CN109453089A - Exquisite anti-age corrective eye treatment cream and preparation method thereof - Google Patents

Exquisite anti-age corrective eye treatment cream and preparation method thereof Download PDF

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CN109453089A
CN109453089A CN201811633506.0A CN201811633506A CN109453089A CN 109453089 A CN109453089 A CN 109453089A CN 201811633506 A CN201811633506 A CN 201811633506A CN 109453089 A CN109453089 A CN 109453089A
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parts
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eye treatment
treatment cream
corrective eye
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CN109453089B (en
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吕飞
王华英
黄刚
汪华斌
沈鸿
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Abstract

A kind of exquisiteness anti-age corrective eye treatment cream and preparation method thereof, exquisite anti-age corrective eye treatment cream includes that each component of following mass parts is prepared: dimethyl silicone polymer, polymethylsilsesquioxane, phytosterols oletate, tocopherol acetate, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, carbomer, PEG-240/HDI copolymer pair--20 ether of decyl tetradecyl alcohol polyethers, inulin lauryl carbamate, polyglutamic acid, cyclomethicone/dimethiconol mixture, triethanolamine, caffeine, glucityl aurantiamarin, bigarabe flower extract, inositol, oat beta-glucan, thallus laminariae extract, instant smoothing wrinkle essence, starfish regenerates repair factor, Gotu Kola P.E, centella polypeptide, two split yeast tunning lysis object, antiallergic active peptide, Phenoxyethanol and fragrant fresh ketone.The salubrious non-greasy of quality can be effectively improved 7 big problems of eye circumference skin: microgroove, wrinkle, relaxation, eye pouch, edema, black eye, drying.

Description

Exquisite anti-age corrective eye treatment cream and preparation method thereof
Technical field
The present invention relates to a kind of skin care item, more particularly to a kind of exquisite anti-age corrective eye treatment cream and preparation method thereof.
Background technique
Eye pouch is medically known as skin of lower eyelid sagging disease.Be due to the age increase cause skin of lower eyelid relaxation, skin with Fibr tissue between orbicular muscle of eye, which connects, to be weakened, at the same under eye socket diaphragm and intraocular adipose tissue through socket of the eye every weak part it is outside It is prominent, so that eyelid is subcutaneously formed too fat to move bag shaped structure, therefore claims eye pouch.Eye pouch is a kind of physiological change of normal person.
With advancing age, work and rest time is irregular, and eye skin metabolism slows down, collagen and elasticity Fiber starts slowly to be lost, and the fat for nursing eyeball starts slowly to deposit, finally, eye pouch just produces.
The cause of disease that eye pouch is formed: 1) the aging regression cause of disease is said: (1) skin of lower eyelid elasticity weakens, is loose sagging;(2) lower eyelid Orbicular muscle of eye degenerative change, elasticity weaken, relaxation atrophy;(3) socket of the eye diaphragm denaturation relaxation, holding power weaken;(4) Orbitalis fat becomes Property displacement or Orbitalis fat hyperproliferative.2) inherited pathogenic factor is said: part young man also have occur aging lower eyelid blepharoptosis person, mostly with familial inheritance Factor is related.
Heredity eye pouch is bad using conservative treatment effect, can only pass through operative correction.The eye pouch of vast majority of people belongs to It is acquired.Eye pouch shaping is divided into papebral conjunctiva approach (interior notch) and incision on dermatology (outer notch) two methods, interior notch eye pouch are whole Shape is fair suitable for skin of lower eyelid elasticity, only Orbital septum fat sockdolager, does a notch for being about 0.5CM in papebral conjunctiva, plucks Except superabundant fats, operation wound is small, restores fast, no operation trace.Outer notch eye pouch shaping can remove loose skin simultaneously, Loose orbicular muscle of eye and extra capsula adiposa bulbi, is suitable for various types of eye pouch shapings, surgical effect is more preferably.
The classification of eye pouch: 1) simple Dermatochalasia type: with simple Dermatochalasia, wrinkle increases mainly to show, no socket of the eye every Fatty protrusion and orbicular muscle of eye are plump;2) simple orbicular muscle of eye hypertrophic: it is mainly shown as orbicular muscle of eye plumpness in palpebra inferior shape At it is too fat to move, skin does not relax, it is more between young man Yu;3) Orbital septum fat hernia goes out type: Orbital septum fat, which has no, increased significantly, but socket of the eye Every outer organizational slack, tension is reduced, and is formed Orbital septum fat hernia and is gone out;4) Orbital septum fat increases type: being mainly shown as Orbital septum fat Tissue increases, and exists simultaneously the relaxation of Pi Fu ﹑ orbicular muscle of eye, forms apparent sagging in palpebra inferior;5) mixed type: eyelid bag hair is accounted for Raw majority has the weakness relaxation of skin, orbicular muscle of eye, and has socket of the eye every weak, Orbitalis fat bulging, person in middle and old age are common.
Because there are certain risks for eye pouch plastic operation, even if finishing plastic operation, eye cream is still used in the nursing in later period Nursing is consolidated.The present invention is effective to the first and second class eye pouches, has improvement to rear three classes eye pouch, to eye pouch postoperative care It is effective.
Therefore, it is necessary to a kind of anti-age corrective eye treatment cream be developed, with improve eye circumference skin 7 big problems: microgroove, wrinkle, relaxation, eye Bag, edema, black eye, drying.
Summary of the invention
The purpose of the present invention is overcoming shortcoming in the prior art, provide that a kind of quality is slim and graceful, water profit, energy after use Enough skin is made to take on an entirely new look, the ability for resisting free radical resisting is enhanced, puts down and comfort wrinkle, taking on a new look, restore elasticity, skin profit Damp fine and smooth compact exquisite anti-age corrective eye treatment cream and preparation method thereof.
The purpose of the present invention is achieved through the following technical solutions:
The exquisite anti-age corrective eye treatment cream of one embodiment, each component including following mass parts are prepared:
A phase: 0.05 part~0.8 part of Natrulon H-10 stearate, 0.5 part~5.0 parts of dimethyl silicone polymer, poly- methyl 0.05 part~2.0 parts of silsesquioxane, 0.5 part~5.0 parts of hydrogenated coco-glyceride class, 0.05 part of phytosterols oletate~ 2.0 parts, 0.05 part~2.0 parts of tocopherol acetate;
B phase: 50.0 parts~100.0 parts of deionized water, 1.0 parts~11.0 parts of glycerol, 0.1 part~0.8 part of hydrolecithin, 0.1 part~1.0 parts of hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, 0.2 part of carbomer~0.6 part, PEG- 240/HDI copolymer pair -0.1 part~0.8 part of -20 ether of decyl tetradecyl alcohol polyethers, 0.1 part of inulin lauryl carbamate~ 1.0 part;
C phase: 0.01 part~0.5 part of polyglutamic acid, cyclomethicone/dimethiconol mixture 0.1 Part~2.0 parts;
D phase: 0.15 part~0.55 part of triethanolamine;
E phase: 0.5 part~5.0 parts of caffeine, 0.1 part~2.0 parts of glucityl aurantiamarin, 0.0 part of bigarabe flower extract~ 5.0 parts, 0.5 part~10.0 parts of inositol, 0.5 part~5.0 parts of oat beta-glucan, 0.0 part~4.0 parts of thallus laminariae extract, immediately 0.0 part~3.0 parts of smoothing wrinkle essence, 0.1 part~3.0 parts of repair factor of starfish regeneration, 0.1 part~3.0 parts of Gotu Kola P.E, product Careless 0.1 part~3.0 parts of the polypeptide of snow, two split 0.1 part~3.0 parts of yeast tunning lysis object, antiallergic active peptide 0.1 part~1.5 Part;
F phase: 0.2 part~0.8 part of Phenoxyethanol, 0.1 part~0.5 part of fragrant fresh ketone, 0.01 part~0.1 part of essence.
The exquisite anti-age corrective eye treatment cream of another embodiment, each component including following mass parts are prepared:
A phase: 0.1 part~0.6 part of Natrulon H-10 stearate, 1.0 parts~4.0 parts of dimethyl silicone polymer, poly- methyl silicon 0.1 part~1.0 parts of sesquioxyalkane, 0.8 part~4.0 parts of hydrogenated coco-glyceride class, phytosterols oletate 0.15 part~1.8 Part, 0.2 part~1.7 parts of tocopherol acetate;
B phase: 52.0 parts~90.0 parts of deionized water, 3.0 parts~11.0 parts of glycerol, 0.2 part~0.6 part of hydrolecithin, 0.4 part~1.0 parts of hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, 0.2 part of carbomer~0.5 part, PEG- 240/HDI copolymer pair -0.3 part~0.7 part of -20 ether of decyl tetradecyl alcohol polyethers, 0.2 part of inulin lauryl carbamate~ 0.8 part;
C phase: 0.05 part~0.3 part of polyglutamic acid, cyclomethicone/dimethiconol mixture 0.2 Part~1.0 parts;
D phase: 0.16 part~0.35 part of triethanolamine;
E phase: 1.5 parts~3.0 parts of caffeine, 0.2 part~1.7 parts of glucityl aurantiamarin, 1.0 parts of bigarabe flower extract~ 4.0 parts, 2.5 parts~7.0 parts of inositol, 1.5 parts~4.0 parts of oat beta-glucan, 1.2 parts~3.0 parts of thallus laminariae extract, remove immediately 0.6 part~2.0 parts of essence of wrinkle, starfish regenerate 1.1 parts~2.0 parts of repair factor, 0.8 part of Gotu Kola P.E~2.0 parts, accumulated snow 0.4 part~2.0 parts of careless polypeptide, two split 0.4 part~2.5 parts of yeast tunning lysis object, 0.3 part~1.1 parts of antiallergic active peptide;
F phase: 0.3 part~0.6 part of Phenoxyethanol, 0.1 part~0.4 part of fragrant fresh ketone, 0.01 part~0.07 part of essence.
The exquisite anti-age corrective eye treatment cream of a further embodiment, each component including following mass parts are prepared:
A phase: 0.3 part of Natrulon H-10 stearate, 2.0 parts of dimethyl silicone polymer, 0.5 part of polymethylsilsesquioxane, 3.0 parts of hydrogenated coco-glyceride class, 0.5 part of phytosterols oletate, 0.5 part of tocopherol acetate;
B phase: 58.84 parts of deionized water, 10 parts of glycerol, 0.3 part of hydrolecithin, hydroxy-ethyl acrylate/acryloyl diformazan 0.8 part of base Taurate Copolymer, 0.3 part of carbomer, PEG-240/HDI copolymer pair--20 ether 0.5 of decyl tetradecyl alcohol polyethers Part, 0.3 part of inulin lauryl carbamate;
C phase: 0.1 part of polyglutamic acid, cyclomethicone/0.5 part of dimethiconol mixture;
D phase: 0.25 part of triethanolamine;
E phase: 2.0 parts of caffeine, 0.5 part of glucityl aurantiamarin, 2.0 parts of bigarabe flower extract, 5.0 parts of inositol, oat Portugal 2.0 parts of glycan, 2.0 parts of thallus laminariae extract, 1.0 parts of instant smoothing wrinkle essence, 1.6 parts of repair factor of starfish regeneration, centella mention 1.0 parts of object, 1.0 parts of centella polypeptide, two are taken to split 2.0 parts, 0.5 part of antiallergic active peptide of yeast tunning lysis object;
F phase: 0.5 part of Phenoxyethanol, fragrant 0.2 part of fresh ketone, 0.01 part of essence.
In one of the embodiments, the Gotu Kola P.E be asiaticosid, madecassoside, asiatic acid and Brahmic acid.
The instant smoothing wrinkle essence is Alteromonad tunning extract in one of the embodiments,.
The preparation method of the exquisite anti-age corrective eye treatment cream of one embodiment, comprising the following steps:
Simultaneously sterilizing equipment decontaminating apparatus is cleaned, it is spare;
By Natrulon H-10 stearate, dimethyl silicone polymer, polymethylsilsesquioxane and hydrogenated coco-glyceride class Oily phase pot is added, carries out the first heating stirring operation, constant temperature to material is kept to be completely dissolved, add phytosterols oletate and Tocopherol acetate obtains oil mixture after mixing, wherein the Natrulon H-10 stearate, the poly- diformazan Radical siloxane, the polymethylsilsesquioxane, the hydrogenated coco-glyceride class, the phytosterols oletate and the life The mass ratio for educating phenol acetic acid esters is (0.05~0.8): (0.5~5.0): (0.05~2.0): (0.5~5.0): (0.05~ 2.0): (0.05~2.0);
By deionized water, glycerol, hydrolecithin, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, card Emulsion pot is added in wave nurse, PEG-240/HDI copolymer pair--20 ether of decyl tetradecyl alcohol polyethers and inulin lauryl carbamate, After carrying out the second heating stirring operation, constant temperature is kept for 9 minutes~12 minutes, is carried out the first homogeneous operation, is added polyglutamic acid It is stirred with cyclomethicone/dimethiconol mixture and the oil mixture, in vacuum condition The second homogeneous operation of lower progress, after then carrying out defoaming operation again, be added triethanolamine simultaneously stir evenly, wherein it is described go from It is sub- water, the glycerol, the hydrolecithin, the hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, described Carbomer, PEG-240/HDI copolymer be double-and it is -20 ether of decyl tetradecyl alcohol polyethers, the inulin lauryl carbamate, described Polyglutamic acid, the cyclomethicone/dimethiconol mixture, the oil mixture and three second The mass ratio of hydramine is (50.0~100.0): (1.0~11.0): (0.1~0.8): (0.1~1.0): (0.2~0.6): (0.1~0.8): (0.1~1.0): (0.01~0.5): (0.1~2.0): (1.2~16.8): (0.15~0.55);
After carrying out the first cooling operation, caffeine, glucityl aurantiamarin, bigarabe flower extract, inositol, swallow are sequentially added Wheat glucan, thallus laminariae extract, instant smoothing wrinkle essence, starfish regeneration repair factor, Gotu Kola P.E, centella polypeptide, Two split yeast tunning lysis object and antiallergic active peptide, carry out third stirring operation, and constant temperature keeps to material being completely dissolved, In, it is the caffeine, the glucityl aurantiamarin, the bigarabe flower extract, the inositol, the oat beta-glucan, described Thallus laminariae extract, the instant smoothing wrinkle essence, the starfish regenerate repair factor, the Gotu Kola P.E, the accumulated snow Careless polypeptide, described two split the mass ratio of yeast tunning lysis object and the antiallergic active peptide for (0.5~5.0): (0.1 ~2.0): (0.0~5.0): (0.5~10.0): (0.5~5.0): (0.0~4.0): (0.0~3.0): (0.1~3.0): (0.1~3.0): (0.1~3.0): (0.1~3.0): (0.1~1.5);
After carrying out the second cooling operation, the Phenoxyethanol dissolved in advance and fragrant fresh ketone and essence, stirring are sequentially added Uniformly, anti-age corrective eye treatment cream precursor is obtained;
After carrying out third cooling operation, the anti-age corrective eye treatment cream precursor is subjected to detection operation, carries out filtering and discharging after qualified, Obtain exquisite anti-age corrective eye treatment cream.
The temperature of the first heating stirring operation is 70 DEG C~75 DEG C in one of the embodiments,.
The temperature of the second heating stirring operation is 80 DEG C~85 DEG C in one of the embodiments,.
It is 42 DEG C~44 DEG C by temperature control in one of the embodiments, after the second cooling operation.
It is 38 DEG C~39 DEG C by temperature control in one of the embodiments, after the third cooling operation.
Above-mentioned exquisiteness anti-age corrective eye treatment cream, each component including following mass parts are prepared: dimethyl silicone polymer, poly- methyl Silsesquioxane, phytosterols oletate, tocopherol acetate, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymerization Object, carbomer, PEG-240/HDI copolymer pair--20 ether of decyl tetradecyl alcohol polyethers, inulin lauryl carbamate, polyglutamic Acid, cyclomethicone/dimethiconol mixture, triethanolamine, caffeine, glucityl aurantiamarin, bigarabe Flower extract, inositol, oat beta-glucan, thallus laminariae extract, instant smoothing wrinkle essence, starfish regeneration repair factor, centella mention Object, centella polypeptide, two are taken to split yeast tunning lysis object, antiallergic active peptide, Phenoxyethanol and fragrant fresh ketone.Quality is clearly not It is greasy, 7 big problems of eye circumference skin: microgroove, wrinkle, relaxation, eye pouch, edema, black eye, drying can be effectively improved.
Detailed description of the invention
In order to illustrate the technical solution of the embodiments of the present invention more clearly, below will be to needed in the embodiment attached Figure is briefly described, it should be understood that the following drawings illustrates only certain embodiments of the present invention, therefore is not construed as pair The restriction of range for those of ordinary skill in the art without creative efforts, can also be according to this A little attached drawings obtain other relevant attached drawings.
Fig. 1 is the step flow chart of the preparation method of the exquisite anti-age corrective eye treatment cream of one embodiment of the invention;
Fig. 2 is the step schematic diagram of the application method of the exquisite anti-age corrective eye treatment cream of one embodiment of the invention.
Specific embodiment
To facilitate the understanding of the present invention, a more comprehensive description of the invention is given in the following sections with reference to the relevant attached drawings.In attached drawing Give better embodiment of the invention.But the invention can be realized in many different forms, however it is not limited to herein Described embodiment.On the contrary, the purpose of providing these embodiments is that making to understand more the disclosure Add thorough and comprehensive.
It should be noted that it can directly on the other element when element is referred to as " being fixed on " another element Or there may also be elements placed in the middle.When an element is considered as " connection " another element, it, which can be, is directly connected to To another element or it may be simultaneously present centering elements.Term as used herein " vertical ", " horizontal ", " left side ", " right side " and similar statement for illustrative purposes only, are not meant to be the only embodiment.
Unless otherwise defined, all technical and scientific terms used herein and belong to technical field of the invention The normally understood meaning of technical staff is identical.Term as used herein in the specification of the present invention is intended merely to description tool The purpose of the embodiment of body, it is not intended that in the limitation present invention.Term " and or " used herein includes one or more Any and all combinations of relevant listed item.
In one embodiment, a kind of exquisiteness anti-age corrective eye treatment cream, each component including following mass parts is prepared:
A phase: 0.05 part~0.8 part of Natrulon H-10 stearate, 0.5 part~5.0 parts of dimethyl silicone polymer, poly- methyl 0.05 part~2.0 parts of silsesquioxane, 0.5 part~5.0 parts of hydrogenated coco-glyceride class, 0.05 part of phytosterols oletate~ 2.0 parts, 0.05 part~2.0 parts of tocopherol acetate;
B phase: 50.0 parts~100.0 parts of deionized water, 1.0 parts~11.0 parts of glycerol, 0.1 part~0.8 part of hydrolecithin, 0.1 part~1.0 parts of hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, 0.2 part of carbomer~0.6 part, PEG- 240/HDI copolymer pair -0.1 part~0.8 part of -20 ether of decyl tetradecyl alcohol polyethers, 0.1 part of inulin lauryl carbamate~ 1.0 part;
C phase: 0.01 part~0.5 part of polyglutamic acid, cyclomethicone/dimethiconol mixture 0.1 Part~2.0 parts;
D phase: 0.15 part~0.55 part of triethanolamine;
E phase: 0.5 part~5.0 parts of caffeine, 0.1 part~2.0 parts of glucityl aurantiamarin, 0.0 part of bigarabe flower extract~ 5.0 parts, 0.5 part~10.0 parts of inositol, 0.5 part~5.0 parts of oat beta-glucan, 0.0 part~4.0 parts of thallus laminariae extract, immediately 0.0 part~3.0 parts of smoothing wrinkle essence, 0.1 part~3.0 parts of repair factor of starfish regeneration, 0.1 part~3.0 parts of Gotu Kola P.E, product Careless 0.1 part~3.0 parts of the polypeptide of snow, two split 0.1 part~3.0 parts of yeast tunning lysis object, antiallergic active peptide 0.1 part~1.5 Part;
F phase: 0.2 part~0.8 part of Phenoxyethanol, 0.1 part~0.5 part of fragrant fresh ketone, 0.01 part~0.1 part of essence.
It is appreciated that Natrulon H-10 stearate (Polyaldo 10-1-S) is also known as ten polyglycerol monostearates, it is Good dispersing agent, stabilizer and protective agent enable to the exquisite anti-age corrective eye treatment cream to have the qualities such as better stability, into One step, the production firm of the Natrulon H-10 stearate is Long Sha group, in this way, using the Natrulon H-10 stearic acid Ester is conducive to improve the stability of the exquisite anti-age corrective eye treatment cream.Dimethyl silicone polymer (DC200) is as base oil ingredient, and texture is light Be full of, clearly, non-greasy, formula and sense of touch can be improved, and remain without permanence, be the common desirable feedstock of cosmetic formulations, into One step, the dimethyl silicone polymer production firm is Dow corning company, in this way, using the dimethyl silicone polymer It enables to that the quality of the exquisite anti-age corrective eye treatment cream is slim and graceful, water profit, is taken on an entirely new look using rear skin.Polymethylsilsesquioxane is The organic siliconresin of ball-type, minitype particle diameter be 4 microns~6 microns, the smear of skin care item can be improved, can enhance described in The ductility and smoothness of exquisite anti-age corrective eye treatment cream.Hydrogenated coco-glyceride class is the triglyceride of C10-C18 saturated vegetable fatty acid, It is used as oxidation resistant tallow in the exquisite anti-age corrective eye treatment cream, it is similar to skin texture, it is odorless, do not glue, skin radiance And high-quality skin sense, it can be improved the ability of imperial free radical resisting of the exquisite anti-age corrective eye treatment cream, moistened using rear skin, shine light It is color.Phytosterols oletate is generally made with fatty acid by esterification or transesterification by phytosterol, in the essence It causes to use in anti-age corrective eye treatment cream as conditioner and softening agent.With anti-inflammatory effect, sitosterol has similar to hydrocortisone and hydroxyl The stronger anti-inflammatory effect such as base phenylbutazone, but the side effect without cortisone class;There are also the effects of skin barrier function reparation: iuntercellular Liposome is that ceramide, cholesterol and fatty acid are formed with 1:1:1 molar ratio, and phytosterin ester is similar with cholesterol structure, Alternative cholesterol effect, plays the effect for repairing skin barrier function.Tocopherol acetate is in the exquisite anti-age corrective eye treatment cream It is used as antioxidant, there is good antioxidant effect, tocopherol acetate prevents carefully during body metabolism The readily oxidizable substances such as after birth and intracellular unsaturated fatty acid are oxidized, and prevent the effect of aging;It is also used as internal antioxidant, is disappeared Except interior free yl, injury of the ultraviolet light to human body is reduced.Therefore each component in A phase is used, the exquisiteness can be effectively improved The slim and graceful water profit of anti-age corrective eye treatment cream quality, the ability that eye skin can be made to resist free radical resisting after use are enhanced, put down and comfort microgroove With wrinkle, alleviate relaxation, eye pouch and edema, Vitamin K and solves the problems, such as to dry.
It is appreciated that deionized water is used as solvent, the degree of purity of the exquisite anti-age corrective eye treatment cream is further improved.It is sweet Oil is common moisturizer, and hydrolecithin is a kind of stable emulsification that lecithin adds hydrogen to be formed under the effect of the catalyst Agent, moisturizer, can be improved the performance of keeping humidity of the exquisite anti-age corrective eye treatment cream, while promote emulsification.Hydroxy-ethyl acrylate/the third Alkene acyl dimethyltaurine sodium copolymer (EMT 15) makees emulsifier, thickener, viscosity-adjusting agent in the exquisite anti-age corrective eye treatment cream Agent uses, and further, the manufacturer of the hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers is France SNF Company.Carbomer has efficient thickening effect, can generate as clear as crystal water gel, rheological characteristic is very short, can make institute It states exquisite anti-age corrective eye treatment cream and is easier skin permeation, promote to absorb.PEG-240/HDI copolymer pair--20 ether of decyl tetradecyl alcohol polyethers (ADEKA Nol GT-730) is that non-ionic emulsifier stablizes thickener, and without neutralizing, good film-forming property can be formed transparent on the skin Smooth skin sense as matter acid;Resistance to polyelectrolyte;It still can stable homogeneous when high temperature resistant, resistance to heating, high viscosity;With especially sensitive Shear shinning characteristic, thixotropy is splendid, energy Fast Restoration, so, it is possible the rheological characteristic for greatly improving the exquisite anti-age corrective eye treatment cream And stability.Further, the PEG-240/HDI copolymer pair--20 ether of decyl tetradecyl alcohol polyethers manufacturer is Japan ADEKA company.Inulin lauryl carbamate (INUTEC SL1) is used as emulsion stabilizer in the exquisite anti-age corrective eye treatment cream It is used with dispersing agent, is capable of the stability and uniformity of the significantly described exquisite anti-age corrective eye treatment cream.Further, the inulin lauryl base The manufacturer of carbamate is Xian Ting company, France.In this way, can be improved the exquisite anti-age corrective eye treatment cream using each component of B phase Emulsifiability, improve stability and dispersion performance, additionally it is possible to improve performance of keeping humidity and rheological characteristic, there is pleasant skin sense Feel and low sticky sense.
It is appreciated that polyglutamic acid is also known as Bacillus natto glue, polyglutamic acid, it is a kind of water solubility, and biodegrade is free of Toxicity uses boiomacromolecule made from microbe fermentation method.With good performance of keeping humidity, the exquisite maintenance can be improved The moisture retention of eye cream.Cyclomethicone/dimethiconol mixture (DC1403) is hyperviscosity dimethyl 13% strength solution of the siloxanes alcohol in volatile cyclomethicone enables to the mousse frost to have soft smooth Skin sense reduces sticky sense, further, the cyclomethicone/dimethiconol mixture manufacturer For Dow corning company.In this way, can be improved performance of keeping humidity and the absorption of the exquisite anti-age corrective eye treatment cream using each component of C phase Performance, enhancing eye skin barrier and the performance for restoring elasticity.
It is to be particularly noted that the triglyceride in fat cell can be resolved into fatty acid and sweet by caffeine Oil, the accumulation for mitigating ocular edema and causing space between cells body fluid excessive because of cellulitis, additionally it is possible to stimulate microcirculation and Into metabolism, accelerate local microcirculation, enables to the exquisite anti-age corrective eye treatment cream that relaxation, eye pouch and edema is effectively relieved and ask Topic.Glucityl aurantiamarin can be protected and be repaired to capillary, and blood leakage and inflammation diffusion are reduced, and improved blood vessel and relaxed It opens and promotes microcirculation and nutritional supplementation, additionally it is possible to promote fat metabolism, can be improved the maintenance performance of the exquisite anti-age corrective eye treatment cream, It is effectively improved microgroove, wrinkle, relaxation, eye pouch, edema, black eye and the dry problem of eye circumference skin.Bigarabe flower extract (Remoduline) it is rich in methoxy flavone and flavanones, can be reduced fat: the triglyceride in fat cell is decomposed At fatty acid and glycerol, additionally it is possible to improve vasodilation and promote microcirculation, to promote discharge fatty in skin histology, energy That enough improves the exquisite anti-age corrective eye treatment cream solves the problems, such as relaxation, eye pouch and edema.Further, the life of the bigarabe flower extract Business men is SILAB company, France.Inositol can adjust Premeabilisation of cells pressure, maintain horn cell oil-water balance, and excitation corium is dry thin Born of the same parents, corium stem cell differentiate come fibroblast can generate corium constituent such as collagen, elastin laminin and Hyaluronic acid enables to skin inherently to be improved, and increases moisture-keeping function, so enables to the essence using inositol It causes anti-age corrective eye treatment cream to improve the oil-water balance of skin, improves elasticity and moistening effect.Oat beta-glucan has good moisturizing and resists Allergy effect, is able to suppress histamine release of mast cell, mitigates the proliferation of allergic reaction, wound healing promoting and macrophage, releases Various cell factors such as EGF and AF are put, can be improved the anti-aging, free radical resisting and promotion collagen egg of the exquisite anti-age corrective eye treatment cream The performance of bletilla fibroblast proliferation.Thallus laminariae extract can reactivate and elastin laminin, collagen, hyaluronic acid Relevant 14 genes are assembled and linked to synthesis, at maturation, mentions compacting effect with significantly repairing, drawing, recovery skin vigor makes Skin is younger, can be improved the lifting tightening effect of the exquisite anti-age corrective eye treatment cream, is conducive to improve eye circumference skin problem.Immediately Smoothing wrinkle essence can greatly improve the performance of the smooth out wrinkles of the exquisite anti-age corrective eye treatment cream, for example, in one of the embodiments, The instant smoothing wrinkle essence is Alteromonad tunning extract, the activity of the Alteromonad tunning extract Ingredient is exocellular polysaccharide, is made of galactolipin, galacturonic acid, glucose, glucuronic acid and mannose, can Fast Filling wrinkle Line, Rosemary Extract;Have the effect of remarkably promoting collagen, elastin laminin, hyaluronic acid synthesis, reduces wrinkle from skin inside Line tightens collagen lattice to anti-aging, and the ability for enabling to the exquisite anti-age corrective eye treatment cream to resist free radical resisting is increased By force, it puts down and comforts that wrinkle, taking on a new look, to restore elasticity, skin moist fine and smooth compact.It is different rich in four kinds that starfish regenerates repair factor Starfish saponin wins peptide and free amino acid, minerals by a narrow margin.It is very strong anti-ageing active constituent, the natural substitute of retinol, With it is colourless, tasteless, do not stimulate, performance without side-effects, can promote skin update and regeneration, repair skin barrier function, Promotion wound healing, so that the exquisiteness anti-age corrective eye treatment cream has crease-resistant, enhancing elasticity of skin, consolidation skin and promotion skin hydration The performance of effect.Gotu Kola P.E has the effect of that remarkably promoting collagen, elastin laminin, hyaluronic acid synthesizes from skin Wrinkle is reduced in inside, to anti-aging;Accelerate skin repair healing, to rebuild impaired skin.In one of the embodiments, The Gotu Kola P.E is asiaticosid, madecassoside, asiatic acid and brahmic acid, can be further increased The exquisiteness anti-age corrective eye treatment cream reduces wrinkle, to the performance of anti-aging.Centella polypeptide carrys out the totipotent cell of self asiatic petiole Concentrating secreted object, this secretion have plant polypeptide abundant, can reversing skin ageing process, induced cell proliferation, It stimulates cell detoxification, inducing cell to protect DNA, cell remodeling, the exquisite anti-age corrective eye treatment cream is enabled to using centella polypeptide With skin elasticity and compact, reverse skin aging is improved, restore the performance of youthful appearance.Two split yeast tunning lysis object Metabolite include small molecular organic acid (lactic acid, acetic acid, propionic acid, butyric acid etc.), vitamin (B1, B2, B6, B12), amino acid (alanine, valine, aspartic acid, threonine);Breakdown products include cell secreta (polysaccharide composite body, small-molecular peptides), Cellular content (nucleic acid, albumen, cytoplasmic fragment), cell rigid structure (teichoic acid, peptide glycan, Cell membrane lipids), and it is rich Prebiotics containing Bifidobacterium enable to the exquisite anti-age corrective eye treatment cream to have the performance for repairing damaged skin barrier, improve skin The microbial environment on surface, free radical resisting and the performance for promoting collagen and fibroblast proliferation.Ceramide liposome Skin moisture loss can be adjusted, moisture content of skin is improved, repairs the performance of damaged skin barrier, so that the exquisiteness maintenance eye Frost can be improved the barrier function and autoimmune ability of skin, improve coarse and dry skin, promote skin elasticity.Antiallergic is living Property peptide be active material in the exquisite anti-age corrective eye treatment cream, can effectively delaying senility and antiallergy, further, wherein one In a embodiment, the antiallergic active peptide is oligopeptides -29, so, it is possible so that the exquisiteness anti-age corrective eye treatment cream have resist it is anti-from Be enhanced by the ability of base, the performance of antiallergy and anti-aging further, the manufacturer of the oligopeptides -29 is South Korea CAREGEN company.In this way, can effectively improve the exquisite anti-age corrective eye treatment cream using the active material of each component in D phase and resist The ability of free radical resisting also enables the exquisite anti-age corrective eye treatment cream to be effectively improved 7 big problems of eye circumference skin: microgroove, wrinkle, Relaxation, eye pouch, edema, black eye and dry problem.
It is appreciated that Phenoxyethanol and fragrant fresh ketone usually play the effect of preservative, energy in cosmetics and skin care item Enough improve the storge quality of the exquisite anti-age corrective eye treatment cream.Essence can remove offending smell in original product, also have excitement And sedation, improve the use feeling of the exquisite anti-age corrective eye treatment cream.In this way, can be improved the essence using each component of E phase Cause the storage stability and use feeling of anti-age corrective eye treatment cream.
The exquisite anti-age corrective eye treatment cream of another embodiment, each component including following mass parts are prepared:
A phase: 0.1 part~0.6 part of Natrulon H-10 stearate, 1.0 parts~4.0 parts of dimethyl silicone polymer, poly- methyl silicon 0.1 part~1.0 parts of sesquioxyalkane, 0.8 part~4.0 parts of hydrogenated coco-glyceride class, phytosterols oletate 0.15 part~1.8 Part, 0.2 part~1.7 parts of tocopherol acetate;
B phase: 52.0 parts~90.0 parts of deionized water, 3.0 parts~11.0 parts of glycerol, 0.2 part~0.6 part of hydrolecithin, 0.4 part~1.0 parts of hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, 0.2 part of carbomer~0.5 part, PEG- 240/HDI copolymer pair -0.3 part~0.7 part of -20 ether of decyl tetradecyl alcohol polyethers, 0.2 part of inulin lauryl carbamate~ 0.8 part;
C phase: 0.05 part~0.3 part of polyglutamic acid, cyclomethicone/dimethiconol mixture 0.2 Part~1.0 parts;
D phase: 0.16 part~0.35 part of triethanolamine;
E phase: 1.5 parts~3.0 parts of caffeine, 0.2 part~1.7 parts of glucityl aurantiamarin, 1.0 parts of bigarabe flower extract~ 4.0 parts, 2.5 parts~7.0 parts of inositol, 1.5 parts~4.0 parts of oat beta-glucan, 1.2 parts~3.0 parts of thallus laminariae extract, remove immediately 0.6 part~2.0 parts of essence of wrinkle, starfish regenerate 1.1 parts~2.0 parts of repair factor, 0.8 part of Gotu Kola P.E~2.0 parts, accumulated snow 0.4 part~2.0 parts of careless polypeptide, two split 0.4 part~2.5 parts of yeast tunning lysis object, 0.3 part~1.1 parts of antiallergic active peptide;
F phase: 0.3 part~0.6 part of Phenoxyethanol, 0.1 part~0.4 part of fragrant fresh ketone, 0.01 part~0.07 part of essence.
By advanced optimizing the proportion of each component of the exquisite anti-age corrective eye treatment cream, the exquisiteness can be further enhanced and repaired The maintenance performance of eyeshield frost, being more advantageous to improves eye circumference skin problem.
The exquisite anti-age corrective eye treatment cream of a further embodiment, each component including following mass parts are prepared:
A phase: 0.3 part of Natrulon H-10 stearate, 2.0 parts of dimethyl silicone polymer, 0.5 part of polymethylsilsesquioxane, 3.0 parts of hydrogenated coco-glyceride class, 0.5 part of phytosterols oletate, 0.5 part of tocopherol acetate;
B phase: 58.84 parts of deionized water, 10 parts of glycerol, 0.3 part of hydrolecithin, hydroxy-ethyl acrylate/acryloyl diformazan 0.8 part of base Taurate Copolymer, 0.3 part of carbomer, PEG-240/HDI copolymer pair--20 ether 0.5 of decyl tetradecyl alcohol polyethers Part, 0.3 part of inulin lauryl carbamate;
C phase: 0.1 part of polyglutamic acid, cyclomethicone/0.5 part of dimethiconol mixture;
D phase: 0.25 part of triethanolamine;
E phase: 2.0 parts of caffeine, 0.5 part of glucityl aurantiamarin, 2.0 parts of bigarabe flower extract, 5.0 parts of inositol, oat Portugal 2.0 parts of glycan, 2.0 parts of thallus laminariae extract, 1.0 parts of instant smoothing wrinkle essence, 1.6 parts of repair factor of starfish regeneration, centella mention 1.0 parts of object, 1.0 parts of centella polypeptide, two are taken to split 2.0 parts, 0.5 part of antiallergic active peptide of yeast tunning lysis object;
F phase: 0.5 part of Phenoxyethanol, fragrant 0.2 part of fresh ketone, 0.01 part of essence.
By further optimizing the proportion of each component of the exquisite anti-age corrective eye treatment cream, it can further optimize the essence The maintenance performance for causing anti-age corrective eye treatment cream, being more advantageous to improves eye circumference skin problem.
Referring to Fig. 1, the preparation method of the exquisite anti-age corrective eye treatment cream of an embodiment, comprising the following steps:
S110, cleaning and sterilizing equipment decontaminating apparatus, it is spare.
In order to guarantee the quality for the exquisite anti-age corrective eye treatment cream being prepared, not contaminated object is infected, is needed first to system The equipment to be used carries out cleaning and sterilizing operation in standby.
It is S120, Natrulon H-10 stearate, dimethyl silicone polymer, polymethylsilsesquioxane and hydrogenated coco is sweet Oily phase pot is added in grease class, carries out the first heating stirring operation, and constant temperature to material is kept to be completely dissolved, and adds phytosterol oil Acid esters and tocopherol acetate obtain oil mixture after mixing, wherein the Natrulon H-10 stearate, described Dimethyl silicone polymer, the polymethylsilsesquioxane, the hydrogenated coco-glyceride class, the phytosterols oletate and The mass ratio of the tocopherol acetate is (0.05~0.8): (0.5~5.0): (0.05~2.0): (0.5~5.0): (0.05~2.0): (0.05~2.0).
By by Natrulon H-10 stearate, dimethyl silicone polymer, polymethylsilsesquioxane and hydrogenated coco glycerol The oily phase pot of esters addition, carries out the first heating stirring operation, can speed up the dissolution of each component under the high temperature conditions and uniformly mixes It closes, then constant temperature to material is kept to be completely dissolved, add phytosterols oletate and tocopherol acetate, be uniformly mixed Afterwards, oil mixture can be obtained, in addition, by the proportion of control each component, it is also better conducive to maintenance performance is prepared The exquisiteness anti-age corrective eye treatment cream.
The temperature of the first heating stirring operation is 70 DEG C~75 DEG C in one of the embodiments,.By by temperature 70 DEG C~75 DEG C are risen to, Natrulon H-10 stearate, dimethyl silicone polymer, polymethylsilsesquioxane and hydrogen can be promoted Change the dissolution of sodium cocoglyceryl esters and is uniformly dispersed.
S130, deionized water, glycerol, hydrolecithin, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate are copolymerized Cream is added in object, carbomer, PEG-240/HDI copolymer pair--20 ether of decyl tetradecyl alcohol polyethers and inulin lauryl carbamate Change pot, after carrying out the second heating stirring operation, constant temperature is kept for 9 minutes~12 minutes, is carried out the first homogeneous operation, is added poly- paddy Propylhomoserin and cyclomethicone/dimethiconol mixture and the oil mixture are stirred, in vacuum Under the conditions of carry out the second homogeneous operation, after then carrying out defoaming operation again, be added triethanolamine simultaneously stir evenly, wherein it is described Deionized water, the glycerol, the hydrolecithin, the hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, The carbomer, PEG-240/HDI copolymer be double--20 ether of decyl tetradecyl alcohol polyethers, the inulin lauryl carbamate, The polyglutamic acid, the cyclomethicone/dimethiconol mixture, the oil mixture and described The mass ratio of triethanolamine is (50.0~100.0): (1.0~11.0): (0.1~0.8): (0.1~1.0): (0.2~ 0.6): (0.1~0.8): (0.1~1.0): (0.01~0.5): (0.1~2.0): (1.2~16.8): (0.15~0.55).
By the way that deionized water, glycerol, hydrolecithin, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate are copolymerized Cream is added in object, carbomer, PEG-240/HDI copolymer pair--20 ether of decyl tetradecyl alcohol polyethers and inulin lauryl carbamate Change pot, after carrying out the second heating stirring operation, above-mentioned each component is enabled to preferably to be dissolved and divided under the high temperature conditions It dissipates, the temperature of the second heating stirring operation is 80 DEG C~85 DEG C in one of the embodiments, be so, it is possible further Each component is promoted to be dissolved and occurred emulsion reaction, then constant temperature is kept for 9 minutes~12 minutes again, so that each component is filled Divide dissolution and emulsification, then carries out the first homogeneous operation and then add polyglutamic so that each component is sufficiently mixed and is uniformly dispersed Acid and cyclomethicone/dimethiconol mixture and the oil mixture are stirred, in vacuum item The second homogeneous operation is carried out under part, after then carrying out defoaming operation again, triethanolamine is added and stirs evenly.It is appreciated that Under vacuum condition, each component can be stirred and be eliminated with the bubble generated in emulsion process, and some of generation are waved Body of getting angry is extracted out, then carries out defoaming operation again, can further be eliminated the bubble in emulsion pot, described in raising The quality and maintenance performance of exquisite anti-age corrective eye treatment cream, in addition, by the proportion of control each component being also conducive to that maintenance performance is prepared The preferably exquisite anti-age corrective eye treatment cream.
S140, after carrying out the first cooling operation, caffeine, glucityl aurantiamarin, bigarabe flower extract, flesh are sequentially added Alcohol, oat beta-glucan, thallus laminariae extract, instant smoothing wrinkle essence, starfish regenerate repair factor, Gotu Kola P.E, centella Polypeptide, two split yeast tunning lysis object and antiallergic active peptide, carry out third stirring operation, and constant temperature keeps completely molten to material Solution, wherein the caffeine, the glucityl aurantiamarin, the bigarabe flower extract, the inositol, the oat beta-glucan, It is the thallus laminariae extract, the instant smoothing wrinkle essence, starfish regeneration repair factor, the Gotu Kola P.E, described Centella polypeptide, described two split the mass ratio of yeast tunning lysis object and the antiallergic active peptide for (0.5~5.0): (0.1~2.0): (0.0~5.0): (0.5~10.0): (0.5~5.0): (0.0~4.0): (0.0~3.0): (0.1~ 3.0): (0.1~3.0): (0.1~3.0): (0.1~3.0): (0.1~1.5).
By carrying out the first cooling operation, the temperature in reaction system can be reduced, avoid to be easy because of high temperature And each component for reducing activity even loss of activity is destroyed, and caffeine, glucityl aurantiamarin, bigarabe are then sequentially added Flower extract, inositol, oat beta-glucan, thallus laminariae extract, instant smoothing wrinkle essence, starfish regeneration repair factor, centella mention It takes object, centella polypeptide, two to split yeast tunning lysis object and antiallergic active peptide, carries out third stirring operation, constant temperature is kept It is completely dissolved to material, for example, carrying out the first cooling operation in one of the embodiments, cools the temperature to 52 DEG C~55 DEG C, The activity of each component is able to maintain because high temperature is destroyed, moreover it is possible to energy consumption is reduced, in addition, by the proportion of control each component, it is also sharp In the maintenance performance preferably exquisite anti-age corrective eye treatment cream is prepared.
S150, after carrying out the second cooling operation, the Phenoxyethanol and fragrant fresh ketone dissolved in advance is sequentially added, and fragrant Essence stirs evenly, and obtains anti-age corrective eye treatment cream precursor.
By carrying out the second cooling operation, temperature is further decreased, for example, in one of the embodiments, dropping temperature To 42 DEG C~44 DEG C, the Phenoxyethanol dissolved in advance and fragrant fresh ketone and essence is sequentially added, and be uniformly mixed, guaranteed While each component performance is not destroyed, moreover it is possible to reduce energy consumption, after mixing evenly, anti-age corrective eye treatment cream precursor can be obtained.
S160, after carrying out third cooling operation, the anti-age corrective eye treatment cream precursor is subjected to detection operation, is filtered after qualified Discharging, obtains exquisite anti-age corrective eye treatment cream.
After the mixing homogeneous for completing each component, then third cooling operation is carried out, further decreases the anti-age corrective eye treatment cream precursor Temperature, be able to maintain the stability of the anti-age corrective eye treatment cream precursor, carry out detection operation, carry out filtering and discharging after qualified, can Obtain exquisite anti-age corrective eye treatment cream.For example, being 38 DEG C by temperature control in one of the embodiments, after the third cooling operation ~39 DEG C, the activity for being able to maintain the anti-age corrective eye treatment cream precursor is not destroyed, and improves stability.
Here is specific embodiment part.
Embodiment 1
Simultaneously sterilizing equipment decontaminating apparatus is cleaned, it is spare;
By Natrulon H-10 stearate 0.3kg, dimethyl silicone polymer 2.0kg, polymethylsilsesquioxane 0.5kg, hydrogen Change sodium cocoglyceryl esters 3.0kg and oily phase pot is added, under the conditions of 70 DEG C of temperature, carries out the first heating stirring operation, keep constant temperature It is completely dissolved to material, adds phytosterols oletate 0.5kg, tocopherol acetate 0.8kg obtains oil after mixing Phase mixture;
By deionized water 59.24kg, glycerol 10kg, hydrolecithin 0.3kg, hydroxy-ethyl acrylate/acryloyldimethyl Taurate Copolymer 0.8kg, carbomer 0.3kg, PEG-240/HDI copolymer be double--20 ether 0.5kg of decyl tetradecyl alcohol polyethers, Emulsion pot is added in inulin lauryl carbamate 0.3kg, under the conditions of 80 DEG C of temperature, after carrying out the second heating stirring operation, Constant temperature is kept for 9 minutes, is carried out the first homogeneous operation, is added polyglutamic acid 0.2kg and cyclomethicone/poly dimethyl Siloxanes alcohol mixture 1.0kg and the oil mixture stir within 1 minute, carry out the second of 10 minutes under vacuum conditions Homogeneous operation, after then carrying out defoaming operation again, adds triethanolamine 0.25kg and stirs evenly;
After carrying out the first cooling operation, temperature is reduced to 55 DEG C, sequentially adds caffeine 2.0kg, glucityl aurantiamarin 0.8kg, bigarabe flower extract 1.0kg, inositol 5.0kg, oat beta-glucan 2.0kg, thallus laminariae extract 2.0kg, instant smoothing wrinkle Essence 1.0kg, starfish regeneration repair factor 1.6kg, Gotu Kola P.E 0.5kg, centella polypeptide 1.5kg, two split yeast hair Ferment product lysis object 1.5kg and antiallergic active peptide 0.5kg, carries out third stirring operation, and constant temperature keeps to material being completely dissolved;
After carrying out the second cooling operation, temperature is reduced to 44 DEG C, sequentially adds the Phenoxyethanol 0.5kg dissolved in advance With fragrant fresh ketone 0.2kg and essence 0.01kg, stirs evenly, obtain anti-age corrective eye treatment cream precursor;
After carrying out third cooling operation, temperature is reduced to 39 DEG C, the anti-age corrective eye treatment cream precursor is subjected to detection operation, it is qualified After carry out filtering and discharging, obtain the exquisite anti-age corrective eye treatment cream of embodiment 1.
Embodiment 2
Simultaneously sterilizing equipment decontaminating apparatus is cleaned, it is spare;
By Natrulon H-10 stearate 0.3kg, dimethyl silicone polymer 2.0kg, polymethylsilsesquioxane 0.5kg, hydrogen Change sodium cocoglyceryl esters 3.0kg and oily phase pot is added, under the conditions of 70 DEG C of temperature, carries out the first heating stirring operation, keep constant temperature It is completely dissolved to material, adds phytosterols oletate 0.5kg, tocopherol acetate 0.5kg obtains oil after mixing Phase mixture;
By deionized water 58.84kg, glycerol 10kg, hydrolecithin 0.3kg, hydroxy-ethyl acrylate/acryloyldimethyl Taurate Copolymer 0.8kg, carbomer 0.3kg, PEG-240/HDI copolymer be double--20 ether 0.5kg of decyl tetradecyl alcohol polyethers, Emulsion pot is added in inulin lauryl carbamate 0.3kg, under the conditions of 80 DEG C of temperature, after carrying out the second heating stirring operation, Constant temperature is kept for 9 minutes, is carried out the first homogeneous operation, is added polyglutamic acid 0.2kg and cyclomethicone/poly dimethyl Siloxanes alcohol mixture 0.5kg and the oil mixture stir within 1 minute, carry out the second of 10 minutes under vacuum conditions Homogeneous operation, after then carrying out defoaming operation again, adds triethanolamine 0.25kg and stirs evenly;
After carrying out the first cooling operation, temperature is reduced to 55 DEG C, sequentially adds caffeine 2.0kg, glucityl aurantiamarin 0.5kg, bigarabe flower extract 2.0kg, inositol 5.0kg, oat beta-glucan 2.0kg, thallus laminariae extract 2.0kg, instant smoothing wrinkle Essence 1.0kg, starfish regeneration repair factor 1.6kg, Gotu Kola P.E 1.0kg, centella polypeptide 1.0kg, two split yeast hair Ferment product lysis object 2.0kg and antiallergic active peptide 0.5kg, carries out third stirring operation, and constant temperature keeps to material being completely dissolved;
After carrying out the second cooling operation, temperature is reduced to 44 DEG C, sequentially adds the Phenoxyethanol 0.5kg dissolved in advance With fragrant fresh ketone 0.2kg and essence 0.01kg, stirs evenly, obtain anti-age corrective eye treatment cream precursor;
After carrying out third cooling operation, temperature is reduced to 39 DEG C, the anti-age corrective eye treatment cream precursor is subjected to detection operation, it is qualified After carry out filtering and discharging, obtain the exquisite anti-age corrective eye treatment cream of embodiment 2.
Here is the result being tested for the property to the cosmetics of the promotion skin hydration effect:
1, skin hydration acts on
Test crowd: 50 people, 40-65 years old women tester are repaired using exquisiteness made from the embodiment of the present invention 2 sooner or later daily Eyeshield frost 2 times measures assessment moistening effect with skin keratin tester.After 28 days, facial skin aquation increases by 13.2%, Skin more healthy water is moistened.
2, senile-resistant efficacy
Test crowd: 50 people, 40-65 years old women tester test 28 days, are made sooner or later using the embodiment of the present invention 2 daily Exquisite anti-age corrective eye treatment cream 2 times obtained.
Test parameter: wrinkle depth, skin firmness, skin elasticity.Using skin elasticity tester MAP580, continuously make After 28 days, result is as shown in table 1 below:
Skin performance Compared with the control group of unused exquisite anti-age corrective eye treatment cream
Skin firmness Increase by 16.9%
Skin elasticity Increase by 7.8%
Wrinkle depth Reduce 12.3%
Table 1
3, oedema, black eye
Test crowd: 50 people, 40-65 years old women tester test 28 days, are made sooner or later using the embodiment of the present invention 2 daily Exquisite anti-age corrective eye treatment cream 2 times obtained.
After 3 hours, there is apparent skin circulation and accelerates in 86% tester, and shows the exclusion of vein siltation.
After 14 days, 88% tester feedback is effective, and 12% tester feeds back no effect, 62% tester's feedback effects It is good.
After 28 days, 74% tester's skin circulation weakens and is restored to normal level, shows that oedema has obtained solution gradually It removes.
4, eye pouch
Test crowd: 50 people, 40-65 years old women tester test 56 days, are made sooner or later using the embodiment of the present invention 2 daily Exquisite anti-age corrective eye treatment cream 2 times obtained.
After 56 days, 66% tester feedback eye pouch is effective, and 34% tester feeds back eye pouch and has no change, 42% test Person, which feeds back eye pouch, preferable effect, hence it is evident that it can be seen that eye pouch has reduction.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.

Claims (10)

1. a kind of exquisiteness anti-age corrective eye treatment cream, which is characterized in that each component including following mass parts is prepared:
A phase: 0.05 part~0.8 part of Natrulon H-10 stearate, 0.5 part~5.0 parts of dimethyl silicone polymer, poly- methyl silicon times Half 0.05 part of oxygen alkane~2.0 parts, 0.5 part~5.0 parts of hydrogenated coco-glyceride class, 0.05 part~2.0 parts of phytosterols oletate, 0.05 part~2.0 parts of tocopherol acetate;
B phase: 50.0 parts~100.0 parts of deionized water, 1.0 parts~11.0 parts of glycerol, 0.1 part of hydrolecithin~0.8 part, propylene 0.1 part~1.0 parts of sour hydroxyl ethyl ester/sodium acryloyldimethyl taurate copolymers, 0.2 part of carbomer~0.6 part, PEG-240/ HDI copolymer pair -0.1 part~0.8 part of -20 ether of decyl tetradecyl alcohol polyethers, 0.1 part~1.0 parts of inulin lauryl carbamate;
C phase: 0.01 part~0.5 part of polyglutamic acid, cyclomethicone/0.1 part of dimethiconol mixture~ 2.0 part;
D phase: 0.15 part~0.55 part of triethanolamine;
E phase: 0.5 part~5.0 parts of caffeine, 0.1 part~2.0 parts of glucityl aurantiamarin, 0.0 part~5.0 parts of bigarabe flower extract, 0.5 part~10.0 parts of inositol, 0.5 part~5.0 parts of oat beta-glucan, 0.0 part~4.0 parts of thallus laminariae extract, instant smoothing wrinkle essence 0.0 part~3.0 parts of China, 0.1 part~3.0 parts of repair factor of starfish regeneration, 0.1 part~3.0 parts of Gotu Kola P.E, centella are more 0.1 part~3.0 parts of peptide, two split 0.1 part~3.0 parts of yeast tunning lysis object, 0.1 part~1.5 parts of antiallergic active peptide;
F phase: 0.2 part~0.8 part of Phenoxyethanol, 0.1 part~0.5 part of fragrant fresh ketone, 0.01 part~0.1 part of essence.
2. exquisiteness anti-age corrective eye treatment cream according to claim 1, which is characterized in that each component including following mass parts is prepared into It arrives:
A phase: 0.1 part~0.6 part of Natrulon H-10 stearate, 1.0 parts~4.0 parts of dimethyl silicone polymer, poly- methyl silicon sesquialter 0.1 part~1.0 parts of oxygen alkane, 0.8 part~4.0 parts of hydrogenated coco-glyceride class, 0.15 part~1.8 parts of phytosterols oletate, life Educate 0.2 part~1.7 parts of phenol acetic acid esters;
B phase: 52.0 parts~90.0 parts of deionized water, 3.0 parts~11.0 parts of glycerol, 0.2 part of hydrolecithin~0.6 part, propylene 0.4 part~1.0 parts of sour hydroxyl ethyl ester/sodium acryloyldimethyl taurate copolymers, 0.2 part of carbomer~0.5 part, PEG-240/ HDI copolymer pair -0.3 part~0.7 part of -20 ether of decyl tetradecyl alcohol polyethers, 0.2 part~0.8 part of inulin lauryl carbamate;
C phase: 0.05 part~0.3 part of polyglutamic acid, cyclomethicone/0.2 part of dimethiconol mixture~ 1.0 part;
D phase: 0.16 part~0.35 part of triethanolamine;
E phase: 1.5 parts~3.0 parts of caffeine, 0.2 part~1.7 parts of glucityl aurantiamarin, 1.0 parts~4.0 parts of bigarabe flower extract, 2.5 parts~7.0 parts of inositol, 1.5 parts~4.0 parts of oat beta-glucan, 1.2 parts~3.0 parts of thallus laminariae extract, instant smoothing wrinkle essence 0.6 part~2.0 parts, starfish regeneration 1.1 parts~2.0 parts of repair factor, 0.8 part~2.0 parts of Gotu Kola P.E, centella polypeptide 0.4 part~2.0 parts, two split 0.4 part~2.5 parts of yeast tunning lysis object, 0.3 part~1.1 parts of antiallergic active peptide;
F phase: 0.3 part~0.6 part of Phenoxyethanol, 0.1 part~0.4 part of fragrant fresh ketone, 0.01 part~0.07 part of essence.
3. exquisiteness anti-age corrective eye treatment cream according to claim 2, which is characterized in that each component including following mass parts is prepared into It arrives:
A phase: 0.3 part of Natrulon H-10 stearate, 2.0 parts of dimethyl silicone polymer, 0.5 part of polymethylsilsesquioxane, hydrogenation 3.0 parts of sodium cocoglyceryl esters, 0.5 part of phytosterols oletate, 0.5 part of tocopherol acetate;
B phase: 58.84 parts of deionized water, 10 parts of glycerol, 0.3 part of hydrolecithin, hydroxy-ethyl acrylate/acryloyldimethyl ox 0.8 part of sodium sulfonate copolymers, 0.3 part of carbomer, PEG-240/HDI copolymer pair -0.5 part of -20 ether of decyl tetradecyl alcohol polyethers, chrysanthemum 0.3 part of powder lauryl carbamate;
C phase: 0.1 part of polyglutamic acid, cyclomethicone/0.5 part of dimethiconol mixture;
D phase: 0.25 part of triethanolamine;
E phase: 2.0 parts of caffeine, 0.5 part of glucityl aurantiamarin, 2.0 parts of bigarabe flower extract, 5.0 parts of inositol, oat beta-glucan 2.0 parts, 2.0 parts of thallus laminariae extract, 1.0 parts of instant smoothing wrinkle essence, starfish regeneration 1.6 parts of repair factor, Gotu Kola P.E 1.0 parts, 1.0 parts of centella polypeptide, two split 2.0 parts, 0.5 part of antiallergic active peptide of yeast tunning lysis object;
F phase: 0.5 part of Phenoxyethanol, fragrant 0.2 part of fresh ketone, 0.01 part of essence.
4. it is according to claim 1 exquisiteness anti-age corrective eye treatment cream, which is characterized in that the Gotu Kola P.E be asiaticosid, Madecassoside, asiatic acid and brahmic acid.
5. exquisiteness anti-age corrective eye treatment cream according to claim 1, which is characterized in that the instant smoothing wrinkle essence is Alteromonad Tunning extract.
6. a kind of preparation method of exquisiteness anti-age corrective eye treatment cream, which comprises the following steps:
Simultaneously sterilizing equipment decontaminating apparatus is cleaned, it is spare;
Natrulon H-10 stearate, dimethyl silicone polymer, polymethylsilsesquioxane and hydrogenated coco-glyceride class are added Oily phase pot carries out the first heating stirring operation, keeps constant temperature to material to be completely dissolved, adds phytosterols oletate and fertility Phenol acetic acid esters obtains oil mixture after mixing, wherein the Natrulon H-10 stearate, the poly dimethyl silicon Oxygen alkane, the polymethylsilsesquioxane, the hydrogenated coco-glyceride class, the phytosterols oletate and the tocopherol The mass ratio of acetic acid esters is (0.05~0.8): (0.5~5.0): (0.05~2.0): (0.5~5.0): (0.05~2.0): (0.05~2.0);
By deionized water, glycerol, hydrolecithin, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, card wave Emulsion pot is added in nurse, PEG-240/HDI copolymer pair--20 ether of decyl tetradecyl alcohol polyethers and inulin lauryl carbamate, into The second heating stirring of row operation after, constant temperature keep 9 minutes~12 minutes, carry out the first homogeneous operation, add polyglutamic acid and Cyclomethicone/dimethiconol mixture and the oil mixture are stirred, under vacuum conditions The second homogeneous operation is carried out, after then carrying out defoaming operation again, triethanolamine is added and stirs evenly, wherein the deionization Water, the glycerol, the hydrolecithin, the hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers, the card Wave nurse, PEG-240/HDI copolymer be double-and it is -20 ether of decyl tetradecyl alcohol polyethers, the inulin lauryl carbamate, described poly- Glutamic acid, the cyclomethicone/dimethiconol mixture, the oil mixture and three ethyl alcohol The mass ratio of amine is (50.0~100.0): (1.0~11.0): (0.1~0.8): (0.1~1.0): (0.2~0.6): (0.1 ~0.8): (0.1~1.0): (0.01~0.5): (0.1~2.0): (1.2~16.8): (0.15~0.55);
After carrying out the first cooling operation, caffeine, glucityl aurantiamarin, bigarabe flower extract, inositol, oat Portugal are sequentially added Glycan, thallus laminariae extract, instant smoothing wrinkle essence, starfish regeneration repair factor, Gotu Kola P.E, centella polypeptide, two are split Yeast tunning lysis object and antiallergic active peptide, carry out third stirring operation, and constant temperature keeps to material being completely dissolved, wherein The caffeine, the glucityl aurantiamarin, the bigarabe flower extract, the inositol, the oat beta-glucan, the opotism Dish extract, the instant smoothing wrinkle essence, starfish regeneration repair factor, the Gotu Kola P.E, the centella are more Peptide, described two split the mass ratio of yeast tunning lysis object and the antiallergic active peptide for (0.5~5.0): (0.1~ 2.0): (0.0~5.0): (0.5~10.0): (0.5~5.0): (0.0~4.0): (0.0~3.0): (0.1~3.0): (0.1 ~3.0): (0.1~3.0): (0.1~3.0): (0.1~1.5);
After carrying out the second cooling operation, the Phenoxyethanol dissolved in advance and fragrant fresh ketone and essence are sequentially added, stirring is equal It is even, obtain anti-age corrective eye treatment cream precursor;
After carrying out third cooling operation, the anti-age corrective eye treatment cream precursor is subjected to detection operation, filtering and discharging is carried out after qualified, obtains Exquisite anti-age corrective eye treatment cream.
7. the preparation method of exquisiteness anti-age corrective eye treatment cream according to claim 6, which is characterized in that the first heating stirring behaviour The temperature of work is 70 DEG C~75 DEG C.
8. the preparation method of exquisiteness anti-age corrective eye treatment cream according to claim 6, which is characterized in that the second heating stirring behaviour The temperature of work is 80 DEG C~85 DEG C.
9. the preparation method of exquisiteness anti-age corrective eye treatment cream according to claim 6, which is characterized in that the second cooling operation It afterwards, is 42 DEG C~44 DEG C by temperature control.
10. the preparation method of exquisiteness anti-age corrective eye treatment cream according to claim 6, which is characterized in that the third cooling operation It afterwards, is 38 DEG C~39 DEG C by temperature control.
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CN110897989A (en) * 2019-12-24 2020-03-24 广州蜜妆生物科技有限公司 Sensitive skin repair emulsion
CN111658557A (en) * 2020-06-22 2020-09-15 泉后(广州)生物科技研究院有限公司 Nano-structure liposome capable of eliminating eye bags immediately and preparation method and application thereof
CN111939114A (en) * 2019-05-14 2020-11-17 西安博和医疗科技有限公司 Eye care composition
CN112353725A (en) * 2020-11-19 2021-02-12 广州领衔生物科技有限公司 Efficacy composition in eye cream, eye cream and preparation method thereof
CN113018223A (en) * 2021-03-24 2021-06-25 湖北省麦诗特生物科技有限公司 Eye tightening fatigue immunity eye cream composition containing coral algae compound and preparation method thereof
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CN113813205A (en) * 2021-09-10 2021-12-21 仙婷(广州)科技研发有限公司 Multifunctional eye care composition and application thereof
CN113876656A (en) * 2021-10-29 2022-01-04 湖北省麦诗特生物科技有限公司 Black eye and pouch removing soluble beautifying microneedle patch composition and preparation method thereof
CN114028245A (en) * 2021-11-29 2022-02-11 浙江宜格企业管理集团有限公司 Mild cutin-removing composition and preparation method thereof
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CN111658557A (en) * 2020-06-22 2020-09-15 泉后(广州)生物科技研究院有限公司 Nano-structure liposome capable of eliminating eye bags immediately and preparation method and application thereof
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CN113679646B (en) * 2021-08-09 2023-07-21 深圳市护家科技有限公司 Caffeine tightening and repairing eye cream and preparation method thereof
CN113813205A (en) * 2021-09-10 2021-12-21 仙婷(广州)科技研发有限公司 Multifunctional eye care composition and application thereof
CN113876656A (en) * 2021-10-29 2022-01-04 湖北省麦诗特生物科技有限公司 Black eye and pouch removing soluble beautifying microneedle patch composition and preparation method thereof
CN114028245A (en) * 2021-11-29 2022-02-11 浙江宜格企业管理集团有限公司 Mild cutin-removing composition and preparation method thereof
CN114028245B (en) * 2021-11-29 2024-03-26 浙江宜格企业管理集团有限公司 Mild exfoliating composition and preparation method thereof
CN114632045B (en) * 2022-04-18 2024-05-31 蔻蔻琪生物科技(杭州)有限公司 Anti-aging composition, preparation method and application
CN114796050A (en) * 2022-04-27 2022-07-29 蓓悠清(广东)健康科技有限公司 Efficient moisturizing and relieving gel mask and preparation method thereof

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