CN107242982A - A kind of fair-skinned bright Virgin's milk liquid and preparation method thereof - Google Patents
A kind of fair-skinned bright Virgin's milk liquid and preparation method thereof Download PDFInfo
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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Abstract
The invention belongs to cosmetic technical field, and in particular to a kind of fair-skinned bright Virgin's milk liquid and preparation method thereof.The fair-skinned bright Virgin's milk liquid that the present invention is provided contains water, dimethyl silicone polymer, polyglycereol 10, glycerine, propane diols, caprylic/capric triglyceride, cetostearyl alcohol/cetearyl glucoside, the stearates of stearine/PEG 100, niacinamide, Laurocapram, Symwhite-337,3 O ethylascorbyls, thyme extract, tree peony whitening elite, Chinese gooseberry berry extract and tocopherol acetate.The fair-skinned bright Virgin's milk liquid system that the present invention is provided is stable, and easy osmotic absorption, effective moisturizing improves pigment deposition and dark and gloomy skin quality, makes whitening skin, and be applicable to the patient of skin injury.
Description
Technical field
The invention belongs to cosmetic technical field, and in particular to a kind of fair-skinned bright Virgin's milk liquid and preparation method thereof.
Background technology
In recent years with the raising of people's living standard and aesthetical standard, increasing people pursues, thirsts for pale and clean
The skin of profit.Therefore, with prevent the color spot as caused by sunray and other reasons, pigmentation whitening class make up
The research and development of product and skin-whitening preparation, are just being increasingly subject to various countries' cosmetic Manufacture business and the attention of researcher, whitening
Cosmetics turn into one of main flow kind of skin-care cosmetics.Find efficiently and human body is had no side effect or Small side effects U.S.
White nti-freckle product turns into a study hotspot of current pharmacy and cosmetic field.
The formation mechenism of melanin is that in melanocyte, tyrosine is in the presence of tyrosinase, by each in environment
The influence of the factor of kind, is gradually oxidized to DOPA, DOPA quinone, dopachrome, 5,6 dihydroindoles, indoles 5,6 quinones etc., final conversion
For pigment granule.The catalytic action of tyrosinase occurs mainly in tyrosine and changes into Dopa and Dopa turns in this course of reaction
Turn to Dopaquinone the two reaction in.
The effect of whitening product is mainly by suppressing tyrosinase activity or blocking the oxygen of tyrosine generation melanin
Change approach, so as to reduce the effect that melanin generation reaches skin whitening.Skin-whitening product is exactly to act on dermal melanin
In generation, metabolic process, suppress melanin generation and meet the material of specification, but traditional skin-whitening product, often use
Chemical substance, such as has the mercury salt of whitening effect and the quinhydrones of effect of dispelling spots.Although these compounds are rapidly achieved whitening
The effect of, but to skin toxic side effect, long-term use can cause contact dermatitis or cause the ill-effects such as permanent decolouring,
Many countries are disabled.The skin-whitening product currently required that should comply with two standards：One is had to tyrosinase activity
Higher inhibiting rate, can significantly reduce the generation of melanin；Two be to have higher security, nontoxic stingless with human body skin
Swash.Ursin, VitC derivatives and kojic acid are the whitening compositions more often used in skin-lightening cosmetic both at home and abroad at present.In order to develop
Meet the cosmetics of " going back to nature " requirement, particularly safe, the whitening product having no side effect, there is fine whitening to imitate for some
The natural plant composition of fruit is increasingly paid attention to by the green grass or young crops of consumer at present.Find exploitation efficiently and human body is had no side effect or secondary work
With small natural plants skin-whitening and speckle eliminating product as one of the current cosmetic field problem being relatively taken seriously.
Chinese patent application CN105640841A discloses a kind of anti-ageing freckle-removing mask liquid and preparation method thereof, it include with
Lower component：Water, glycerine, propane diols, ursin, polyglutamic acid sodium, cyclomethicone, dimethyl silicone polymer crosslinking are poly-
Compound, 3-O- ethylascorbyls, AVC, Bo Lashi mushroom extracts, sweet orange flower are carried
Take thing, pale flag extract, Herba Saussureae Involueratae extract, carbomer, triethanolamine, Sodium Hyaluronate, methyl hydroxybenzoate, Phenoxyethanol
And essence.The facial mask liquid has replenishing water and preserving moisture, desalinates color spot, whitening effect.
Chinese patent application CN106176347A discloses a kind of man and moistened maintenance elite breast, and the man moistens maintenance
Elite breast includes water, glycerine, propane diols, atoleine, cyclomethicone, ethylhexyl palmitate, poly dimethyl silicon
Oxygen alkane, cetostearyl alcohol, trehalose, mango extract, Fragaia ananassa Duchesne extract, ethoxy urea, C20-22 alcohol phosphate, C20-22
Alcohol, triethanolamine, PAA/sodium acryloyldimethyl taurate copolymers, isohexadecane, carbomer and emulsifying agent.The essence
Magnificent breast has moisturizing, repairs, effect of anti-aging.
Whitening is also a nursing engineering from inside to outside.The a set of suitable whitening product of oneself of selection is first had to, because
Whitening composition is different, so can so prevent difference with a series of product preferably using same brand in theory
Whitening composition conflicts mutually the adverse reaction of generation.Therefore, it is necessary to research and develop a kind of natural safety, moisturizing, moisturizing, whitening effect
Good whitening emulsion.
The content of the invention
In order to solve problems of the prior art, it is an object of the invention to provide the fair-skinned bright Virgin's milk liquid of one kind and its
Preparation method.The fair-skinned bright Virgin's milk liquid system that the present invention is provided is stable, easy osmotic absorption, effective moisturizing, improve pigment deposition and
Dark and gloomy skin quality, makes whitening skin, and be applicable to the patient of skin injury.
The invention provides the fair-skinned bright Virgin's milk liquid of one kind, including following components：
Dimethyl silicone polymer, Natrulon H-10, glycerine, propane diols, caprylic/capric triglyceride, cetostearyl alcohol/whale
Wax stearyl glucoside, stearine/PEG-100 stearates, niacinamide, Laurocapram, Symwhite-337,
3-O- ethylascorbyls, thyme extract, tree peony whitening elite, Chinese gooseberry berry extract, PAA/acryloyl
The dimethyltaurine sodium copolymer/smooth oleate/Polyoxyethylene Sorbitan Monooleate of isohexadecane/water/sorb, cetanol palmitate,
C20-22 alcohol phosphate/C20-22 alcohol, glycine betaine, allantoin, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymerization
Thing/saualane/smooth the isostearate of the sorb of polysorbate -60/, carbomer, triethanolamine, tocopherol acetate, sulfurous acid
Hydrogen sodium, Sodium Hyaluronate, CI 19140, methyl hydroxybenzoate, parahydroxyacet-ophenone, essence and water.Dimethyl silicone polymer CAS is
63148-62-9；Natrulon H-10 CAS is 9041-07-0；Cetearyl glucoside CAS is 246159-33-1；PEG-
100 stearates CAS are 9004-99-3；Thyme extract is purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd, article No. B-
658；Chinese gooseberry berry extract is purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd, article No. N-562；Acryloyldimethyl ox sulphur
Sour sodium copolymer CAS is 111286-86-3；Polyoxyethylene Sorbitan Monooleate CAS is 9005-65-6；C20-22 alcohol phosphate/
C20-22 alcohol is purchased from Guangzhou Run Pu Chemical Industry Science Co., Ltd；Glycine betaine CAS is 107-43-7；The CAS of polysorbate -60
Number be 9005-67-8；Carbomer CAS is 9007-20-9.
Further, described fair-skinned bright Virgin's milk liquid is made up of following components and its percentage by weight：
Dimethyl silicone polymer 2-4%, Natrulon H-10 2-4%, glycerine 2-4%, propane diols 2-4%, caprylic/capric are sweet
Three ester 1-3% of oil, cetostearyl alcohol/cetearyl glucoside 0.5-1.5%, stearine/PEG-100 stearates
0.5-1.5%, niacinamide 0.5-1.5%, Laurocapram 0.6-1.5%, Symwhite-337 0.5-1.4%, 3-O- second
Base ascorbic acid 0.5-1.4%, thyme extract 0.3-0.8%, tree peony whitening elite 0.3-0.8%, Chinese gooseberry fruit
Extract 0.01-0.03%, PAA/sodium acryloyldimethyl taurate copolymers/isohexadecane/smooth oleic acid of water/sorb
Ester/Polyoxyethylene Sorbitan Monooleate 0.4-0.8%, cetanol palmitate 0.4-0.7%, C20-22 alcohol phosphate/C20-22 alcohol 0.3-
0.7%th, glycine betaine 0.3-0.7%, allantoin 0.1-0.3%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymerization
The smooth isostearate 0.1-0.3% of thing/saualane/sorb of polysorbate -60/, carbomer 0.1-0.2%, triethanolamine
0.05-0.15%, tocopherol acetate 0.05-0.15%, sodium hydrogensulfite 0.06-0.14%, Sodium Hyaluronate 0.01-
0.03%th, CI 191400.025-0.03%, methyl hydroxybenzoate 0.12-0.18%, parahydroxyacet-ophenone 0.4-0.5%, essence
0.008-0.012% and water 69.678-86.867%.
Further, described fair-skinned bright Virgin's milk liquid is made up of following components and its percentage by weight：
Dimethyl silicone polymer 3%, Natrulon H-10 3%, glycerine 3%, propane diols 3%, caprylic/capric triglyceride
2%th, cetostearyl alcohol/cetearyl glucoside 1%, stearine/PEG-100 stearates 1%, niacinamide 1%,
Laurocapram 1%, Symwhite-337 1%, 3-O- ethylascorbyls 1%, thyme extract 0.6%, tree peony are beautiful
Bai Jinghua 0.5%, Chinese gooseberry berry extract 0.02%, PAA/sodium acryloyldimethyl taurate copolymers/different ten
Smooth oleate/the Polyoxyethylene Sorbitan Monooleate 0.6% of six alkane/water/sorb, cetanol palmitate 0.5%, C20-22 alcohol phosphate/
C20-22 alcohol 0.5%, glycine betaine 0.5%, allantoin 0.2%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymerization
The smooth isostearate 0.2% of thing/saualane/sorb of polysorbate -60/, carbomer 0.12%, triethanolamine 0.1%, fertility
Phenol acetic acid esters 0.1%, sodium hydrogensulfite 0.1%, Sodium Hyaluronate 0.02%, CI 191400.028%, methyl hydroxybenzoate
0.15%th, parahydroxyacet-ophenone 0.4%, essence 0.01% and water 75.352%.
Competitive inhibition of the Symwhite-337 to tyrosinase can prevent the generation of melanin；Meanwhile,
Symwhite-337 has stronger antioxidation activity, is conducive to the regression of melanin, improves colour of skin inequality, and reduction skin
Color.
Described 3-O- ethylascorbyls are synthesized using the production technology (one-step synthesis) for possessing national patent
High-purity vitamin C derivative.Vc is got the nod with its efficient whitening function and high security, but itself is easily oxidized, no
Easily really absorbed by skin, skin availability is low.For Vc, 3-O- ethylascorbyls readily penetrate through cuticula and entered
Enter skin corium, into skin after by biology enzyme decompose play VC effect, improve VC availability.It can suppress tyrosinase
Activity, suppress melanin formation, reduction melanin be colourless, efficient skin whitening.3-O- ethylascorbyls enter true
Skin Cell activity is repaired in the synthesis that collagen is directly participated in after cortex, is collagen increase, so that skin becomes to fill
It is full of high resilience, makes skin moist.There is the antioxidant effect of brilliance in cosmetics, it is ensured that VC availability, with respect to VC
For, 3-O- ethylascorbyls are highly stable, and nondiscolouring, are really achieved whitening spot-removing, the effect of potent antibacterial anti-inflammatory, energy
Inflammation caused by antisum.
Described thyme extract can prevent " step " of melanin, be a kind of brand-new whitening raw material, for brand-new
Lightening mechanism.Due to the environmental stimuli of ultraviolet etc., substantial amounts of melanin can be produced in melanocyte.These melanin
Epidermal cell can be transported to by " porter ".In environmental stimuli duration, can constantly it be produced newly in melanocyte
Melanin, then epidermal cell is arrived by " carrying ".If if " porter " disappears, it is thin that melanin will be stuck in melanin
Intracellular.When melanin savings arrives a certain amount, melanocyte would not produce melanin again.The melanin that savings gets up also can
It is digested.There is a kind of driving albumen in melanocyte, they are that melanin is carried into epidermal cell " porter ".
The tree peony whitening elite contains the different flavones ingredient of kind more than 20：Anthocyanidin, flavonols, flavones, resin, fat
Fat acid and sterol, the ability with high anti-oxidation activity and anti-inflammatory, can suppress the effect of tyrosinase, so as to suppress melanin
Horn cell is transferred to, so as to reduce Skin pigmentation, profit is highlighted in vain from inside to outside, makes skin become clear pure and fresh.Tree peony whitening
Elite is purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd, article No. S-636.
The Chinese gooseberry berry extract, is referred to as the king of Vc, can effectively reduce the pigment of pitch-dark skin quality, and deep layer is extensive
Moisten white skin texture again, meanwhile, promote the synthesis of collagen, make skin water moisten bullet and slide.
Meanwhile, present invention provides a kind of preparation method of fair-skinned bright Virgin's milk liquid, comprise the following steps：
S1, by cetostearyl alcohol/cetearyl glucoside, stearine/PEG-100 stearates, cetanol
Palmitate, C20-22 alcohol phosphate/C20-22 alcohol, tocopherol acetate, caprylic/capric triglyceride, polydimethylsiloxanes
Alkane, methyl hydroxybenzoate are added in oil phase pot, are heated with stirring to 75-85 DEG C, are completely dissolved, obtain material A；
S2, carbomer, water with hanging homogenizer homogeneous, to being uniformly dispersed, obtained into material B；
S3, step S2 resulting materials B and water, Sodium Hyaluronate, Natrulon H-10, glycerine, glycine betaine, allantoin added
In main cooker, 80-90 DEG C is heated with stirring to, heating and thermal insulation 10-20 minutes obtains material C；
S4, unlatching homogeneous, step S1 resulting materials are added in step S3 resulting materials C, while adding acrylic acid hydroxyl
Ethyl ester/sodium acryloyldimethyl taurate copolymers/saualane/smooth the isostearate of the sorb of polysorbate -60/, three ethanol
Amine, the PAA/sodium acryloyldimethyl taurate copolymers/smooth oleate/polysorbate of isohexadecane/water/sorb,
To emulsifying uniformly, insulation stirs cooling to matter after 5-15 minutes, is down to 50-60 DEG C, obtains material D within 5-8 minutes；
S5, step S4 resulting materials D added into pre- solvent water, parahydroxyacet-ophenone and essence, phenethyl isophthalic two
Phenol, niacinamide, Chinese gooseberry berry extract, 3-O- ethylascorbyls, Laurocapram, sodium hydrogensulfite, thyme are carried
Thing, tree peony whitening elite, CI 19140 are taken, is stirred until homogeneous, obtains material E；
S6, step S5 resulting materials E is down to normal temperature, sampling inspection is qualified to discharge again, produces.
Wherein, CI 19140 is lemon yellow (yellow 4), is purchased from this trade Co., Ltd of Qingdao Shanks.
Further, heating-up temperature is 80 DEG C in the step S1.
Further, heating-up temperature is 85 DEG C in the step S3, and the heating and thermal insulation time is 15 minutes.
Further, soaking time is 10 minutes in the step S4, is cooled to 55 DEG C.
In the fair-skinned bright Virgin's milk liquid of the present invention containing Symwhite-337,3-O- ethylascorbyls, thyme extract,
A variety of small molecules and the active skull cap components such as tree peony whitening elite, Chinese gooseberry berry extract, can effectively penetrate cuticula,
Moisturizing is preferably played, wrinkle, anti-aging effect are gone in whitening.
Compared with prior art, the present invention has the advantage that：
(1) the fair-skinned bright Virgin's milk liquid system that the present invention is provided is stable, easy osmotic absorption, effective replenishing water and preserving moisture, Kohakuhi,
Improve obscure, repair skin, delay skin aging makes skin distribute charming brilliance from inside to outside, and water is tender glossy, pale crystal-clear bright；
(2) the fair-skinned bright Virgin's milk liquid that the present invention is provided has bacteriostasis, it is adaptable to which the patient that skin has damage uses,
Skin injury will not be aggravated；
(3) the fair-skinned bright Virgin's milk liquid safety and stability that the present invention is provided, good penetrability easily absorbs, salubrious not using rear skin
It is sticky；And the preparation method of the fair-skinned bright Virgin's milk liquid of the present invention is simple, condition is controllable, process stabilizing, can be applicable.
Embodiment
Below by specific embodiment, the present invention will be further described, and these embodiments are served only for the purpose of illustration, and
Do not limit the scope of the invention.
A kind of fair-skinned bright Virgin's milk liquid of embodiment 1
The fair-skinned bright Virgin's milk liquid is made up of following components and its percentage by weight：
Dimethyl silicone polymer 2%, Natrulon H-10 2%, glycerine 2%, propane diols 2%, caprylic/capric triglyceride
1%th, cetostearyl alcohol/cetearyl glucoside 0.5%, stearine/PEG-100 stearates 0.5%, niacinamide
0.5%th, Laurocapram 0.6%, Symwhite-337 0.5%, 3-O- ethylascorbyls 0.5%, thyme extract
0.3%th, tree peony whitening elite 0.3%, Chinese gooseberry berry extract 0.01%, PAA/acryloyldimethyl taurine
Sodium copolymer/smooth oleate/the Polyoxyethylene Sorbitan Monooleate 0.4% of isohexadecane/water/sorb, cetanol palmitate 0.4%, C20-
22 alcohol phosphates/C20-22 alcohol 0.3%, glycine betaine 0.3%, allantoin 0.1%, hydroxy-ethyl acrylate/acryloyldimethyl ox
The smooth isostearate 0.1% of sodium sulfonate copolymers/saualane/sorb of polysorbate -60/, carbomer 0.1%, triethanolamine
0.05%th, tocopherol acetate 0.05%, sodium hydrogensulfite 0.06%, Sodium Hyaluronate 0.01%, CI 191400.025%,
Methyl hydroxybenzoate 0.12%, parahydroxyacet-ophenone 0.4%, essence 0.008% and water 86.867%.
Preparation method：
S1, by cetostearyl alcohol/cetearyl glucoside, stearine/PEG-100 stearates, cetanol
Palmitate, C20-22 alcohol phosphate/C20-22 alcohol, tocopherol acetate, caprylic/capric triglyceride, polydimethylsiloxanes
Alkane, methyl hydroxybenzoate are added in oil phase pot, are heated with stirring to 80 DEG C, are completely dissolved, obtain material A；
S2, carbomer, water with hanging homogenizer homogeneous, to being uniformly dispersed, obtained into material B；
S3, step S2 resulting materials B and water, Sodium Hyaluronate, Natrulon H-10, glycerine, glycine betaine, allantoin added
In main cooker, 85 DEG C are heated with stirring to, heating and thermal insulation 15 minutes obtains material C；
S4, unlatching homogeneous, step S1 resulting materials A is added in step S3 resulting materials C, while adding acrylic acid hydroxyl
Ethyl ester/sodium acryloyldimethyl taurate copolymers/saualane/smooth the isostearate of the sorb of polysorbate -60/, three ethanol
Amine, the PAA/sodium acryloyldimethyl taurate copolymers/smooth oleate/polysorbate of isohexadecane/water/sorb,
To emulsifying uniformly, insulation stirs cooling to matter after 10 minutes, is down to 55 DEG C, obtains material D within 6 minutes；
S5, step S4 resulting materials D added into pre- solvent water, parahydroxyacet-ophenone and essence, phenethyl isophthalic two
Phenol, niacinamide, Chinese gooseberry berry extract, 3-O- ethylascorbyls, Laurocapram, sodium hydrogensulfite, thyme are carried
Thing, tree peony whitening elite, CI 19140 are taken, is stirred until homogeneous, obtains material E；
S6, step S5 resulting materials E is down to normal temperature, sampling inspection is qualified to discharge again, produces.
A kind of fair-skinned bright Virgin's milk liquid of embodiment 2
The fair-skinned bright Virgin's milk liquid is made up of following components and its percentage by weight：
Dimethyl silicone polymer 3%, Natrulon H-10 3%, glycerine 3%, propane diols 3%, caprylic/capric triglyceride
2%th, cetostearyl alcohol/cetearyl glucoside 1%, stearine/PEG-100 stearates 1%, niacinamide 1%,
Laurocapram 1%, Symwhite-337 1%, 3-O- ethylascorbyls 1%, thyme extract 0.6%, tree peony are beautiful
Bai Jinghua 0.5%, Chinese gooseberry berry extract 0.02%, PAA/sodium acryloyldimethyl taurate copolymers/different ten
Smooth oleate/the Polyoxyethylene Sorbitan Monooleate 0.6% of six alkane/water/sorb, cetanol palmitate 0.5%, C20-22 alcohol phosphate/
C20-22 alcohol 0.5%, glycine betaine 0.5%, allantoin 0.2%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymerization
The smooth isostearate 0.2% of thing/saualane/sorb of polysorbate -60/, carbomer 0.12%, triethanolamine 0.1%, fertility
Phenol acetic acid esters 0.1%, sodium hydrogensulfite 0.1%, Sodium Hyaluronate 0.02%, CI 191400.028%, methyl hydroxybenzoate
0.15%th, parahydroxyacet-ophenone 0.4%, essence 0.01% and water 75.352%.
Preparation method is similar to Example 1.
A kind of fair-skinned bright Virgin's milk liquid of embodiment 3
The fair-skinned bright Virgin's milk liquid is made up of following components and its percentage by weight：
Dimethyl silicone polymer 4%, Natrulon H-10 4%, glycerine 4%, propane diols 4%, caprylic/capric triglyceride
3%th, cetostearyl alcohol/cetearyl glucoside 1.5%, stearine/PEG-100 stearates 1.5%, niacinamide
1.5%th, Laurocapram 1.5%, Symwhite-337 1.4%, 3-O- ethylascorbyls 1.4%, thyme extract
0.8%th, tree peony whitening elite 0.8%, Chinese gooseberry berry extract 0.03%, PAA/acryloyldimethyl taurine
Sodium copolymer/smooth oleate/the Polyoxyethylene Sorbitan Monooleate 0.8% of isohexadecane/water/sorb, cetanol palmitate 0.7%, C20-
22 alcohol phosphates/C20-22 alcohol 0.7%, glycine betaine 0.7%, allantoin 0.3%, hydroxy-ethyl acrylate/acryloyldimethyl ox
The smooth isostearate 0.3% of sodium sulfonate copolymers/saualane/sorb of polysorbate -60/, carbomer 0.2%, triethanolamine
0.15%th, tocopherol acetate 0.15%, sodium hydrogensulfite 0.14%, Sodium Hyaluronate 0.03%, CI 191400.03%, hydroxyl
Benzene methyl 0.18%, parahydroxyacet-ophenone 0.5%, essence 0.012% and water 69.678%.
Preparation method is similar to Example 1.
A kind of fair-skinned bright Virgin's milk liquid of comparative example 1
The fair-skinned bright Virgin's milk liquid is made up of following components and its percentage by weight：
Dimethyl silicone polymer 3%, Natrulon H-10 3%, glycerine 3%, propane diols 3%, caprylic/capric triglyceride
2%th, cetostearyl alcohol/cetearyl glucoside 1%, stearine/PEG-100 stearates 1%, niacinamide 1%,
Laurocapram 1%, Symwhite-337 1%, 3-O- ethylascorbyls 1%, dulse elite 0.6%, tree peony whitening
Elite 0.5%, Chinese gooseberry berry extract 0.02%, PAA/sodium acryloyldimethyl taurate copolymers/different 16
Smooth oleate/the Polyoxyethylene Sorbitan Monooleate 0.6% of alkane/water/sorb, cetanol palmitate 0.5%, C20-22 alcohol phosphate/C20-
22 alcohol 0.5%, glycine betaine 0.5%, allantoin 0.2%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers/angle
The smooth isostearate 0.2% of shark alkane/sorb of polysorbate -60/, carbomer 0.12%, triethanolamine 0.1%, tocopherol second
It is acid esters 0.1%, sodium hydrogensulfite 0.1%, Sodium Hyaluronate 0.02%, CI 191400.028%, methyl hydroxybenzoate 0.15%, right
Hydroxy acetophenone 0.4%, essence 0.01% and water 75.352%.
Preparation method is similar to Example 1.
Difference with embodiment 2 is, thyme extract is replaced with into dulse elite.
A kind of fair-skinned bright Virgin's milk liquid of comparative example 2
The fair-skinned bright Virgin's milk liquid is made up of following components and its percentage by weight：
Dimethyl silicone polymer 3%, Natrulon H-10 3%, glycerine 3%, propane diols 3%, caprylic/capric triglyceride
2%th, cetostearyl alcohol/cetearyl glucoside 1%, stearine/PEG-100 stearates 1%, niacinamide 1%,
Laurocapram 1%, Symwhite-337 1%, 3-O- ethylascorbyls 1%, thyme extract 0.6%, radix glycyrrhizae carry
Take thing 0.5%, Chinese gooseberry berry extract 0.02%, PAA/sodium acryloyldimethyl taurate copolymers/different 16
Smooth oleate/the Polyoxyethylene Sorbitan Monooleate 0.6% of alkane/water/sorb, cetanol palmitate 0.5%, C20-22 alcohol phosphate/C20-
22 alcohol 0.5%, glycine betaine 0.5%, allantoin 0.2%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers/angle
The smooth isostearate 0.2% of shark alkane/sorb of polysorbate -60/, carbomer 0.12%, triethanolamine 0.1%, tocopherol second
It is acid esters 0.1%, sodium hydrogensulfite 0.1%, Sodium Hyaluronate 0.02%, CI 191400.028%, methyl hydroxybenzoate 0.15%, right
Hydroxy acetophenone 0.4%, essence 0.01% and water 75.352%.
Preparation method is similar to Example 1.
Difference with embodiment 2 is, tree peony whitening elite is replaced with into licorice.
A kind of fair-skinned bright Virgin's milk liquid of comparative example 3
The fair-skinned bright Virgin's milk liquid is made up of following components and its percentage by weight：
Dimethyl silicone polymer 3%, Natrulon H-10 3%, glycerine 3%, propane diols 3%, caprylic/capric triglyceride
2%th, cetostearyl alcohol/cetearyl glucoside 1%, stearine/PEG-100 stearates 1%, niacinamide 1%,
Laurocapram 1%, Symwhite-337 1%, 3-O- ethylascorbyls 1%, thyme extract 0.6%, tree peony are beautiful
Bai Jinghua 0.5%, Chinese gooseberry berry extract 0.02%, PAA/sodium acryloyldimethyl taurate copolymers/different ten
Smooth oleate/the Polyoxyethylene Sorbitan Monooleate 0.6% of six alkane/water/sorb, cetanol palmitate 0.5%, glycine betaine 0.5%, allantois
Element 0.2%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers/saualane/sorb of polysorbate -60/ are smooth different
Stearate 0.2%, carbomer 0.12%, triethanolamine 0.1%, tocopherol acetate 0.1%, sodium hydrogensulfite 0.1%, thoroughly
The sour sodium 0.02% of bright matter, CI 191400.028%, methyl hydroxybenzoate 0.15%, parahydroxyacet-ophenone 0.4%, the and of essence 0.01%
Water 75.852%.
Preparation method is similar to Example 1.
Difference with embodiment 2 is, is not added with C20-22 alcohol phosphate/C20-22 alcohol, adds the consumption of water.
Test example one, safety evaluatio
1. test material：Fair-skinned bright Virgin's milk liquid prepared by embodiment 1-3.
2. subjects：60 people, women, 25-50 Sui, skin health, no skin disease allergies.
3. test method：
1) subject is randomly divided into 3 groups, every group of 20 people are denoted as embodiment 1-3 groups；
2) from qualified spot examination device, with closed patch experiment method, by tested material, (prepared by embodiment 1-3 fair-skinned
Brilliant white emulsion) about 0.2-0.3mL drops in spot examination device in, external application special adhesive tape be covered on after subject back, 24h remove it is tested
Thing, respectively remove after 0.5,6,12,24,48h observation dermoreaction, according to《Cosmetics health specification》Middle dermoreaction classification mark
Standard records its result.
4 result of the tests：
As a result show, after the fair-skinned bright Virgin's milk liquid that each group subject is prepared using embodiment 1-3,0.5,6,12,24,
48h observes dermoreaction, and skin has no adverse reaction, and illustrates that fair-skinned bright Virgin's milk liquid prepared by the present invention is safe and non-stimulating.
Test example two, whitening effect evaluation
1. test material：Fair-skinned bright Virgin's milk liquid prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：180 people, women, 22-50 Sui, skin is dim, no skin disease allergies.
3. test method：
1) subject is randomly divided into 6 groups, every group of 30 people are denoted as embodiment 1-3 groups and comparative example 1-3 groups；
2) the fair-skinned bright Virgin's milk liquid respectively prepared sooner or later using an embodiment 1-3 and comparative example 1-3 daily, continuously using 3
Individual month, the melanin content (choosing at facial same spot position is tested using German CK companies dermal melanin test probe MX18
Take cheek cheekbone peak position), average.
4. result of the test：Melanin content test result is shown in Table 1.
The melanin content of table 1 changes
| Melanin content | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Before use | 504 | 554 | 525 | 532 | 496 | 516 |
| After use | 308 | 337 | 324 | 367 | 322 | 334 |
| Changing value | 196 | 217 | 201 | 165 | 174 | 182 |
Known by table 1, fair-skinned bright Virgin's milk liquid whitening effect prepared by the present invention is preferable.Compared with comparative example 1-3, the present invention is real
Apply a fair-skinned bright Virgin's milk liquid of 1-3 preparations more apparent using melanin content minimizing effect after 3 months, illustrate that compatibility of the present invention is closed
Reason, science, each component interacts plays the effect of whitening jointly.
Test example three, moisturizing effect assessment
1. test material：Fair-skinned bright Virgin's milk liquid prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：180 people, women, 22-50 Sui, skin health, no skin disease allergies.
3. test method：
1) subject is randomly divided into 6 groups, every group of 30 people are denoted as embodiment 1-3 groups and comparative example 1-3 groups；
2) after subject's clear water washes one's face, using Fes Kai Er SK-III skin moistures detectors test respectively forehead, left face,
The moisture of right face and chin skin, and arithmetic mean of instantaneous value is taken, subject reuses above-mentioned elite breast, is uniformly applied to face
Portion, is gently massaged into the skin for testing forehead, left face, right face and chin same location after absorption, 24h with skin moisture tester
Moisture, and take arithmetic mean of instantaneous value.
4. result of the test：Moisture test result is shown in Table 2.
The moisture result of table 2
Known by table 2, fair-skinned bright Virgin's milk liquid replenishing water and preserving moisture effect prepared by the present invention is preferable.Compared with comparative example 1-3, this hair
Fair-skinned bright Virgin's milk liquid prepared by bright embodiment 1-3 increases more apparent using rear water content, illustrate that compatibility of the present invention is reasonable, science,
Each component interacts plays the effect of moisturizing jointly.
Test example four, fungistatic effect evaluation
1. test material：Fair-skinned bright Virgin's milk liquid prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：Micrococcus scarlatinae, propionibacterium acnes, MRSE, staphylococcus aureus.
3. test method：
1) experiment bacteria suspension is prepared
Concentration is：With 100 μ L drops on to photo, it is 1 × 10 to reclaim clump count4-1×109Cfu/ pieces.
2) microbiological contamination print is prepared
Above-mentioned bacteria suspension is taken, 100 μ L is added dropwise in coupons and control print each respectively, acts on 20min.
3) print is put into the test tube of the phosphate buffer solution containing 5mL respectively, fully mixed, diluted 2-3 dilution factor, take
0.5mL is placed in plate, is poured into 40-50 DEG C of nutrient agar (bacterium) 15mL, rotates plate, it is fully mixed
It is even, flat board is overturn after agar solidification, culture is inverted, 37 DEG C, cultivates 48h.4) bacteriostasis rate is calculated, formula is as follows：
Wherein, X- bacteriostasis rates, %；A- compares print average colony number；B- is by coupons average colony number.
4. result of the test：Bacteriostasis rate the results are shown in Table 3.
The bacteriostasis rate result of table 3
Known by table 3, fair-skinned bright Virgin's milk liquid prepared by the present invention has preferable bacteriostasis, it is adaptable to which skin has damage
Patient, will not cause the further damage of skin.Compared with comparative example 1-3, fair-skinned bright Virgin's milk liquid prepared by the present invention is to suppurating
Property streptococcus, propionibacterium acnes, MRSE, staphylococcus aureus has good inhibiting effect, illustrates this hair
The fair-skinned bright Virgin's milk liquid of bright preparation can suppress small pox and the effectively impaired skin of protection.
Test example five, freckle effect evaluation
1. test material：Fair-skinned bright Virgin's milk liquid prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：300, female, 30-50 Sui, with chloasma.
3. test method：
Subject is randomly divided into 6 groups, every group 50, respectively embodiment 1-3 and comparative example 1-3 groups；Subject cleans
After face, face is applied to, twice daily, is used sooner or later, it is continuous to use 2 months.
Evaluation criterion：
Recovery from illness：Naked eyes regard color spot area regression ＞ 90%, and color disappears substantially；
It is effective：Naked eyes regard color spot area regression ＞ 60%, and color is substantially thin out；
Take a turn for the better：Naked eyes regard color spot area regression ＞ 30%, and color disappears substantially；
It is invalid：Naked eyes regard color spot area regression ＜ 30%, and color change is not obvious；
Obvious effective rate=(recovery from illness number of cases+effective number of cases)/total number of cases × 100%；
Total effective rate=(recovery from illness number of cases+effective number of cases+improvement number of cases)/total number of cases × 100%.
4. result of the test：Fair-skinned bright Virgin's milk liquid freckle effect evaluation result is shown in Table 4.
The freckle effect evaluation result of table 4
| Group | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Subject/example | 50 | 50 | 50 | 50 | 50 | 50 |
| Recovery from illness/example | 32 | 36 | 33 | 24 | 23 | 25 |
| Effective/example | 12 | 12 | 13 | 6 | 5 | 8 |
| Improvement/example | 3 | 1 | 2 | 11 | 10 | 9 |
| Invalid/example | 3 | 1 | 2 | 9 | 12 | 8 |
| Obvious effective rate/% | 88 | 96 | 92 | 60 | 56 | 66 |
| Total effective rate/% | 94 | 98 | 96 | 82 | 76 | 84 |
As shown in Table 4, the freckle effect of fair-skinned bright Virgin's milk liquid prepared by the present invention is preferable.Compared with comparative example 1-3 groups, this
The nti-freckle total effective rate of fair-skinned bright Virgin's milk liquid prepared by inventive embodiments 1-3 is up to more than 94%, illustrates that the present invention can be effective
Elimination color spot, go back skin fair-skinned bright white.
Test example six, sensory evaluation
1. test material：Fair-skinned bright Virgin's milk liquid prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：120 people, women, 22-50 Sui, skin health, no skin disease allergies.
3. test method：
Subject is randomly divided into 6 groups, every group of 20 people are denoted as embodiment 1-3 and comparative example 1-3 groups.Each group is used respectively
Fair-skinned bright Virgin's milk liquid prepared by embodiment 1-3 and comparative example 1-3, is used for situation daily once in the morning and once at night, after January and beats
Divide and evaluate.Standards of grading：Using ten point system, 10 points best, and 0 point worst, and fraction more high effect is better.
4. result of the test：Analyses Methods for Sensory Evaluation Results is shown in Table 5.
The Analyses Methods for Sensory Evaluation Results of table 5
Known by table 5, fair-skinned bright Virgin's milk liquid prepared by the present invention has preferable moistness, salubrious property, absorbability.With implementation
Example 1-3 contrasts, the effect that the present invention is strength 1-3 is preferable, illustrates the reasonable science of compatibility of the present invention, each component interaction collaboration
Play a part of moist, salubrious, good absorbing, and subject does not occur allergic phenomena.
Claims (7)
1. a kind of fair-skinned bright Virgin's milk liquid, it is characterised in that including following components：
Dimethyl silicone polymer, Natrulon H-10, glycerine, propane diols, caprylic/capric triglyceride, cetostearyl alcohol/spermaceti are hard
Aliphatic radical glucoside, stearine/PEG-100 stearates, niacinamide, Laurocapram, Symwhite-337,3-O-
Ethylascorbyl, thyme extract, tree peony whitening elite, Chinese gooseberry berry extract, PAA/acryloyl diformazan
Base Taurate Copolymer/smooth oleate/the Polyoxyethylene Sorbitan Monooleate of isohexadecane/water/sorb, cetanol palmitate, C20-22
Alcohol phosphate/C20-22 alcohol, glycine betaine, allantoin, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers/spiny dogfish
Alkane/smooth the isostearate of the sorb of polysorbate -60/, carbomer, triethanolamine, tocopherol acetate, sodium hydrogensulfite, thoroughly
The sour sodium of bright matter, CI 19140, methyl hydroxybenzoate, parahydroxyacet-ophenone, essence and water.
2. fair-skinned bright Virgin's milk liquid as claimed in claim 1, it is characterised in that be made up of following components and its percentage by weight：
Dimethyl silicone polymer 2-4%, Natrulon H-10 2-4%, glycerine 2-4%, propane diols 2-4%, caprylic/capric glycerine three
Ester 1-3%, cetostearyl alcohol/cetearyl glucoside 0.5-1.5%, stearine/PEG-100 stearates 0.5-
1.5%th, niacinamide 0.5-1.5%, Laurocapram 0.6-1.5%, Symwhite-337 0.5-1.4%, 3-O- ethyl resist
Bad hematic acid 0.5-1.4%, thyme extract 0.3-0.8%, tree peony whitening elite 0.3-0.8%, Chinese gooseberry fruit are extracted
Thing 0.01-0.03%, PAA/sodium acryloyldimethyl taurate copolymers/isohexadecane/smooth oleate of water/sorb/poly-
Sorbitol ester -800.4-0.8%, cetanol palmitate 0.4-0.7%, C20-22 alcohol phosphate/C20-22 alcohol 0.3-
0.7%th, glycine betaine 0.3-0.7%, allantoin 0.1-0.3%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymerization
The smooth isostearate 0.1-0.3% of thing/saualane/sorb of polysorbate -60/, carbomer 0.1-0.2%, triethanolamine
0.05-0.15%, tocopherol acetate 0.05-0.15%, sodium hydrogensulfite 0.06-0.14%, Sodium Hyaluronate 0.01-
0.03%th, CI 191400.025-0.03%, methyl hydroxybenzoate 0.12-0.18%, parahydroxyacet-ophenone 0.4-0.5%, essence
0.008-0.012% and water 69.678-86.867%.
3. fair-skinned bright Virgin's milk liquid as claimed in claim 2, it is characterised in that be made up of following components and its percentage by weight：
Dimethyl silicone polymer 3%, Natrulon H-10 3%, glycerine 3%, propane diols 3%, caprylic/capric triglyceride 2%, whale
Wax stearyl alcohol/cetearyl glucoside 1%, stearine/PEG-100 stearates 1%, niacinamide 1%, bay nitrogen
Tall and erect ketone 1%, Symwhite-337 1%, 3-O- ethylascorbyls 1%, thyme extract 0.6%, tree peony whitening elite
0.5%th, Chinese gooseberry berry extract 0.02%, PAA/sodium acryloyldimethyl taurate copolymers/isohexadecane/
Smooth oleate/the Polyoxyethylene Sorbitan Monooleate 0.6% of water/sorb, cetanol palmitate 0.5%, C20-22 alcohol phosphate/C20-22
Alcohol 0.5%, glycine betaine 0.5%, allantoin 0.2%, hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers/spiny dogfish
The smooth isostearate 0.2% of alkane/sorb of polysorbate -60/, carbomer 0.12%, triethanolamine 0.1%, tocopheryl acetate
Ester 0.1%, sodium hydrogensulfite 0.1%, Sodium Hyaluronate 0.02%, CI 191400.028%, methyl hydroxybenzoate 0.15%, to hydroxyl
Benzoylformaldoxime 0.4%, essence 0.01% and water 75.352%.
4. the preparation method of the fair-skinned bright Virgin's milk liquid as described in claim 1-3 is any, it is characterised in that comprise the following steps：
S1, by cetostearyl alcohol/cetearyl glucoside, stearine/PEG-100 stearates, cetanol palm
Acid esters, C20-22 alcohol phosphate/C20-22 alcohol, tocopherol acetate, caprylic/capric triglyceride, dimethyl silicone polymer, hydroxyl
Benzene methyl is added in oil phase pot, is heated with stirring to 75-85 DEG C, is completely dissolved, obtains material A；
S2, carbomer, water with hanging homogenizer homogeneous, to being uniformly dispersed, obtained into material B；
S3, step S2 resulting materials B and water, Sodium Hyaluronate, Natrulon H-10, glycerine, glycine betaine, allantoin added into main cooker
In, 80-90 DEG C is heated with stirring to, heating and thermal insulation 10-20 minutes obtains material C；
S4, unlatching homogeneous, step S1 resulting materials A is added in step S3 resulting materials C, while adding acrylic acid hydroxyl second
Ester/sodium acryloyldimethyl taurate copolymers/saualane/smooth the isostearate of the sorb of polysorbate -60/, triethanolamine,
PAA/sodium acryloyldimethyl taurate copolymers/smooth oleate/polysorbate of isohexadecane/water/sorb, homogeneous
5-8 minutes uniform to emulsifying, and insulation stirs cooling after 5-15 minutes, is down to 50-60 DEG C, obtains material D；
S5, step S4 resulting materials D added into pre- solvent water, parahydroxyacet-ophenone and essence, Symwhite-337, cigarette
Acid amides, Chinese gooseberry berry extract, 3-O- ethylascorbyls, Laurocapram, sodium hydrogensulfite, thyme extract,
Tree peony whitening elite, CI 19140, are stirred until homogeneous, and obtain material E；
S6, step S5 resulting materials E is down to normal temperature, sampling inspection is qualified to discharge again, produces.
5. the preparation method of fair-skinned bright Virgin's milk liquid as claimed in claim 4, it is characterised in that heating-up temperature in the step S1
For 80 DEG C.
6. the preparation method of fair-skinned bright Virgin's milk liquid as claimed in claim 4, it is characterised in that heating-up temperature in the step S3
For 85 DEG C, the heating and thermal insulation time is 15 minutes.
7. the preparation method of fair-skinned bright Virgin's milk liquid as claimed in claim 4, it is characterised in that soaking time in the step S4
For 10 minutes, 55 DEG C are cooled to.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0283309A (en) * | 1988-09-19 | 1990-03-23 | Kanebo Ltd | Creamy or milky lotion-like water-on-oil type emulsified cosmetic |
| CN106176566A (en) * | 2016-08-23 | 2016-12-07 | 上海新高姿化妆品有限公司 | Cosmetic composition with white-skinned face function and preparation method thereof |
| CN106265121A (en) * | 2016-10-08 | 2017-01-04 | 广州丹奇日用化工厂有限公司 | Leaf mustard polypeptide repairs the application in cosmetics in preparation whitening |
| CN106420445A (en) * | 2016-09-19 | 2017-02-22 | 广东丸美生物技术股份有限公司 | Skin care matrix with moisture preserving and oxidation resisting effects as well as preparation method and application of skin care matrix |
| CN106726769A (en) * | 2016-12-27 | 2017-05-31 | 广州赛莱拉干细胞科技股份有限公司 | A kind of peony seed oil anti-apolexis composition and preparation method thereof |
-
2017
- 2017-06-07 CN CN201710425317.3A patent/CN107242982B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0283309A (en) * | 1988-09-19 | 1990-03-23 | Kanebo Ltd | Creamy or milky lotion-like water-on-oil type emulsified cosmetic |
| CN106176566A (en) * | 2016-08-23 | 2016-12-07 | 上海新高姿化妆品有限公司 | Cosmetic composition with white-skinned face function and preparation method thereof |
| CN106420445A (en) * | 2016-09-19 | 2017-02-22 | 广东丸美生物技术股份有限公司 | Skin care matrix with moisture preserving and oxidation resisting effects as well as preparation method and application of skin care matrix |
| CN106265121A (en) * | 2016-10-08 | 2017-01-04 | 广州丹奇日用化工厂有限公司 | Leaf mustard polypeptide repairs the application in cosmetics in preparation whitening |
| CN106726769A (en) * | 2016-12-27 | 2017-05-31 | 广州赛莱拉干细胞科技股份有限公司 | A kind of peony seed oil anti-apolexis composition and preparation method thereof |
Cited By (13)
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|---|---|---|---|---|
| CN107496190A (en) * | 2017-10-15 | 2017-12-22 | 广州汀兰生物科技有限公司 | A kind of whitening spot-eliminating composition and its application |
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| CN108245458A (en) * | 2018-03-28 | 2018-07-06 | 广州科玛大健康产业有限公司 | It is a kind of to repair tender skin lotion and preparation method thereof |
| CN110840771A (en) * | 2018-08-20 | 2020-02-28 | 天津美臣生物科技有限公司 | Skin-refreshing essence milk |
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| CN110123678A (en) * | 2019-06-25 | 2019-08-16 | 深圳市仙迪化妆品有限公司 | Cosmetic composition and preparation method thereof containing Chilean rose hip oil |
| CN110680769A (en) * | 2019-10-25 | 2020-01-14 | 张赞红 | Whitening essence of neroli extracting solution and preparation method thereof |
| CN111067838A (en) * | 2020-01-15 | 2020-04-28 | 广州市逸轩精细化工有限公司 | Whitening and freckle-removing composition, whitening and freckle-removing cream and preparation method thereof |
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