CN106344465A - Moisturizing lotion without preservative - Google Patents
Moisturizing lotion without preservative Download PDFInfo
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- CN106344465A CN106344465A CN201611008967.XA CN201611008967A CN106344465A CN 106344465 A CN106344465 A CN 106344465A CN 201611008967 A CN201611008967 A CN 201611008967A CN 106344465 A CN106344465 A CN 106344465A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a moisturizing lotion without a preservative, and a preparation method thereof. The moisturizing lotion is prepared from the following components in percentage by weight: 10 to 20 percent of oil substance, 1 to 5 percent of emulgator, 0.1 to 1 percent of carbomer, 1 to 15 percent of polyhydric alcohol, 0.01 to 0.2 percent of sodium hyaluronate, 0.05 to 3 percent of panthenol, 0.05 to 3 percent of allantoin, 0.1 to 1 percent of glycerol caprylate, 0.1 to 2 percent of isooctyl glycerinum, 0.01 to 0.2 percent of disodium EDTA, 0.1 to 5 percent of traditional Chinese medicine extract composite, 0.01 to 1 percent of aminomethyl propanol, 0.01 to 0.5 percent of essence, and the balance of water to reach 100 percent. The moisturizing lotion without the preservative does not contain any preservative specified by Cosmetic Safety Technology Standard (Edition 2015), and is good in moisture retention, low in irritation, and safer to a human body.
Description
Technical field
The present invention relates to a kind of moisturizing emulsion without preservative, belong to cosmetic field.
Background technology
The use of cosmetics has a long history, now constantly carrying with expanding economy and people's living standard
Height, cosmetics have become an indispensable part in people's daily life.The cosmetics great majority of mankind's early application are all
Natural mineral matter, these materials inherently have the ability of antibacterial, there is not Anticorrosion.With social progress, science and technology
Development, former, the adjuvant of cosmetics are no longer limited to natural materials, but with the addition of various nutrient substance, cosmetics
In abundant nutritional labeling be easily subject to microorganism pollution, in addition the extraneous factor such as production equipment, packaging, storage also results in product
Product microorganism pollution, in order that cosmetics do not occur microorganism pollution within the shelf-life and in consumer's validity period, rationally prolongs
The long products shelf-life, various cosmetics must add certain preservative to prevent cosmetics from deterioration.
The cosmetics preservative of regulation definition is it is simply that refer to add in cosmetics to suppress microorganism to grow in this cosmetics
For the purpose of material." cosmetics safety technical specification " (2015) define preservative used in cosmetics must be this specification
In listed material, the meeting that these cosmetics preservatives using at present have produces stimulations, allergy etc. to skin and reacts, have to ring
Border has than larger harm.In recent years, state food drug regulatory department proposes increasingly to the safety of cosmetics
High requirement, safe and non-stimulating cosmetics progressively become focus of concern, and the safety of Preservative Technology for Personal Care is always
Enjoy query.With the raising of living standards of the people, for cosmetic allergic contact dermatitis problem pay attention to day by day.In order to comply with the consumption of the people
Demand, the research for the cosmetics without preservative has become as focus.
Content of the invention
It is an object of the invention to provide a kind of moisturizing emulsion without preservative and preparation method thereof.
To achieve the object of the present invention, present invention employs following technical scheme:
A kind of moisturizing emulsion without preservative is it is characterised in that be made up of the component of following percentage by weight: oily matter 10-
20%th, emulsifying agent 1-5%, Carbomer 0.1-1%, polyhydric alcohol 1-15%, hyaluronate sodium 0.01-0.2%, pantothenylol 0.05-3%, allantois
Plain 0.05-0.3%, glycerol caprylate 0.1-1%, iso-octyl glycerol 0.1-2%, edta disodium 0.01-0.2%, Chinese medicine extraction combination
Thing 0.1-5%, aminomethyl propanol 0.01-1%, essence 0.01-0.5%, water add to 100%.
Combinations of the above thing, wherein said oily matter is spermol, stearyl alcohol, cetearyl alcohol, behenyl alcohol, cocos nucifera oil
Alcohol-caprylate/decanoin, hydrogenated olive oil decanol esters, dicaprylyl carbonate, caprylic/capric triglyceride, Butyrospermum parkii fruit
Fat, olive oil, jojoba seed oil, white Limnanthes Alba Seed Oil, hydrogenated olive oil decanol esters, shea butter, glyceryl stearate,
Isopropyl palmitate, isopropyl myristate, isononyl isononanoate, tocopherol acetass, Ascorbyl Tetraisopalmitate, poly-
The combination of any more than three kinds in dimethyl siloxane and dimethiconol, Cyclomethicone, mineral oil
Thing.
Combinations of the above thing, wherein said emulsifying agent is polysorbate -20, c12-20 alkyl androstanediol, arachidic alcohol
Glucoside, cetearyl glucoside, Coco-Glucoside, Natrulon H-10 five stearate, cetearyl alcohol Fructus Canarii albi Oleic acid
Ester, Pyrusussuriensiss smooth Fructus Canarii albi oleate, cetyl peg/ppg-10/1 polydimethylsiloxane, lecithin, methyl times semihard
Any one or more combination in fat acid ester, peg-10 polydimethylsiloxane, hydrolecithin.
Combinations of the above thing, wherein said polyhydric alcohol is glycerol, propylene glycol, butanediol, dipropylene glycol, 1,2- penta 2
Any one or more combination in alcohol, Sorbitol, PEG-8.
Combinations of the above thing, wherein said Chinese medicine extraction compositionss are to make Flos Lonicerae by the plant of following parts by weight
30-50 part, Flos Hibisci Mutabilis 20-45 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 20-45 part, Dendrobium nobile 20-30 part.Preparation method is as follows: plant pulverized, point
Do not sieved with 20～100 mesh sieve, mixing, be that 5:1～20:1 adds Extraction solvent by liquid material mass ratio, after soaking 1～5h,
10～100mpa extracts and carries out extract at room temperature with high pressure homogenization method machine under pressure, after extracting solution is centrifuged, with membrance concentration,
Concentrated solution macroporous resin adsorption, the more multiple eluting of ethanol being 10～95% with volume fraction, collect eluent, membrance concentration is extremely
Extracting solution is 1:0.1～1:5 with the mass ratio of plant amedica, adds butanediol dissolving, filters, prepared plant drug composition；Carry
Take solvent to be water, ethanol or ethanol water.
A kind of moisturizing emulsion without preservative of the present invention does not contain " cosmetics safety technical specification " (2015
Year) any preservative of defined.
A kind of preparation method of moisturizing emulsion without preservative of the present invention is it is characterised in that concretely comprise the following steps:
(1) oil-soluble constitents such as oily matter, oil soluble emulsifying agent, glycerol caprylate are put into oil cauldron and be heated to 80 DEG C, stir
Mix mix homogeneously so as to be completely dissolved, be oil phase, stand-by.
(2) by water, water soluble emulsifier, polyhydric alcohol, iso-octyl glycerol, Carbomer, hyaluronate sodium, pantothenylol, allantoin,
The water-soluble components such as edta disodium, citric acid are put into emulsifying pot and are heated to 85 DEG C, are uniformly mixed so as to be completely dissolved,
For aqueous phase, stand-by.
(3) control homogenizing speed in 1000-8000r/min, mixing speed is in 200-500r/min.Quickly oil phase is put into
Emulsifying pot, homogenizing 3-10min.
(4) stop homogenizing, maintain the temperature at 80 DEG C, control mixing speed in 200-500r/min, stir 10min.
(5) it is kept stirring for speed in 200-500r/min, lower the temperature.
(6) cool to 40 DEG C and Chinese medicine extraction compositionss, essence, aminomethyl propanol are added emulsifying pot, evacuation, stirring is all
Even.
(7) stir, cool to 35 DEG C of dischargings, fill is sealed up for safekeeping.
Specific embodiment
Below by way of specific embodiment come the present invention is further illustrated, but these embodiments simply to illustrate that,
It is not limitation of the present invention.
Embodiment 1 does not contain the moisturizing emulsion () of preservative
The moisturizing emulsion formula not containing preservative is shown in Table 1.
Table 1
Preparation method is as follows:
(1) oil-soluble constitents such as oily matter, oil soluble emulsifying agent, glycerol caprylate are put into oil cauldron and be heated to 80 DEG C, stir
Mix mix homogeneously so as to be completely dissolved, be oil phase, stand-by.
(2) by water, water soluble emulsifier, polyhydric alcohol, iso-octyl glycerol, Carbomer, hyaluronate sodium, pantothenylol, allantoin,
The water-soluble components such as edta disodium, citric acid are put into emulsifying pot and are heated to 85 DEG C, are uniformly mixed so as to be completely dissolved,
For aqueous phase, stand-by.
(3) control homogenizing speed in 1000-8000r/min, mixing speed is in 200-500r/min.Quickly oil phase is put into
Emulsifying pot, homogenizing 3-10min.
(4) stop homogenizing, maintain the temperature at 80 DEG C, control mixing speed in 200-500r/min, stir 10min.
(5) it is kept stirring for speed in 200-500r/min, lower the temperature.
(6) cool to 40 DEG C and Chinese medicine extraction compositionss, essence, aminomethyl propanol are added emulsifying pot, evacuation, stirring is all
Even.
(7) stir, cool to 35 DEG C of dischargings, fill is sealed up for safekeeping.
The moisturizing emulsion containing preservative for the comparative example 1
Containing the most frequently used preservative of cosmetics (by methyl parahydroxybenzoate, propyl p-hydroxybenzoate, phenoxyethanol together
Composition conventional emulsion protective system) moisturizing emulsion formula be shown in Table 1
Preparation method is consistent with embodiment 1.
Embodiment 2 moisturizing emulsion ()
Formula is shown in Table 2.
Table 2
Preparation method is consistent with embodiment 1.
Test example 1 moisture-keeping efficacy evaluation experimental
According to light industry standard qb/t 4256-2011 cosmetics moisture-keeping efficacy evaluation guide, measure the guarantor of embodiment 1 preparation
The moistening effect of wet emulsion ().
1st, experimental principle: the moisture using capacitance method mensure human skin keratinocyte's layer is based on water and other materials
Difference in dielectric constant is notable, and according to the difference of keratodermatitis moisture, the capacitance of the skin recording is different, and its parameter can
Represent skin moisture content.
2nd, experimental apparatus: courage+khazaha company of comermeter cm825(Germany
3rd, experimental technique: healthy volunteer 30, male 20, women 10, the age is in 25-50 year.Isoperibol (20 ~
22 DEG C), relative humidity 50 ± 10%, after 1 hour of rest.It is respectively adopted the sample of embodiment 1, by (2.0 ± 0.1) mg/ 2
Consumption is coated in inside experimenter's left hand inner forearm (3cm × 3cm) and right forearm (3cm × 3cm).Blank (not applying) is simultaneously
Test.It is being painted with 1 hour of sample, 2 hours, 4 hours, the degree of hydration state of 6 hours test skin respectively.
4th, experimental result: be shown in Table 3.
Table 3
Result shows, the moisturizing emulsion of the present invention has more preferable moistening effect than comparative example 1, longer to the moisture preserving time of skin.
Test example 2 preservation challenge is tested
With the moisturizing emulsion of system described in embodiment 1, common mixed cell (Staphylococcus aureus in the work of single inoculation cosmetics
Bacterium sa, escherichia coli ec, Pseudomonas aeruginosa pa), mixed fungus (Aspergillus niger an, white vacation screw mandrel bacterium ca), according to cosmetic
Product, toilet articles and fragrance association (ctfa) Microbial Challenge test method, the sample monitoring cycle is 28 days, and period exists respectively
Carry out within 2nd, 7,14 and 28 days sample detection, calculate the clump count (cfu) of every ml.Result is as shown in table 4
Table 4 bacteriostatic experiment result
| Strain | 0 day | 7 days | 14 days | 21 days | 28 days |
| Mixed cell | 3×107 | 0 | 0 | 0 | 0 |
| Mixed fungus | 5×105 | 0 | 0 | 0 | 0 |
Table 1 result shows, with the moisturizing emulsion obtaining described in embodiment 1, can pass through preservation challenge, fully achieve anti-corrosion effect
Really.
Test example 3 patch is tested
With the moisturizing emulsion of system described in embodiment 1, carry out patch test and test its anaphylaxis to skin, method is: select
Qualified speckle tries device, and sample uniform application is tried in device in speckle, then spreads on the back of experimenter, is allowed to uniformly docile and obedient with the light pressure of palm
On skin, continue 72h.It is spaced 30min after removing tested material speckle examination device, after impression disappears, observe dermoreaction.With reference to " change
Cosmetic technical specification of security " dermoreaction grade scale record reaction result in (version in 2015).Negative control: deionized water.
Experimenter totally 30 people, male 20, women 10.Face test result on probation is as shown in table 5.
Table 5
| Phenomenon | Skin pruritus | Skin irritation | Red swelling of the skin | Skin generates heat | Other untoward reaction | Amount to |
| Comparative example 1 | 1 | 1 | 0 | 0 | 2 | |
| Embodiment 1 | 0 | 0 | 0 | 0 | 0 | 0 |
Table 5 result shows, with the moisturizing emulsion of system described in embodiment 1, any allergic phenomena and bad in trier
Reaction.
Claims (7)
1. a kind of moisturizing emulsion without preservative it is characterised in that: be made up of the component of following percentage by weight: oily matter
10-20%, emulsifying agent 1-5%, Carbomer 0.1-1%, polyhydric alcohol 1-15%, hyaluronate sodium 0.01-0.2%, pantothenylol 0.05-3%, urine
Bursin 0.05-0.3%, glycerol caprylate 0.1-1%, iso-octyl glycerol 0.1-2%, edta disodium 0.01-0.2%, Chinese medicine extraction group
Compound 0.1-5%, aminomethyl propanol 0.01-1%, essence 0.01-0.5%, water add to 100%；Described a kind of without preservative
Moisturizing emulsion, does not contain any preservative of " cosmetics safety technical specification " (version in 2015) defined.
2. the oily matter described in claim 1 be spermol, stearyl alcohol, cetearyl alcohol, behenyl alcohol, cocoanut oil alcohol-caprylate/
Decanoin, hydrogenated olive oil decanol esters, dicaprylyl carbonate, caprylic/capric triglyceride, Butyrospermum parkii fruit fat, olea europaea fruit
Oil, jojoba seed oil, white Limnanthes Alba Seed Oil, hydrogenated olive oil decanol esters, shea butter, glyceryl stearate, Palmic acid isopropyl
Ester, isopropyl myristate, isononyl isononanoate, tocopherol acetass, Ascorbyl Tetraisopalmitate, polydimethylsiloxanes
The compositionss of any more than three kinds in alkane and dimethiconol, Cyclomethicone, mineral oil.
3. the emulsifying agent described in claim 1 is polysorbate -20, c12-20 alkyl androstanediol, arachidic alcohol glucoside, whale
Wax stearyl glucoside, Coco-Glucoside, Natrulon H-10 five stearate, cetearyl alcohol Fructus Canarii albi oleate, Pyrusussuriensiss are smooth
Fructus Canarii albi oleate, cetyl peg/ppg-10/1 polydimethylsiloxane, lecithin, methyl sesquistearate,
Any one or more combination in peg-10 polydimethylsiloxane, hydrolecithin.
4. the polyhydric alcohol described in claim 1 be glycerol, propylene glycol, butanediol, dipropylene glycol, 1,2- pentanediol, Sorbitol, poly-
Any one or more combination in ethylene glycol -8.
5. the Chinese medicine extraction compositionss described in claim 1 are to make Flos Lonicerae 30-50 part, cottonrose hibiscus by the plant of following parts by weight
Rong spends 20-45 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 20-45 part, Dendrobium nobile 20-30 part.
6. preparation method is as follows: plant is pulverized, is sieved with 20～100 mesh sieve respectively, mixing, be 5:1 by liquid material mass ratio
～20:1 adds Extraction solvent, after soaking 1～5h, extracts in 10～100mpa and carries out room temperature with high pressure homogenization method machine under pressure
Extract, after extracting solution is centrifuged, with membrance concentration, concentrated solution macroporous resin adsorption, then be 10～95% with volume fraction
The multiple eluting of ethanol, collects eluent, and membrance concentration to extracting solution is 1:0.1～1:5 with the mass ratio of plant amedica, adds fourth two
Alcohol dissolves, and filters, prepared plant drug composition；Extraction solvent is water, ethanol or ethanol water.
7. a kind of described in claim 1 one preparation method of the moisturizing emulsion without preservative is it is characterised in that concrete steps
For:
(1) oil-soluble constitents such as oily matter, oil soluble emulsifying agent, glycerol caprylate, iso-octyl glycerol are put into oil cauldron to add
Heat, to 80 DEG C, is uniformly mixed so as to be completely dissolved, is oil phase, stand-by；
(2) by water, water soluble emulsifier, polyhydric alcohol, Carbomer, hyaluronate sodium, pantothenylol, allantoin, edta disodium, citric acid
Put into emulsifying pot Deng water-soluble component and be heated to 85 DEG C, be uniformly mixed so as to be completely dissolved, be aqueous phase, stand-by；
(3) control homogenizing speed in 1000-8000r/min, oil phase, in 200-500r/min, is quickly put into emulsifying by mixing speed
Pot, homogenizing 3-10min；
(4) stop homogenizing, maintain the temperature at 80 DEG C, control mixing speed in 200-500r/min, stir 10min；
(5) it is kept stirring for speed in 200-500r/min, lower the temperature；
(6) cool to 40 DEG C and Chinese medicine extraction compositionss, essence are added emulsifying pot, evacuation, stir；
(7) stir, cool to 35 DEG C of dischargings, fill is sealed up for safekeeping.
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| CN201611008967.XA CN106344465A (en) | 2016-11-16 | 2016-11-16 | Moisturizing lotion without preservative |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107184410A (en) * | 2017-04-28 | 2017-09-22 | 广州瑞誉化工科技有限公司 | A kind of skin cream with steroid dependent dermatitis repair function |
| CN107375029A (en) * | 2017-08-01 | 2017-11-24 | 广东芭薇生物科技股份有限公司 | A kind of camellia seed oil antiallergic moisturizing emulsion |
| CN107669500A (en) * | 2017-11-28 | 2018-02-09 | 广州市花安堂生物科技有限公司 | A kind of moisturizing elite breast and preparation method thereof |
| CN108261382A (en) * | 2018-02-27 | 2018-07-10 | 广州彤博士健康科技有限公司 | Subset moisturizing emulsion formulations and preparation method |
| CN108294979A (en) * | 2017-12-29 | 2018-07-20 | 青岛百瑞吉生物工程有限公司 | A kind of moisturizing gel emulsion and preparation method thereof |
| CN108451855A (en) * | 2018-04-26 | 2018-08-28 | 佛山市芊茹化妆品有限公司 | A kind of Dead Sea clay mask of tender skin |
| CN108524386A (en) * | 2018-03-30 | 2018-09-14 | 广东巴松那生物科技有限公司 | A kind of antiallergic skin care milk and preparation method thereof of releiving without chemical preservative |
| CN108785141A (en) * | 2018-09-14 | 2018-11-13 | 广州优刻生物科技有限公司 | A kind of beautifying liquid, preparation method and applications |
| CN109464308A (en) * | 2018-11-15 | 2019-03-15 | 广东轻工职业技术学院 | A kind of essential oil composition and application with anti-blue light skin-care effect |
| CN110585044A (en) * | 2019-10-14 | 2019-12-20 | 遵义医科大学 | Compound traditional Chinese medicine composition containing dendrobium stem and preparation method thereof |
| CN111728892A (en) * | 2020-08-14 | 2020-10-02 | 宋家豪 | Oil-control cosmetic cream for improving oily skin and preparation method thereof |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107184410A (en) * | 2017-04-28 | 2017-09-22 | 广州瑞誉化工科技有限公司 | A kind of skin cream with steroid dependent dermatitis repair function |
| CN107375029A (en) * | 2017-08-01 | 2017-11-24 | 广东芭薇生物科技股份有限公司 | A kind of camellia seed oil antiallergic moisturizing emulsion |
| CN107669500A (en) * | 2017-11-28 | 2018-02-09 | 广州市花安堂生物科技有限公司 | A kind of moisturizing elite breast and preparation method thereof |
| CN108294979A (en) * | 2017-12-29 | 2018-07-20 | 青岛百瑞吉生物工程有限公司 | A kind of moisturizing gel emulsion and preparation method thereof |
| CN108261382A (en) * | 2018-02-27 | 2018-07-10 | 广州彤博士健康科技有限公司 | Subset moisturizing emulsion formulations and preparation method |
| CN108524386A (en) * | 2018-03-30 | 2018-09-14 | 广东巴松那生物科技有限公司 | A kind of antiallergic skin care milk and preparation method thereof of releiving without chemical preservative |
| CN108451855A (en) * | 2018-04-26 | 2018-08-28 | 佛山市芊茹化妆品有限公司 | A kind of Dead Sea clay mask of tender skin |
| CN108785141A (en) * | 2018-09-14 | 2018-11-13 | 广州优刻生物科技有限公司 | A kind of beautifying liquid, preparation method and applications |
| CN109464308A (en) * | 2018-11-15 | 2019-03-15 | 广东轻工职业技术学院 | A kind of essential oil composition and application with anti-blue light skin-care effect |
| CN110585044A (en) * | 2019-10-14 | 2019-12-20 | 遵义医科大学 | Compound traditional Chinese medicine composition containing dendrobium stem and preparation method thereof |
| CN110585044B (en) * | 2019-10-14 | 2022-06-17 | 遵义医科大学 | Compound traditional Chinese medicine composition containing dendrobium stem and preparation method thereof |
| CN111728892A (en) * | 2020-08-14 | 2020-10-02 | 宋家豪 | Oil-control cosmetic cream for improving oily skin and preparation method thereof |
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Application publication date: 20170125 |
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