CN108085518A - 一种真空蒸馏设备及超高纯铟的制备方法 - Google Patents
一种真空蒸馏设备及超高纯铟的制备方法 Download PDFInfo
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- CN108085518A CN108085518A CN201711391555.3A CN201711391555A CN108085518A CN 108085518 A CN108085518 A CN 108085518A CN 201711391555 A CN201711391555 A CN 201711391555A CN 108085518 A CN108085518 A CN 108085518A
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- vacuum distillation
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- 238000005292 vacuum distillation Methods 0.000 title claims abstract description 78
- 229910052738 indium Inorganic materials 0.000 title claims abstract description 38
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 title claims abstract description 38
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 107
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 93
- 239000010439 graphite Substances 0.000 claims abstract description 93
- 238000010438 heat treatment Methods 0.000 claims abstract description 43
- 239000010453 quartz Substances 0.000 claims abstract description 42
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 42
- 239000003708 ampul Substances 0.000 claims abstract description 33
- 238000007711 solidification Methods 0.000 claims abstract description 33
- 230000008023 solidification Effects 0.000 claims abstract description 33
- 238000001816 cooling Methods 0.000 claims abstract description 21
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 14
- 238000004321 preservation Methods 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims description 7
- 238000000746 purification Methods 0.000 claims description 5
- 238000004821 distillation Methods 0.000 abstract description 12
- 230000006698 induction Effects 0.000 abstract description 9
- 239000012535 impurity Substances 0.000 description 13
- 238000000034 method Methods 0.000 description 9
- 239000000463 material Substances 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 7
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- 229910052802 copper Inorganic materials 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 239000013078 crystal Substances 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000005457 optimization Methods 0.000 description 2
- PXXKQOPKNFECSZ-UHFFFAOYSA-N platinum rhodium Chemical compound [Rh].[Pt] PXXKQOPKNFECSZ-UHFFFAOYSA-N 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- GPXJNWSHGFTCBW-UHFFFAOYSA-N Indium phosphide Chemical compound [In]#P GPXJNWSHGFTCBW-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 238000012644 addition polymerization Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000001036 glow-discharge mass spectrometry Methods 0.000 description 1
- 150000002366 halogen compounds Chemical class 0.000 description 1
- 238000001095 inductively coupled plasma mass spectrometry Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052745 lead Inorganic materials 0.000 description 1
- 239000007769 metal material Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 125000002524 organometallic group Chemical group 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 229910052716 thallium Inorganic materials 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 238000004857 zone melting Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B58/00—Obtaining gallium or indium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/02—Refining by liquating, filtering, centrifuging, distilling, or supersonic wave action including acoustic waves
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/25—Process efficiency
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Acoustics & Sound (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
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CN201711391555.3A CN108085518B (zh) | 2017-12-21 | 2017-12-21 | 一种真空蒸馏设备及超高纯铟的制备方法 |
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CN201711391555.3A CN108085518B (zh) | 2017-12-21 | 2017-12-21 | 一种真空蒸馏设备及超高纯铟的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN108085518A true CN108085518A (zh) | 2018-05-29 |
CN108085518B CN108085518B (zh) | 2020-06-26 |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110195164A (zh) * | 2019-06-28 | 2019-09-03 | 昆山祁御新材料科技有限公司 | 以粗钪为原料制备高纯钪的装置及方法 |
CN110257648A (zh) * | 2019-07-05 | 2019-09-20 | 上海大学 | 一种制备超高纯铟的装置及其制备方法 |
CN111286755A (zh) * | 2020-04-10 | 2020-06-16 | 云南锡业集团(控股)有限责任公司研发中心 | 一种电解-区域法制备高纯铟的方法 |
CN111593211A (zh) * | 2020-07-10 | 2020-08-28 | 楚雄川至电子材料有限公司 | 一种高纯铟提纯方法 |
CN113648672A (zh) * | 2021-09-01 | 2021-11-16 | 云南锡业集团(控股)有限责任公司研发中心 | 一种蒸馏冷凝的装置及超高纯铟的制备方法 |
CN117051266A (zh) * | 2023-08-29 | 2023-11-14 | 昆明理工大学 | 一种高纯铟的制备方法 |
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CN101270959A (zh) * | 2007-03-21 | 2008-09-24 | 中国科学院理化技术研究所 | 快速反应合成式高温气氛炉以及合成陶瓷粉末的方法 |
CN201497336U (zh) * | 2009-07-30 | 2010-06-02 | 株洲红亚电热设备有限公司 | 卧式连续高温石墨化炉 |
CN102168919A (zh) * | 2011-04-14 | 2011-08-31 | 张森 | 制备高纯和超纯材料的感应冷坩埚区熔提纯设备及方法 |
CN103160855A (zh) * | 2011-12-15 | 2013-06-19 | 广东先导稀材股份有限公司 | 高纯铟的制备方法 |
CN103184339A (zh) * | 2011-12-29 | 2013-07-03 | 广东先导稀材股份有限公司 | 砷化镓的处理设备及处理方法 |
CN104501580A (zh) * | 2014-12-01 | 2015-04-08 | 咸阳华光窑炉设备有限公司 | 电加热超高温内热式回转窑炉 |
CN104534864A (zh) * | 2014-12-01 | 2015-04-22 | 咸阳华光窑炉设备有限公司 | 电加热连续内热式高温回转窑炉 |
CN204388576U (zh) * | 2014-12-01 | 2015-06-10 | 咸阳华光窑炉设备有限公司 | 电加热连续内热式高温回转窑炉 |
CN106591599A (zh) * | 2017-02-08 | 2017-04-26 | 磐石创新(北京)电子装备有限公司 | 一种砷化镓废料分离回收装置及方法 |
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2017
- 2017-12-21 CN CN201711391555.3A patent/CN108085518B/zh active Active
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CN101270959A (zh) * | 2007-03-21 | 2008-09-24 | 中国科学院理化技术研究所 | 快速反应合成式高温气氛炉以及合成陶瓷粉末的方法 |
CN201497336U (zh) * | 2009-07-30 | 2010-06-02 | 株洲红亚电热设备有限公司 | 卧式连续高温石墨化炉 |
CN102168919A (zh) * | 2011-04-14 | 2011-08-31 | 张森 | 制备高纯和超纯材料的感应冷坩埚区熔提纯设备及方法 |
CN103160855A (zh) * | 2011-12-15 | 2013-06-19 | 广东先导稀材股份有限公司 | 高纯铟的制备方法 |
CN103184339A (zh) * | 2011-12-29 | 2013-07-03 | 广东先导稀材股份有限公司 | 砷化镓的处理设备及处理方法 |
CN104501580A (zh) * | 2014-12-01 | 2015-04-08 | 咸阳华光窑炉设备有限公司 | 电加热超高温内热式回转窑炉 |
CN104534864A (zh) * | 2014-12-01 | 2015-04-22 | 咸阳华光窑炉设备有限公司 | 电加热连续内热式高温回转窑炉 |
CN204388576U (zh) * | 2014-12-01 | 2015-06-10 | 咸阳华光窑炉设备有限公司 | 电加热连续内热式高温回转窑炉 |
CN106591599A (zh) * | 2017-02-08 | 2017-04-26 | 磐石创新(北京)电子装备有限公司 | 一种砷化镓废料分离回收装置及方法 |
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李冬生: "真空蒸馏—区域熔炼联合法制备高纯铟的研究", 《工程科技I辑》 * |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110195164A (zh) * | 2019-06-28 | 2019-09-03 | 昆山祁御新材料科技有限公司 | 以粗钪为原料制备高纯钪的装置及方法 |
CN110257648A (zh) * | 2019-07-05 | 2019-09-20 | 上海大学 | 一种制备超高纯铟的装置及其制备方法 |
CN111286755A (zh) * | 2020-04-10 | 2020-06-16 | 云南锡业集团(控股)有限责任公司研发中心 | 一种电解-区域法制备高纯铟的方法 |
CN111593211A (zh) * | 2020-07-10 | 2020-08-28 | 楚雄川至电子材料有限公司 | 一种高纯铟提纯方法 |
CN111593211B (zh) * | 2020-07-10 | 2021-04-23 | 楚雄川至电子材料有限公司 | 一种高纯铟提纯方法 |
CN113648672A (zh) * | 2021-09-01 | 2021-11-16 | 云南锡业集团(控股)有限责任公司研发中心 | 一种蒸馏冷凝的装置及超高纯铟的制备方法 |
CN117051266A (zh) * | 2023-08-29 | 2023-11-14 | 昆明理工大学 | 一种高纯铟的制备方法 |
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CN108085518B (zh) | 2020-06-26 |
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Effective date of registration: 20211217 Address after: 511517 workshop a, No.16, Chuangxing Third Road, high tech Zone, Qingyuan City, Guangdong Province Patentee after: Guangdong lead Microelectronics Technology Co.,Ltd. Address before: 511517 area B, no.27-9 Baijia Industrial Park, Qingyuan high tech Zone, Guangdong Province Patentee before: FIRST SEMICONDUCTOR MATERIALS Co.,Ltd. |
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Effective date of registration: 20231121 Address after: 221100 Xuzhou High tech Industrial Development Zone, Xuzhou City, Jiangsu Province, North of Fifth Ring Road and West of Tongchuang Road, No. 1 Qianfeng South Road Patentee after: Pioneer Electronic Technology Co.,Ltd. Address before: 511517 workshop a, No.16, Chuangxing Third Road, high tech Zone, Qingyuan City, Guangdong Province Patentee before: Guangdong lead Microelectronics Technology Co.,Ltd. |