CN107375029B - Anti-allergy moisturizing emulsion containing camellia seed oil - Google Patents

Anti-allergy moisturizing emulsion containing camellia seed oil Download PDF

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CN107375029B
CN107375029B CN201710649750.5A CN201710649750A CN107375029B CN 107375029 B CN107375029 B CN 107375029B CN 201710649750 A CN201710649750 A CN 201710649750A CN 107375029 B CN107375029 B CN 107375029B
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seed oil
camellia seed
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allergy
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CN107375029A (en
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陈效芳
刘瑞学
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Guangdong Bawei Biotechnology Co ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59—Mixtures
    • A61K2800/592—Mixtures of compounds complementing their respective functions

Abstract

The invention discloses camellia seed oil anti-allergy moisturizing emulsion which comprises the following components in parts by weight: 2-4 parts of camellia seed oil and 3-5 parts of a component A, wherein the component A is at least one of coconut oil alcohol-caprylate/caprate, C12-15 alcohol benzoate and glycerol tri (ethyl hexanoate). The camellia seed oil anti-allergy moisturizing emulsion disclosed by the invention adopts a very simple formula, is low in cost, has good anti-allergy moisturizing effects under the combined action of all components, can enhance the skin tolerance, is mild, is not irritant, and can be used for a long time.

Description

Anti-allergy moisturizing emulsion containing camellia seed oil
Technical Field
The invention relates to an emulsion, in particular to an anti-allergy moisturizing emulsion of camellia seed oil.
Background
With the increasingly severe air pollution and the increasing pressure of life in society, more and more human skin has a series of symptoms such as dryness, darkness, sensitivity and the like. Along with the increase of attention of people to skin care problems, the requirements of people on the functions and the quality of skin care products are continuously improved, so that the skin care emulsion with the characteristics of high efficiency, moisture retention, mildness and allergy resistance has larger market demand.
The traditional moisturizing skin care product has the moisturizing effect, is added with more chemical components, has certain toxic and side effects on a human body, can generate anaphylactic reaction after being used for a long time, and can cause damage to the skin barrier function and sensitive skin due to the use of unsuitable skin care products.
The skin care product can bring great burden to the skin by adding excessive raw materials, and a high-quality skin care product is made by using a simple formula to provide the best maintenance and repair to the skin, so that the skin care product is in line with the development trend of the skin care industry. Component selection is often a very critical factor in order to achieve efficacy, safety and stability of skin care products.
Disclosure of Invention
Based on the above, the invention aims to overcome the defects of the prior art and provide the camellia oil anti-allergy moisturizing emulsion.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows: the camellia seed oil anti-allergy moisturizing emulsion comprises the following components in parts by weight: 2-4 parts of camellia seed oil and 3-5 parts of a component A, wherein the component A is at least one of coconut oil alcohol-caprylate/caprate, C12-15 alcohol benzoate and glycerol tri (ethyl hexanoate).
The emulsion disclosed by the invention adopts a very simple formula, has excellent effects, enhances the skin tolerance, does not contain silicone oil, but can achieve the effect of the silicone oil, wherein:
the camellia seed oil is rich in unsaturated fatty acid, has remarkable nourishing effect on skin, can supplement nutrient components required by skin repair, and has the effects of reducing wrinkles, improving skin elasticity and the like.
The component A can provide a lubricating skin feel similar to silicone oil and can be used as a softening agent and a lubricant.
Wherein:
the coconut oil alcohol-caprylate/caprate is an emollient with fresh skin feeling, has no irritation, low viscosity, excellent spreadability and moisturizing effect, and excellent compatibility with skin.
Tri (ethyl hexanoate) is a colorless and odorless liquid oil and fat, and can be used as emollient for providing refreshing and smooth skin feeling.
Preferably, the camellia oil anti-allergy moisturizing emulsion further comprises 0.5-0.7 part by weight of a component B, wherein the component B is at least one of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, acrylic acid (ester)/vinyl isodecanoate cross-linked polymer, and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer sodium.
Wherein:
the hydroxyethyl acrylate/acryloyl dimethyl sodium taurate copolymer is a novel emulsifier, and has excellent emulsifying, dispersing, film forming and thickening capabilities.
The acrylic acid (ester)/isodecyl vinyl ester cross-linked polymer is a high-purity high-efficiency acrylic acid derivative, has mild property and excellent emulsifying property and ion resistance.
Acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer sodium is used as an emulsifier, and has excellent emulsifying, dispersing, thickening, film forming, water retaining and water absorbing capacities.
Preferably, the camellia oil anti-allergy moisturizing emulsion further comprises 0.5-1.5 parts by weight of component C, wherein the component C is at least one of sorbitan olive oleate, glyceryl stearate citrate and coco glucoside.
The component C of the invention is used as a liquid crystal emulsifier, so that the emulsion has better skin-friendly feeling.
More preferably, the camellia seed oil anti-allergy moisturizing emulsion further comprises 2-4 parts by weight of hydrogenated polyisobutene.
Preferably, the camellia oil anti-allergy moisturizing emulsion further comprises 9-11 parts by weight of glycerin.
Preferably, the camellia seed oil anti-allergy moisturizing emulsion further comprises 0.5-0.7 parts by weight of p-hydroxyacetophenone.
More preferably, the camellia oil anti-allergy moisturizing emulsion further comprises 0.5-0.7 part by weight of 1, 2-hexanediol.
Preferably, the weight ratio of the component A, the component B and the component C is as follows: and (2) component A: and (B) component: component C is 4:0.6: 1.5.
The component A, the component B and the component C in the proportion play a role in synergy, so that the stability of the emulsion can be better improved, and simultaneously the skin refreshing feeling can be better achieved.
Preferably, the weight ratio of the camellia seed oil, the hydrogenated polyisobutene and the component A is as follows: and (3) camellia seed oil: hydrogenated polyisobutene: component a is 3:3: 4.
The inventor discovers through a great deal of creative work that the three components in the proportion can play a synergistic effect to achieve better moisture-preserving and anti-allergy effects.
Preferably, the weight ratio of the glycerol to the p-hydroxyacetophenone to the 1, 2-hexanediol is as follows: glycerol: p-hydroxyacetophenone: 1, 2-hexanediol ═ 10:0.6: 0.6.
The inventor discovers through a great deal of creative work that the three components in the proportion can play a synergistic effect to achieve a better moisturizing effect.
In addition, the camellia oil anti-allergy moisturizing emulsion further comprises a proper amount of water, and a person skilled in the art can uniformly mix the components according to a conventional preparation method to prepare the camellia oil anti-allergy moisturizing emulsion.
Compared with the prior art, the invention has the beneficial effects that:
the camellia seed oil anti-allergy moisturizing emulsion disclosed by the invention adopts a very simple formula, is low in cost, does not bring burden to skin, provides fresh and non-greasy skin feeling under the combined action of all components, has good anti-allergy moisturizing effect and stability, can enhance the skin tolerance, is mild, does not irritate, and is suitable for long-term use.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.
The content of each component in the camellia oil anti-allergy moisturizing emulsion of the invention in the embodiments 1-5 is as follows 1:
TABLE 1 contents of the respective components in examples 1 to 5
Figure BDA0001367288440000041
Figure BDA0001367288440000051
And (3) uniformly mixing the components in the phase (1), the phase (2) and the phase (3) to obtain the camellia oil anti-allergy moisturizing emulsion disclosed by the embodiment 1-5 of the invention.
Example 6 moisturizing Performance test
20 female consumers aged 18-50 years are selected to respectively test the moisturizing performance of the emulsions described in examples 1-5, and during the test, the forehead is used as a test part, and a fixed area with the size of 2 square centimeters is drawn on the forehead of the face to be used as a test area. In an indoor environment with the temperature of 20 ℃ and the relative humidity of 50%, a CorneometerCM820 skin Moisture meter is used for testing the Moisture content of the skin of the forehead of 20 female consumers with the age of 18-50 years in each group, the result is represented by a set humidity Measurement Value (MMV), the final MMV Value is represented by an average result to evaluate the moisturizing performance of the product, and the moisturizing performance test of the camellia oil anti-sensitivity moisturizing emulsion in the examples 1-5 is shown in the table 2:
wherein: MMV 1-MMV value of skin before applying moisturizing sunscreen lotion, MMV 2-MMV value of skin within 1 minute after applying moisturizing sunscreen lotion, MMV 3-MMV value of skin after 1 hour after applying moisturizing sunscreen lotion; the water supplement rate is MMV2/MMV1 multiplied by 100 percent; moisture retention rate is MMV3/MMV2 × 100%.
Table 2 test results of water replenishing and moisturizing performances of camellia oil anti-allergy moisturizing emulsions in examples 1-5
Figure BDA0001367288440000052
Figure BDA0001367288440000061
As can be seen from the data in Table 2, the emulsions in the embodiments 1-5 of the invention have good moisturizing effect.
Example 7 anti-sensitivity Property test
100 women with sensitive skin are randomly selected, and the emulsion is used once before sleeping every night and after 3 months, no side effect or allergy is found. Therefore, the emulsion of the invention has no side effect on skin and has better anti-allergy performance.
Example 8 skin-refreshing effect test
The test was divided into a control group and an experimental group, the experimental group 7(a1) -7 (a3) were emulsions prepared in examples 3-5, the control group was 6, the emulsions of the control group 7(B1) -7 (B6) contained the same components as in example 5 except for the content of the three components, component a, component B and component C, and the specific control group 7(B1) -7 (B6) contained the components a, B and C in parts by weight as shown in table 3:
TABLE 3 content of component A, component B and component C in the control emulsion
Group of 7(b1) 7(b2) 7(b3) 7(b4) 7(b5) 7(b6)
Component A 4 0 0 4 0 4
Component B 0 0.6 0 0.6 0.6 0
Component C 0 0 1.5 0 1.5 1.5
Note: the contents of the respective components in table 3 are mass numbers in 100g of the product.
The emulsions of control groups 7(b1) to 7(b6) were prepared in the same manner as in example 5.
In the control group and the experimental group, each group randomly selected 100 women of 20-45 years old with sensitive skin as test subjects, the test subjects of the experimental groups 7(a1) -7 (a3) respectively used the emulsions prepared in the examples 3-5, and the test subjects of the control groups 7(b1) -7 (b6) respectively used the emulsions prepared in the control groups 7(b1) -7 (b6), the using method is to use the emulsions once every night before sleep, and after 3 months of use, the using feeling condition is counted, if the tested person feels fresh skin and is not hypersensitive, the result is shown in table 4.
Table 4 usage perception statistics
Figure BDA0001367288440000071
Figure BDA0001367288440000081
As can be seen from table 4, the emulsions of the control groups 7(B1) to 7(B6) contained only one or two of the three components of component a, component B, and component C, and did not have a very good skin-refreshing effect. The emulsions of experimental groups 7(a1) to 7(a3) contained three components and had very good skin-refreshing effect, especially the best skin-refreshing effect of experimental group 7(a 3). Therefore, the emulsion of the invention has the advantages that the three components of the component A, the component B and the component C have the mutual promotion and mutual synergy effects, and have the obvious skin refreshing effect and the enhanced use sensitivity.
Example 9 moisturizing Effect test
The test was divided into a control group and an experimental group, the experimental group 8(a1) to 8(a3) were emulsions prepared in examples 3 to 5, the control group was 6, the emulsions of the control group 8(b1) to 8(b6) contained the same components as in example 5 except for the content of glycerin, p-hydroxyacetophenone, and 1, 2-hexanediol, and the contents of the specific control group 8(b1) to 8(b6) in parts by weight of glycerin, p-hydroxyacetophenone, and 1, 2-hexanediol were as shown in table 5:
TABLE 5 content of glycerin, p-hydroxyacetophenone, and 1, 2-hexanediol in control emulsion
Group of 8(b1) 8(b2) 8(b3) 8(b4) 8(b5) 8(b6)
Glycerol 10 0 0 10 0 10
P-hydroxyacetophenone 0 0.6 0 0.6 0.6 0
1, 2-hexanediol 0 0 0.6 0 0.6 0.6
Note: the contents of the respective components in table 5 are mass numbers in 100g of the product.
The emulsions of control groups 8(b1) to 8(b6) were prepared in the same manner as in example 5.
In the control group and the experimental group, 100 women of 20-45 years old with sensitive and dry skin were randomly selected as test subjects for each group, the emulsions prepared in examples 3-5 were respectively used for the test subjects of the experimental groups 8(a1) -8 (a3), and the emulsions prepared in control groups 8(b1) -8 (b6) were respectively used for the test subjects of the control groups 8(b1) -8 (b6), and the results are shown in table 6 if the moisturizing rate is 80% or more and is not too sensitive, which is measured and calculated according to the measuring and calculating method of the moisturizing rate in example 6.
TABLE 6 statistical results of moisturizing effect
Group of Number of effective persons High efficiency
Control group 8(b1) 23 23％
Control group 8(b2) 22 22％
Control group 8(b3) 29 29％
Control group 8(b4) 34 34％
Control group 8(b5) 38 38％
Control group 8(b6) 35 35％
Experimental group 8(a1) 73 73％
Experimental group 8(a2) 71 71％
Experimental group 8(a3) 86 86％
As can be seen from table 6, the emulsions of the control groups 8(b1) to 8(b6) contained only one or two of glycerin, p-hydroxyacetophenone, and 1, 2-hexanediol, and did not have a good moisturizing effect. The emulsions of experimental groups 8(a1) to 8(a3) contain three components, and have a good moisturizing effect, particularly the moisturizing effect of experimental group 8(a3) is the best. Therefore, the emulsion of the invention has the effects of mutual promotion and mutual synergy of the three components of glycerol, p-hydroxyacetophenone and 1, 2-hexanediol, and has a remarkable moisturizing effect.
Example 10 test of moisturizing and anti-allergic Effect
The test was divided into a control group and an experimental group, the experimental group 9(a1) -9 (a3) were respectively the emulsions prepared in examples 3-5, the control group was 6, the emulsions of the control group 9(b1) -9 (b6) contained the same components as in example 5 except for the contents of camellia oil, hydrogenated polyisobutene and component a, and the contents of the three components of camellia oil, hydrogenated polyisobutene and component a in the control group 9(b1) -9 (b6) in parts by weight are shown in table 7:
TABLE 7 content of camellia seed oil, hydrogenated polyisobutene, component A in the control emulsion
Group of 9(b1) 9(b2) 9(b3) 9(b4) 9(b5) 9(b6)
Camellia seed oil 3 0 0 3 0 3
Hydrogenated polyisobutenes 0 3 0 3 3 0
Component A 0 0 4 0 4 4
Note: the contents of the respective components in Table 7 are mass numbers in 100g of the product.
The emulsions of control groups 9(b1) to 9(b6) were prepared in the same manner as in example 5.
In the control group and the experimental group, 100 women of 20-45 years old with sensitive and dry skin were randomly selected as test subjects for each group, the emulsions prepared in examples 3-5 were respectively used for the test subjects of the experimental groups 9(a1) -9 (a3), and the emulsions prepared in control groups 9(b1) -9 (b6) were respectively used for the test subjects of the control groups 9(b1) -9 (b6), and the results are shown in table 8 if the moisturizing rate is 80% or more and no allergy is considered to be effective according to the measurement and calculation method of the moisturizing rate in example 6.
TABLE 8 statistical results of the moisturizing and anti-allergic effects used
Figure BDA0001367288440000101
Figure BDA0001367288440000111
As can be seen from Table 8, the emulsions of the control groups 9(b1) to 9(b6) contained only one or two of camellia oil, hydrogenated polyisobutene and component A, and did not have a good moisturizing and anti-allergy effect. The emulsions of experimental groups 9(a1) to 9(a3) contain three components, and have good moisturizing and anti-allergy effects, especially the moisturizing and anti-allergy effects of experimental group 9(a3) are the best. Therefore, the camellia seed oil, the hydrogenated polyisobutene and the component A in the emulsion have the mutual promotion and mutual synergy effects, and have the obvious effects of moisture retention and allergy resistance.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.

Claims (4)

1. The camellia seed oil anti-allergy moisturizing emulsion is characterized by comprising the following components in parts by weight: 2-4 parts of camellia seed oil, 3-5 parts of a component A, 0.5-0.7 part of a component B, 0.5-1.5 parts of a component C, 2-4 parts of hydrogenated polyisobutene, 9-11 parts of glycerol, 0.5-0.7 part of p-hydroxyacetophenone and 0.5-0.7 part of 1, 2-hexanediol, wherein the component A is at least one of coconut oil alcohol-caprylate/caprate, C12-15 alcohol benzoate and glycerol tri (ethyl hexanoate); the component B is at least one of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, acrylic acid (ester)/vinyl isodecanoate cross-linked polymer and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer sodium; the component C is at least one of sorbitan olive oleate, glycerol stearate citrate and coco glucoside.
2. The camellia seed oil anti-allergy moisturizing emulsion as claimed in claim 1, wherein the weight ratio of the component A, the component B and the component C is as follows: and (2) component A: and (B) component: component C is 4:0.6: 1.5.
3. The camellia seed oil anti-allergy moisturizing emulsion as claimed in claim 1, wherein the camellia seed oil, the hydrogenated polyisobutene and the component A are in a weight ratio of: and (3) camellia seed oil: hydrogenated polyisobutene: component a is 3:3: 4.
4. The camellia seed oil anti-allergy moisturizing emulsion as claimed in claim 1, wherein the weight ratio of the glycerol to the p-hydroxyacetophenone to the 1, 2-hexanediol is: glycerol: p-hydroxyacetophenone: 1, 2-hexanediol ═ 10:0.6: 0.6.
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