the protection scope of the claims.
Claims (10)
1. The oil-control capillary pore-collecting composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract.
2. The oil control capillary composition of claim 1, wherein the oil control capillary composition comprises, in parts by weight:
1 part of cinnamon bark extract;
0.2-10 parts of sanguisorba root extract;
0.2-20 parts of crowtoe seed extract.
3. The oil control pore composition according to claim 1 or 2, wherein the oil control pore composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract;
0.02-1000 parts of zostera marina extract.
4. The oil control capillary composition of claim 3, wherein the oil control capillary composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract;
0.02-1000 parts of zostera marina extract;
0.002-1000 parts of red clover flower extract.
5. The oil control capillary composition of claim 4, wherein the oil control capillary composition comprises the following components in parts by weight:
1 part of cinnamon bark extract;
0.002-100 parts of sanguisorba root extract;
0.002-2000 parts of crowtoe seed extract;
0.02-1000 parts of zostera marina extract;
0.002-1000 parts of red clover flower extract;
0.002-200 parts of rosewood seed extract.
6. An oil-control capillary Kong Jinghua liquid comprises the following components in percentage by mass:
0.01 to 5 percent of cinnamon bark extract;
0.01 to 10 percent of sanguisorba root extract;
0.01-20% of crowtoe seed extract;
0-10% of zostera marina extract;
0-10% of red clover flower extract;
0-2% of rosewood seed extract;
0% -2% of polyquaternium-51, lecithin, hydrogenated lecithin, phosphatidylcholine or a combination thereof;
0-8% of humectant;
0-8% of preservative;
0.1-8% of thickening agent;
0 to 5 percent of pH regulator
6 to 99.85 percent of water.
7. The oil-control capillary Kong Jinghua liquid of claim 6, wherein the oil-control capillary essence comprises the following components in percentage by mass:
1% -5% of cinnamon bark extract;
1-10% of sanguisorba root extract;
1-20% of crowtoe seed extract;
1-5% of zostera marina extract;
1-10% of red clover flower extract;
1% -2% of rosewood seed extract;
0.1% -2% of polyquaternium-51, lecithin, hydrogenated lecithin, phosphatidylcholine or a combination thereof;
0.1-5% of humectant;
0.1-5% of preservative;
0.1-5% of thickening agent;
0.1-3% of pH regulator;
30 to 93.7 percent of water.
8. The oil-controlling capillary Kong Jinghua liquid of claim 6 or 7, wherein the humectant is selected from glycerin, butylene glycol, 1,3-propanediol, 1,2-pentanediol, caprylyl glycol, and sodium hyaluronate, or a combination thereof; and/or the presence of a gas in the gas,
the preservative is selected from phenoxyethanol, p-hydroxyacetophenone, 1,2-pentanediol, 1,2-hexanediol, caprylyl glycol, ethylhexyl glycerol, benzoic acid, sodium benzoate, caprylyl hydroxamic acid, or combinations thereof; and/or the presence of a gas in the atmosphere,
the thickening agent is selected from carbomer, acrylic acid cross-linked polymer with C10-C30 alkanol acrylate, xanthan gum or combination thereof; and/or the presence of a gas in the gas,
the pH regulator is selected from arginine, tromethamine, sodium hydroxide water emulsion or the combination thereof; and 5% of sodium hydroxide water emulsion can be selected.
9. A method of preparing the oil-control harvested fine hair Kong Jinghua liquid of any of claims 6-8, comprising:
preparing an aqueous phase solution: mixing humectant, antiseptic, thickener and water;
mixing the aqueous phase solution, cinnamon bark extract, sanguisorba officinalis root extract, crowtoe seed extract, zostera marina extract, red clover flower extract and rosewood seed extract, homogenizing and emulsifying, and adding a pH regulator to obtain the oil-controlling and capillary pore-collecting essence.
10. An oil-controlling cosmetic or pharmaceutical composition comprising: the oil control pore composition of any one of claims 1-5 and a cosmetically acceptable adjuvant.
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Citations (5)
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| KR20020093364A (en) * | 2001-06-08 | 2002-12-16 | 애경산업(주) | Additive compositions including laminaria saccharina extract for cosmetics and cosmetics containing the same |
| CN109330953A (en) * | 2018-12-25 | 2019-02-15 | 广州艾蓓生物科技有限公司 | A kind of oil-control receipts pore Essence |
| CN109718138A (en) * | 2019-02-28 | 2019-05-07 | 北昊干细胞与再生医学研究院有限公司 | Acne-eliminating cosmetic composition and its application |
| CN111297754A (en) * | 2020-02-18 | 2020-06-19 | 广州艾蓓生物科技有限公司 | Day-tightening oil-control essence and preparation method thereof |
| CN115337243A (en) * | 2022-09-14 | 2022-11-15 | 上海臻臣化妆品有限公司 | Blackhead removing composition and cosmetic |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR20020093364A (en) * | 2001-06-08 | 2002-12-16 | 애경산업(주) | Additive compositions including laminaria saccharina extract for cosmetics and cosmetics containing the same |
| CN109330953A (en) * | 2018-12-25 | 2019-02-15 | 广州艾蓓生物科技有限公司 | A kind of oil-control receipts pore Essence |
| CN109718138A (en) * | 2019-02-28 | 2019-05-07 | 北昊干细胞与再生医学研究院有限公司 | Acne-eliminating cosmetic composition and its application |
| CN111297754A (en) * | 2020-02-18 | 2020-06-19 | 广州艾蓓生物科技有限公司 | Day-tightening oil-control essence and preparation method thereof |
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