CN108309829A - Skin care milk and preparation method thereof containing camellia seed oil - Google Patents
Skin care milk and preparation method thereof containing camellia seed oil Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses a kind of skin care milks containing camellia seed oil,Including 100 parts of water,0.5 5 parts of parahydroxyacet-ophenone,18 parts of trehalose,5 15 parts of glycerine,5 15 parts of butanediol,0.05 0.3 parts of Sodium Hyaluronate,1 10 parts of niacinamide,0.05 0.5 parts of dipotassium glycyrrhizinate,5 25 parts of camellia seed oil,5 15 parts of mink oil,15 parts of cetostearyl alcohol and/or cocoyl glucoside,2 10 parts of jojoba seed oil,2 10 parts of Queensland nut seed oil,2 10 parts of olive oil,2 10 parts of ring five dimethyl silicone polymer,2 10 parts of saualane,2 10 parts of dimethyl silicone polymer,2 10 parts of isononyl isononanoate,2 10 parts of glycerine three (thylhexoic acid) ester,1 10 parts of tocopherol,0.5 3 parts of hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers and 1,2 0.5 5 parts of hexylene glycols；Also disclose preparation method.By each component raw material scientific compatibility, realize that moisturizing, crease-resistant, anti-aging and sun-proof maintenance multiple efficacies, salubrious non-greasy are suitable for various skin quality.
Description
Technical field
The invention belongs to household chemicals technical field more particularly to a kind of skin care milk containing camellia seed oil and its preparations
Method.
Background technology
With advancing age, epidermal cell division, growth and differentiation efficiency are lower, the lipid synthesis energy of keratoderma
Power declines, while the influence of the multi-party factor such as life stress, environmental pollution growing day by day, and skin problem is caused to frequently occur.
For example, skin water loss can be caused by lacking moisturizing factor and lipid, the water content of cuticula is reduced, when water content is down to 10%
When following, skin seems dry, coarse, tarnishes and elasticity；Undesirable environmental factor, such as dry air, pollutant, purple
The infringements such as outside line, radiation can make skin become drier, further speed up skin aging.Water be skin important composition at
Point, it is conducive to maintain epidermal cell normally metabolic, keeps skin tender, plentiful, soft, glossy.For example, adult skin
Water content is the 18%-20% of human body water requirement, and the water content of infant skin is up to 80%, therefore infant's skin delicacy light
It is sliding.On the contrary, the moisture content of skin of the elderly is far below adult, therefore has dry skin, withers that flat, wrinkle is more.Therefore, how skin is kept
It is particularly significant in cosmetics research and development to reduce moisture loss for the moisture of skin.The skin care item with moisture-keeping efficacy are non-on the market at present
Chang Duo, but the molecular structure due to moisturizing ingredient differs greatly with sebum, it is difficult to it is absorbed by the skin, influences instead normal raw
Reason metabolism.
Other than the influence of moisture, collagen and elastic fibers albumen, hyaluronic acid and glycoprotein in skin corium
Also skin can be supported, its is made full to compact.Increased by the age, internal system or immune function decline are influenced, the conjunction of albumen
Change at reducing or arranging, the various problems such as skin elasticity decline, obscure, the wrinkle hyperplasia of the colour of skin can be caused.
Camellia seed oil mid-oleic is about 80~83%, and linoleic acid is about 7~13%, also contains multivitamin, tea
Polyphenol, squalene, ketone isoreactivity substance, have the function of moisturizing, skin care and anti-aging.For example, the parent of oleic acid and skin
It is good with property, it is easily absorbed by the skin, to cell Yellow Gentian Extract；Active material can make skin restore natural elasticity, gloss and tender,
Skin corrugation and coarse is prevented, and has special absorbability to ultraviolet light.Tea oil has preliminary in the application of skin care field
Research, however existing tea oil extraction process is squeezed mainly to produce based on crude oil, or by high temperature, or use a large amount of chemistry
Preparation, the active material in tea oil are easily destroyed, and active component content is limited, and there are chemical residuals, influence cosmetics work(
Effect.In addition, tea oil viscosity is big, bad dispersibility, it is thick and heavy to easily cause white matter, is unfavorable for absorbing.
Invention content
In order to solve the above technical problem, the present invention provides a kind of skin care milk and preparation method thereof containing camellia seed oil.
To achieve the goals above, the present invention uses following technical scheme：
A kind of skin care milk containing camellia seed oil, including following raw material by weight：
(1) component A：
100 parts of water, 0.5-5 parts of parahydroxyacet-ophenone, 1-8 parts of trehalose, 5-15 parts of glycerine, 5-15 parts of butanediol are transparent
0.05-0.3 parts of matter acid sodium, 1-10 parts of niacinamide, 0.05-0.5 parts of dipotassium glycyrrhizinate；
(2) B component：
1-5 parts of 5-25 parts of camellia seed oil, 5-15 parts of mink oil, cetostearyl alcohol and/or cocoyl glucoside, Jojoba seed
It is 2-10 parts oily, 2-10 parts of Queensland nut seed oil, 2-10 parts of olive oil, 2-10 parts of ring five dimethyl silicone polymer, saualane
2-10 parts, 2-10 parts of dimethyl silicone polymer, 2-10 parts of isononyl isononanoate, 2-10 parts of (thylhexoic acid) ester of glycerine three, fertility
1-10 parts of phenol；
(3) component C：Hydroxy-ethyl acrylate/0.5-3 parts of sodium acryloyldimethyl taurate copolymers；
(4) D components：0.5-5 parts of 1,2- hexylene glycols.
Preferably, the camellia seed oil is using the camellia seed of organic farming as raw material, at 35 DEG C or less through cold pressing, filter plate
Filtering, activated carbon filtering are made；Further, camellia seed oil mid-oleic ＞ 85%, the palmitic acid content ＞ 9%, firmly
Resin acid content ＞ 2.5%, iodine number 75-85gI2/ 100g, saponification number 185-195mgKOH/g, unsaponifiable matter≤1%.Wherein, oily
Sour penetrating power and moisture-keeping function are strong, have bactericidal effect, can prevent pachylosis, keep skin water profit clean；Palmitic acid is flat
The grease that weighs generates, and help forms sebum film, reduces scattering and disappearing for moisture, effective delay skin aging；Stearic acid inhibit gelatin enzyme A and
B is generated, and reduces protein breakdown, is played the role of improving skin and is increased skin elasticity.In addition, there are many also containing in camellia seed oil
Vitamin, it is highly beneficial to nourishing skin, such as vitamin A can moisten dry skin, prevent skin from wrinkling；Vitamin D promotees
Into body metabolism, skin elasticity, pre- anti-wrinkle is kept to generate；Vitamin C and E inhibit skin aging and flexibility decrease.
In above-mentioned raw materials, mink oil is natural triglyceride, nontoxic, non-stimulated, physicochemical property and body fat pole
It is similar, it is easy to be absorbed by the skin, permeability and ductility are good, have good emulsifiability, anti-oxidant and ultraviolet-absorbing
Can, to heat, oxidation stability, wrinkled skin and aging can be prevented, keep skin tender and flexible, especially accommodate dry skin.
Jojoba seed oil：Molecules align and human body grease are very similar, are easily absorbed by the skin, and have excellent stabilization
Property, ductility, permeability and certain hydrophily, fat secretion can be adjusted, moisten and moistening effect is good.Jojoba seed oil is rich in
Vitamin D and protein, are particularly suitable for ripe and sensitive skin, energy cutin-softening, and pre- anti-wrinkle generates.
Trehalose：It is a kind of irreducibility disaccharide of stabilization, can helps to maintain the original nutrition of skin and moisture, avoid skin
Solarization injures melanin deposition, is effective against skin aging.
Macadimia nut oil：Moisturizing, ductility and good penetrability are moistened, does not stimulate mildly, but has certain greasy feeling.
Olive oil：Rich in unsaturated fatty acid, multivitamin and phenols polyphenoils, it is easy to absorb, can prevents
Skin wrinkles and coarse, delay skin aging, moreover it is possible to absorb certain ultraviolet light, prevent tanned sunburn.
Saualane：Closest to a kind of lipid of human sebaceous, skin-friendly and moisture retention are good, mild non-stimulated, easily absorb, energy
Promote blood microcirculation, promote the metabolism of cell, damaged cell is repaired in help.Saualane moistens chemical property and stablizes, right
Mould has inhibiting effect.
Hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers：As thickener and emulsion stabilizer, breast is promoted
The texture of liquid is smooth to the touch not sticky.
A method of the above-mentioned skin care milk containing camellia seed oil is prepared, is included the following steps：
(1) prepared by component A：
Raw material is weighed by weight, and water, parahydroxyacet-ophenone are put into water phase pot, are heated to 70-80 DEG C, stirring and dissolving,
Trehalose, glycerine, butanediol, Sodium Hyaluronate, niacinamide and dipotassium glycyrrhizinate is added, is warming up to 80-85 DEG C, stirring and dissolving,
Component A is obtained, it is spare；
(2) prepared by B component：
Raw material is weighed by weight, by camellia seed oil, mink oil, cetostearyl alcohol and/or cocoyl glucoside, Jojoba
Seed oil, Queensland nut seed oil, olive oil, ring five dimethyl silicone polymer, saualane, dimethyl silicone polymer, isononanoic acid
Different nonyl ester, glycerine three (thylhexoic acid) ester, tocopherol sequentially add oil phase pot, are heated to 80-85 DEG C, stirring and dissolving obtains B groups
Point, it is spare；
(3) by A made from step (1), (2), B component input emulsification pot, 2- is stirred with 1000-3000r/min rotating speeds
5min；
(4) step (3) is added in 0.5-3 parts by weight of acrylic acid hydroxyl ethyl ester/sodium acryloyldimethyl taurate copolymers to make
In the material obtained, stir evenly, homogeneous 3-5min keeps emulsification more abundant, and lotion is finer and smoother；
(5) it is warming up to 80-85 DEG C, constant temperature emulsifies 25-40min under 500-1000r/min rotating speeds, adjusts rotating speed to 100-
500r/min, stirring are cooled to 40-50 DEG C；
(6) by 0.5-5 parts by weight 1,2- hexylene glycols are added in material made from step (5), with 100-500r/min rotating speeds
10-20min is stirred, is cooled to room temperature；
(7) it examines, discharges, packaging obtains product.
Beneficial effects of the present invention：
(1) present invention realizes moisturizing, crease-resistant, anti-aging and sun-proof maintenance by the reasonable compatibility of each component raw material
Multiple efficacies, the salubrious non-greasy of product are suitable for various skin quality.Wherein, the oleic acid in camellia seed oil and mink oil, Jojoba seed
The property of oil and saualane is easy to be absorbed by the skin close to human sebaceous, arranges in pairs or groups and uses with macadimia nut oil, overcomes spiny dogfish
The defect that alkane spreadability is general and macadimia nut oil is greasy, realize it is excellent moisten, moisturizing and the effect of adjust fat secretion；Mountain
Tea-seed oil, jojoba seed oil, olive oil are rich in multivitamin and active material, arrange in pairs or groups and use with niacinamide, anti-oxidant
Property it is good, play the role of promoting cell metabolism, reduce protein breakdown and cutin-softening, can tough cell membrane, slow down aging, keep
Skin elasticity, pre- anti-wrinkle generate；Camellia seed oil has what is cooperateed with to form isolated protective layer in skin surface with olive oil
Effect, can under the adverse circumstances such as high temperature, drying, intensive ultraviolet radiation effective protection cell membrane；
(2) camellia seed oil has the inhibiting effect cooperateed with saualane to mould, and product is not necessarily to preservative, mild stingless
Swash, is suitable for sensitive skin type；
(3) camellia seed oil content of the present invention is high, solves the problems, such as that camellia seed oil is sticky, is not easy to disperse, and is conducive to nutrients
The full effect of matter absorbs, technical target of the product meet QB/T 1857-2013 and《Cosmetics safety technical specification》(version in 2015)
It is required that.
Specific implementation mode
With reference to specific embodiment, the present invention will be described in detail.
The skin care milk formula (unit/parts by weight) of table 1 embodiment 1-3 and comparative example 1-3
Embodiment 1-3
Raw material is weighed by the formula of table 1, the preparation process of above-mentioned skin care milk is as follows：
(1) prepared by component A：
Water, parahydroxyacet-ophenone are put into water phase pot, are heated to 70 DEG C, trehalose, glycerine, fourth two is added in stirring and dissolving
Alcohol, Sodium Hyaluronate, niacinamide and dipotassium glycyrrhizinate are warming up to 85 DEG C, and stirring and dissolving obtains component A, spare；
(2) prepared by B component：
By camellia seed oil, mink oil, cetostearyl alcohol and/or cocoyl glucoside, jojoba seed oil, Queensland nut seed
Oil, olive oil, ring five dimethyl silicone polymer, saualane, dimethyl silicone polymer, isononyl isononanoate, three (second of glycerine
Base caproic acid) ester, tocopherol sequentially add oil phase pot, 85 DEG C are heated to, stirring and dissolving obtains B component, spare；
(3) by A made from step (1), (2), B component input emulsification pot, 5min is stirred with 1500r/min rotating speeds；
(4) hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers are added in material made from step (3),
It stirs evenly, homogeneous 5min keeps emulsification more abundant, and lotion is finer and smoother；
(5) 80 DEG C are warming up to, constant temperature emulsifies 30min under 800r/min rotating speeds, adjusts rotating speed to 150r/min, stirring is cold
But to 50 DEG C；
(6) 1,2- hexylene glycols are added in the material of step (5), 15min is at the uniform velocity stirred with 150r/min rotating speeds, is cooled to
Room temperature；
(7) it examines, discharges, packaging obtains product.
Comparative example 1
Product is prepared as described in Example 1, unlike, the water of mink oil equivalent therein is substituted.
Comparative example 2
Product is prepared as described in Example 1, unlike, the water of olive oil equivalent therein is substituted.
Comparative example 3
Product is prepared as described in Example 1, unlike, the water of saualane equivalent therein is substituted.
Test case
(1) moisture retention and sense of touch evaluation
Subject：5-10 Sui 10 people of juvenile, young 10-18 Sui 10 people, 20-50 Sui 40 people of adult female；
Evaluation method：Sample is smeared in subject's cheek, is evaluated after 2h, test result is as shown in table 2.
Table 2
It can be seen from the above result that mink oil and saualane can significantly improve moisture retention and sense of touch, product is mildly non-stimulated, right
Juvenile is also applicable in.
(2) stability test
The skin care milk sample of Example 1-3 and comparative example 1-3 is placed in 45 DEG C of insulating boxs, weekly to lotion color into
Row evaluation, continues one month, test result is as follows：The last fortnight, all samples are unchanged；Third week, only comparative example 2 and 3 samples
Product light discolouration；4th week, embodiment 2 and 3 samples are without significant change, the 1 sample light discolouration of embodiment 1 and comparative example, comparison
Example 2 and 3 color samples obviously deepen.As can be seen from the above results, olive oil or saualane is added, or improves camellia seed
Oil content can significantly improve the stability of product.
The preferred embodiment of the present invention has been described above in detail, still, during present invention is not limited to the embodiments described above
Detail, a variety of equivalent substitutes that those skilled in the art carries out within the scope of the technical concept of the present invention or simple become
Type mode, all belongs to the scope of protection of the present invention.
Claims (4)
1. a kind of skin care milk containing camellia seed oil, which is characterized in that including following raw material by weight：
(1) component A：
100 parts of water, 0.5-5 parts of parahydroxyacet-ophenone, 1-8 parts of trehalose, 5-15 parts of glycerine, 5-15 parts of butanediol, hyaluronic acid
0.05-0.3 parts of sodium, 1-10 parts of niacinamide, 0.05-0.5 parts of dipotassium glycyrrhizinate；
(2) B component：
1-5 parts of 5-25 parts of camellia seed oil, 5-15 parts of mink oil, cetostearyl alcohol and/or cocoyl glucoside, jojoba seed oil 2-
10 parts, 2-10 parts of Queensland nut seed oil, 2-10 parts of olive oil, 2-10 parts of ring five dimethyl silicone polymer, saualane 2-10
Part, 2-10 parts of dimethyl silicone polymer, 2-10 parts of isononyl isononanoate, 2-10 parts of (thylhexoic acid) ester of glycerine three, tocopherol 1-
10 parts；
(3) component C：Hydroxy-ethyl acrylate/0.5-3 parts of sodium acryloyldimethyl taurate copolymers；
(4) D components：0.5-5 parts of 1,2- hexylene glycols.
2. skin care milk according to claim 1, which is characterized in that the camellia seed oil is original with the camellia seed of organic farming
Material is filtered through cold pressing, filter plates, activated carbon at 35 DEG C or less and is made.
3. skin care milk according to claim 2, which is characterized in that the camellia seed oil mid-oleic ＞ 85%, palm
Acid content ＞ 9%, stearic acid content ＞ 2.5%, iodine number 75-85gI2/ 100g, saponification number 185-195mgKOH/g, unsaponifiable matter
≤ 1%.
4. a kind of method preparing the skin care milk described in any one of claim 1-3, which is characterized in that include the following steps：
(1) prepared by component A：
Raw material is weighed by weight, and water, parahydroxyacet-ophenone are put into water phase pot, are heated to 70-80 DEG C, stirring and dissolving is added
Trehalose, glycerine, butanediol, Sodium Hyaluronate, niacinamide and dipotassium glycyrrhizinate, are warming up to 80-85 DEG C, and stirring and dissolving obtains A
Component, it is spare；
(2) prepared by B component：
Raw material is weighed by weight, by camellia seed oil, mink oil, cetostearyl alcohol and/or cocoyl glucoside, Jojoba seed
Oil, Queensland nut seed oil, olive oil, ring five dimethyl silicone polymer, saualane, dimethyl silicone polymer, isononanoic acid are different
Nonyl ester, glycerine three (thylhexoic acid) ester, tocopherol sequentially add oil phase pot, are heated to 80-85 DEG C, stirring and dissolving obtains B groups
Point, it is spare；
(3) by A made from step (1), (2), B component input emulsification pot, 2-5min is stirred with 1000-3000r/min rotating speeds；
(4) 0.5-3 parts by weight of acrylic acid hydroxyl ethyl ester/sodium acryloyldimethyl taurate copolymers are added made from step (3)
It in material, stirs evenly, homogeneous 3-5min；
(5) it is warming up to 80-85 DEG C, constant temperature emulsifies 25-40min under 500-1000r/min rotating speeds, adjusts rotating speed to 100-
500r/min, stirring are cooled to 40-50 DEG C；
(6) by 0.5-5 parts by weight 1,2- hexylene glycols are added in material made from step (5), are stirred with 100-500r/min rotating speeds
10-20min is cooled to room temperature；
(7) it examines, discharges, packaging obtains product.
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| CN114259433A (en) * | 2022-01-13 | 2022-04-01 | 湖北杰讯文化传媒有限公司 | Camellia skin-moistening oil and preparation method thereof |
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Application publication date: 20180724 |