CN106214515A - A kind of oil-containing moisturizing astringent and preparation method thereof - Google Patents
A kind of oil-containing moisturizing astringent and preparation method thereof Download PDFInfo
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- CN106214515A CN106214515A CN201610693725.2A CN201610693725A CN106214515A CN 106214515 A CN106214515 A CN 106214515A CN 201610693725 A CN201610693725 A CN 201610693725A CN 106214515 A CN106214515 A CN 106214515A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The invention belongs to cosmetic field, be specifically related to a kind of oil-containing moisturizing astringent and preparation method thereof.This oil-containing moisturizing astringent, comprise the raw material components of following percentage by weight: acceptable carrier 0.1 5% on oils and fats 0.1 10%, thickening agent 0.001 1%, polyalcohols wetting agent 1 30%, surfactant 0.001~1%, cosmeceutical, surplus is that water is to 100%.The present invention is by adding oils composition in astringent, and formula is reasonable, can form protective barrier at skin surface; the moisture making skin is difficult to evaporation and scatters and disappears, and skin absorptance is high, and moistening effect is good; can effectively prevent scaly dry skin, make the tender smooth pliable of skin water, strengthen skin elasticity.Comparing common astringent more moist, skinfeel is more soft and moist, and moisturizing effect is more more longlasting than common astringent.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to the moisturizing astringent being not required to emulsifying homogeneous and the system thereof of a kind of oil-containing
Preparation Method.
Background technology
Now astringent major part the most on the market is transparent water preparation, contains only water soluble humectants, and water solublity moisturizing
Agent basic function brings the replenishing water and preserving moisture effect of skin short time, and along with the volatilization of moisture, facial skin quickly can become
Drier.We need instantaneous moisturizing can have again the astringent of permanent moisturizing effect, reaches real moisturizing effect
Really.
At present, there is not yet the moisturizing astringent Related product being not required to emulsifying homogeneous or the document report of oil-containing.
Summary of the invention
In order to overcome the defect of prior art, the invention provides a kind of oil-containing moisturizing astringent and preparation method thereof.
Therefore, it is an object of the invention to provide a kind of oil-containing moisturizing astringent and preparation method thereof.
In order to solve above-mentioned technical problem, the technical solution used in the present invention is as follows:
A kind of oil-containing moisturizing astringent of the present invention, comprises the raw material components of following percentage by weight:
Described oils and fats is natural oil or synthetic ester oil;Wherein, described natural plant grease selected from squalane, olive oil,
Macadimia nut oil, argan oil, almond oil, shea butter, Oleum Vitis viniferae etc.;Preferably, described natural plant grease is
Macadimia nut oil, the mixture of Oleum Vitis viniferae.Described synthetic ester oil selected from Parleam, caprylic/capric triglyceride,
C12-15 alkyl benzoate, hydrogenated polydecene, polydimethylsiloxane, ethylhexyl palmitate, isopropyl myristate, poly-
Dimethyl siloxane, phenyl trimethicone, ring five polydimethylsiloxane, cyclohexasiloxane etc.;Preferably, described conjunction
One-tenth oils and fats is Parleam, polydimethylsiloxane, the mixture of ring five polydimethylsiloxane.
Described surfactant is Natrulon H-10 laurate or Natrulon H-10 myristinate.
Described thickening agent is selected from carbomer, xanthan gum, hydroxyethyl cellulose, ammonium acryloyldime-thyltaurate/ethylene pyrrole
Pyrrolidone copolymer, carrageenan, 2-(Acryloyloxy)ethanol/sodium acryloyldimethyl taurate copolymers, sodium polyacrylate, polypropylene
Acid esters cross linked polymer-6, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer (PEMULEN TR-1) etc..Excellent
Choosing, described thickening agent is carbomer, xanthan gum, hydroxyethyl cellulose and acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters
The mixture of cross linked polymer.
Described polyalcohols wetting agent is selected from glycerol, 1,3 butylene glycol, glycine betaine, 1,3-propylene glycol, dipropylene glycol, poly-second
Glycol-8, Polyethylene Glycol-32, Sorbitol etc..Preferably, described polyalcohols wetting agent is glycerol, 1,3 butylene glycol and sweet
The mixture of dish alkali.
On described cosmeceutical, acceptable carrier is selected from metal-chelator, pH adjusting agent (sodium hydroxide, citric acid, lemon
Lemon acid sodium etc.), essence, preservative (methyl parahydroxybenzoate, phenoxyethanol, parahydroxyacet-ophenone, benzoic acid, potassium sorbate,
Sodium benzoate, benzyl alcohol, chlorphenesin etc.), moisturizing antioxidation isoreactivity material (saccharide isomers, Semen Coicis extract,
Herba portulacae extract, Semen Pisi sativi extract, olive leaf extract, Flos Chrysanthemi extract, Echinacea purpurea Moench flower/leaf/stem extract, flesh
Peptide, hydrolytic collagen) etc..
Described metal-chelator is EDTA-2Na.
Preferably, described oil-containing moisturizing astringent, comprise the raw material components of following percentage by weight:
The second object of the present invention is providing the preparation method of above-mentioned oil-containing moisturizing astringent, including:
(1) by surfactant and part polyalcohols wetting agent mixing and stirring, stirring adds oils and fats, and mixing is all
Even, prepare prefabricated oil phase, standby;Wherein, described part polyalcohols wetting agent accounts for the 1-of polyalcohols wetting agent gross weight
5%;
(2) water and thickening agent stirring and dissolving is uniform, be heated to 85 DEG C continuously stirred 20-50 minute, the most while stirring
Being cooled to less than 45 DEG C, addition residue polyalcohols wetting agent 10-20r/min stirring continues for 10-20 minute to mix homogeneously
Continuous cooling;
(3) it is cooled to 25-40 DEG C, is slowly homogeneously added into prefabricated oil phase prepared by step (1), and on cosmeceutical
Acceptable carrier, after stirring, to obtain final product.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention is by adding oils composition in astringent, and formula is reasonable, can form protective barrier at skin surface,
The moisture making skin is difficult to evaporation and scatters and disappears, and skin absorptance is high, and moistening effect is good, can effectively prevent scaly dry skin, make skin water
Tender smooth pliable, strengthens skin elasticity.Comparing common astringent more moist, skinfeel is more soft and moist, and moisturizing effect ratio is general
Logical astringent is more longlasting.
By experimental test, the moisturizing astringent of the present invention will not make skin the situation such as allergy, inflammation, safety non-toxic occur
Side effect, makes skin beauty water tender smooth, fine and smooth, lubricious glossy, makes the flexible health of skin, instant effect.
The preparation method of the present invention is simple, and economic benefit is friendly, is suitable to commercial introduction application.
Accompanying drawing explanation
Fig. 1 is the moistening effect evaluation figure of embodiment 4.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described.Should be understood that following example are merely to illustrate this
Invent not for limiting the scope of the present invention.
In following example, raw materials used all by commercially available acquisition.
Embodiment 1 oil-containing moisturizing astringent
The formula (percentage by weight) of the oil-containing moisturizing astringent in the present embodiment is as follows:
The preparation technology of the oil-containing moisturizing astringent in the present embodiment is as follows:
The most prefabricated oil phase: by Natrulon H-10 laurate and the glycerol mixing and stirring of 1%, stirring adds ring five and gathers
Dimethyl siloxane, mix homogeneously, standby.
2., by water and EDTA-2Na, PEMULEN TR-1, xanthan gum, dispersed with stirring is uniform, is heated to 85 DEG C, continues stirring
30 minutes.
3. it is cooled to 45 DEG C, adds 1,3 butylene glycol, residue glycerol (glycerol of i.e. 9%), glycine betaine, PEG-8,10-
20r/min stirs 10-20 minute to mix homogeneously, continuation cooling.
4. being cooled to 40 DEG C, add prefabricated oil phase, preservative, essence, 10-20r/min stirs 10-20 minute to mixing all
Even, cooling.
5. being cooled to 32 DEG C, add citric acid, sodium citrate, stirring and dissolving is uniform, adds sodium hydroxide, and stirring is all
Even, allotment terminates.
Embodiment 2 oil-containing moisturizing astringent
The formula (percentage by weight) of the oil-containing moisturizing astringent in the present embodiment is as follows:
The preparation technology of the oil-containing moisturizing astringent in the present embodiment is as follows:
The most prefabricated oil phase: by Natrulon H-10 laurate and the glycerol mixing and stirring of 1%, stirring adds squalane,
Mix homogeneously, standby.
2., by water and EDTA-2Na, PEMULEN TR-1, xanthan gum, dispersed with stirring is uniform, is heated to 85 DEG C, continues stirring
30 minutes.
3. it is cooled to 45 DEG C, adds 1,3 butylene glycol, residue glycerol (glycerol of i.e. 9%), glycine betaine, PEG-8,10-
20r/min stirs 10-20 minute to mix homogeneously, continuation cooling.
4. being cooled to 40 DEG C, add prefabricated oil phase, preservative, essence, 10-20r/min stirs 10-20 minute to mixing all
Even, cooling.
5. being cooled to 32 DEG C, add citric acid, sodium citrate, stirring and dissolving is uniform, adds sodium hydroxide, and stirring is all
Even, allotment terminates.
Embodiment 3 oil-containing moisturizing astringent
The formula (percentage by weight) of the oil-containing moisturizing astringent in the present embodiment is as follows:
The preparation technology of the oil-containing moisturizing astringent in the present embodiment is as follows:
The most prefabricated oil phase: by Natrulon H-10 laurate and the glycerol mixing and stirring of 1%, it is hard that stirring adds Australia
Fruit oil, mix homogeneously, standby.
2., by water and EDTA-2Na, PEMULEN TR-1, xanthan gum, dispersed with stirring is uniform, is heated to 85 DEG C, continues stirring
30 minutes.
3. it is cooled to 45 DEG C, adds 1,3 butylene glycol, residue glycerol (glycerol of i.e. 9%), glycine betaine, PEG-8,10-
20r/min stirs 10-20 minute to mix homogeneously, continuation cooling.
4. being cooled to 40 DEG C, add prefabricated oil phase, preservative, essence, 10-20r/min stirs 10-20 minute to mixing all
Even, cooling.
5. being cooled to 32 DEG C, add citric acid, sodium citrate, stirring and dissolving is uniform, adds sodium hydroxide, and stirring is all
Even, allotment terminates.
Embodiment 4 oil-containing moisturizing astringent moisturizing contrast test
Choose the moisturizing astringent (choosing the formula of embodiment 1, remove oils composition as a comparison case) of not oil-containing, contain
Oil moisturizing astringent contrast (formula of embodiment 1), chooses 10 volunteers and tests, and same tester cleans facial skin
After, dry, with hands, astringent is patted on facial skin.Every left face of bit test person uses the astringent of not oil-containing, and right face makes
With the astringent of oil-containing.Then the moisture of skin measuring instrument that COURAGE+KHAZAKA (CK) company of Germany produces is used
(Cornemeter CM825) face left and right to experimenter carries out keratodermatitis moisture determination, and result is as shown in table 1 and Fig. 1.
Table 1, moistening effect comparing result
From table 1 and Fig. 1 it can be seen that the astringent of oil-containing instant replenishing water and preserving moisture effect is slightly better than the astringent of not oil-containing,
But from replenishing water and preserving moisture long-lasting for, the astringent of oil-containing is substantially better than the astringent of not oil-containing.
Embodiment 5 oil-containing moisturizing astringent moisture-keeping efficacy is evaluated
The oil-containing moisturizing astringent actually used efficacy assessment method of the present invention is as follows: choose 12 volunteers as tested
Person, wherein 6 men and 6 Mies, age bracket is 20~50 years old, uses one week oil-containing according to embodiment 3 preparation continuously
Moisturizing astringent product (using method: sooner or later after face cleaning, by normal skin protection program, uses astringent and other skin care item), one
Zhou Hou, is estimated astringent properties according to actually used impression.
Evaluation item includes: skin moisture content, sebum secretion amount, skin coarseness, enlarged pores number etc..
Pass judgment on rule as follows: moisture content of skin moisture of skin measuring instrument (Cornemeter CM825) is tested, and sebum divides
The amount of secreting, skin coarseness, enlarged pores number are described according to practical situation assessment by experimenter oneself, and result is as shown in table 2.
Table 2, oil-containing moisturizing astringent efficacy assessment
Being found out by the result of table 2, after using one week oil-containing astringent, moisture content of skin has significantly increase, and sebum
Secretory volume has reduced, and the most smooth exquisiteness of skin, additionally pore also has the trend reduced.Illustrate that the astringent of oil-containing is to changing
Kind skin serves good effect.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.The technology of the industry
Personnel, it should be appreciated that the present invention is not restricted to the described embodiments, simply illustrating this described in above-described embodiment and description
The principle of invention, the present invention also has various changes and modifications without departing from the spirit and scope of the present invention, and these become
Change and improvement both falls within scope of the claimed invention.Claimed scope by appending claims and
Equivalent defines.
Claims (10)
1. an oil-containing moisturizing astringent, comprises the raw material components of following percentage by weight:
A kind of oil-containing moisturizing astringent the most according to claim 1, it is characterised in that: described oils and fats is natural oil or conjunction
Become oils and fats;Wherein, described natural plant grease selected from squalane, olive oil, macadimia nut oil, argan oil, almond oil,
One or more in shea butter, Oleum Vitis viniferae;Described synthetic ester oil is selected from Parleam, caprylic/capric triglycerin
Ester, C12-15 alkyl benzoate, hydrogenated polydecene, polydimethylsiloxane, ethylhexyl palmitate, myristic acid isopropyl
One in ester, polydimethylsiloxane, phenyl trimethicone, ring five polydimethylsiloxane, cyclohexasiloxane or
Several.
A kind of oil-containing moisturizing astringent the most according to claim 1, it is characterised in that: described surfactant is for poly-sweet
Oil-10 laurates or Natrulon H-10 myristinate.
A kind of oil-containing moisturizing astringent the most according to claim 1, it is characterised in that: described thickening agent selected from carbomer,
Xanthan gum, hydroxyethyl cellulose, ammonium acryloyldime-thyltaurate/nvp copolymer, carrageenan, acrylic acid hydroxyl second
Ester/sodium acryloyldimethyl taurate copolymers, sodium polyacrylate, polyacrylate cross linked polymer-6, acrylic acid (ester) class/
One or more in C10-30 alkylol acrylamide acid esters cross linked polymer.
A kind of oil-containing moisturizing astringent the most according to claim 1, it is characterised in that: described polyalcohols wetting agent is selected from
In glycerol, 1,3 butylene glycol, glycine betaine, 1,3-propylene glycol, dipropylene glycol, PEG-8, Polyethylene Glycol-32, Sorbitol
One or more.
6. a kind of oil-containing moisturizing astringent as claimed in claim 1, it is characterised in that: acceptable load on described cosmeceutical
One or more in metal-chelator, pH adjusting agent, essence, preservative, moisturizing anti-oxidation active substance of body.
7. a kind of oil-containing moisturizing astringent as claimed in claim 6, it is characterised in that: described preservative is selected from para hydroxybenzene first
One in acid methyl ester, phenoxyethanol, parahydroxyacet-ophenone, benzoic acid, potassium sorbate, sodium benzoate, benzyl alcohol, chlorphenesin
Or it is multiple.
8. a kind of oil-containing moisturizing astringent as claimed in claim 6, it is characterised in that: described moisturizing anti-oxidation active substance selects
From selected from saccharide isomers, Semen Coicis extract, Herba portulacae extract, Semen Pisi sativi extract, olive leaf extract, Flos Matricariae chamomillae
One or more in flower extract, Echinacea purpurea Moench flower/leaf/stem extract, carnosine, hydrolytic collagen.
9. a kind of oil-containing moisturizing astringent as claimed in claim 1, it is characterised in that: described oil-containing moisturizing astringent, comprise
The raw material components of following percentage by weight:
10. according to the preparation method of the oil-containing moisturizing astringent described in any one of claim 1-9, including:
(1) by surfactant and part polyalcohols wetting agent mixing and stirring, stirring adds oils and fats, mix homogeneously, system
Obtain prefabricated oil phase, standby;Wherein, described part polyalcohols wetting agent accounts for the 1-5% of polyalcohols wetting agent gross weight;
(2) water and thickening agent stirring and dissolving is uniform, be heated to 85 DEG C continuously stirred 20-50 minute, cool down the most while stirring
To less than 45 DEG C, addition residue polyalcohols wetting agent 10-20r/min stirring continues cold to mix homogeneously in 10-20 minute
But;
(3) it is cooled to 25-40 DEG C, is slowly homogeneously added into prefabricated oil phase prepared by step (1), and can connect on cosmeceutical
The carrier being subject to, after stirring, to obtain final product.
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CN114762660A (en) * | 2021-01-12 | 2022-07-19 | 新生活化妆品科技(上海)有限公司 | Cosmetic composition and cosmetic |
CN114788804A (en) * | 2021-06-04 | 2022-07-26 | 广州一一生物技术有限公司 | High-efficiency moisturizing double-layer water and preparation method thereof |
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