CN107213062B - Fair, transparent and white facial cleanser and preparation method thereof - Google Patents
Fair, transparent and white facial cleanser and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to fair and bright facial cleanser and a preparation method thereof. The fair, transparent and white facial cleanser provided by the invention comprises the following components: disodium lauryl sulfosuccinate, sodium methyl lauroyl taurate, lauramidopropyl betaine, sodium laureth sulfate, sodium chloride, cocamide, acrylic acid (ester) copolymer, caprylic/capric glyceride-10 esters, betaine, laurocapram, 3-O-ethyl ascorbic acid, arbutin, peony whitening essence, thyme extract, Palettia japonica, PEG-120 methyl glucose dioleate, di (hydrogenated tallow) phthalamide, panthenol, niacinamide, tranexamic acid, DMDM, essence, and water. The fair, bright and white facial cleanser provided by the invention is mild and skin-friendly, safe and non-irritant, and has the effects of deeply cleaning skin, moisturizing and whitening skin, repairing damaged skin, diminishing inflammation and moisturizing.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to fair and bright facial cleanser and a preparation method thereof.
Background
In recent years, as the living standard and aesthetic standard of people are improved, more and more people seek and desire white and moist skin. Therefore, research and development of whitening cosmetics and skin whitening preparations having the effect of preventing color spots and pigmentation caused by solar rays and other causes are receiving increasing attention from cosmetic manufacturers and researchers in various countries, and the whitening cosmetics have become one of the main types of skin care cosmetics. The search for a whitening and freckle-removing preparation which is efficient and has no side effect or little side effect on human bodies becomes a research hotspot in the fields of pharmacy and cosmetics at present.
The whitening product has the main function of whitening the skin by inhibiting the activity of tyrosinase or blocking the oxidation pathway of the tyrosine to generate melanin so as to reduce the generation of the melanin. The skin whitening product is a substance which acts on the skin in the processes of melanin generation and metabolism, inhibits the generation of melanin and meets the specification, but the traditional skin whitening product usually adopts chemical substances, such as mercuric salt with whitening effect and hydroquinone with freckle removing effect. Although the compounds have the effect of quickly whitening skin, the compounds have toxic and side effects on skin, and can cause contact dermatitis or permanent decoloration after long-term use, and the compounds are forbidden in many countries. The currently required skin lightening agents should meet two criteria: firstly, the tyrosinase activity is inhibited at a high rate, and the generation of melanin can be obviously reduced; secondly, the safety is higher, and the skin of the human body is nontoxic and non-irritant. Arbutin, VitC derivatives and kojic acid are the whitening components which are commonly used in the whitening cosmetics at home and abroad at present. In order to develop cosmetics that meet the requirements of "returning to nature", particularly whitening products that are safe and free of side effects, some natural plant ingredients having a good whitening effect are currently being regarded by consumers more and more. The search for and development of natural plant skin whitening and freckle removing preparations which are efficient and have no side effects or small side effects on human bodies has become a more important subject in the field of cosmetics at present.
Chinese patent application CN105640841A discloses an anti-aging and freckle-removing mask liquid and a preparation method thereof, wherein the anti-aging and freckle-removing mask liquid comprises the following components: water, glycerin, propylene glycol, arbutin, sodium polyglutamate, cyclomethicone, dimethicone crosspolymer, 3-O-ethyl ascorbic acid, ammonium acryloyldimethyl taurate/VP copolymer, Agaricus campestris extract, Citrus sinensis flower extract, Iris communis extract, snow lotus herb extract, carbomer, triethanolamine, sodium hyaluronate, methylparaben, phenoxyethanol, and essence. The facial mask liquid has effects of moisturizing, removing color spots, and whitening skin.
Chinese patent application CN105832608A discloses an anti-aging whitening facial cleanser and a preparation method thereof, the anti-aging whitening facial cleanser is prepared by dahurian angelica root, pilose asiabell root, balsam pear, rose, white paeony root, peony, carrot, winged euonymus twig, himalayan teasel root, lotus root, coconut oleic acid monoethanolamide, triethanolamine, polysorbate, squalane, hyaluronic acid, hydroxypropyl methyl cellulose and glycerin monostearate, the dahurian angelica root, the pilose asiabell root, the balsam pear, rose, white paeony root, peony, carrot, winged euonymus twig, teasel root and lotus root are respectively cleaned, aired, crushed and mixed, the mixture is added into an ethanol-water solution for extraction, the extract liquid is concentrated and evaporated under a vacuum environment, then the hydroxypropyl methyl cellulose is added for stirring, the rest raw materials are sequentially added, the mixture is fully stirred and emulsified. The facial cleanser disclosed by the invention is high in safety and good in skin cleaning effect, has good effects of resisting oxidation and delaying skin aging, promotes facial circulation, improves and repairs damaged skin, enables the facial skin to be fresh and bright, and is whitening and dialyzing.
Whitening is also a care process from the inside out. Firstly, a set of whitening products suitable for the user needs to be selected, and because the whitening components are different, the user preferably uses products of the same brand and the same series theoretically, so that adverse reactions caused by the mutual conflict of different whitening components can be prevented. Aiming at the problems that the cleaning and whitening effects of the whitening facial cleanser on the market are not satisfactory and the skin problem cannot be fundamentally improved, the whitening facial cleanser in the market is necessary to be developed, and the whitening facial cleanser is natural, safe, good in cleaning, moisturizing and whitening effects.
Disclosure of Invention
In order to solve the problems in the prior art, the invention aims to provide a fair, transparent and white facial cleanser and a preparation method thereof. The fair, bright and white facial cleanser provided by the invention is mild and skin-friendly, safe and non-irritant, and has the effects of deeply cleaning skin, moisturizing and whitening skin, repairing damaged skin, diminishing inflammation and moisturizing.
The invention provides fair, transparent and white facial cleanser which comprises the following components:
disodium lauryl sulfosuccinate, sodium methyl lauroyl taurate, lauramidopropyl betaine, sodium laureth sulfate, sodium chloride, cocamide, acrylic acid (ester) copolymer, caprylic/capric glyceride-10 esters, betaine, laurocapram, 3-O-ethyl ascorbic acid, arbutin, peony whitening essence, thyme extract, Palettia japonica, PEG-120 methyl glucose dioleate, di (hydrogenated tallow) phthalamide, panthenol, niacinamide, tranexamic acid, DMDM, essence, and water. Lauramidopropyl betaine CAS No.: 4292-10-8; sodium laureth sulfate CAS number: 1335-72-4; cocamide CAS number: 61789-19-3; acrylic copolymer CAS No.: 25035-69-2; caprylic/capric glyceride polyglycerol-10 esters were purchased from Jiaxing Zhongcheng environmental protection science and technology, Inc.; the peony whitening essence is purchased from Guangzhou Ming Hui Fine chemical Co., Ltd, product number S-636, and the thyme extract is purchased from Guangzhou Ming Hui Fine chemical Co., Ltd, product number B-658; blatania pearl algae is purchased from Nanjing Zeron pharmaceutical science and technology, Inc.; PEG-120 methyl glucose dioleate CAS number: 86893-19-8.
Further, the fair, transparent and white facial cleanser comprises the following components in percentage by weight:
46-50% of disodium lauryl alcohol sulfosuccinate, 7-9% of sodium methyl lauroyl taurate, 4-6% of lauramidopropyl betaine, 2.5-3.6% of sodium laureth sulfate, 2.5-3.5% of sodium chloride, 1.5-2.5% of cocamide DEA, 0.6-1.5% of acrylic acid (ester) copolymer, 0.6-1.5% of caprylic/capric glyceride type polyglycerol-10 esters, 0.6-1.5% of betaine, 0.01-0.1% of laurocapram, 0.05-0.2% of 3-O-ethyl ascorbic acid, 0.05-0.2% of arbutin, 0.6-1% of peony whitening essence, 0.5-1% of thyme extract, 0.4-0.8% of Botrytis algae, 0.4-0.8% of PEG-120% of methyl glucose dioleate, and 0.3-0.7% of di (hydrogenated tallow) phthalic acid amide, 0.3-0.7% of panthenol, 0.3-0.7% of nicotinamide, 0.05-0.2% of tranexamic acid, 0.25-0.35% of DMDM hydantoin, 0.25-0.35% of essence and 13.8-31.24% of water.
Further, the fair, transparent and white facial cleanser comprises the following components in percentage by weight:
disodium lauryl sulfosuccinate 48%, sodium methyl lauroyl taurate 8%, lauramidopropyl betaine 5%, sodium laureth sulfate 3%, sodium chloride 3%, cocamide DEA 2%, acrylic acid (ester) copolymer 1%, caprylic/capric glyceride-10 esters 1%, betaine 1%, laurocapram 0.05%, 3-O-ethyl ascorbic acid 0.1%, arbutin 0.1%, peony whitening essence 0.8%, thyme extract 0.7%, Pearl shell-weed 0.6%, PEG-120-methyl glucose dioleate 0.6%, di (hydrogenated tallow) phthalic acid amide 0.5%, panthenol 0.5%, nicotinamide 0.5%, tranexamic acid 0.1%, DMDM hydantoin 0.3%, essence 0.3%, and water 22.85%.
According to the technical scheme, 3-O-ethyl ascorbic acid, arbutin, peony whitening essence, thyme extract and Blattella bubonii are added, wherein the 3-O-ethyl ascorbic acid can inhibit the activity of tyrosinase and the formation of melanin, reduce the melanin to be colorless, efficiently whiten skin and also has an excellent antioxidant effect. The arbutin can rapidly penetrate into skin, effectively inhibit the activity of tyrosinase in the skin, block the formation of melanin, and accelerate the decomposition and excretion of melanin through the direct combination of the arbutin and the tyrosinase, thereby reducing skin pigmentation and removing color spots and freckles. The thyme extract can prevent melanin from 'walking', and reduce the amount of kinesin for transporting melanin to epidermal cells to inhibit the transportation of melanin, thereby whitening skin. The peony whitening essence can inhibit tyrosinase, thereby inhibiting melanin from transferring to keratinocytes, inhibiting melanin generation, improving skin glossiness, and reducing visible spots. The pearl algae of Butyrospermum parkeri can clean and shrink pores and improve skin texture; regulating sebum secretion; the skin is prevented from being oily and glossy, and the skin luster is improved; relieving irritation to skin, and protecting skin.
The fair and bright white facial cleanser disclosed by the invention contains 3-O-ethyl ascorbic acid, arbutin, peony whitening essence, thyme extract, pearl algae and other active ingredients, and is combined with the basic raw materials such as disodium lauryl sulfosuccinate, methyl lauroyl taurate, lauramidopropyl betaine, sodium laureth sulfate, sodium chloride, cocamide DEA, acrylic acid (ester) copolymer, caprylic/capric glyceride polyglycerol-10 esters, betaine, laurocapram and the like, and the components have synergistic effects, so that the fair and bright white facial cleanser disclosed by the invention has the advantages of delicate and rich foam, close contact with the skin, effective cleaning, retention of necessary moisture on the skin, loose cleaning factors after washing, deep penetration of the skin, mild and soft washing to remove dirt, and one-day fatigue and turbidity washing. The weak acid formula has strong skin-friendly property and no damage to skin. Fine texture, small molecule penetration, deep pore cleaning, multiple essence components, skin whitening channel opening, and white and fair skin.
Meanwhile, the invention also provides a preparation method of the fair, transparent and white facial cleanser, which comprises the following steps:
s1, sequentially adding water, sodium laureth sulfate, cocamide DEA, disodium laurylsulfosuccinate, lauramidopropyl betaine, di (hydrogenated tallow) phthalic acid amide, PEG-120 methyl glucose dioleate and methyl lauroyl sodium taurate into a main pot, stirring and heating to 80-85 ℃, completely dissolving the materials, and preserving heat for 20-40 minutes to obtain a material A;
s2, adding the pre-dissolved acrylic acid (ester) copolymer and water into the material A obtained in the step S1, and stirring uniformly to obtain a material B;
s3, cooling the material B obtained in the step S2 to 55-65 ℃, adding sodium chloride, water and caprylic/capric glyceride polyglycerol-10 esters and betaine which are heated and dissolved completely in advance, and stirring uniformly to obtain a material C;
s4, cooling the material C obtained in the step S3 to 45-50 ℃, adding 3-O-ethyl ascorbic acid, tranexamic acid, arbutin, panthenol, laurocapram, nicotinamide, DMDM hydantoin, essence, peony whitening essence, thyme extract and pearl algae, and stirring uniformly to obtain a material D;
s5, cooling the material D obtained in the step S4 to 38 ℃, sampling, checking, and discharging after the material is qualified.
Further, in the step S1, the heating temperature is 83 ℃ and the holding time is 30 minutes.
Further, in the step S3, the temperature is decreased to 60 ℃.
Further, in the step S4, the temperature is decreased to 48 ℃.
Compared with the prior art, the invention has the following advantages:
(1) the fair, transparent and white facial cleanser can effectively remove dirt, dust, residual makeup and grease, sweep skin component malabsorption, reduce melanin, fade spots and darkness and make the skin fair and active after washing;
(2) the fair, transparent and white facial cleanser also has the functions of repairing damaged skin, replenishing water, moisturizing, diminishing inflammation and inhibiting bacteria, effectively inhibits acnes and protects the damaged skin;
(3) the preparation method of the fair, transparent and white facial cleanser is simple, controllable in conditions, stable in process and capable of being popularized and applied.
Detailed Description
The present invention is further illustrated by the following specific examples, which are provided for illustrative purposes only and do not limit the scope of the present invention.
Example 1 fair, transparent and white cleanser
The fair, transparent and white facial cleanser comprises the following components in percentage by weight:
disodium lauryl sulfosuccinate 46%, sodium methyl lauroyl taurate 7%, lauramidopropyl betaine 4%, sodium laureth sulfate 2.5%, sodium chloride 2.5%, cocamide DEA 1.5%, acrylic acid (ester) copolymer 0.6%, caprylic/capric glyceride polyglycerol-10 esters 0.6%, betaine 0.6%, laurocapram 0.01%, 3-O-ethyl ascorbic acid 0.05%, arbutin 0.05%, peony whitening essence 0.6%, thyme extract 0.5%, Pearl oyster shell-grass 0.4%, PEG-120-methylglucdioleate 0.4%, di (hydrogenated tallow) phthalic acid amide 0.3%, panthenol 0.3%, niacinamide 0.3%, tranexamic acid 0.05%, DMDM hydantoin 0.25%, essence 0.25%, and water 31.24%.
The preparation method comprises the following steps:
s1, sequentially adding water, sodium laureth sulfate, cocamide DEA, disodium laurylsulfosuccinate, lauramidopropyl betaine, di (hydrogenated tallow) phthalic acid amide, PEG-120 methyl glucose dioleate and methyl lauroyl sodium taurate into a main pot, stirring and heating to 83 ℃, completely dissolving the materials, and preserving the temperature for 30 minutes to obtain a material A;
s2, adding the pre-dissolved acrylic acid (ester) copolymer and water into the material A obtained in the step S1, and stirring uniformly to obtain a material B;
s3, cooling the material B obtained in the step S2 to 60 ℃, adding sodium chloride, water and caprylic/capric glyceride polyglycerol-10 esters and betaine which are heated and dissolved completely in advance, and stirring uniformly to obtain a material C;
s4, cooling the material C obtained in the step S3 to 48 ℃, adding 3-O-ethyl ascorbic acid, tranexamic acid, arbutin, panthenol, laurocapram, nicotinamide, DMDM hydantoin, essence, peony whitening essence, thyme extract and pearly alga of Tanonia, and uniformly stirring to obtain a material D;
s5, cooling the material D obtained in the step S4 to 38 ℃, sampling, checking, and discharging after the material is qualified.
Example 2 fair, transparent and white facial cleanser
The fair, transparent and white facial cleanser comprises the following components in percentage by weight:
disodium lauryl sulfosuccinate 48%, sodium methyl lauroyl taurate 8%, lauramidopropyl betaine 5%, sodium laureth sulfate 3%, sodium chloride 3%, cocamide DEA 2%, acrylic acid (ester) copolymer 1%, caprylic/capric glyceride-10 esters 1%, betaine 1%, laurocapram 0.05%, 3-O-ethyl ascorbic acid 0.1%, arbutin 0.1%, peony whitening essence 0.8%, thyme extract 0.7%, Pearl shell-weed 0.6%, PEG-120-methyl glucose dioleate 0.6%, di (hydrogenated tallow) phthalic acid amide 0.5%, panthenol 0.5%, nicotinamide 0.5%, tranexamic acid 0.1%, DMDM hydantoin 0.3%, essence 0.3%, and water 22.85%.
The preparation method is similar to example 1.
Example 3 fair, transparent and white cleanser
The fair, transparent and white facial cleanser comprises the following components in percentage by weight:
disodium lauryl sulfosuccinate 50%, sodium methyl lauroyl taurate 9%, lauramidopropyl betaine 6%, sodium laureth sulfate 3.6%, sodium chloride 3.5%, cocamide DEA 2.5%, acrylic acid (ester) copolymer 1.5%, caprylic/capric glyceride polyglycerol-10 esters 1.5%, betaine 1.5%, laurocapram 0.1%, 3-O-ethyl ascorbic acid 0.2%, arbutin 0.2%, peony whitening essence 1%, thyme extract 1%, pearl alga buntania 0.8%, PEG-120-methyl glucose dioleate 0.8%, di (hydrogenated tallow) phthalic acid amide 0.7%, panthenol 0.7%, niacinamide 0.7%, tranexamic acid 0.2%, DMDM hydantoin 0.35%, essence 0.35%, and water 13.8%.
The preparation method is similar to example 1.
Comparative example 1 fair, transparent and white facial cleanser
The fair, transparent and white facial cleanser comprises the following components in percentage by weight:
disodium lauryl sulfosuccinate 48%, sodium methyl lauroyl taurate 8%, lauramidopropyl betaine 5%, sodium laureth sulfate 3%, sodium chloride 3%, cocamide DEA 2%, acrylic acid (ester) copolymer 1%, glyceryl caprylate/caprate polyglycerin-10 esters 1%, betaine 1%, laurocapram 0.05%, 3-O-ethyl ascorbic acid 0.1%, arbutin 0.1%, peony whitening essence 0.8%, thyme extract 0.7%, Pearl seaweed 0.6%, PEG-120-methyl glucose dioleate 0.6%, di (hydrogenated tallow) phthalic acid amide 0.5%, niacinamide 0.5%, tranexamic acid 0.1%, DMDM hydantoin 0.3%, essence 0.3%, and water 23.35%.
The preparation method is similar to example 1.
The difference from example 2 is that the amount of water was increased without adding panthenol.
Comparative example 2 fair, transparent and white facial cleanser
The fair, transparent and white facial cleanser comprises the following components in percentage by weight:
disodium lauryl sulfosuccinate 48%, sodium methyl lauroyl taurate 8%, lauramidopropyl betaine 5%, sodium laureth sulfate 3%, sodium chloride 3%, cocamide DEA 2%, acrylic acid (ester) copolymer 1%, caprylic/capric glyceride-10 esters 1%, betaine 1%, laurocapram 0.05%, 3-O-ethyl ascorbic acid 0.1%, arbutin 0.1%, angelica dahurica extract 0.8%, thyme extract 0.7%, pearly seaweed bubonii 0.6%, PEG-120-methyl glucose dioleate 0.6%, di (hydrogenated tallow) phthalic acid amide 0.5%, panthenol 0.5%, niacinamide 0.5%, tranexamic acid 0.1%, DMDM hydantoin 0.3%, essence 0.3%, and water 22.85%.
The preparation method is similar to example 1.
The difference from example 2 is that the peony whitening essence is replaced with an angelica dahurica extract.
Comparative example 3 fair, transparent and white facial cleanser
The fair, transparent and white facial cleanser comprises the following components in percentage by weight:
disodium lauryl sulfosuccinate 48%, sodium methyl lauroyl taurate 8%, lauramidopropyl betaine 5%, sodium laureth sulfate 3%, sodium chloride 3%, cocamide DEA 2%, acrylic acid (ester) copolymer 1%, glyceryl caprylate/caprate polyglycerin-10 esters 1%, betaine 1%, laurocapram 0.05%, 3-O-ethyl ascorbic acid 0.2%, arbutin 0.1%, peony whitening essence 0.8%, thyme extract 0.7%, Pearl seaweed 0.6%, PEG-120-methylglucdioleate 0.6%, di (hydrogenated tallow) phthalic acid amide 0.5%, panthenol 0.5%, nicotinamide 0.5%, DMDM hydantoin 0.3%, essence 0.3%, and water 22.85%.
The preparation method is similar to example 1.
The difference from example 2 is that the amount of 3-O-ethyl ascorbic acid was increased without adding tranexamic acid.
Test example I, safety evaluation
1. Test materials: the fair, clear and white facial cleansers prepared in examples 1-3.
2. Test subjects: 60 women, 25-50 years old, have healthy skin and no history of skin allergy.
3. The test method comprises the following steps:
1) subjects were randomized into 3 groups of 20 individuals each, designated as examples 1-3;
2) selecting a qualified spot tester, placing a tested object (the fair and bright facial cleanser prepared in examples 1-3) with the length of about 1-2cm in the spot tester in a closed spot patch experimental mode, externally applying a special adhesive tape to the back of the tested object, removing the tested object after 24h, observing skin reactions after 0.5, 6, 12, 24 and 48h respectively, and recording the result according to the skin reaction grading standard in the cosmetic hygiene Specification.
4, test results:
the results showed that after each group of subjects used the fair whitening facial cleanser prepared in examples 1-3, no adverse reaction occurred on the skin when the skin reactions were observed for 0.5, 6, 12, 24, and 48 hours, indicating that the fair whitening facial cleanser prepared by the present invention was safe and non-irritant.
Test example two evaluation of whitening Effect
1. Test materials: fair and white facial cleanser prepared in examples 1-3 and comparative examples 1-3.
2. Test subjects: 120 women, 22-40 years old, with dull skin and no history of skin allergy.
3. The test method comprises the following steps:
1) subjects were randomized into 6 groups of 20 individuals each, designated as examples 1-3 and comparative examples 1-3;
2) the fair, transparent and white facial cleanser prepared in examples 1 to 3 and comparative examples 1 to 3 was used for washing the face once every day in the morning and evening for 3 months, the melanin content of the same spot on the face (the highest point of cheekbones of the cheek was selected) was measured by using a skin melanin test probe MX18 from CK company, Germany, and the average value was taken.
4. And (3) test results: the results of the melanin content test are shown in table 1.
TABLE 1 changes in melanin content
Content of melanin | Example 1 | Example 2 | Example 3 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
Before use | 492 | 487 | 501 | 488 | 496 | 476 |
After use | 360 | 323 | 356 | 370 | 384 | 371 |
Variation value | 132 | 164 | 145 | 118 | 112 | 105 |
As shown in Table 1, the fair, transparent, white and whitening facial cleanser prepared by the invention has better whitening effect. Compared with comparative examples 1-3, the fair and bright whitening facial cleanser prepared in examples 1-3 of the invention has obvious effect of reducing melanin content after being used for 3 months, which shows that the invention has reasonable and scientific compatibility and the components interact with each other to play a whitening effect.
Test example III evaluation of Water-replenishing Effect
1. Test materials: fair and white facial cleanser prepared in examples 1-3 and comparative examples 1-3.
2. Test subjects: 120 people and women, 22-40 years old, have healthy skin and no history of skin allergy.
3. The test method comprises the following steps:
1) subjects were randomized into 6 groups of 20 individuals each, designated as examples 1-3 and comparative examples 1-3;
2) after the subjects washed their faces with the fair, bright, white, cleansing milky water prepared in examples 1 to 3 and comparative examples 1 to 3, the skin moisture contents of the forehead, left face, right face and chin were measured respectively using a Fischerer SK-III skin moisture meter and arithmetically averaged, and after 24 hours, the skin moisture contents of the forehead, left face, right face and chin at the same positions were measured using a skin moisture meter and arithmetically averaged.
4. And (3) test results: the moisture content test results are shown in table 2.
TABLE 2 moisture content results
As shown in Table 2, the fair, transparent and white facial cleanser prepared by the invention has better moisturizing effect. Compared with comparative examples 1-3, the fair, transparent and white facial cleanser prepared in examples 1-3 of the invention has obvious water content increase after use, which shows that the invention has reasonable and scientific compatibility and the components interact with each other to play a role in moisturizing.
Test example four evaluation of bacteriostatic Effect
1. Test materials: fair and white facial cleanser prepared in examples 1-3 and comparative examples 1-3.
2. Test subjects: streptococcus pyogenes, Propionibacterium acnes, Staphylococcus epidermidis, Staphylococcus aureus.
3. The test method comprises the following steps:
1) preparation of test bacterial suspension
The concentration was 100. mu.L of the suspension was dropped on a control plate, and the number of recovered colonies was 1 × 104-1×109cfu/tablet.
2) Preparation of a specimen for contamination of bacteria
100 μ L of the above bacterial suspension was added dropwise to each of the test sample and the control sample, and the reaction was carried out for 20 min.
3) Respectively putting the sample slices into test tubes containing 5mL of phosphoric acid buffer solution, fully and uniformly mixing, diluting for 2-3 dilutions, putting 0.5mL into a plate, pouring 15mL of nutrient agar culture medium (bacteria) at 40-50 ℃, rotating the plate to fully and uniformly mix, turning over the plate after agar is solidified, and carrying out inverted culture at 37 ℃ for 48 hours.
4) Calculating the bacteriostasis rate by the following formula:
wherein, the X-bacteriostasis rate is percent; a-average colony number of control sample; b-average colony number of test piece.
4. And (3) test results: results of the bacteriostatic rate are shown in table 3.
TABLE 3 results of bacteriostatic rate
As shown in Table 3, the fair, transparent and white facial cleanser prepared by the invention has better bacteriostatic action. Compared with comparative examples 1-3, the fair and bright white facial cleanser prepared by the invention has better inhibiting effect on streptococcus pyogenes, propionibacterium acnes, staphylococcus epidermidis and staphylococcus aureus, and shows that the fair and bright white facial cleanser prepared by the invention can inhibit acnes and effectively protect damaged skin.
Test example five sensory evaluation test
1. Test materials: fair and white facial cleanser prepared in examples 1-3 and comparative examples 1-3.
2. Test subjects: 120 people, male and female halves, with lesions or scars on the face, 18-40 years old.
3. The test method comprises the following steps:
subjects were randomized into 6 groups of 20 individuals each, and designated as examples 1-3 and comparative examples 1-3. The fair, transparent and white facial cleansers prepared in examples 1 to 3 and comparative examples 1 to 3 were used for each group, and the use condition was evaluated after one month every morning and evening. Grading standard: the product is divided into 10 parts, the 10 parts are the best, the 0 part is the worst, and the higher the fraction is, the better the effect is.
4. And (3) test results: the sensory evaluation results are shown in Table 4.
TABLE 4 sensory evaluation results
As shown in Table 4, the fair, transparent and white cleanser prepared by the invention has better repairing effect. The repairing effect of the fair, transparent and white facial cleanser prepared in the comparative examples 1-3 is poorer than that of the fair, transparent and white facial cleanser prepared in the examples 1-3, which shows that the compatibility of the invention is reasonable and scientific, and the components interact and cooperate to play a repairing role. Meanwhile, the fair, transparent and white facial cleanser prepared by the invention also has the effects of cleaning, moisturizing and diminishing inflammation, and feels moist and fresh after being used, and no allergy phenomenon occurs to a subject.
Claims (1)
1. The fair-skinning, transparent and white facial cleanser comprises the following components in percentage by weight:
disodium lauryl sulfosuccinate 48%, sodium methyl lauroyl taurate 8%, lauramidopropyl betaine 5%, sodium laureth sulfate 3%, sodium chloride 3%, cocamide DEA 2%, acrylic acid (ester) copolymer 1%, caprylic/capric glyceride-10 esters 1%, betaine 1%, laurocapram 0.05%, 3-O-ethyl ascorbic acid 0.1%, arbutin 0.1%, peony whitening essence 0.8%, thyme extract 0.7%, pearl algae 0.6%, PEG-120-methyl glucose dioleate 0.6%, di (hydrogenated tallow) phthalic acid amide 0.5%, panthenol 0.5%, nicotinamide 0.5%, tranexamic acid 0.1%, DMDM hydantoin 0.3%, essence 0.3%, and water 22.85%;
the preparation method of the fair, transparent and white facial cleanser comprises the following steps:
s1, sequentially adding water, sodium laureth sulfate, cocamide DEA, disodium laurylsulfosuccinate, lauramidopropyl betaine, di (hydrogenated tallow) phthalic acid amide, PEG-120 methyl glucose dioleate and methyl lauroyl sodium taurate into a main pot, stirring and heating to 83 ℃, completely dissolving the materials, and preserving the temperature for 30 minutes to obtain a material A;
s2, adding the pre-dissolved acrylic acid (ester) copolymer and water into the material A obtained in the step S1, and stirring uniformly to obtain a material B;
s3, cooling the material B obtained in the step S2 to 60 ℃, adding sodium chloride, water and caprylic/capric glyceride polyglycerol-10 esters and betaine which are heated and dissolved completely in advance, and stirring uniformly to obtain a material C;
s4, cooling the material C obtained in the step S3 to 48 ℃, adding 3-O-ethyl ascorbic acid, tranexamic acid, arbutin, panthenol, laurocapram, nicotinamide, DMDM hydantoin, essence, peony whitening essence, thyme extract and pearly alga of Tanonia, and uniformly stirring to obtain a material D;
s5, cooling the material D obtained in the step S4 to 38 ℃, sampling, checking, and discharging after the material is qualified.
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CN110037937B (en) * | 2019-03-06 | 2023-05-12 | 曼秀雷敦(中国)药业有限公司 | Mild amino acid facial cleanser and preparation method thereof |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104983604A (en) * | 2015-06-30 | 2015-10-21 | 江苏奇力康皮肤药业有限公司 | Degreasing and moisturizing cleanser and preparation method thereof |
CN106176566A (en) * | 2016-08-23 | 2016-12-07 | 上海新高姿化妆品有限公司 | Cosmetic composition with white-skinned face function and preparation method thereof |
CN106265236A (en) * | 2016-08-15 | 2017-01-04 | 广州澳希亚实业有限公司 | Whitening composition and skin care product containing same |
CN106727083A (en) * | 2015-11-20 | 2017-05-31 | 周丽 | A kind of manufacture method of tree peony whitening cleansing facial milk containing |
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CN106727083A (en) * | 2015-11-20 | 2017-05-31 | 周丽 | A kind of manufacture method of tree peony whitening cleansing facial milk containing |
CN106265236A (en) * | 2016-08-15 | 2017-01-04 | 广州澳希亚实业有限公司 | Whitening composition and skin care product containing same |
CN106176566A (en) * | 2016-08-23 | 2016-12-07 | 上海新高姿化妆品有限公司 | Cosmetic composition with white-skinned face function and preparation method thereof |
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