CN109097841A - 一种各向异性纳米纤维聚偏氟乙烯基复合介质及其制备方法 - Google Patents
一种各向异性纳米纤维聚偏氟乙烯基复合介质及其制备方法 Download PDFInfo
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- CN109097841A CN109097841A CN201810819906.4A CN201810819906A CN109097841A CN 109097841 A CN109097841 A CN 109097841A CN 201810819906 A CN201810819906 A CN 201810819906A CN 109097841 A CN109097841 A CN 109097841A
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- 239000002131 composite material Substances 0.000 title claims abstract description 39
- 239000002121 nanofiber Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 27
- 239000002033 PVDF binder Substances 0.000 claims abstract description 105
- 229920002981 polyvinylidene fluoride Polymers 0.000 claims abstract description 105
- 238000011049 filling Methods 0.000 claims abstract description 32
- 238000010041 electrostatic spinning Methods 0.000 claims abstract description 29
- 238000000034 method Methods 0.000 claims abstract description 21
- 239000011259 mixed solution Substances 0.000 claims abstract description 11
- 239000003989 dielectric material Substances 0.000 claims abstract 2
- 239000000243 solution Substances 0.000 claims description 41
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 claims description 32
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- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 12
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 11
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 11
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 9
- 238000001035 drying Methods 0.000 claims description 8
- 238000013019 agitation Methods 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000001291 vacuum drying Methods 0.000 claims description 6
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims description 4
- ZUDYPQRUOYEARG-UHFFFAOYSA-L barium(2+);dihydroxide;octahydrate Chemical compound O.O.O.O.O.O.O.O.[OH-].[OH-].[Ba+2] ZUDYPQRUOYEARG-UHFFFAOYSA-L 0.000 claims description 4
- YHWCPXVTRSHPNY-UHFFFAOYSA-N butan-1-olate;titanium(4+) Chemical compound [Ti+4].CCCC[O-].CCCC[O-].CCCC[O-].CCCC[O-] YHWCPXVTRSHPNY-UHFFFAOYSA-N 0.000 claims description 4
- 239000011575 calcium Substances 0.000 claims description 4
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 4
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 4
- 239000000920 calcium hydroxide Substances 0.000 claims description 4
- 239000000919 ceramic Substances 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 4
- 230000003247 decreasing effect Effects 0.000 claims description 4
- 238000004090 dissolution Methods 0.000 claims description 4
- 238000004321 preservation Methods 0.000 claims description 4
- 238000003825 pressing Methods 0.000 claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- 238000005245 sintering Methods 0.000 claims description 3
- 239000010408 film Substances 0.000 claims 10
- 239000010409 thin film Substances 0.000 claims 1
- 239000011159 matrix material Substances 0.000 abstract description 11
- 229920000642 polymer Polymers 0.000 abstract description 7
- 239000002114 nanocomposite Substances 0.000 abstract description 3
- 238000011161 development Methods 0.000 abstract description 2
- 238000010791 quenching Methods 0.000 abstract description 2
- 230000000171 quenching effect Effects 0.000 abstract description 2
- 238000003980 solgel method Methods 0.000 abstract description 2
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 21
- 230000015556 catabolic process Effects 0.000 description 12
- 238000004146 energy storage Methods 0.000 description 8
- 230000005684 electric field Effects 0.000 description 7
- 238000009987 spinning Methods 0.000 description 7
- 150000001875 compounds Chemical class 0.000 description 5
- 230000005611 electricity Effects 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
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- 229910052710 silicon Inorganic materials 0.000 description 2
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- 238000001228 spectrum Methods 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- FQNGWRSKYZLJDK-UHFFFAOYSA-N [Ca].[Ba] Chemical compound [Ca].[Ba] FQNGWRSKYZLJDK-UHFFFAOYSA-N 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 239000013064 chemical raw material Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 125000002573 ethenylidene group Chemical group [*]=C=C([H])[H] 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
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Classifications
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/0007—Electro-spinning
- D01D5/0015—Electro-spinning characterised by the initial state of the material
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/62227—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
- C04B35/62231—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on oxide ceramics
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4374—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece using different kinds of webs, e.g. by layering webs
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/54—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by welding together the fibres, e.g. by partially melting or dissolving
- D04H1/558—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by welding together the fibres, e.g. by partially melting or dissolving in combination with mechanical or physical treatments other than embossing
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/70—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
- D04H1/72—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged
- D04H1/728—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being randomly arranged by electro-spinning
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/70—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres
- D04H1/74—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres characterised by the method of forming fleeces or layers, e.g. reorientation of fibres the fibres being orientated, e.g. in parallel (anisotropic fleeces)
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Ceramic Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Fixed Capacitors And Capacitor Manufacturing Machines (AREA)
- Nonwoven Fabrics (AREA)
- Artificial Filaments (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
Abstract
Description
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Priority Applications (1)
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CN201810819906.4A CN109097841B (zh) | 2018-07-24 | 2018-07-24 | 一种各向异性纳米纤维聚偏氟乙烯基复合介质及其制备方法 |
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CN201810819906.4A CN109097841B (zh) | 2018-07-24 | 2018-07-24 | 一种各向异性纳米纤维聚偏氟乙烯基复合介质及其制备方法 |
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CN109097841A true CN109097841A (zh) | 2018-12-28 |
CN109097841B CN109097841B (zh) | 2021-10-22 |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109893680A (zh) * | 2019-03-07 | 2019-06-18 | 宁波光远致信生物科技有限公司 | 一种修复纤维膜、修复套接管及其制备方法和用途 |
CN110331520A (zh) * | 2019-07-11 | 2019-10-15 | 哈尔滨理工大学 | 一种二氧化硅包覆钛酸钡/聚醚酰亚胺复合材料及其制备方法与应用 |
CN112030369A (zh) * | 2020-07-22 | 2020-12-04 | 哈尔滨理工大学 | 一种一维铁磁填料-铁电聚合物的多铁复合介质及其制备方法 |
CN112980188A (zh) * | 2021-05-07 | 2021-06-18 | 哈尔滨理工大学 | 一种锆钛酸钡钙纤维/聚醚砜基复合电介质制备及储能性能优化 |
CN113061341A (zh) * | 2021-05-08 | 2021-07-02 | 哈尔滨理工大学 | 一种表面修饰的无机填充相/聚醚砜基复合电介质制备 |
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JP2008015054A (ja) * | 2006-07-04 | 2008-01-24 | Dainippon Printing Co Ltd | ホログラム異方性反射複合媒体 |
CN104327433A (zh) * | 2013-10-30 | 2015-02-04 | 东莞市长安东阳光铝业研发有限公司 | 一种聚偏氟乙烯基薄膜的制备方法 |
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CN107177144A (zh) * | 2017-06-27 | 2017-09-19 | 哈尔滨理工大学 | 一种三明治结构纳米纤维/聚偏氟乙烯复合介质及其制备方法 |
CN107195836A (zh) * | 2017-05-10 | 2017-09-22 | 东南大学 | 一种压电驱动自充电电池隔膜及其制备方法 |
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2018
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CN105884350A (zh) * | 2016-04-08 | 2016-08-24 | 江苏大学 | 一种锆钛酸钡钙无铅压电陶瓷材料及其制备方法 |
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CN107090088A (zh) * | 2017-05-25 | 2017-08-25 | 陕西科技大学 | 高β晶体含量的聚偏氟乙烯复合取向介电膜及制备方法 |
CN107177144A (zh) * | 2017-06-27 | 2017-09-19 | 哈尔滨理工大学 | 一种三明治结构纳米纤维/聚偏氟乙烯复合介质及其制备方法 |
Non-Patent Citations (2)
Title |
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CHI QINGGUO等: "Microstructure and dielectric properties of BZT-BCT/PVDF nanocomposites", 《RESULTS IN PHYSICS》 * |
张昌海: "高储能密度聚偏氟乙烯基复合介质的制备与性能研究", 《中国博士学位论文全文数据库 工程科技Ⅰ辑》 * |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109893680A (zh) * | 2019-03-07 | 2019-06-18 | 宁波光远致信生物科技有限公司 | 一种修复纤维膜、修复套接管及其制备方法和用途 |
CN109893680B (zh) * | 2019-03-07 | 2021-10-08 | 宁波光远致信生物科技有限公司 | 一种修复纤维膜、修复套接管及其制备方法和用途 |
CN110331520A (zh) * | 2019-07-11 | 2019-10-15 | 哈尔滨理工大学 | 一种二氧化硅包覆钛酸钡/聚醚酰亚胺复合材料及其制备方法与应用 |
CN112030369A (zh) * | 2020-07-22 | 2020-12-04 | 哈尔滨理工大学 | 一种一维铁磁填料-铁电聚合物的多铁复合介质及其制备方法 |
CN112980188A (zh) * | 2021-05-07 | 2021-06-18 | 哈尔滨理工大学 | 一种锆钛酸钡钙纤维/聚醚砜基复合电介质制备及储能性能优化 |
CN113061341A (zh) * | 2021-05-08 | 2021-07-02 | 哈尔滨理工大学 | 一种表面修饰的无机填充相/聚醚砜基复合电介质制备 |
CN113061341B (zh) * | 2021-05-08 | 2023-02-21 | 哈尔滨理工大学 | 一种表面修饰的无机填充相/聚醚砜基复合电介质制备 |
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