CN107213062A - A kind of fair-skinned bright white mildy wash and preparation method thereof - Google Patents
A kind of fair-skinned bright white mildy wash and preparation method thereof Download PDFInfo
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- CN107213062A CN107213062A CN201710424002.7A CN201710424002A CN107213062A CN 107213062 A CN107213062 A CN 107213062A CN 201710424002 A CN201710424002 A CN 201710424002A CN 107213062 A CN107213062 A CN 107213062A
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Abstract
The invention belongs to cosmetic technical field, and in particular to a kind of fair-skinned bright white mildy wash and preparation method thereof.The fair-skinned bright white mildy wash that the present invention is provided includes following components：Laruyl alcohol sulfosuccinate disodium, methyl lauroyl sodium taurocholate, lauroylamidopropyl betaine, laureth sodium sulfovinate, sodium chloride, coconut oleoyl amine, acrylic acid (ester) analog copolymer, the esters of caprylic/capric glyceride type polyglycereol 10, glycine betaine, Laurocapram, 3 O ethylascorbyls, ursin, tree peony whitening elite, thyme extract, Brittany Asia pearl algae, the methyl dioleates of PEG 120, two (hydrogenated-tallow group) phthalic acid amides, panthenol, niacinamide, tranexamic acid, DMDMH, essence and water.The fair-skinned bright white gentle pro-skin of mildy wash that the present invention is provided, safe and non-stimulating, with deep layer cleaning skin, impaired skin, the effect of anti-inflammatory moisturizing are repaired in moisturizing whitening.
Description
Technical field
The invention belongs to cosmetic technical field, and in particular to a kind of fair-skinned bright white mildy wash and preparation method thereof.
Background technology
In recent years with the raising of people's living standard and aesthetical standard, increasing people pursues, thirsts for pale and clean
The skin of profit.Therefore, with prevent the color spot as caused by sunray and other reasons, pigmentation whitening class make up
The research and development of product and skin-whitening preparation, are just being increasingly subject to various countries' cosmetic Manufacture business and the attention of researcher, whitening
Cosmetics turn into one of main flow kind of skin-care cosmetics.Find efficiently and human body is had no side effect or Small side effects U.S.
White nti-freckle preparation turns into a study hotspot of current pharmacy and cosmetic field.
The effect of whitening product is mainly by suppressing tyrosinase activity or blocking the oxygen of tyrosine generation melanin
Change approach, so as to reduce the effect that melanin generation reaches skin whitening.Skin-whitening product is exactly to act on dermal melanin
In generation, metabolic process, suppress melanin generation and meet the material of specification, but traditional skin-whitening product, often use
Chemical substance, such as has the mercury salt of whitening effect and the quinhydrones of effect of dispelling spots.Although these compounds are rapidly achieved whitening
The effect of, but to skin toxic side effect, long-term use can cause contact dermatitis or cause the ill-effects such as permanent decolouring,
Many countries are disabled.The skin-whitening agents currently required that should comply with two standards：One be have to tyrosinase activity compared with
High inhibiting rate, can significantly reduce the generation of melanin；Two be to have higher security, nontoxic non-stimulated with human body skin.
Ursin, VitC derivatives and kojic acid are the whitening compositions more often used in skin-lightening cosmetic both at home and abroad at present.In order to develop symbol
The cosmetics that " going back to nature " requires, particularly safety, the whitening product having no side effect are closed, some have fine whitening effect
Natural plant composition increasingly paid attention at present by the green grass or young crops of consumer.Find exploitation efficiently and human body is had no side effect or side effect
Small natural plants skin-whitening and speckle eliminating preparation is as one of the current cosmetic field problem being relatively taken seriously.
Chinese patent application CN105640841A discloses a kind of anti-ageing freckle-removing mask liquid and preparation method thereof, it include with
Lower component：Water, glycerine, propane diols, ursin, polyglutamic acid sodium, cyclomethicone, dimethyl silicone polymer crosslinking are poly-
Compound, 3-O- ethylascorbyls, AVC, Bo Lashi mushroom extracts, sweet orange flower are carried
Take thing, pale flag extract, Herba Saussureae Involueratae extract, carbomer, triethanolamine, Sodium Hyaluronate, methyl hydroxybenzoate, Phenoxyethanol
And essence.The facial mask liquid has replenishing water and preserving moisture, desalinates color spot, whitening effect.
Chinese patent application CN105832608A discloses a kind of anti-aging whitening cleansing facial milk containing and preparation method thereof, by white
The root of Dahurian angelica, Radix Codonopsis, balsam pear, rose, the root of herbaceous peony, tree peony, carrot, Ramulus euonymi, teasel root, lotus rhizome, coconut monoethanolamide, three second
Hydramine, polysorbate, saualane, hyaluronic acid, hydroxypropyl methyl cellulose and glycerin monostearate are prepared from, will be white
The root of Dahurian angelica, Radix Codonopsis, balsam pear, rose, the root of herbaceous peony, tree peony, carrot, Ramulus euonymi, teasel root, lotus rhizome are respectively washed, dry, crush, mixed,
Add and extracted in ethanol-water solution, by extract concentration and evaporation under vacuum conditions, then add hydroxypropyl methyl fiber
Element is stirred, and sequentially adds surplus stock, is sufficiently stirred for, emulsification to emulsifiable paste shape, you can.The invention mildy wash security
Height, clean skin effect is good, with good anti-oxidant, delaying skin aging effect, promotes face circulation, improves and repairs impaired flesh
Skin so that the fresh light of skin of face, whitening dialysis.
Whitening is also a nursing engineering from inside to outside.The a set of suitable whitening product of oneself of selection is first had to, because
Whitening composition is different, so can so prevent difference with a series of product preferably using same brand in theory
Whitening composition conflicts mutually the adverse reaction of generation.For whitening cleansing milk in the market cleaning whitening effect not to the utmost such as
People's will, could not fundamentally improve skin problem etc., therefore, it is necessary to a kind of natural safety is researched and developed, cleaning, moisturizing, whitening effect
Really good whitening cleansing milk.
The content of the invention
In order to solve problems of the prior art, it is an object of the invention to provide the fair-skinned bright white mildy wash of one kind and
Its preparation method.The fair-skinned bright white gentle pro-skin of mildy wash that the present invention is provided, it is safe and non-stimulating, with deep layer cleaning skin, mend
Water whitening, repairs impaired skin, the effect of anti-inflammatory moisturizing.
The invention provides the fair-skinned bright white mildy wash of one kind, including following components：
Laruyl alcohol sulfosuccinate disodium, methyl lauroyl sodium taurocholate, lauroylamidopropyl betaine, laruyl alcohol
Polyethers sodium sulfovinate, sodium chloride, coconut oleoyl amine, acrylic acid (ester) analog copolymer, caprylic/capric glyceride type Natrulon H-10 ester
Class, glycine betaine, Laurocapram, 3-O- ethylascorbyls, ursin, tree peony whitening elite, thyme extract, Boulez tower
Buddhist nun Asia pearl algae, PEG-120 methyls dioleate, two (hydrogenated-tallow group) phthalic acid amides, panthenol, niacinamide,
Tranexamic acid, DMDMH, essence and water.Lauroylamidopropyl betaine CAS：4292-10-8；Laureth sulfuric acid
Ester sodium CAS：1335-72-4；Coconut oleoyl amine CAS：61789-19-3；Acrylic acid (ester) analog copolymer CAS：25035-
69-2；Caprylic/capric glyceride type Natrulon H-10 esters are purchased from Jiaxing really environmentally friendly Science and Technology Co., Ltd.；Tree peony whitening
Elite is purchased from Guangzhou Ming Hui Fine Chemical Co., Ltd, article No. S-636, and thyme extract, which is purchased from Guangzhou tender tea leaves luxuriant growth fine chemistry industry, to be had
Limit company, article No. B-658；Pearl algae is purchased from Nanjing Zelang Pharmaceutical Technology Inc. for Brittany Asia；PEG-120 methyls
Dioleate CAS：86893-19-8.
Further, described fair-skinned bright white mildy wash is made up of following components and its percentage by weight：
Laruyl alcohol sulfosuccinate disodium 46-50%, methyl lauroyl sodium taurocholate 7-9%, dodecanamide propyl
Glycine betaine 4-6%, laureth sodium sulfovinate 2.5-3.6%, sodium chloride 2.5-3.5%, coconut oleoyl amine DEA 1.5-
2.5%th, acrylic acid (ester) analog copolymer 0.6-1.5%, caprylic/capric glyceride type Natrulon H-10 esters 0.6-1.5%, sweet tea
Dish alkali 0.6-1.5%, Laurocapram 0.01-0.1%, 3-O- ethylascorbyl 0.05-0.2%, ursin 0.05-
0.2%th, sub- pearl algae 0.4-0.8%, PEG- of tree peony whitening elite 0.6-1%, thyme extract 0.5-1%, Brittany
120 methyl dioleate 0.4-0.8%, two (hydrogenated-tallow group) phthalic acid amide 0.3-0.7%, panthenol 0.3-
0.7%th, niacinamide 0.3-0.7%, tranexamic acid 0.05-0.2%, DMDMH 0.25-0.35%, essence 0.25-
0.35% and water 13.8-31.24%.
Further, described fair-skinned bright white mildy wash is made up of following components and its percentage by weight：
Laruyl alcohol sulfosuccinate disodium 48%, methyl lauroyl sodium taurocholate 8%, lauroylamidopropyl betaine
5%th, laureth sodium sulfovinate 3%, sodium chloride 3%, coconut oleoyl amine DEA 2%, acrylic acid (ester) analog copolymer 1%, pungent
Acid/glycerol decanoate class Natrulon H-10 esters 1%, glycine betaine 1%, Laurocapram 0.05%, 3-O- ethylascorbyls
0.1%th, the sub- pearl algae 0.6% of ursin 0.1%, tree peony whitening elite 0.8%, thyme extract 0.7%, Brittany,
PEG-120 methyls dioleate 0.6%, two (hydrogenated-tallow group) phthalic acid amide 0.5%, panthenol 0.5%, nicotinoyl
Amine 0.5%, tranexamic acid 0.1%, DMDMH 0.3%, essence 0.3% and water 22.85%.
3-O- ethylascorbyls, ursin, tree peony whitening elite, thyme is with the addition of in technical solution of the present invention to carry
The sub- pearl algae of thing, Brittany is taken, wherein 3-O- ethylascorbyls can suppress the activity of tyrosinase, suppress melanin
Formed, reduction melanin is colourless, efficient skin whitening, also has remarkable antioxidant effect.Ursin can rapidly permeate into flesh
Skin, effectively suppresses the activity of the tyrosinase in skin, blocks the formation of melanin, directly tied with tyrosinase by itself
Close, accelerate the decomposition and excretion of melanin, so that Skin pigmentation is reduced, dispelling stain and freckle.Thyme extract energy
" step " of melanin is prevented, melanin quilt is suppressed by the amount for reducing the driving albumen that melanin is carried into epidermal cell
Carry, so as to reach whitening effect.Tree peony whitening elite can suppress the effect of tyrosinase, so as to suppress melanin transfer to angle
Cell plastid, suppresses melanin and produces, highlight the glossiness of skin, reduce visual spot.Brittany Asia pearl algae, can clean
And pore refining, improve skin pattern；Adjust sebum secretion；Skin bellding light is avoided, improves skin gloss；Excitant of releiving flesh
Skin, protects the hyaluronic acid of skin.
The fair-skinned bright white mildy wash of the present invention contains 3-O- ethylascorbyls, ursin, tree peony whitening elite, thyme and carried
The various active compositions such as the sub- pearl algae of thing, Brittany are taken, in conjunction with laruyl alcohol sulfosuccinate disodium of the present invention, methyl month
Osmanthus acyl taurines sodium, lauroylamidopropyl betaine, laureth sodium sulfovinate, sodium chloride, coconut oleoyl amine DEA, propylene
The basic materials such as sour (ester) analog copolymer, caprylic/capric glyceride type Natrulon H-10 esters, glycine betaine, Laurocapram, respectively
Component acts synergistically so that the fair-skinned bright white mildy wash foam exquisiteness of the present invention is abundant, is close to skin, effectively cleaning, keeps skin here
Necessary moisture, not tight after washing, JKS lotions go deep into skin, and tenderness washes away dirt, and a step washes away the fatigue and turbidity of one day.It is weak
Acidity formula, skin-friendly is extremely strong, and skin zero is damaged.Quality is fine and smooth, small molecule infiltration, deep layer cleaning pore, a variety of elite into
Point, the net white passage of skin is opened, the pale good colour of skin is washed out.
Meanwhile, present invention provides a kind of preparation method of fair-skinned bright white mildy wash, comprise the following steps：
S1, Jiang Shui, laureth sodium sulfovinate, coconut oleoyl amine DEA, laruyl alcohol sulfosuccinate disodium, lauroyl
Amine CAB, two (hydrogenated-tallow group) phthalic acid amides, PEG-120 methyls dioleate, methyl lauroyl
Base sodium taurocholate is sequentially added in main cooker, is heated with stirring to 80-85 DEG C, is made its dissolving complete, is incubated 20-40 minutes, obtains material
A；
S2, acrylic acid (ester) analog copolymer and water for adding into step S1 resulting materials A predissolve, and stir to equal
It is even, obtain material B；
S3, when step S2 resulting materials B is cooled into 55-65 DEG C, addition dissolve by heating in advance complete sodium chloride, water and
The caprylic/capric glyceride type Natrulon H-10 esters that dissolve by heating in advance, glycine betaine, and be stirred until homogeneous, obtain material C；
S4, when step S3 resulting materials C is cooled into 45-50 DEG C, add 3-O- ethylascorbyls, tranexamic acid, black bearberry
Glycosides, panthenol, Laurocapram, niacinamide and DMDMH, essence, tree peony whitening elite, thyme extract, Boulez tower
Pearl algae is stirred until homogeneous for Buddhist nun Asia, obtains material D；
S5, step S4 resulting materials D is cooled to 38 DEG C, sampling inspection is qualified to discharge again.
Further, heating-up temperature is 83 DEG C in the step S1, and soaking time is 30 minutes.
Further, 60 DEG C are cooled in the step S3.
Further, 48 DEG C are cooled in the step S4.
Compared with prior art, the present invention has the advantage that：
(1) the fair-skinned bright white mildy wash of the present invention can effectively take out stains, dust, residual adornment, grease, cleaning skin composition inhales
Obstacle is received, it is not tight to wash Hou Shuirun, reduce melanin, that skin and muscles are fair is moving for the obscure order of Kohakuhi；
(2) the fair-skinned bright white mildy wash of the present invention also there is maintenance to be damaged skin, and replenishing water and preserving moisture, the antibacterial effect of anti-inflammatory has
Effect suppresses small pox, the impaired skin of protection；
(3) preparation method of the fair-skinned bright white mildy wash of the present invention is simple, and condition is controllable, process stabilizing, can be applicable.
Embodiment
Below by specific embodiment, the present invention will be further described, and these embodiments are served only for the purpose of illustration, and
Do not limit the scope of the invention.
A kind of fair-skinned bright white mildy wash of embodiment 1
Described fair-skinned bright white mildy wash is made up of following components and its percentage by weight：
Laruyl alcohol sulfosuccinate disodium 46%, methyl lauroyl sodium taurocholate 7%, lauroylamidopropyl betaine
4%th, laureth sodium sulfovinate 2.5%, sodium chloride 2.5%, coconut oleoyl amine DEA 1.5%, acrylic acid (ester) analog copolymer
0.6%th, caprylic/capric glyceride type Natrulon H-10 esters 0.6%, glycine betaine 0.6%, Laurocapram 0.01%, 3-O- second
Base ascorbic acid 0.05%, ursin 0.05%, tree peony whitening elite 0.6%, thyme extract 0.5%, Brittany are sub-
It is pearl algae 0.4%, PEG-120 methyls dioleate 0.4%, two (hydrogenated-tallow group) phthalic acid amide 0.3%, general
Alcohol 0.3%, niacinamide 0.3%, tranexamic acid 0.05%, DMDMH 0.25%, essence 0.25% and water 31.24%.
Preparation method：
S1, Jiang Shui, laureth sodium sulfovinate, coconut oleoyl amine DEA, laruyl alcohol sulfosuccinate disodium, lauroyl
Amine CAB, two (hydrogenated-tallow group) phthalic acid amides, PEG-120 methyls dioleate, methyl lauroyl
Base sodium taurocholate is sequentially added in main cooker, is heated with stirring to 83 DEG C, is made its dissolving complete, is incubated 30 minutes, obtains material A；
S2, acrylic acid (ester) analog copolymer and water for adding into step S1 resulting materials A predissolve, and stir to equal
It is even, obtain material B；
S3, when step S2 resulting materials B is cooled into 60 DEG C, addition dissolves by heating complete sodium chloride, water and pre- in advance
The caprylic/capric glyceride type Natrulon H-10 esters that first dissolve by heating, glycine betaine, and be stirred until homogeneous, obtain material C；
S4, when step S3 resulting materials C is cooled into 48 DEG C, add 3-O- ethylascorbyls, tranexamic acid, ursin,
Panthenol, Laurocapram, niacinamide and DMDMH, essence, tree peony whitening elite, thyme extract, Brittany
Sub- pearl algae is stirred until homogeneous, and obtains material D；
S5, step S4 resulting materials D is cooled to 38 DEG C, sampling inspection is qualified to discharge again.
A kind of fair-skinned bright white mildy wash of embodiment 2
Described fair-skinned bright white mildy wash is made up of following components and its percentage by weight：
Laruyl alcohol sulfosuccinate disodium 48%, methyl lauroyl sodium taurocholate 8%, lauroylamidopropyl betaine
5%th, laureth sodium sulfovinate 3%, sodium chloride 3%, coconut oleoyl amine DEA 2%, acrylic acid (ester) analog copolymer 1%, pungent
Acid/glycerol decanoate class Natrulon H-10 esters 1%, glycine betaine 1%, Laurocapram 0.05%, 3-O- ethylascorbyls
0.1%th, the sub- pearl algae 0.6% of ursin 0.1%, tree peony whitening elite 0.8%, thyme extract 0.7%, Brittany,
PEG-120 methyls dioleate 0.6%, two (hydrogenated-tallow group) phthalic acid amide 0.5%, panthenol 0.5%, nicotinoyl
Amine 0.5%, tranexamic acid 0.1%, DMDMH 0.3%, essence 0.3% and water 22.85%.
Preparation method is similar to Example 1.
A kind of fair-skinned bright white mildy wash of embodiment 3
Described fair-skinned bright white mildy wash is made up of following components and its percentage by weight：
Laruyl alcohol sulfosuccinate disodium 50%, methyl lauroyl sodium taurocholate 9%, lauroylamidopropyl betaine
6%th, laureth sodium sulfovinate 3.6%, sodium chloride 3.5%, coconut oleoyl amine DEA 2.5%, acrylic acid (ester) analog copolymer
1.5%th, caprylic/capric glyceride type Natrulon H-10 esters 1.5%, glycine betaine 1.5%, Laurocapram 0.1%, 3-O- second
The sub- pearl algae of base ascorbic acid 0.2%, ursin 0.2%, tree peony whitening elite 1%, thyme extract 1%, Brittany
0.8%th, PEG-120 methyls dioleate 0.8%, two (hydrogenated-tallow group) phthalic acid amide 0.7%, panthenol
0.7%th, niacinamide 0.7%, tranexamic acid 0.2%, DMDMH 0.35%, essence 0.35% and water 13.8%.
Preparation method is similar to Example 1.
A kind of fair-skinned bright white mildy wash of comparative example 1
Described fair-skinned bright white mildy wash is made up of following components and its percentage by weight：
Laruyl alcohol sulfosuccinate disodium 48%, methyl lauroyl sodium taurocholate 8%, lauroylamidopropyl betaine
5%th, laureth sodium sulfovinate 3%, sodium chloride 3%, coconut oleoyl amine DEA 2%, acrylic acid (ester) analog copolymer 1%, pungent
Acid/glycerol decanoate class Natrulon H-10 esters 1%, glycine betaine 1%, Laurocapram 0.05%, 3-O- ethylascorbyls
0.1%th, the sub- pearl algae 0.6% of ursin 0.1%, tree peony whitening elite 0.8%, thyme extract 0.7%, Brittany,
It is PEG-120 methyls dioleate 0.6%, two (hydrogenated-tallow group) phthalic acid amide 0.5%, niacinamide 0.5%, solidifying
Hematic acid 0.1%, DMDMH 0.3%, essence 0.3% and water 23.35%.
Preparation method is similar to Example 1.
Difference with embodiment 2 is, is not added with panthenol, adds the consumption of water.
A kind of fair-skinned bright white mildy wash of comparative example 2
Described fair-skinned bright white mildy wash is made up of following components and its percentage by weight：
Laruyl alcohol sulfosuccinate disodium 48%, methyl lauroyl sodium taurocholate 8%, lauroylamidopropyl betaine
5%th, laureth sodium sulfovinate 3%, sodium chloride 3%, coconut oleoyl amine DEA 2%, acrylic acid (ester) analog copolymer 1%, pungent
Acid/glycerol decanoate class Natrulon H-10 esters 1%, glycine betaine 1%, Laurocapram 0.05%, 3-O- ethylascorbyls
0.1%th, the sub- pearl algae 0.6% of ursin 0.1%, Angelica Dahurica extract 0.8%, thyme extract 0.7%, Brittany,
PEG-120 methyls dioleate 0.6%, two (hydrogenated-tallow group) phthalic acid amide 0.5%, panthenol 0.5%, nicotinoyl
Amine 0.5%, tranexamic acid 0.1%, DMDMH 0.3%, essence 0.3% and water 22.85%.
Preparation method is similar to Example 1.
Difference with embodiment 2 is, tree peony whitening elite is replaced with into Angelica Dahurica extract.
A kind of fair-skinned bright white mildy wash of comparative example 3
Described fair-skinned bright white mildy wash is made up of following components and its percentage by weight：
Laruyl alcohol sulfosuccinate disodium 48%, methyl lauroyl sodium taurocholate 8%, lauroylamidopropyl betaine
5%th, laureth sodium sulfovinate 3%, sodium chloride 3%, coconut oleoyl amine DEA 2%, acrylic acid (ester) analog copolymer 1%, pungent
Acid/glycerol decanoate class Natrulon H-10 esters 1%, glycine betaine 1%, Laurocapram 0.05%, 3-O- ethylascorbyls
0.2%th, the sub- pearl algae 0.6% of ursin 0.1%, tree peony whitening elite 0.8%, thyme extract 0.7%, Brittany,
PEG-120 methyls dioleate 0.6%, two (hydrogenated-tallow group) phthalic acid amide 0.5%, panthenol 0.5%, nicotinoyl
Amine 0.5%, DMDMH 0.3%, essence 0.3% and water 22.85%.
Preparation method is similar to Example 1.
Difference with embodiment 2 is, is not added with tranexamic acid, adds the consumption of 3-O- ethyl Vitamin Cs.
Test example one, safety evaluatio
1. test material：Fair-skinned bright white mildy wash prepared by embodiment 1-3.
2. subjects：60 people, women, 25-50 Sui, skin health, no skin disease allergies.
3. test method：
1) subject is randomly divided into 3 groups, every group of 20 people are denoted as embodiment 1-3 groups；
2) from qualified spot examination device, with closed patch experiment method, by tested material, (prepared by embodiment 1-3 fair-skinned
Brilliant white mildy wash) length about 1-2cm in spot examination device in, external application special adhesive tape be covered on after subject back, 24h remove it is tested
Thing, respectively remove after 0.5,6,12,24,48h observation dermoreaction, according to《Cosmetics health specification》Middle dermoreaction classification mark
Standard records its result.
4 result of the tests：
As a result show, after the fair-skinned bright white mildy wash that each group subject is prepared using embodiment 1-3,0.5,6,12,24,
48h observes dermoreaction, and skin has no adverse reaction, and illustrates that fair-skinned bright white mildy wash prepared by the present invention is safe and non-stimulating.
Test example two, whitening effect evaluation
1. test material：Fair-skinned bright white mildy wash prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：120 people, women, 22-40 Sui, skin is dim, no skin disease allergies.
3. test method：
1) subject is randomly divided into 6 groups, every group of 20 people are denoted as embodiment 1-3 groups and comparative example 1-3 groups；
2) respectively washed one's face sooner or later using an embodiment 1-3 and comparative example 1-3 fair-skinned bright white mildy wash prepared daily, continuously
Using 3 months, contained using the German CK companies dermal melanin test probe MX18 melanin for testing facial same spot position
Amount (chooses cheek cheekbone peak position), averages.
4. result of the test：Melanin content test result is shown in Table 1.
The melanin content of table 1 changes
| Melanin content | Embodiment 1 | Embodiment 2 | Embodiment 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
| Before use | 492 | 487 | 501 | 488 | 496 | 476 |
| After use | 360 | 323 | 356 | 370 | 384 | 371 |
| Changing value | 132 | 164 | 145 | 118 | 112 | 105 |
Known by table 1, fair-skinned bright white mildy wash whitening effect prepared by the present invention is preferable.Compared with comparative example 1-3, the present invention
Melanin content minimizing effect is more apparent after fair-skinned bright white mildy wash prepared by embodiment 1-3 is used 3 months, illustrates that the present invention matches somebody with somebody
5 is reasonable, science, and each component interacts plays the effect of whitening jointly.
Test example three, moisturizing effect assessment
1. test material：Fair-skinned bright white mildy wash prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：120 people, women, 22-40 Sui, skin health, no skin disease allergies.
3. test method：
1) subject is randomly divided into 6 groups, every group of 20 people are denoted as embodiment 1-3 groups and comparative example 1-3 groups；
2) after subject is washed one's face with the embodiment 1-3 and comparative example 1-3 fair-skinned bright white face cleaning whey waters prepared, Fes is used
Kai Er SK-III skin moistures detectors test the moisture of forehead, left face, right face and chin skin respectively, and take arithmetic to put down
The skin moisture content of forehead, left face, right face and chin same location is tested after average, 24h with skin moisture tester, and is taken
Arithmetic mean of instantaneous value.
4. result of the test：Moisture test result is shown in Table 2.
The moisture result of table 2
Known by table 2, fair-skinned bright white mildy wash replenishing water and preserving moisture effect prepared by the present invention is preferable.Compared with comparative example 1-3, this
Fair-skinned bright white mildy wash prepared by inventive embodiments 1-3 increases more apparent using rear water content, illustrate that compatibility of the present invention is reasonable, section
Learn, each component interacts plays the effect of moisturizing jointly.
Test example four, fungistatic effect evaluation
1. test material：Fair-skinned bright white mildy wash prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：Micrococcus scarlatinae, propionibacterium acnes, MRSE, staphylococcus aureus.
3. test method：
1) experiment bacteria suspension is prepared
Concentration is：With 100 μ L drops on to photo, it is 1 × 10 to reclaim clump count4-1×109Cfu/ pieces.
2) microbiological contamination print is prepared
Above-mentioned bacteria suspension is taken, 100 μ L is added dropwise in coupons and control print each respectively, acts on 20min.
3) print is put into the test tube of the phosphate buffer solution containing 5mL respectively, fully mixed, diluted 2-3 dilution factor, take
0.5mL is placed in plate, is poured into 40-50 DEG C of nutrient agar (bacterium) 15mL, rotates plate, it is fully mixed
It is even, flat board is overturn after agar solidification, culture is inverted, 37 DEG C, cultivates 48h.
4) bacteriostasis rate is calculated, formula is as follows：
Wherein, X- bacteriostasis rates, %；A- compares print average colony number；B- is by coupons average colony number.
4. result of the test：Bacteriostasis rate the results are shown in Table 3.
The bacteriostasis rate result of table 3
Known by table 3, fair-skinned bright white mildy wash prepared by the present invention has preferable bacteriostasis.Compared with comparative example 1-3,
Fair-skinned bright white mildy wash prepared by the present invention is to micrococcus scarlatinae, propionibacterium acnes, MRSE, golden yellow grape
Coccus has good inhibiting effect, illustrate the fair-skinned bright white mildy wash for preparing of the present invention can suppress small pox and effectively protection by
Damage skin.
Test example five, sensory evaluation experiment
1. test material：Fair-skinned bright white mildy wash prepared by embodiment 1-3 and comparative example 1-3.
2. subjects：120 people, men and women half and half, and there are damage or scar, 18-40 Sui in face.
3. test method：
Subject is randomly divided into 6 groups, every group of 20 people are denoted as embodiment 1-3 and comparative example 1-3 groups.Each group is used respectively
Fair-skinned bright white mildy wash prepared by embodiment 1-3 and comparative example 1-3, daily once in the morning and once at night, is used for situation after January
Marking is evaluated.Standards of grading：Using ten point system, 10 points best, and 0 point worst, and fraction more high effect is better.
4. result of the test：Analyses Methods for Sensory Evaluation Results is shown in Table 4.
The Analyses Methods for Sensory Evaluation Results of table 4
Known by table 4, fair-skinned bright white mildy wash repairing effect prepared by the present invention is preferable.And comparative example 1-3 preparations is fair-skinned
Brilliant white mildy wash repairing effect is poorer than the effect of the embodiment 1-3 fair-skinned bright white mildy wash prepared, illustrates that compatibility of the present invention is reasonable
Science, each component interaction collaboration plays a part of to repair.Meanwhile, fair-skinned bright white mildy wash prepared by the present invention also has clear
Clean, moisturizing, the effect of anti-inflammatory, feel to moisten, clearly, and subject does not occur allergic phenomena after use.
Claims (7)
1. a kind of fair-skinned bright white mildy wash, it is characterised in that including following components：
Laruyl alcohol sulfosuccinate disodium, methyl lauroyl sodium taurocholate, lauroylamidopropyl betaine, laureth
Sodium sulfovinate, sodium chloride, coconut oleoyl amine, acrylic acid (ester) analog copolymer, caprylic/capric glyceride type Natrulon H-10 esters, sweet tea
Dish alkali, Laurocapram, 3-O- ethylascorbyls, ursin, tree peony whitening elite, thyme extract, Brittany are sub-
Pearl algae, PEG-120 methyls dioleate, two (hydrogenated-tallow group) phthalic acid amides, panthenol, niacinamide, blood coagulation
Acid, DMDMH, essence and water.
2. fair-skinned bright white mildy wash as claimed in claim 1, it is characterised in that by following components and its percentage by weight group
Into：
Laruyl alcohol sulfosuccinate disodium 46-50%, methyl lauroyl sodium taurocholate 7-9%, dodecanamide propyl beet
Alkali 4-6%, laureth sodium sulfovinate 2.5-3.6%, sodium chloride 2.5-3.5%, coconut oleoyl amine DEA1.5-2.5%, propylene
Sour (ester) analog copolymer 0.6-1.5%, caprylic/capric glyceride type Natrulon H-10 esters 0.6-1.5%, glycine betaine 0.6-
1.5%th, Laurocapram 0.01-0.1%, 3-O- ethylascorbyls 0.05-0.2%, ursin 0.05-0.2%, tree peony are beautiful
Bai Jinghua 0.6-1%, thyme extract 0.5-1%, Brittany Asia pearl algae 0.4-0.8%, PEG-120 methyl two
Oleate 0.4-0.8%, two (hydrogenated-tallow group) phthalic acid amide 0.3-0.7%, panthenol 0.3-0.7%, niacinamide
0.3-0.7%, tranexamic acid 0.05-0.2%, DMDMH 0.25-0.35%, essence 0.25-0.35% and water 13.8-
31.24%.
3. fair-skinned bright white mildy wash as claimed in claim 2, it is characterised in that by following components and its percentage by weight group
Into：
Laruyl alcohol sulfosuccinate disodium 48%, methyl lauroyl sodium taurocholate 8%, lauroylamidopropyl betaine 5%,
Laureth sodium sulfovinate 3%, sodium chloride 3%, coconut oleoyl amine DEA 2%, acrylic acid (ester) analog copolymer 1%, the octanoic acid/last of the ten Heavenly stems
Acid glyceride class Natrulon H-10 esters 1%, glycine betaine 1%, Laurocapram 0.05%, 3-O- ethylascorbyls 0.1%,
The sub- pearl algae 0.6% of ursin 0.1%, tree peony whitening elite 0.8%, thyme extract 0.7%, Brittany, PEG-120
Methyl dioleate 0.6%, two (hydrogenated-tallow group) phthalic acid amide 0.5%, panthenol 0.5%, niacinamide
0.5%th, tranexamic acid 0.1%, DMDMH 0.3%, essence 0.3% and water 22.85%.
4. the preparation method of the fair-skinned bright white mildy wash as described in claim 1-3 is any, it is characterised in that including following step
Suddenly：
S1, Jiang Shui, laureth sodium sulfovinate, coconut oleoyl amine DEA, laruyl alcohol sulfosuccinate disodium, lauramide third
Base glycine betaine, two (hydrogenated-tallow group) phthalic acid amides, PEG-120 methyls dioleate, methyl lauroyl ox
Sodium sulfonate is sequentially added in main cooker, is heated with stirring to 80-85 DEG C, is made its dissolving complete, is incubated 20-40 minutes, obtains material A；
S2, acrylic acid (ester) analog copolymer and water for adding into step S1 resulting materials A predissolve, and are stirred until homogeneous, obtain
Material B；
S3, when step S2 resulting materials B is cooled into 55-65 DEG C, addition dissolves by heating complete sodium chloride, water and in advance in advance
The caprylic/capric glyceride type Natrulon H-10 esters of heating for dissolving, glycine betaine, and be stirred until homogeneous, obtain material C；
S4, when step S3 resulting materials C is cooled into 45-50 DEG C, add 3-O- ethylascorbyls, tranexamic acid, ursin, general
Alcohol, Laurocapram, niacinamide and DMDMH, essence, tree peony whitening elite, thyme extract, Brittany are sub-
Pearl algae is stirred until homogeneous, and obtains material D；
S5, step S4 resulting materials D is cooled to 38 DEG C, sampling inspection is qualified to discharge again.
5. the preparation method of fair-skinned bright white mildy wash as claimed in claim 4, it is characterised in that temperature is heated in the step S1
Spend for 83 DEG C, soaking time is 30 minutes.
6. the preparation method of fair-skinned bright white mildy wash as claimed in claim 4, it is characterised in that be cooled in the step S3
60℃。
7. the preparation method of fair-skinned bright white mildy wash as claimed in claim 4, it is characterised in that be cooled in the step S4
48℃。
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| CN110037937A (en) * | 2019-03-06 | 2019-07-23 | 曼秀雷敦(中国)药业有限公司 | A kind of mild amino acid cleansing cream and preparation method thereof |
| CN110693748A (en) * | 2019-11-04 | 2020-01-17 | 木芷秋山(广州)化妆品研究开发有限公司 | Amino acid bubble cleanser and preparation method thereof |
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