CN106473099A - Functional food or alternative tea that effect improves - Google Patents
Functional food or alternative tea that effect improves Download PDFInfo
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- CN106473099A CN106473099A CN201610888845.8A CN201610888845A CN106473099A CN 106473099 A CN106473099 A CN 106473099A CN 201610888845 A CN201610888845 A CN 201610888845A CN 106473099 A CN106473099 A CN 106473099A
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- KRDDWVMTVMSFAV-UHFFFAOYSA-N [S].OC(=O)C=C Chemical compound [S].OC(=O)C=C KRDDWVMTVMSFAV-UHFFFAOYSA-N 0.000 description 1
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- 239000002250 absorbent Substances 0.000 description 1
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- 239000000853 adhesive Substances 0.000 description 1
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- 150000001298 alcohols Chemical class 0.000 description 1
- 229940072056 alginate Drugs 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 125000003368 amide group Chemical group 0.000 description 1
- 150000001412 amines Chemical class 0.000 description 1
- UIERETOOQGIECD-ARJAWSKDSA-N angelic acid Chemical compound C\C=C(\C)C(O)=O UIERETOOQGIECD-ARJAWSKDSA-N 0.000 description 1
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- 150000001450 anions Chemical class 0.000 description 1
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- 230000000903 blocking effect Effects 0.000 description 1
- 210000004556 brain Anatomy 0.000 description 1
- 210000000481 breast Anatomy 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 150000001244 carboxylic acid anhydrides Chemical class 0.000 description 1
- 235000010418 carrageenan Nutrition 0.000 description 1
- 229920001525 carrageenan Polymers 0.000 description 1
- 239000000679 carrageenan Substances 0.000 description 1
- 229940113118 carrageenan Drugs 0.000 description 1
- 229920006317 cationic polymer Polymers 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 229930016911 cinnamic acid Natural products 0.000 description 1
- 235000013985 cinnamic acid Nutrition 0.000 description 1
- GTZCVFVGUGFEME-IWQZZHSRSA-N cis-aconitic acid Chemical compound OC(=O)C\C(C(O)=O)=C\C(O)=O GTZCVFVGUGFEME-IWQZZHSRSA-N 0.000 description 1
- HNEGQIOMVPPMNR-IHWYPQMZSA-N citraconic acid Chemical compound OC(=O)C(/C)=C\C(O)=O HNEGQIOMVPPMNR-IHWYPQMZSA-N 0.000 description 1
- 229940018557 citraconic acid Drugs 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000002079 cooperative effect Effects 0.000 description 1
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- 238000007598 dipping method Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000005293 duran Substances 0.000 description 1
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- 241000411851 herbal medicine Species 0.000 description 1
- 229920006158 high molecular weight polymer Polymers 0.000 description 1
- 239000000416 hydrocolloid Substances 0.000 description 1
- 238000005213 imbibition Methods 0.000 description 1
- 125000001841 imino group Chemical group [H]N=* 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
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- 239000011976 maleic acid Substances 0.000 description 1
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
- 239000001771 mentha piperita Substances 0.000 description 1
- HNEGQIOMVPPMNR-NSCUHMNNSA-N mesaconic acid Chemical compound OC(=O)C(/C)=C/C(O)=O HNEGQIOMVPPMNR-NSCUHMNNSA-N 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- LVHBHZANLOWSRM-UHFFFAOYSA-N methylenebutanedioic acid Natural products OC(=O)CC(=C)C(O)=O LVHBHZANLOWSRM-UHFFFAOYSA-N 0.000 description 1
- HNEGQIOMVPPMNR-UHFFFAOYSA-N methylfumaric acid Natural products OC(=O)C(C)=CC(O)=O HNEGQIOMVPPMNR-UHFFFAOYSA-N 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 235000019426 modified starch Nutrition 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 235000014571 nuts Nutrition 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 150000002894 organic compounds Chemical class 0.000 description 1
- 210000004681 ovum Anatomy 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 125000002467 phosphate group Chemical group [H]OP(=O)(O[H])O[*] 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920002401 polyacrylamide Polymers 0.000 description 1
- 238000006068 polycondensation reaction Methods 0.000 description 1
- 239000001205 polyphosphate Substances 0.000 description 1
- 235000011176 polyphosphates Nutrition 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
- UIIIBRHUICCMAI-UHFFFAOYSA-N prop-2-ene-1-sulfonic acid Chemical compound OS(=O)(=O)CC=C UIIIBRHUICCMAI-UHFFFAOYSA-N 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- 238000010526 radical polymerization reaction Methods 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000002829 reductive effect Effects 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 125000000467 secondary amino group Chemical group [H]N([*:1])[*:2] 0.000 description 1
- 235000008113 selfheal Nutrition 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 150000003385 sodium Chemical class 0.000 description 1
- UAJTZZNRJCKXJN-UHFFFAOYSA-M sodium;2-dodecoxy-2-oxoethanesulfonate Chemical compound [Na+].CCCCCCCCCCCCOC(=O)CS([O-])(=O)=O UAJTZZNRJCKXJN-UHFFFAOYSA-M 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 125000001302 tertiary amino group Chemical group 0.000 description 1
- 229940126680 traditional chinese medicines Drugs 0.000 description 1
- GTZCVFVGUGFEME-UHFFFAOYSA-N trans-aconitic acid Natural products OC(=O)CC(C(O)=O)=CC(O)=O GTZCVFVGUGFEME-UHFFFAOYSA-N 0.000 description 1
- WBYWAXJHAXSJNI-VOTSOKGWSA-N trans-cinnamic acid Chemical compound OC(=O)\C=C\C1=CC=CC=C1 WBYWAXJHAXSJNI-VOTSOKGWSA-N 0.000 description 1
- NLVXSWCKKBEXTG-UHFFFAOYSA-N vinylsulfonic acid Chemical compound OS(=O)(=O)C=C NLVXSWCKKBEXTG-UHFFFAOYSA-N 0.000 description 1
- 210000001835 viscera Anatomy 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F3/00—Tea; Tea substitutes; Preparations thereof
- A23F3/34—Tea substitutes, e.g. matè; Extracts or infusions thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
Present invention is disclosed a kind of edible or/and pharmaceutical (powder) product (/ composition) of performance improvement, the product (/ composition) contains particulate matter (or powder) the I and AAP value one (or more) hydrophilic polymer (particulate matter (or powder)) II higher than particulate matter (or powder) I of polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer comprising one (or more).The product (/ composition) dispersive property improves, particularly following performance improvement:Food synthetic performance that caking capacity, powder are not made under stripping property of the active ingredient in (warm) water, powder high humidity environment in dispersiveness of the powder in (warm) water, powder etc.).
Description
Technical field
The present invention relates to functional food (or alternative tea).It particularly relates to effect improves or enhanced feature food
Product (or alternative tea).
Technical background
The products (or its intermediate products) such as food, feed, health treatment (or functional food (or alternative tea)), medicine,
Relate generally to powder.Powder in these food or functional food contain polysaccharide (particularly starch, viscous polysaccharide) class,
Peptides or high molecular polymer and small molecule carbohydrate, low molecule carbohydrate, amino acid, the low molecule with high viscosity such as protein-based
The hygroscopic component such as peptide, thus, these powders have stronger hygroscopicity, water imbibition, after powder moisture absorption, water suction under mobility
Drop, caking, stickness, this will make these (powder) products using front or/and using when be difficult to keep preferable dispersity, from
And there are various problems.The performance of these (powder) products, often directly related with its degree of scatter.For example using front
Or/and after luming during use, will result in powder and be difficult to disperse, there is edible difficult, mouthfeel decline, bioactive ingredients and be difficult to
The problems such as dissolution, biologically active decline, so as to directly affect the performance of its effect.
Polysaccharide (particularly starch, viscous polysaccharide) class, peptides in particularly above-mentioned powder or the macromolecule such as protein-based
Polymeric adhesive material, after contact with water when using can water absorption and swelling, easy generation " gel blockage " effect, particularly in pressure-bearing
(reaction force of other periphery powders " four walls " when expanding, can be subject to) under state, herein " gel blockage " effect (lower section
In implication herewith) refer to that the hydrophilic polymer particles for contacting swellable with water are wetted and swelling, it is suppressed that fluid is to grain
Other regions such as interior shifting of son the phenomenon for inhibiting particle swelling further are so-called " not with the face that opens just as being formed
The phenomenon of group ", will be more serious particularly under artesian condition.After the main cause of generation gel blocking phenomenon is swelling, special
It is not that the space between particle is reduced and viscosity increases under artesian condition.
After there is " gel blockage " effect, moisture is difficult to reach powder nexine region, the active component of nexine region powder
It is difficult to ooze out by moisture, thus, functional food effect declines.
In theory, powder granule is thinner, and particularly after ultra micro efflorescence, functional food effect is more beneficial for playing, however,
More thin easier generation the problems referred to above of powder granule in reality, particularly after ultra micro efflorescence, the decline of functional food effect is more, more
It is difficult to play.
Therefore, also needing to effect in reality improves or enhanced functional food.
Following patent is provided as reference.
Chinese patent CN1079698C (or US5714156) is disclosed has different AAP values by mixing two classes
The hydrogel of (Absorption Against Pressure value, sucting wet gel material absorb the important parameter of the ability of liquid)
Type particle, can obtain cooperative effect, and wherein the AAP value of mixture is predicted than the weight percent of component based on mixture
Value is high.There is AAP value that different TCC values can make mixture with the aquogel type particle of identical AAP value unexpectedly by mixing two classes
Increase.But the patent does not refer to the application in food, feed, health treatment, medicine and other fields.
Content of the invention
The present invention relates to a kind of effect improve or strengthen (stripping property of in other words, contained (effective) composition in () water (/
Amount) improve or strengthen) functional food (or alternative tea), the functional food (or alternative tea) contains comprising one (or more)
Have polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer with physiologically active (or
Pharmacological action) food grain thing (or powder) I and AAP value (i.e. Absorption Against Pressure value, or claim to hold
Compression swelling (swelling) value, the Swelling Capacity under the value reflection polymer renitency, similarly hereinafter) than the food grain thing (or powder)
The one (or more) of I high (it is preferred that 1.25 times of height (containing)) is (it is preferred that water-insoluble (including " omiting on ordinary meaning
Molten ", " slightly soluble ", the meaning such as " almost insoluble " or " fairly insoluble ", " water-insoluble " implication is all herewith below)) hydrophilic polymeric
Thing (particulate matter (or powder)) II.
The present invention relates to a kind of use of (it is preferred that non-water-soluble) hydrophilic polymer (particulate matter (or powder)) II
On the way, hydrophilic polymer (particulate matter (or powder)) II is used for improving or strengthening containing polysaccharide (spy comprising one (or more)
Starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer with biologically active (or pharmacologically active)
Food grain thing (or powder) I functional food (or alternative tea) effect, strengthen the functional food (or generation in other words
With tea) in stripping property of contained (effective) composition in () water (/ measure), above-mentioned hydrophilic polymer (particulate matter (or powder))
II AAP value is higher (it is preferred that 1.25 times of height (containing)) than the food grain thing (or powder) I.
More preferably, the AAP value of II particle of above-mentioned hydrophilic polymer is at least the AAP of above-mentioned food grain thing (or powder) I
1.5 (preferably 2, more preferably 3, more preferably 5, more preferably 10, most preferably 15) times of value.
It is preferred that above-mentioned food grain thing (or powder) I is AAP with respect to the absorption value under a pressure1, above-mentioned hydrophilic poly-
II particle of compound is AAP with respect to the absorption value under a pressure2, the two mixture with respect to the absorption value under a pressure be
AAP1,2, AAP1,2> (w AAP1+p·AAP2) (more preferably >=1.25 (w AAP1+p·AAP2)), wherein, w is above-mentioned edible
Particulate matter (or powder) I accounts for the percentage of above-mentioned food grain thing (or powder) I and II particle gross weight of above-mentioned hydrophilic polymer,
P accounts for above-mentioned food grain thing (or powder) I and II particle gross weight of above-mentioned hydrophilic polymer for II particle of above-mentioned hydrophilic polymer
Percentage, and p+w=1, above-mentioned absorption value AAP with respect to pressure be in 21.1g/cm2(0.3psi) and 70.3g/cm2
(1psi) between, preferably in 35.2g/cm2(0.5psi) and 56.2g/cm2(0.8psi) measurement, (explanation under the pressure between:
For comparativity, the measure of all absorption values AAP for comparing is carried out under identical conditions (pressure) herein).
It is preferred that TCC value of the TCC value of II particle of above-mentioned hydrophilic polymer higher than above-mentioned food grain thing (or powder) I,
The AAP value of the mixture of the two is higher than any one in above-mentioned food grain thing (or powder) I and II particle of above-mentioned hydrophilic polymer
AAP value, the wherein described absorption value with respect to pressure be in 21.1g/cm2(0.3psi) and 70.3g/cm2Between (1psi),
It is preferred that in 35.2g/cm2(0.5psi) and 56.2g/cm2(0.8psi) measurement under the pressure between.
It is preferred that the weight of above-mentioned food grain thing (or powder) I accounts for above-mentioned food grain thing (or powder) I and above-mentioned parent
At least the 10% of II particle gross weight of aqueous polymer.
It is preferred that half mass particle size of above-mentioned food grain thing (or powder) I is substantially not less than above-mentioned hydrophilic poly-
Half mass particle size of II particle of compound.
It is preferred that the difference at least 2 of the AAP value of above-mentioned hydrophilic polymer II and above-mentioned food grain thing (or powder) I is (preferably
5, more preferably 10, more preferably 20, most preferably 40) gram gram.
It is preferred that in 49.2g/cm2(0.7psi), under pressure, the AAP value of II particle of above-mentioned hydrophilic polymer is at least 8
(preferably 15, more preferably 25) gram gram.
It is preferred that the TCC value of II material of above-mentioned hydrophilic polymer is at least 10 (preferably 20, more preferably 30) gram gram.
It is preferred that it is preferred that the content of above-mentioned food grain thing (or powder) I is in above-mentioned food grain thing (or powder) I
With 10% and the 97% of II material gross weight of above-mentioned hydrophilic polymer (preferably 20% and 90%, more preferably 20% and 85%, more excellent
Select 30% and 75%, most preferably 30% and 65%) between.
It is preferred that half mass particle size (or particle diameter) of II particle of above-mentioned hydrophilic polymer is less than 212 microns (70 mesh),
Preferably less than 106 microns (140 mesh), more preferably less than 53 microns (270 mesh), more preferably less than 20 microns (700 mesh), most preferably
Ground is less than 10 microns (1250 mesh);Half mass particle size (or particle diameter) of above-mentioned food grain thing (or powder) I particle is less than
300 microns (50 mesh), preferably less than 150 microns (100 mesh), more preferably less than 75 microns (200 mesh), more preferably less than 32 is micro-
Rice (450 mesh), most preferably less than 18 microns (800 mesh).
During " TTC value " (Teabag Centrifuge Capacity) and " AAP value " definition and assay method see below
Determination test method part.
Have been found that by adding a fraction of inhomogeneity AAP value higher (it is preferred that half mass particle size is also less)
Aquogel type particle (hydrophilic polymer II), be particularly conducive to improve low AAP value aquogel type material (food grain thing (or
Powder) I) AAP value.Do not wish to be bound by any theory restrictions, it is believed that have higher AAP value particle absorb liquid when than AAP value
The ability of relatively low " compared with soft " particle deformation resistant is big.In the mixture, the particle of less, " harder " keeps open architecture and prevents
Impermeability barrier is formed when " softer ", larger particle expansion, prevent or prevents generation " gel blockage " effect.
Based on this, it has unexpectedly been found that, add the hydrophilic polymer II of higher AAP value to be prevented from or prevent low AAP value
Food grain thing containing polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer (or
Powder) I generation " gel blockage " effect, so as to improve or strengthen effect (in other words, improvement of functional food (or alternative tea)
Or strengthen stripping property (/ amount) of (effective) composition contained therein in () water).
Specific embodiment
Containing having for polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer
The food grain thing (or powder) I of physiologically active (or pharmacological action)
For the present invention containing polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based macromolecule
The food grain thing (or powder) I with physiologically active (or pharmacological action) of polymer is generally selected from containing polysaccharide (particularly
Starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer with physiologically active (or pharmacological action) can
The crushed material or powder at edible or/and pharmaceutical plant, animal or bacterium algae or its edible or/and pharmaceutical position, or
Which contains the extract powder of polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer.
Above-mentioned plant edible or/and pharmaceutical position include but do not limit seed, fruit, stem (particularly fleshy stem, " i.e. with respect to
For wooden, non-wood, non-highly Fibrotic, below all herewith ", especially underground (meat) stem:Stem tuber is (as Ma Ling
Potato, jerusalem artichoke, Chinese artichoke, rhizome (as ginger, lotus rhizome), bulb (as arrowhead, taro), bulb class (as garlic, lily)), root (especially
Be fleshy root, especially (meat) root tuber such as yam bean and sweet potato), leaf, flower (or pollen (being particularly the crushed material of its broken wall))
Or (meat) plant is all, the edible of above-mentioned fungi or/and pharmaceutical position include but do not limit mycelium, fructification, spore
Sub- powder (being particularly the crushed material of its broken wall), algae thallus, algae bulbous body, algae rhizomorph or bacterium algae are all, and above-mentioned animal can
Edible or/and pharmaceutical position include but do not limit muscle, internal organ, bone, skin, blood, marrow, brains, milk or breast, ovum (or
Egg), seminal fluid or animal all.Edible or/and pharmaceutical plant, animal or bacterium algae for the present invention is so long as not being on the verge of
Species extinction or (wildlife) that be protected by law.
Above-mentioned containing polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer
The edible with biologically active (pharmacologically active) or/and pharmaceutical plant, animal or bacterium algae or its edible or/and doctor
Including but not limited to (I preferred embodiment of particulate matter (or powder) for the present invention includes but does not limit medicinal position preferred embodiment
In following traditional Chinese medicines material (crushed material or powder)):
1), fruit, kind subclass Chinese medicine
Example such as, pericarpium zanthoxyli, the seed of feather cockscomb, semen allii tuberosi, fennel seeds, rice sprout, semen armeniacae amarae, fructus polygoni orientalis, waxgourd seed, waxgourd peel,
Rde bean, linseed, the seed of Chinese dodder, tribulus terrestris, puncture vine, the shell of areca nut, in one's early teens, polished rice, Snakegourd Fruit, cassia seed, Psoralea corylifolia, fire fiber crops
Benevolence, cowpea, tangerine seed, fig, Chinese toona fruit, sandlwood, Kiwi berry, raspberry, Chinese wild pepper, the seed of Oriental arborvitae, evodia rutaecarpa, perilla seed, castor
Pockmarks, longan seed, Chinese honey locust, peanut, frutus cnidii, glutinous rice, franchet groundcherry persistent calyx or fruit, capsicum, tomato, mountain Wu's cornel, fruit Exocarpium Citri Grandis, Wang Buliu
Row, black nightshade seed, Chinese torreyanut, semen astragali complanati, plantain seed, the fruit of Rangoon creeper, sword bean, dried orange peel, rascal, Java brucea, dark plum, Chinese prickly ash, balsam pear, pomegranate
Skin, vomiting nut, dillseed, Perilla frutescens, Semen Lablab Album, Chinese hawthorn seed, barley, citron, fiveleaf akebia fruit, sea-buckthorn, kaladana, lepidium seed, oil
The seeds of a tung oil tree, myrobalan, pepper, light wheat, calyx-shaped daphniphyllum fruit, fructus amomi, Oroxylum indicum, trachycarpi,fructus, Amomum cardamomum, malt, fructus alpiniae oxyphyllae, nutmeg,
Mace, coffee senna fruit or seed, fructus gleditsiae, cassia bud, great burdock achene, radish seed, fructus viticis, Gui Ding, gingko, wax gourd, the fruit of Cherokee rose,
Skin, Fructus meliae toosendan, Momordica grosvenori, the achene of Siberian cocklebur, spina date seed, date, Exocarpium Citri Rubrum, lichee, arillus longan, grape, cherry, coix seed, Yu Li
Benevolence, crotons, the fruit of glossy privet, mulberry fruit, Fructus Aurantii, Gorgon fruit, muskmelon pedicel, peach kernel, semen litchi, the capsule of weeping forsythia, corn stigma, watermelon peel, lotus seeds, walnut
Benevolence, selfheal, tsaoko, Chinese anise, semen brassicae, chingma abutilon seed, betel nut, the dried immature fruit of citron orange, the fruit of Chinese magnoliavine, Fructus Corni, cape jasmine, the fruit of Chinese wolfberry, wood
Melon, jujube core, Semen sesami nigrum, the sterculia seed, hawthorn, Buddha's hand, persimmon, Paper mulberry Fruit, mung bean, papaw, gumbo.
2), plant roots, stem class Chinese medicine
Example such as, Radix Angelicae Sinensis, radix scrophulariae, Dysosma versipellis, the bighead atractylodes rhizome, rhizoma dioscoreae nipponicae, radix aconiti sinensis, RADIX ACONITI KUSNEZIFFII, rattletop, Longstamen Onion Bulb, fritillaria thunbergii, mountain
Arrowhead, the root of gansui, cymose buckwheat rhizome, rhizoma arisaematis, fresh rehmannia root, Radix changii, rhizoma typhonii, rhizoma homalonemae, Kaempferia galanga, flea stop, adder-wort, Radix picrorrhizae, day
Winter, the rhizoma bolbostemmae, aster, bletilla, the rhizome of davallia, monkshood, saline cistanche, blackberry lily, Cynanchum glaucescens, rhizome of cyrtomium, root of Chinese trichosanthes, felwort, blackfruit greenbrier rhizome and leaf,
Achyranthes aspera, Alpinia japonica, RADIX PRZEWALSKIAE TANGUTICAE, the wind-weed, cynomorium songaricum, Jehol Ligusticum Rhizome, corydalis tuber, rhizoma nardostachyos, radix cynanchi atrati, Bulbus Fritillariae Cirrhosae, Morinda officinalis, henry woodbetony root, Rhizoma Sparganii,
Wild pseudo-ginseng, Bi, the tuber of stemona, airpotato yam, adenophora tetraphylla, radix glehniae, hand ginseng, stephanotis, the root of purple-flowered peucedanum, rhizoma zingiberis, Bulbus Allii Fistulosi, pseudo-ginseng, twoleaf platanthera rhizome,
Turmeric, sealwort, galangal, Rhizoma polygoni vivipari, American Ginseng, water chestnut, radix ranunculi ternati, smilax, fritillary bulb, curcuma zedoary, radix polygonati officinalis, the root of straight ladybell, the root of kudzu vine,
Polygala root, the radix paeoniae rubrathe, garlic, thizoma curculiginis, root tuber of aromatic turmeric, the fleece-flower root, decumbent corydalis tuber, rhizoma cyperi, radix ampelopsis, cogongrass rhizome, rhizoma alismatis, the tuber of dwarf lilyturf, bracketplant, rhizoma Gastrodiae,
The tuber of pinellia, Ligusticum wallichii, Chinese yam, Radix Codonopsis, ginger, radix pseudostellariae, prepared rhizome of rehmannia, rheum officinale, Radix Isatidis, pseudo-ginseng, ginseng, red ginseng, hair arrowhead, method half
Summer.
3), leaves of plants class Chinese medicine
Example such as, holly leaf, thick grass, folium lycii, folium isatidis, Japanses beauty-berry, Pittosporum glabratum Lindl. leaf, leaf mustard, chinaroot greenbrier leaf, Fallopia nervosa,
Chinese Photinia Leaf, Pu'er tea, buzhaye, bluish dogbane, mulberry leaf, folium sennae, coffee senna, Ilex Latifolia Thunb, refute greatly bone, perilla leaf, Chinese holly, knotweed
Folium isatidis, lotus leaf, thin evodia leaf, barrenwort, acute turpinia leaf, lily, peppermint, sanchi leaf, folium panacis japonici cum caule, the bark of eucommia, leek, Herba Andrographitis,
Tarragon, loguat leaf, Chinese tamarisk tops, ginkgo leaf, hairyflower actinidia root and leaf, greater celandine, gumbo.
4), plant flowers class Chinese medicine
Example such as, datlily (day lily), globe artichoke, cauliflower, broccoli, tender flower stalk, sophora flower, pollen pini, peach blossom, camellia
Flower, lilac daphne, the flower bud of lily magnolia, inular flower, sanchi flower, honeysuckle, Chinese trumpet creeper, plum blossom, Inula britannica chinensis, balsamine, mother chrysanthemum, Flos Albiziae, rose
Rare flower, flos mume, finger citron flower, Camellia nitidissima, sweet osmanthus, shrub althea flower, flores tiliae, loquat flower, lily, betelnutpalm male flower, FI puerariae, cuckoo
Flower, flower of hyacinth dolichos, stamen nelumbini, cattail pollen, lanatechead saussurea herb with flower, roselle, harlequin glorybower flower, phoenix tree flower, datura flower, gardenia, Flos Magnoliae Officinalis, egg
Flower, jasmine, flower of Panax ginseng, safflower, tussilago, tulip, safflower, wintersweet immature flower, cockscomb, rose, common bombax flower, noisy sheep
Flower, bitter citrus immature flower, globe amaranth, Flos Hibisci Mutabilis, trollflower, China rose, cloves, chrysanthemum, yulan magnolia, Jasmine, fried dough twist.
5), plant entirety Chinese medicine
Example such as, schizonepeta, coriander, bittersweet, black nightshade, Sculellaria barbata, Chinese violet, oriental wormwood, Glabrous Sarcandra Herb, corydlis bungeana, catchweed bedstraw herb,
Sweet wormwood, Artemisia japonica, centella, gerbera, Chinese celery, scouring rush, osbeckia chinensis, savatier monochasma herb, elscholtiza, waterplantain ottelia herb, salvia chinensis, Herba lygodii,
Paniculate swallowwort, lycopodium calvatum, rooted pellionia herb, water hyacinth, milk thistle, Herba Lycopi, unpleasant swallowwort herb, Pogostemon cablin, rosemary, Xi, potentilla chinensis, great Bai
Medicine, birdsfoot trefoil herb and flower, white dead nettle, Chinese mesona herb, Artemisia anomala, lopseed, little groundcherry herb or fruit, gynostemma pentaphylla, meadow pine, bitter ground courage, wartwort, flaccid knotweed herb,
Involucrate balanophora herb, Common Leafflower Herb, setose thistle, broomrape, david gentian herb, eclipta, Lemongrass, pot marigold, desmodium, Centipeda minima, small stream are yellow
Grass, Sambucus thunbergiana, rhodiola root, sensitive plant, kiss-me, affine cudweed, Common Sage Herb, wolf's milk, Canton love-pea vine, Chinese milkwort herb, pipewort, phoenix
Tail grass, acalypha copperleaf, sealwort, mock-strawberry, bitter leaves, geranium wilfordii, ciliate desert-grass, dandelion, oldenlandia diffusa, Rabdosia rubescens, potentilla discolor, little
Ji, motherwort, cordate houttuynia, ardisia japonica, Mongollian Thyme Herb, Chinese penthorum herb, eupatorium, wrinkled giant hyssop, purslane, hairyvein agrimony, short top top, Chinese lobelia, company
Money grass, Verbena officinalis, concave head amaranth, Asiatic plantain, himalayan creeper herb, field pennycress, witchweed, roxburgh anoectochilus terminal bud.
6), Homonemeae Chinese medicine
Example such as, umbellate pore furgus, glossy ganoderma, Lygodium japonicum, white fungus, tabasheer, fushen, fuling peel, poria cocos, agaric, hickory chick, five times
Son, stone-like omphalia, kelp, rainbow conk, marine alga, Lasiosphaera fenzlii, Cordyceps sinensis, Poria cocos, purple sesame.
7), animal tcm material
Sparrow meat, mutton, pig lung, cow's milk, deer horn glue, deer horn, ground bettle, cornu bubali, sea otter, pearl, tortoise plastron, tortoise plastron
Glue, dog meats, mole cricket, rhinoceros horn, mantis egg-case, sea cucumber, toad, goat's horn, pilose antler, turtle shell, jellyfish, Bungarus Parvus, oyster meat,
Centipede, Moschus, cuttlebone, cornu cerve degelatinatum, cow-bezoar, dens draconis, jellyfish, dried scallop, antelope's horn, pallas pit viper, bear gall, mother-of-pearl, honeycomb, the black tip
Snake, earthworm, snake slough, yellow-swallowtail butterfly larva, deer's sinew, toad skin, black-bone chicken, deer tire, pillworm, garter snake gall, cricket, bird's nest, snail, deer blood, white
Stiff silkworm, dog kidney, aspongopus, hedgehog skin, hippocampus, cockroach, gekko, frog, cicada slough, ant, pork tripe, the membrane of a chicken's gizzard, pork liver, Chuan Shan
First, deer's tail, cornu caprae hircus, deer kidney, nutgall, the shell of seaear, Chinese blister beetle, donkey-hide gelatin, honey, silkworm excrement, dung beetle, scorpio, leech, gecko, male
Oyster.
8), other classes contain polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymerization
The Chinese medicine with biologically active (pharmacologically active) of thing
The concentrated dry product of Tabasheer, arisaema cum bile, Divine Comedy, dried human placenta, indigo naturalis, frankincense, aloe leaf juice, catechu (catechu
Tree dry branch add water pan-fried juice concentration dry extract).
Following integration of drinking and medicinal herbs food (crushed material or powder) is preferred for above-mentioned food grain thing (or the powder of the present invention
Not) I:
Cloves, Chinese anise, sword bean, fennel seeds, field thistle, Chinese yam, hawthorn, purslane, zaocys dhumnade, dark plum, pawpaw, fire fiber crops
Benevolence, bitter orange flower, radix polygonati officinalis, Radix Glycyrrhizae, the root of Dahurain angelica, gingko, Semen Lablab Album, Flos Semen Lablab Album, arillus longan (longan), cassia seed, lily, Pork and beans
Cool, Chinese cassia tree, emblic, Buddha's hand, almond (sweet, bitter), sea-buckthorn, oyster, Gorgon fruit, Chinese prickly ash, rde bean, donkey-hide gelatin, the membrane of a chicken's gizzard, malt,
Kelp, jujube (date, wild jujube, dateplum persimmon), Momordica grosvenori, brush-cherry seed, honeysuckle, Chinese olive, cordate houttuynia, ginger (ginger, rhizoma zingiberis), trifoliate orange
Son, the fruit of Chinese wolfberry, cape jasmine, fructus amomi, the sterculia seed, Poria cocos, citron, elscholtiza, peach kernel, mulberry leaf, mulberry fruit, orange, balloonflower root, fructus alpiniae oxyphyllae, lotus
Leaf, radish seed, lotus seeds, galangal, lophatherum gracile, Fermented Soybean, chrysanthemum, witloof, SEMEN SINAPIS ALBAE, sealwort, purple perilla, purple perilla seed, the root of kudzu vine, black
Sesame, black pepper, the sophora bud, sophora flower, dandelion, honey, Chinese torreyanut, spina date seed, fresh Rhizoma Imperatae, fresh Rhizoma Phragmitis, pallas pit viper, orange peel, peppermint,
Coix seed, Longstamen Onion Bulb, raspberry, wrinkled giant hyssop, pueraria root powder, Cordyceps militaris.
Following food (crushed material or powder) with health role is more preferably used for the above-mentioned food grain of the present invention
Thing (or powder) I:
Ginseng, folium panacis japonici cum caule, panax ginseng fruit, pseudo-ginseng, smilax, setose thistle, the fruit of glossy privet, Fructus Corni, radix cyathulae, Bulbus Fritillariae Cirrhosae, Ligusticum wallichii,
Red deer tire, cervus elaphus linnaeus, red deer bone, the red sage root, cortex acanthopanacis, the fruit of Chinese magnoliavine, rattletop, lucid asparagus, rhizoma Gastrodiae, radix pseudostellariae, Morinda officinalis, the banksia rose,
Scouring rush, great burdock achene, radix bardanae, plantain seed, Asiatic plantain, radix glehniae, fritillary bulb, radix scrophulariae, radix rehmanniae recen, Radix Polygoni Multiflori, bletilla, white
Art, the root of herbaceous peony, Amomum cardamomum, the shell of seaear, the stem of noble dendrobium (need to provide can be using proof), the root bark of Chinese wolf-berry, Radix Angelicae Sinensis, caulis bambusae in taenian, safflower, rhodiola root, west
American ginseng, evodia rutaecarpa, radix achyranthis bidentatae, the bark of eucommia, folium cortex eucommiae, semen astragali complanati, moutan bark, aloe, rhizoma atractylodis, Psoralea corylifolia, myrobalan, the radix paeoniae rubrathe, polygala root,
The tuber of dwarf lilyturf, tortoise plastron, eupatorium, cacumen biotae, rhubarb, prepared fleece flower root, wilsonii, rose hip, Herba Lycopi, rhizoma alismatis, rose, rose
Eggplant, the wind-weed, bluish dogbane, Ilex Latifolia Thunb, cymose buckwheat rhizome, the fruit of Cherokee rose, rascal, the bark of official magnolia, Flos Magnoliae Officinalis, turmeric, Fructus Aurantii, the dried immature fruit of citron orange, the seed of Oriental arborvitae, treasure
Pearl, gynostemma pentaphylla, fenugreek, madder, the Bi roots of grass, semen allii tuberosi, the vine of multiflower knotweed, rhizoma cyperi, the rhizome of davallia, Radix Codonopsis, the root bark of white mulberry, ramulus mori, fritillaria thunbergii,
Motherwort, centella, barrenwort, the seed of Chinese dodder, mother chrysanthemum, ginkgo leaf, the Radix Astragali, Hupeh Fritillary Bulb, folium sennae, gekko, cowberry, Chinese scholartree
Reality, cattail pollen, puncture vine, propolis, tamarind, eclipta, prepared RADIX ET RHIZOMA RHEI, prepared rhizome of rehmannia, turtle shell.
Above-mentioned different edible or/and pharmaceutical plant, animal, Homonemeae or its edible or/and pharmaceutical
Position can in any combination, i.e. any mixture of their (crushed material or powder) also can be used for the present invention, these combinations
(with the biologically active (pharmacologically active)) of (mixture) containing polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or
The extract of protein-based high molecular polymer is also preferably used for the present invention.
Hydrophilic polymer II
In the above-mentioned hydrophilic polymer II used by the present invention, be a kind of " pharmaceutically acceptable water-swellable, preferably
Ground, the substantially insoluble polymer of water ".They are preferably meant that a kind of such pharmaceutically acceptable material (polymerization
Thing), when it is exposed in excessive water, it is expanded to its equilibrium volume, but is substantially insoluble in solution, this polymerization
Thing material is also commonly referred to as " hydrocolloid " or " superabsorbent " material.For definition used herein, if a kind of material is recognized
For being water miscible, it is substantially soluble in excessive water formation solution, thus loses which initial, particularly granular
Shape, and be substantially scattered in the aqueous solution with molecular state.Common criterion is that water dissolvable material is handed over nothing substantial extent
Connection, because crosslinking will make material have water-insoluble.
Above-mentioned hydrophilic polymer II is typically crosslinked.The amount of crosslinking should generally be enough to make polymer keep water substantially
On insoluble minimum, but also polymer should be made to keep under swelling enough maximum in water, so that polymer energy
Absorb the desired amount of liquid and and swelling.
The crosslinking of usual polymer is by one of two distinct types of crosslinking agent using realizing.First type
Crosslinking agent is polymerisable crosslinking agent.Suitable polymerizable crosslinking agent to the monomer for preparing polymer be generally in reactivity
, and therefore usually contain at least two can be with the functional group of monomer reaction.The example of suitable polymerizable crosslinking agent, for
Include vinyl-based unsaturated monomer, such as N, N for radical polymerization '-methylene-bisacrylamide, include for polycondensation
Polyamines or polyol.
The crosslinking agent of Second Type is rear crosslinking agents.Rear crosslinking agents are generally not involved in whole polymerization process, but after relatively
Time, it can be with polymer reaction when appropriate cross linking conditions are supplied to.Suitable post-treatment condition is included using heating
Process, such as greater than about 60 DEG C of temperature, is exposed to ultraviolet, be exposed to microwave, steam or high humility are processed, HIGH PRESSURE TREATMENT or with having
Machine solvent is processed.
Rear crosslinking agents suitable for the present invention are usually water miscible.Suitable rear crosslinking agents be at least there are two can be with
A kind of organic compound of any carboxyl, carboxylic acid, the functional group of amino or hydroxyl reaction or degree of functionality on polymer.Suitable
The example of rear crosslinking agents includes but is not limited to diamine, polyamines, dihydroxylic alcohols, polyol, polycarboxylic acid and polyoxide.Another kind of suitable
Suitable rear crosslinking agents contain the metal ion with more than two positive charge, such as Al3+, Fe2+, Ce3+, Ce4+, Ti4+, Zr4+ and
Cr3+.
When polymer is for cationic polymer, suitable crosslinking agent is the material of polymer anion, such as polyacrylic acid
Sodium, carboxymethylcellulose calcium, or polyphosphate.
Above-mentioned hydrophilic polymer II preferably (in molecular structure) contains multiple anionic functional groups, such as sulfonic group, and more allusion quotation
Type ground such as the polymer of carboxyl.Example suitable for this polymer includes to prepare from polymerisable, undersaturated, acidiferous monomer
Those polymer.Therefore, this monomer includes the ethylenic unsaturated acid containing at least one carbon-to-carbon olefinic double bond and acid anhydride.More
Body ground, these monomers are selected from ethylenically unsaturated carboxylic acids and acid anhydrides, olefinic unsaturated sulfonic acid and its mixture.
In above-mentioned hydrophilic polymer II is prepared, may also comprise some generally with less amount of non-acid monomers.This non-
Acid monomers may include the water solubility of such as acidiferous monomer or the dispersible ester of water, and without carboxylic acid or sulfonic monomer.Cause
This optional non-acid monomers may include the monomer containing such as lower class functional group:Carboxylic acid or sulphonic acid ester, hydroxyl, amide groups, amino, nitrile
Base and quaternary ammonium salt base.These non-acid monomers are known material, are described in more detail in the U.S. for for example issuing for 28th for 2 months for 1978
In the United States Patent (USP) 4,062,817 (Westerman) that patent 4,076,663 (Masuda etc.) and on December 13rd, 1977 issue,
The two is all incorporated by reference.
Ethylenically unsaturated carboxylic acids and carboxylic acid anhydride monomer include acrylic compounds, typically acrylic acid itself, methacrylic acid,
Ethylacrylic acid, chloroacrylic acid, alpha-cyanoacrylate, methacrylic acid (crotonic acid), phenylacrylic acid, acryloxy propionic
(- acryloxypropionic acid), sorbic acid, chlorine sorbic acid, angelic acid, cinnamic acid, to chloro-cinnamic acid ,-
Sterylacrylic acid, itaconic acid, citraconic acid, mesaconic acid, glutaconate, aconitic acid, maleic acid, fumaric acid, tricarboxylic second
Alkene and maleic anhydride.
Olefinic unsaturated sulfonic acid monomer includes aliphatic series or aromatic vinyl sulfonic acids such as vinyl sulfonic acid, allyl sulphonic acid, second
Thiazolinyl toluenesulfonic acid and styrene sulfonic acid;Acrylic acid and methacrylic sulfonic acids such as sulfoethyl acrylate, methacrylic acid sulphur second
Ester, acrylic acid sulphur propyl ester, methacrylic acid sulphur propyl ester, 2- hydroxy-3-methyl acryloxypropyl sulfonic acid and 2- acrylamide -2-
Methyl propane sulfonic acid.
More preferably be preferred for the above-mentioned hydrophilic polymer of the present invention II be usually in and/or part neutralization weakly acidic or
Weakly alkaline water-swellable and insoluble polymer.The pKa (or pKb) of these polymer is advisable with about 2~about 12, more favorably
Ground is for about 2~about 10, conveniently about 3~about 6.
It has been found that using pKa (or pKb) less than about 2 or using the expansiveness of pKa (or pKb) greater than about 12, water
Insoluble polymer, generally will appear from the unwanted performance of the present invention, such as low absorption liquid rate, low Release Performance, and
And there may also be larger excitant etc.
Above-mentioned suitable slightly acidic water swellability and insoluble polymer (in molecular structure) are comprising can be used as weak acid
Functional group.These functional groups include but is not limited to carboxyl, sulfate groups, inferior sulfate radical group, and phosphate groups.Suitable
Functional group is carboxyl.Generally, these functional groups are connected on the base polymer of crosslinking.Suitable base polymer includes poly- third
Acrylamide, polyvinyl alcohol, EMA anhydride copolymer, polyvingl ether, polyacrylic acid, poly- carbon number are C1~C4 alkyl
Acrylic acid, poly- hydroxyl carbon atom number are C1~C4 alkyl acrylic, PVP, polyvinyl beautiful jade, and they
Copolymer.Natural polysaccharide (particularly starch, viscous polysaccharide) polymer can also be used, including carboxymethylcellulose calcium, carboxylic
Methyl starch, hydroxypropyl or ethyl cellulose, alginic acid, alginate, humic acid, carrageenan, acrylic acid-grafted starch, third
The cellulose of olefin(e) acid grafting, and their copolymer.Can also be using the polypeptide of synthesis, such as poly-aspartate, polyglutamic acid, poly-
(such as poly- mixing aspartic acid, for example poly-aspartate-aspartic acid-lysine is sour (4: 2: 1) in fact for mixing acidic amino acid;
Poly- mixing glutamic acid, for example polyglutamic acid-lysine is sour (4: 1) in fact.Term " poly- mixing acidic amino acid " refers to chain herein
In containing including the several amino acids including acidic amino acid, and the molal quantity of acidic amino acid (as aspartic acid, glutamic acid)
Poly- several amino acids that are molal quantity more than basic amino acid (as lysine, arginine) and assuming acidity (gather multiple amino
Acid is referring to document:US5247068A).It is preferred that being suitable for the above-mentioned slightly acidic water swellability of the present invention and water-insoluble polymerization
The example of thing is generally greater than about 100000 acroleic acid polymerization including but not limited to (in and/or part neutralization) weight average molecular weight
Thing, poly- carbon number are C1~C4 alkyl acrylic, poly- hydroxyl carbon atom number is C1~C4 alkyl acrylic, acrylic acid-acrylic
Acid ester polymer, polyvinyl alcohol-acrylic block copolymers, starch graft acrylic acid polymer, cellulose graft acrylic acid gather
Compound, humic acid, polycarbophil (Polycarbophil polymers), alginic acid, poly-aspartate, polyglutamic acid, poly- mixed
Close aspartic acid and poly- mixing glutamic acid, and their mixture.
Above-mentioned suitable alkalescent water swellability and insoluble polymer (in molecular structure) are comprising can be used as weak base
Functional group.These functional groups include but is not limited to primary, secondary and tertiary amino, imino group, and acylamino-.Suitable functional group is ammonia
Base.Generally, these functional groups are connected on the matrix polymer of crosslinking.Suitable matrix polymer includes polyamine or polyimides,
Polyethyleneimine, polyethylenepolyamine, polyacrylamide, polypropylene amine, polypropylene carbon number are C1~C4 alkylamine, and poly- carbon is former
Subnumber is C1~C4 alkyl amine, and it is C1~C4 alkylamine that poly- carbon number is C1~C4 alkyl carbon number, poly- hydroxyl
Base carbon number is C1~C4 alkyl amine, and it is C1~C4 alkane that poly- hydroxyl carbon atom number is C1~C4 alkyl carbon number
Base amine, and polyquaternium, and their copolymer.Can also be polymerized using natural polysaccharide (particularly starch, viscous polysaccharide)
Thing, including chitin (particularly starch, viscous polysaccharide) and chitosan (particularly starch, viscous polysaccharide) and other ammonia
Quito sugar (particularly starch, viscous polysaccharide).Can also gather and rely using the polypeptide of synthesis, such as poly-asparagine, polyglutamine
Propylhomoserin, poly arginine, poly- mixed-alkali amino acid (mix lysine as poly-, in fact such as polyglutamic acid-lysine (1: 3);Poly-
Mix arginine, in fact such as poly-aspartate-arginine (1: 4).Term " poly- mixed-alkali amino acid " is referred in chain herein
Contain including the several amino acids including basic amino acid, and the molal quantity of basic amino acid (as lysine, arginine) is more than
Acidic amino acid (as aspartic acid, glutamic acid) molal quantity and assume poly- several amino acids (the poly- several amino acids of alkalescence
Referring to document:US5247068A).It is preferred that being suitable for the above-mentioned alkalescent water swellability of the present invention and water-insoluble polymer
Example including but not limited to (in and/or part neutralization) weight average molecular weight be generally greater than about 100000 polyamine or polyimides,
Polyethyleneimine, polypropylene amine, polyethylenepolyamine, polypropylene carbon number be C1~C4 alkylamine, poly- carbon number be C1~
It is C1~C4 alkylamine, poly- hydroxyl carbon atom number that C4 alkyl amine, poly- carbon number are C1~C4 alkyl carbon number
It is C1~C4 alkylamine, chitin for C1~C4 alkyl amine, poly- hydroxyl carbon atom number for C1~C4 alkyl atomicity
(particularly starch, viscous polysaccharide), chitosan (particularly starch, viscous polysaccharide), other glycosaminoglycans (particularly form sediment
Powder, viscous polysaccharide), poly-asparagine, polyglutamine, polylysine, poly arginine, gather mixing lysine and the smart ammonia of poly- mixing
Acid, and their mixture.
The above-mentioned hydrophilic polymer II for being more preferably preferred for the present invention is selected from containing the water-soluble of carboxyl (in molecular structure)
Swollen property and insoluble polymer.The example of these polymer includes that hydrolyzed starch-acrylonitrile graft copolymer, part are neutralized
Starch-Acrylontirile Graft Copolymer, starch-acrylate graft copolymer, part neutralization starch-acrylate graft copolymer,
Sapond vinyl acetate-acrylate copolymer, the acrylonitrile of hydrolysis or acrylamide copolymer, any of the above described copolymer
Micro- cross-linked network polymer, part neutralization polyacrylic acid and part neutralization polyacrylic micro- cross-linked network polymerization
Thing, (pregelatinated 20-80%'s) partially pregelatinized starch (explanation:After starch pregelatinated, its AAP value is risen from on pregelatinated degree
Now first rise to maximum and then decline, AAP value is very low after complete pregelatinated, and hardly possible AAP value is to survey in cold water and normal-temperature water
Fixed or indeterminacy), and their mixture.These polymer can be used alone or the mixing with two or more different polymer
The form of thing is used.The example of these polymeric materials is disclosed in United States Patent (USP) 3,661,875, United States Patent (USP) 4,076,663, U.S.
In state's patent 4,093,776, United States Patent (USP) 4,666,983 and United States Patent (USP) 4,734,478.
Most preferably it is preferred for preparing above-mentioned hydrophilic polymer II for (part neutralization) polyacrylic micro- cross-linked network
Polymer and its starch derivatives.
The neutralization of weak acid (or alkali) the property functional group in above-mentioned weak acid (or alkali) property water-swellable and insoluble polymer
Degree is for about 5~about 100 moles of %, more advantageously about 30~about 95 moles of %, suitably about 50~about 90 moles of %, optimally
About 70~about 80 moles of %.
Very wide for the molecular weight ranges of the hydrophilic polymer II in the present invention.The water-swellable of relatively high molecular weight and water
Insoluble polymer, is typically favourable for the use in the present invention.Water-swellable and water-insoluble suitable for the present invention
The weight average molecular weight of polymer is generally greater than about 20000, is preferred with being greater than about 100000, and preferably greater than about 200000, more preferably
Greater than about 500000, preferably more than 1000000, up to about 10000000.The method for determining polymer molecular weight generally exists
It is known in the art.
Sometimes more easily the mode of expression polymer molecular weight is at 25 DEG C, the aqueous solutions of polymers of 1.0 weight %
Viscosity.Suitable for the polymer of the present invention, 200~about 80000 centipoises are for about with the viscosity of its 1.0 weight % aqueous solution at 25 DEG C
(mPa s) is advisable, and for about 500~about 80000 centipoises preferably, optimum are for about 1000~about 80000 centipoises.
Currently preferred hydrophilic polymer II is that have higher absorption ability or Teabag Centrifuge Capacity
Value.Absorbability or Teabag Centrifuge Capacity mean to give polymer absorb under the conditions of non-swelling with
The ability of the liquid that it contacts.TCC can be with the way of contact of the property of absorbed liquid and liquid and polymeric material not
Significantly change together.
Determination test method
AAP value (with respect to the absorption value of pressure) determination test
The test measurement superabsorbent is with respect to external pressure between 21.1g/cm (0.3psi) and 70.3g/cm (1psi)
Absorbability, represents so that superabsorbent is swelling with respect to the single shaft of the pressure.Aquogel type to two or more types
The sucting wet gel material mixture of grain, observation Absorption AgainstPressure change with the percentage composition of component of mixture
The curve of change, depends primarily on pressure condition.Adequately reflect use condition, the pressure of AAP value is measured in 21.1g/cm
(0.3psi) and 70.3g/cm (1psi) between.The gel hardness of AAP value reflection hygroscopic material.Grain structure is kept during wetting
The moisture absorption particle of (keeping space) will show good liquid absorption effect and not collapse to impermeability blob of viscose.AAP value
Low aquogel type material to form, by tending to, the Weak Gels that the permeability to liquid is relatively low and subsides under stress.
The ceramic filter plate of 120 millimeters of diameter and porosity are " Zero " (from the ceramic filter that Schott has bought
Duran) it is placed in 150 millimeters of diameter, high 30 millimeters of Petri dish (Petridsh).By 0.9% in distilled water
The sodium-chloride water solution of (weight) adds Petri dish so that filter is capped.By 125 millimeters of circular filter paper of diameter
(from the Schwarzband 589 that Schleicher and Schull has bought) is placed on filter plate, and is chlorinated sodium solution completely
Wetting.
The plexiglass cylinder bottom aperture of internal diameter 60+/- 0.1 millimeter and high 50 millimeters is 36 microns (400 mesh)
Sieving cloth is sealed.0.9000+/- 0.0005 gram superabsorbent is carefully sprinkling upon described heat-resisting organic glass that is clean and drying
On the screen of glass cylinder.Superabsorbent must be made to be uniformly distributed on sieve.
The external diameter of one cover plate is 59+/- 0.1 millimeter, internal diameter is for 51 millimeters and a height of 25 millimeters, and has a diameter of 50 millimeters
With a height of 34 millimeters of additional load, the pre- level pressure in the weight of cover plate and the scope between 21.1g/cm and 70.3g/cm
Power is corresponding, and the pressure is generally default to be set to 49.2g/cm2(0.7psi).Cover plate and load are placed in cylinder, and whole cylinder device exists
Weigh on balance, be accurate to 0.01 gram.Then whole cylinder device is placed on the filter paper of the moistening in Petri dish so as to
Absorb 1 hour.Then the equipment is removed from filter plate, is re-weighed.
Thoroughly cleaning answered by cylinder device and filter plate between measurements, and measurement afterchlorinate sodium solution and filter paper should be changed every time.
AAP value (with respect to the absorption value of pressure) is calculated as below:
AAP value=[(weight of cylinder device after absorption)-(weight of cylinder device when drying)]:(superabsorbent initial
Weight).
TTC value (Teabag Cetrifuge Capacity) determination test
Teabag Centrifuge Capacity test measurement Teabag Centrifuge Capacity value, it is right
Retain the measurement of liquid under static pressure in gel rubber material.
Superabsorbent is placed on 20 minutes in the sodium chloride solution for immerse in " tea bag " 0.9% (weight), is then centrifuged for
3 minutes.The ratio of the weight and the initial weight of dry superabsorbent that retain liquid is the absorbability of superabsorbent.
5 lis of 30 cm x of sodium chloride solution injection a size of 24 cm x by 2 liters of 0.9% (weight) in distilled water
In the disk of rice.Liquid packed height should be about 3 centimetres.
The size of tea bag bag is 6.5 centimetres of 6.5 cm x, can be public from Teekanne in Dusseldorf, Germany
Department obtains.This bag plastic bag sealing device for kitchen use (the VACUPACK PLUS as bought from Krups, Germany) of standard
Heat seal.
Tea bag is opened by carefully partial cut, is then weighed.The superabsorbent of 0.200+/- 0.005 gram is tried
Sample is put in tea bag.Then sealed with heat sealer.Referred to as sample tea bag.
Tea bag is sealed as blank test.
Then each tea bag holding level is made, and vibration sample tea bag is so that superabsorbent is evenly distributed in whole bag
In.Then sample tea bag and blank tea bag are placed on the surface of salt solution, make tea bag submergence 5 seconds with a flat spoon so that its
(tea bag will float over salt solution surface but completely moisten) is moistened completely.Immediately begin to timing.
Sample tea bag and blank tea bag were removed from salt solution, and are put into Bauknecht after 20 minutes by dipping
In the centrifuge (230 millimeters of diameter) of WS130, Bosch 772NZK 096 or equivalence, so that each Bao Jun sticks to centrifuge
On the outer wall of cylinder.The lid of centrifuge is covered, is started centrifuge, and speed is increased to rapidly 1400 revs/min.Centrifuge is 1400
After stablizing under rev/min, timing is immediately begun to.After 3 minutes, centrifuge is closed.
Sample tea bag and blank tea bag is taken out, is weighed respectively.
The Teabag Centrifuge Capacity (TCC value) of aquogel type superabsorbent sample is calculated as below:
TCC value=[(weight of sample tea bag after centrifugation)-(weight of blank tea bag after centrifugation)-(dry becomes hydrogel
The weight of superabsorbent)] ÷ (weight of dry superabsorbent).
The determination of half mass particle size
By the sample of known weight is put in Retsch mechanical sifter, and vibration one is specific under qualifications
Time cycle, determine the particle size distribution of superabsorbent.Weigh the sample parts and chassis being retained on each sieve
Weight, and it is recorded as the percentage of original sample weight.
Specimen mounting is added after superabsorbent polymeric material dry for 100+/- 0.5 gram is weighed, then specimen mounting is covered with cover.
Four sieves are stacked from bottom to up as follows:Stainless steel bottom plate, No. 325, No. 100, No. 50 and No. 20;These
Screen size (ASTM-E-11-61) for the U.S..Sample is delivered to the most top flat of the sieve series, powder is evenly distributed on sieve.
Stainless steel cover is placed on No. 20 sieve.
Stacked sieve is placed on the Retsch testing sieve shaker Vibotronic of timer
Appropriate location on TypeVE1.Guarantee that Retsch lid coordinates with the tight of vibrator as far as possible.Timer is located at
10 minutes, start test.When vibrator stops, bushing screen is removed from vibrator.
Then, for example by different measurements, the retained screening of each sieve is weighed, is accurate to 0.01 gram.
Rapid operation is important to avoid superabsorbent from absorbing moisture in this test.
Half mass particle size of given aquogel type absorbent polymer particle sample is defined as dividing sample according to quality
Become the particle size of half, i.e., the particle size that half sample will have less than half mass size by weight, half sample will have
Particle size more than half mass size.When 50% mass value does not correspond to U.S.A.Standard Testing Sieve (U.S.
National standard testing sieve) size perforate when, lead to working standard particle size method for drafting (wherein on graph paper draw retain
Open with sieve size on given sieve size perforate or by giving the accumulating weight percentage of the particle sample of sieve size perforate
The relation curve in hole) determine half mass particle size.For determine the particle size of aquogel type hygroscopic polymeric composition granule this
A little methods are further described authorizes the United States Patent (USP) 5 of Goldman etc. on October 29th, 1991, and in 061,259, the document is introduced
For reference.
Embodiment
Lower non-limiting examples further describe the preferred embodiment in the scope of the invention.Within the scope of the invention
These embodiments can also have many changes.
Embodiment 1
Seed of Chinese dodder crushed material (200 mesh) and the mixture of chitosan sulfate (250 mesh), the part by weight of the two
For 10:2.
Reference examples 1
In embodiment, chitosan sulfate is replaced by superfine silica gel powder, and other are constant.
Explanation:Above-mentioned crushed material, chitosan sulfate, superfine silica gel powder three APP value be respectively 1.3g/g,
6.5g/g、2.4g/g.
Embodiment 2
Cassia seed powder minces the mixture of (200 mesh) and poly glucosamine hydrochloride (250 mesh), the part by weight of the two
For 10:4.
Reference examples 2
In embodiment, poly glucosamine hydrochloride is replaced by soluble starch, and other are constant.
Explanation:Above-mentioned crushed material, poly glucosamine hydrochloride, soluble starch three APP value be respectively 1.8g/g,
7.7g/g, 0.3g/g, the TCC value of three are respectively 3.1g/g, 13.2g/g, 0.4g/g, and the APP value of the former two's mixture is
9.6g/g, the 1st, the APP value of 3 mixtures be 1.0g/g.
Embodiment 3
Date crushed material (200 mesh) and the mixture of poly-asparagine (200 mesh), the part by weight of the two are 10:2.
Reference examples 3
In embodiment, poly-asparagine is replaced by microcrystalline cellulose, and other are constant.
Explanation:Above-mentioned crushed material, poly-asparagine, microcrystalline cellulose three APP value be respectively 2.1g/g, 8.1g/g,
2.4g/g, the TCC value of three are respectively 4.3g/g, 14.4g/g, 3.8g/g, and the APP value of the former two's mixture is 7.7g/g, the
1st, the APP value of 3 mixtures is 2.2g/g.
Embodiment 4
Medlar powder minces the mixture of (200 mesh) and polyglutamine (200 mesh), and the part by weight of the two is 10:3.
Reference examples 4
In embodiment, polyglutamine is replaced by PEG6000, and other are constant.
Explanation:Above-mentioned crushed material, polyglutamine, PEG6000 three APP value be respectively 2.4g/g, 15.4g/g,
0.1g/g, the APP value of the former two's mixture is 12.5g/g, the 1st, the APP value of 3 mixtures be 1.2g/g.
Embodiment 5
Hawthorn crushed material (100 mesh) and the mixture of polylysine hydrochloride (200 mesh), the part by weight of the two are 10:
2.
Reference examples 5
In embodiment, polylysine hydrochloride is replaced by talcum powder, and other are constant.
Explanation:Above-mentioned crushed material, polylysine hydrochloride, talcum powder three APP value be respectively 2.5g/g, 23.6g/g,
1.2g/g.
Embodiment 6
Mangosteen powder minces the mixture of (200 mesh) and poly arginine dihydric phosphate (200 mesh), the part by weight of the two
For 10:1.
Reference examples 6
In embodiment, poly arginine dihydric phosphate is replaced by white bole (KALIN), and other are constant.
Explanation:Above-mentioned crushed material, poly arginine dihydric phosphate, the APP value of white bole (KALIN) three are respectively
1.6g/g, 23.2g/g, 0.9g/g, the APP value of the former two's mixture is 8.9g/g, the 1st, the APP value of 3 mixtures be 1.3g/
g.
Embodiment 7
Glutinous rice crushed material (250 mesh) and polylysine-glutamic acid (1:1) mixture of (250 mesh), the part by weight of the two
For 10:2.
Reference examples 7
Polylysine-glutamic acid (1 in embodiment:1) replaced by aluminium hydroxide desiccant gel, other are constant.
Explanation:Above-mentioned crushed material, polylysine-glutamic acid (1:1), the APP value difference of aluminium hydroxide desiccant gel three
For 2.1g/g, 17.4g/g, 3.3g/g, the APP value of the former two's mixture is 14.4g/g, the 1st, the APP value of 3 mixtures be
2.4g/g.
Embodiment 8
Psoralea corylifolia crushed material (200 mesh) and poly arginine-Men Dong propylhomoserin (3:1) mixture of hydrochloride (250 mesh), the two
Part by weight be 10:6.
Reference examples 8
Poly arginine-Men Dong propylhomoserin (3 in embodiment:1) hydrochloride is dry waxy corn starch (full pregelatinated) by drum-type
Replace, other are constant.
Explanation:Above-mentioned crushed material, poly arginine-Men Dong propylhomoserin (3:1) hydrochloride, drum-type dry waxy corn starch three
APP value be respectively 1.3g/g, 18.4g/g, 0.2g/g, the TCC value of three respectively 2.4g/g, 27.8g/g, 0.3g/g, front
The APP value of the two mixture is 18.9g/g, the 1st, the APP value of 3 mixtures be 0.7g/g.
Embodiment 9
Bighead atractylodes rhizome crushed material (250 mesh) and the mixture of hydrolyzed starch-acrylonitrile graft copolymer (250 mesh), the weight of the two
Amount ratio is 10:1.
Reference examples 9
In embodiment, hydrolyzed starch-acrylonitrile graft copolymer is replaced by light magnesium oxide, and other are constant.
Explanation:Above-mentioned crushed material, hydrolyzed starch-acrylonitrile graft copolymer, the APP value of light magnesium oxide three are respectively
2.5g/g, 17.3g/g, 1.8g/g, the APP value of the former two's mixture is 6.9g/g, the 1st, the APP value of 3 mixtures be 2.0g/
g.
Embodiment 10
Fritillaria thunbergii crushed material (250 mesh) is mixed with the Starch-Acrylontirile Graft Copolymer (250 mesh) of part neutralization (50%)
Compound, the part by weight of the two are 10:3.
Reference examples 10
In embodiment, the Starch-Acrylontirile Graft Copolymer of partly neutralization (50%) is replaced by beta-schardinger dextrin, and other are constant.
Explanation:Above-mentioned crushed material, the part neutralization Starch-Acrylontirile Graft Copolymer of (50%), beta-schardinger dextrin three
APP value is respectively 2.6g/g, 17.2g/g, 0.5g/g.
Embodiment 11
Saline cistanche crushed material (200 mesh) and the mixture of starch-sodium acrylate graft copolymer (250 mesh), the weight of the two
Amount ratio is 10:2.
Reference examples 11
In embodiment, starch-sodium acrylate graft copolymer is replaced by mannitol, and other are constant.
Explanation:Above-mentioned crushed material, starch-sodium acrylate graft copolymer, the APP value of mannitol three are respectively 2.5g/
G, 23.8g/g, 0.03g/g, the APP value of the former two's mixture is 12.9g/g, the 1st, the APP value of 3 mixtures be 1.2g/g.
Embodiment 12
Sealwort crushed material (200 mesh) neutralizes the mixing of the starch-acrylate graft copolymer (200 mesh) of (70%) with part
Thing, the part by weight of the two are 10:4.
Reference examples 12
In embodiment, the starch-acrylate graft copolymer of partly neutralization (70%) is replaced by lactose, and other are constant.
Explanation:Above-mentioned crushed material, the starch-acrylate graft copolymer of part neutralization (70%), the APP value of lactose three
Respectively 2.3g/g, 15.5g/g, 0.05g/g, the TCC value of three are respectively 3.9g/g, 24.7g/g, 0.07g/g, and the former two mixes
The APP value of compound is 17.4g/g, the 1st, the APP value of 3 mixtures be 1.3g/g.
Embodiment 13
The mixture of Ligusticum wallichii crushed material (200 mesh) and sapond vinyl acetate-acrylate copolymer (200 mesh),
The part by weight of the two is 10:2.
Reference examples 13
In embodiment, sapond vinyl acetate-acrylate copolymer is replaced by stearic acid, and other are constant.
Explanation:Above-mentioned crushed material, sapond vinyl acetate-acrylate copolymer, the APP value point of stearic acid three
Not Wei 2.2g/g, 12.4g/g, 0.4g/g, the TCC value of three is respectively 3.6g/g, 21.3g/g, 0.6g/g, the former two's mixture
APP value be 10.8g/g, the 1st, the APP value of 3 mixtures be 1.3g/g.
Embodiment 14
The mixture of the acrylamide copolymer (200 mesh) of prepared rhizome of rehmannia crushed material (200 mesh) and hydrolysis, the weight ratio of the two
Example is 10:2.
Reference examples 14
The acrylamide copolymer hydrolyzed in embodiment is replaced by Arabic gum, and other are constant.
Explanation:Above-mentioned crushed material, the acrylamide copolymer of hydrolysis, the APP value respectively 1.8g/g of Arabic gum three,
14.6g/g、2.1g/g.
Embodiment 15
Red ginseng crushed material (200 mesh) and the mixture of polyacrylic acid sodium salt (90% degree of neutralization) (200 mesh), the weight of the two
Ratio is 10:1.
Reference examples 15
In embodiment, polyacrylic acid sodium salt (90% degree of neutralization) is replaced by dextrin, and other are constant.
Explanation:Above-mentioned crushed material, polyacrylic acid sodium salt (90% degree of neutralization), dextrin three APP value be respectively 1.7g/g,
19.2g/g, 1.8g/g, the APP value of the former two's mixture is 6.7g/g, the 1st, the APP value of 3 mixtures be 1.5g/g.
Embodiment 16
Dried peppermint leaf crushed material (200 mesh) and the mixture of 60~80% pregelatinized partially pregelatinized starch (250 mesh), two
The part by weight of person is 10:20.
Reference examples 16
In embodiment, 60~80% pregelatinized partially pregelatinized starch are replaced by colloid silicic acid magnalium, and other are constant.
Explanation:Above-mentioned crushed material, 60~80% pregelatinized partially pregelatinized starch, the APP of colloid silicic acid magnalium three
Value is respectively 1.2g/g, 3.5g/g, 1.8g/g, and the TCC value of three is respectively 2.5g/g, 5.8g/g, 2.4g/g, and the former two mixes
The APP value of thing is 4.9g/g, the 1st, the APP value of 3 mixtures be 1.9g/g.
Embodiment 17
Datlily crushed material (200 mesh) and the mixture of sodium carboxymethyl starch (200 mesh), the part by weight of the two are 10:
10.
Reference examples 17
In embodiment, sodium carboxymethyl starch is dry waxy corn starch (full pregelatinated) replacement by drum-type, and other are constant.
Explanation:Above-mentioned crushed material, sodium carboxymethyl starch, drum-type dry the APP value of waxy corn starch three and are respectively
1.1g/g, 5.4g/g, 0.2g/g, the TCC value of three are respectively 2.5g/g, 8.3g/g, 0.3g/g, the APP of the former two's mixture
Be worth for 7.3g/g, the 1st, the APP value of 3 mixtures be 0.6g/g.
Embodiment 18
Platanus hispanica pollen minces the mixture of (200 mesh) and hydroxypropylcellulose (200 mesh), and the part by weight of the two is 10:1.
Reference examples 18
In embodiment, hydroxypropylcellulose is dry waxy corn starch (full pregelatinated) replacement by drum-type, and other are constant.
Explanation:Above-mentioned crushed material, hydroxypropylcellulose, drum-type dry the APP value of waxy corn starch three and are respectively 0.8g/
G, 3.2g/g, 0.2g/g, the APP value of the former two's mixture is 2.4g/g, the 1st, the APP value of 3 mixtures be 0.5g/g.
Embodiment 19
Gynostemma pentaphyllum powder minces the mixture of (200 mesh) and polyvinyl alcohol-PAA block copolymer (200 mesh), the two
Part by weight be 10:2.
Reference examples 19
In embodiment, polyvinyl alcohol-PAA block copolymer is replaced by Bletilla glucomannan, and other are constant.
Explanation:Above-mentioned crushed material, polyvinyl alcohol-PAA block copolymer, the APP value of Bletilla glucomannan three are respectively
1.2g/g, 15.2g/g, 1.6g/g, the APP value of the former two's mixture is 7.3g/g, the 1st, the APP value of 3 mixtures be 1.3g/
g.
Embodiment 20
Earthworm crushed material (200 mesh) and the mixture of polyacrylic acid sulphur propyl ester (200 mesh), the part by weight of the two are 10:
3.
Reference examples 20
In embodiment, polyacrylic acid sulphur propyl ester is replaced by magnesium stearate, and other are constant.
Explanation:Above-mentioned crushed material, polyacrylic acid sulphur propyl ester, the APP value of magnesium stearate three are respectively 2.3g/g, 8.4g/
G, 0.3g/g, the TCC value of three are respectively 4.4g/g, 15.3g/g, 0.5g/g, and the APP value of the former two's mixture is 9.4g/g,
1st, the APP value of 3 mixtures is 1.6g/g.
Embodiment 21
Dry deer blood meal mince (250 mesh) with 85% neutralization poly- ethylacrylic acid (250 mesh) mixture, the weight of the two
Amount ratio is 10:2.
Reference examples 21
In embodiment, the poly- ethylacrylic acid of 85% neutralization is replaced by carboxymethylcellulose calcium, and other are constant.
Explanation:Above-mentioned crushed material, the poly- ethylacrylic acid of 85% neutralization, the APP value of carboxymethylcellulose calcium three are respectively
1.4g/g、17.3g/g、3.5g/g.
Embodiment 22
Scorpio crushed material (300 mesh) and the mixture of sodium carboxymethylcellulose (300 mesh), the part by weight of the two are 10:
2.
Reference examples 22
In embodiment, sodium carboxymethylcellulose is dry waxy corn starch (full pregelatinated) replacement by drum-type, and other are constant.
Explanation:Above-mentioned crushed material, sodium carboxymethylcellulose, drum-type dry the APP value of waxy corn starch three and are respectively
2.5g/g, 4.6g/g, 0.3g/g, the APP value of the former two's mixture is 5.1g/g, the 1st, the APP value of 3 mixtures be 1.5g/
g.
Embodiment 23
Human placenta powder mince (300 mesh) with 50% neutralization starch graft acrylic acid polymer (300 mesh) mixture, two
The part by weight of person is 10:1.
Reference examples 23
In embodiment, the starch graft acrylic acid polymer of 50% neutralization is replaced by calcium phosphate, and other are constant.
Explanation:Above-mentioned crushed material, the starch graft acrylic acid polymer of 50% neutralization, the APP value difference of calcium phosphate three
For 2.6g/g, 12.4g/g, 0.8g/g, the TCC value of three is respectively 2.4g/g, 17.8g/g, 0.3g/g, the former two's mixture
APP value is 8.6g/g, the 1st, the APP value of 3 mixtures be 1.2g/g.
Embodiment 24
Pot marigold herb crushed material (250 mesh) and the mixture of Ac-Di-Sol (250 mesh), the weight of the two
Ratio is 10:1.
Reference examples 24
In embodiment, Ac-Di-Sol is dry waxy corn starch (full pregelatinated) replacement by drum-type, and other are not
Become.
Explanation:Above-mentioned crushed material, Ac-Di-Sol, drum-type dry the APP value point of waxy corn starch three
Not Wei 0.8g/g, 5.4g/g, 0.2g/g, the APP value of the former two's mixture is 3.8g/g, the 1st, the APP value of 3 mixtures be
0.5g/g.
Embodiment 25
Motherwort powder minces the mixture of (200 mesh) and polyoxyethylene (weight average molecular weight 600,000) (200 mesh), the weight of the two
Amount ratio is 10:1.
Reference examples 25
In embodiment, polyoxyethylene (weight average molecular weight 600,000) is dry waxy corn starch (full pregelatinated) replacement by drum-type,
Other are constant.
Explanation:Above-mentioned crushed material, polyoxyethylene (weight average molecular weight 600,000), drum-type dry waxy corn starch three's
APP value is respectively 1.2g/g, 4.2g/g, 0.2g/g.
Embodiment 26
Herba houttuyniae powder minces the mixture of (200 mesh) and PVPP (200 mesh), the part by weight of the two
For 10:3.
Reference examples 26
In embodiment, PVPP is replaced by lactose, and other are constant.
Explanation:Above-mentioned crushed material, PVPP, the APP value of lactose three are respectively 0.9g/g, 3.6g/
G, 0.03g/g, the TCC value of three are respectively 1.4g/g, 5.8g/g, 0.02g/g, and the APP value of the former two's mixture is 4.2g/g,
1st, the APP value of 3 mixtures is 0.5g/g.
Embodiment 27
The mixture of two acid sodium-salt of polypenthylene (250 mesh) that trollflower crushed material (250 mesh) is neutralized with 95%, the weight of the two
Amount ratio is 10:1.
Reference examples 27
In embodiment, two acid sodium-salt of polypenthylene of 95% neutralization is dry waxy corn starch (full pregelatinated) replacement by drum-type,
Other are constant.
Explanation:Above-mentioned crushed material, two acid sodium-salt of polypenthylene of 95% neutralization, drum-type dry waxy corn starch three's
APP value is respectively 0.8g/g, 12.4g/g, 0.3g/g.
Embodiment 28
(weight ratio is 4 for oyster meat (doing), Folium Andrographis, Radix Isatidis mixing:1:1) crushed material (200 mesh) and 45% neutralization
Poly arginine (200 mesh) mixture, the part by weight of the two be 10:4.
Reference examples 28
In embodiment, the poly arginine of 45% neutralization is replaced by hydroxyethyl cellulose, and other are constant.
Explanation:Above-mentioned crushed material, the poly arginine of 45% neutralization, the APP value of hydroxyethyl cellulose three are respectively 2.9g/
G, 13.2g/g, 2.8g/g, the TCC value of three are respectively 4.1g/g, 21.2g/g, 3.8g/g, and the APP value of the former two's mixture is
14.8g/g, the 1st, the APP value of 3 mixtures be 2.7g/g.
Embodiment 29
Radix Angelicae Sinensis mix with American Ginseng (weight ratio be 3:1) the polyacrylic microgrid that crushed material (200 mesh) is neutralized with 60%
The mixture of the polymer (200 mesh) of shape crosslinking, the part by weight of the two are 10:1.
Reference examples 29
In embodiment, the polymer of polyacrylic micro- cross-linked network of 60% neutralization is replaced by polyfructosan, and other are not
Become.
Explanation:Above-mentioned crushed material, the polymer of polyacrylic micro- cross-linked network of 60% neutralization, polyfructosan three
APP value is respectively 0.8g/g, 26.7g/g, 1.7g/g, and the APP value of the former two's mixture is 10.4g/g, and the 1st, 3 mixtures
APP value is 1.0g/g.
Embodiment 30
The fleece-flower root is minced with sealwort mixed powder, and (weight ratio is 1:2) (250 mesh) is formed sediment with the part pregelatinated of pregelatinated 50%
The mixture of powder (250 mesh), the part by weight of the two are 10:2.5.
Reference examples 30
In embodiment, the partially pregelatinized starch of pregelatinated 50% is dry waxy corn starch (full pregelatinated) by drum-type and replaces
Change, other are constant.
Explanation:Above-mentioned crushed material, the partially pregelatinized starch of pregelatinated 50%, drum-type dry waxy corn starch three's
APP value is respectively 1.9g/g, 4.7g/g, 0.2g/g, and the TCC value of three is respectively 3.3g/g, 7.2g/g, 0.3g/g, the former two
The APP value of mixture is 5.3g/g, the 1st, the APP value of 3 mixtures be 1.1g/g.
Embodiment 31
The mixing of the vinyl acetate-acrylic copolymer (300 mesh) that rhizoma pinellinae praeparata crushed material (300 mesh) is neutralized with 60%
Thing, the part by weight of the two are 10:1.
Reference examples 31
In embodiment, the vinyl acetate-acrylic copolymer of 60% neutralization is replaced by carboxymethylcellulose calcium, and other are constant.
Explanation:Above-mentioned crushed material, the vinyl acetate-acrylic copolymer of 60% neutralization, carboxymethylcellulose calcium three
APP value is respectively 2.3g/g, 16.8g/g, 2.8g/g, and the APP value of the former two's mixture is 10.2g/g, and the 1st, 3 mixtures
APP value is 2.4g/g.
Embodiment 32
The mixture of the Starch-Acrylontirile Graft Copolymer (200 mesh) that radix polygonati officinalis crushed material (200 mesh) is neutralized with 80%, two
The part by weight of person is 10:0.5.
Reference examples 32
In embodiment, the Starch-Acrylontirile Graft Copolymer of 80% neutralization is replaced by pectin, and other are constant.
Explanation:Above-mentioned crushed material, the Starch-Acrylontirile Graft Copolymer of 80% neutralization, the APP value of pectin three are respectively
1.2g/g, 16.4g/g, 1.5g/g, the APP value of the former two's mixture is 5.3g/g, the 1st, the APP value of 3 mixtures be 1.2g/
g.
Embodiment 33
Sterculia seed crushed material (200 mesh) and the mixture of calcium alginate (200 mesh), the part by weight of the two are 10:1.
Reference examples 33
In embodiment, calcium alginate is replaced by microcrystalline cellulose, and other are constant.
Explanation:Above-mentioned powder thing, calcium alginate, the APP value of microcrystalline cellulose three are respectively 1.4g/g, 4.7g/g, 2.5g/
g.
Embodiment 34
The mixing of polyvinyl alcohol-acrylic block copolymers (200 mesh) that arisaema cum bile crushed material (200 mesh) is neutralized with 50%
Thing, the part by weight of the two are 10:1.
Reference examples 34
In embodiment, the polyvinyl alcohol-acrylic block copolymers of 50% neutralization are replaced by carboxymethylethylcellulose, its
He is constant.
Explanation:Above-mentioned powder thing, the polyvinyl alcohol-acrylic block copolymers of 50% neutralization, carboxymethylethylcellulose
The APP value of three is respectively 1.7g/g, 17.2g/g, 3.1g/g, and the APP value of the former two's mixture is 7.8g/g, and the 1st, 3 mix
The APP value of compound is 1.9g/g.
Embodiment 35
Gallnut extract minces the mixture of (200 mesh) and poly-asparagine (200 mesh), and the part by weight of the two is 10:1.
Reference examples 35
In embodiment, poly-asparagine is dry waxy corn starch (full pregelatinated) replacement by drum-type, and other are constant.
Explanation:Above-mentioned powder thing, poly-asparagine, drum-type dry the APP value of waxy corn starch three and are respectively 1.5g/
g、13.8g/g、0.1g/g.
Embodiment 36
Cassia seed, hawthorn, the fruit of Chinese wolfberry, chrysanthemum, lotus leaf mixed powder mince, and (each Ingredients Weight ratio is 10:2:2:1:0.5)
The mixture of (200 mesh) and poly-asparagine (200 mesh), the part by weight of the two are 10:3.
Reference examples 36
In embodiment, poly-asparagine is replaced by maltodextrin, and other are constant.
Explanation:Above-mentioned powder thing, poly-asparagine, maltodextrin three APP value be respectively 1.8g/g, 8.8g/g,
0.4g/g, the TCC value of three are respectively 3.1g/g, 15.3g/g, 0.5g/g, and the APP value of the former two's mixture is 9.4g/g, the
1st, the APP value of 3 mixtures is 1.3g/g.
Embodiment 37
Gekko crushed material (200 mesh) and poly-aspartate-arginine (3:1) mixture of (200 mesh), the weight ratio of the two
Example is 10:1.
Reference examples 37
Poly-aspartate-arginine (3 in embodiment:1) waxy corn starch (full pregelatinated) replacement is dry by drum-type, its
He is constant.
Explanation:Above-mentioned powder thing, poly-aspartate-arginine (3:1), drum-type dries the APP of waxy corn starch three
Value is respectively 2.5g/g, 18.6g/g, 0.3g/g, and the APP value of the former two's mixture is 8.1g/g, and the 1st, the APP of 3 mixtures
It is worth for 1.2g/g.
Embodiment 38
Armillaria mellea accreting with Rhizoma Gastrodiae crushed material (300 mesh) and the mixture of polycarbophil (400 mesh), the part by weight of the two are 10:
5.
Reference examples 38
In embodiment, polycarbophil is replaced by starch, and other are constant.
Explanation:Above-mentioned crushed material, polycarbophil, the APP value of starch three are respectively 1.8g/g, 3.9g/g, 1.7g/g, front
The APP value of the two mixture is 5.4g/g, the 1st, the APP value of 3 mixtures be 1.8g/g.
Embodiment 39
The mixture of the cellulose graft acrylate copolymer (200 mesh) that Chinese aloe leaf crushed material (200 mesh) is neutralized with 30%,
The part by weight of the two is 10:2.
Reference examples 39
In embodiment, the cellulose graft acrylate copolymer of 30% neutralization is replaced by methylcellulose, and other are constant.
Explanation:Above-mentioned crushed material, the cellulose graft acrylate copolymer of 30% neutralization, the APP of methylcellulose three
Value is respectively 1.2g/g, 13.2g/g, 1.6g/g.
Embodiment 40
The mixture of purple sesame crushed material (200 mesh) and the polyglutamic acid (200 mesh) of 70% neutralization, the part by weight of the two is
10:3.
Reference examples 40
In embodiment, the polyglutamic acid of 70% neutralization is dry waxy corn starch (full pregelatinated) replacement by drum-type, and other are not
Become.
Explanation:Above-mentioned crushed material, the polyglutamic acid of 70% neutralization, drum-type dry the APP value point of waxy corn starch three
Wei not 1.2g/g, 17.7g/g, 0.2g/g.
Embodiment 41
The mixture of dandelion herb crushed material (200 mesh) and hydroxypropul starch (200 mesh), the part by weight of the two is
10:2.
Reference examples 41
In embodiment, hydroxypropul starch is replaced by microcrystalline cellulose, and other are constant.
Explanation:Above-mentioned crushed material, hydroxypropul starch, microcrystalline cellulose three APP value be respectively 1.2g/g, 4.6g/g,
2.3g/g.
Embodiment 42
The mixture of the poly- fumaric acid (200 mesh) that mother chrysanthemum crushed material (200 mesh) is neutralized with 75%, the part by weight of the two
For 10:2.
Reference examples 42
In embodiment, the poly- fumaric acid of 75% neutralization is replaced by starch, and other are constant.
Explanation:Above-mentioned crushed material, the poly- fumaric acid of 75% neutralization, the APP value of starch three are respectively 0.8g/g, 12.4g/
G, 1.8g/g, the APP value of the former two's mixture is 7.7g/g, the 1st, the APP value of 3 mixtures be 1.2g/g.
Embodiment 43
(weight ratio is 2 for leech, ginkgo leaf:1) mixed powder minces (200 mesh) and the 45% acrylic acid-acrylic acid first for neutralizing
The mixture of ester polymer (200 mesh), the part by weight of the two are 10:3.
Reference examples 43
The acrylic acid-acrylic acid methacrylate polymer of 45% neutralization in embodiment is replaced by bassora gum, and other are constant.
Explanation:Above-mentioned crushed material, the acrylic acid-acrylic acid methacrylate polymer of 45% neutralization, the APP value point of bassora gum three
Not Wei 2.0g/g, 11.8g/g, 2.3g/g, the TCC value of three is respectively 3.4g/g, 18.2g/g, 3.6g/g, the former two's mixture
APP value be 13.3g/g, the 1st, the APP value of 3 mixtures be 2.1g/g.
Embodiment 44
(weight ratio is 3 to indigoplant with rhizoma cyperi:1) the poly- amino fructose hydrochloride that crushed material (200 mesh) is neutralized with 80%
The mixture of (200 mesh), the part by weight of the two are 10:2.
Reference examples 44
In embodiment, the poly- amino fructose hydrochloride of 80% neutralization is dry waxy corn starch (full pregelatinated) by drum-type and replaces
Change, other are constant.
Explanation:Above-mentioned crushed material, the poly- amino fructose hydrochloride of 80% neutralization, drum-type dry waxy corn starch three's
APP value is respectively 1.3g/g, 14.7g/g, 0.1g/g.
Embodiment 45
GL-B (200 mesh) and the mixture of calcium carboxymethylcellulose (200 mesh), the part by weight of the two are 10:2.
Reference examples 45
In embodiment, calcium carboxymethylcellulose is dry waxy corn starch (full pregelatinated) replacement by drum-type, and other are constant.
Explanation:Above-mentioned crushed material, calcium carboxymethylcellulose, drum-type dry the APP value of waxy corn starch three and are respectively
1.5g/g, 3.6g/g, 0.4g/g, the TCC value of three are respectively 3.1g/g, 5.2g/g, 0.3g/g, the APP of the former two's mixture
Be worth for 5.1g/g, the 1st, the APP value of 3 mixtures be 1.0g/g.
Embodiment 46
Hickory chick crushed material (200 mesh) and the mixture of (pregelatinated 65%) partially pregelatinized starch (200 mesh), the two
Part by weight be 10:2.
Reference examples 46
In embodiment, (pregelatinated 65%) partially pregelatinized starch is dry waxy corn starch (full pregelatinated) by drum-type
Replace, other are constant.
Explanation:Above-mentioned crushed material, (pregelatinated 65%) partially pregelatinized starch, drum-type dry waxy corn starch three
APP value be respectively 2.1g/g, 6.8g/g, 0.3g/g, the APP value of the former two's mixture is 7.9g/g, the 1st, 3 mixtures
APP value is 1.1g/g.
Embodiment 47
Hickory chick crushed material (200 mesh) and the mixture of (pregelatinated 85%) partially pregelatinized starch (200 mesh), the two
Part by weight be 10:2.
Reference examples 47
In embodiment, (pregelatinated 85%) partially pregelatinized starch is dry waxy corn starch (full pregelatinated) by drum-type
Replace, other are constant.
Explanation:Above-mentioned crushed material, (pregelatinated 85%) partially pregelatinized starch, drum-type dry waxy corn starch three
APP value be respectively 2.1g/g, 4.8g/g, 0.3g/g, the APP value of the former two's mixture is 5.2g/g, the 1st, 3 mixtures
APP value is 1.1g/g.
Embodiment 48
Hickory chick crushed material (200 mesh) and the mixture of (pregelatinated 25%) partially pregelatinized starch (200 mesh), the two
Part by weight be 10:2.
Reference examples 48
In embodiment, (pregelatinated 25%) partially pregelatinized starch is dry waxy corn starch (full pregelatinated) by drum-type
Replace, other are constant.
Explanation:Above-mentioned crushed material, (pregelatinated 25%) partially pregelatinized starch, drum-type dry waxy corn starch three
APP value be respectively 2.1g/g, 2.8g/g, 0.3g/g, the APP value of the former two's mixture is 3.1g/g, the 1st, 3 mixtures
APP value is 1.1g/g.
Contained (effective) the composition stripping property detection in the hot water of detection example powder
Powder dispersive property in the hot water is better, performance more prevented from caking, and contained (effective) composition in powder is easier
Dissolution.Hot water oneself be widely used solvent in (effective) composition dissolution contained by Chinese herbal medicine, this time experiment detection hot water conduct
Solvent.
Take the hot water that the embodiment of identical weight, reference examples sample powder are scattered in the same temperature of 5 times of its weight respectively
In (75~95 DEG C), stirring is filtered (first with filter paper coarse filtration (elimination slag) then smart with 0.22 micron pore size miillpore filter after 5 minutes
Filter), the filtrate frozen drying of identical weight is taken respectively to moisture less than 1%, determine the weight of gained filtrate dried object
Amount (deducting container weight), the ratio for calculating embodiment filtrate dried object weight and reference examples filtrate dried object weight (set
Reference examples filtrate dried object weight is 1).The results are shown in Table 1.
1 embodiment of table and reference examples sample contained (effective) composition dissolving out capability testing result in the hot water
Embodiment 1 | 1.94 | Embodiment 2 | 2.25 | Embodiment 3 | 2.53 | Embodiment 4 | 2.62 |
Reference examples 1 | 1 | Reference examples 2 | 1 | Reference examples 3 | 1 | Reference examples 4 | 1 |
Embodiment 5 | 2.75 | Embodiment 6 | 2.53 | Embodiment 7 | 2.42 | Embodiment 8 | 1.73 |
Reference examples 5 | 1 | Reference examples 6 | 1 | Reference examples 7 | 1 | Reference examples 8 | 1 |
Embodiment 9 | 2.16 | Embodiment 10 | 2.46 | Embodiment 11 | 2.37 | Embodiment 12 | 2.54 |
Reference examples 9 | 1 | Reference examples 10 | 1 | Reference examples 11 | 1 | Reference examples 12 | 1 |
Embodiment 13 | 3.46 | Embodiment 14 | 2.63 | Embodiment 15 | 2.38 | Embodiment 16 | 1.84 |
Reference examples 13 | 1 | Reference examples 14 | 1 | Reference examples 15 | 1 | Reference examples 16 | 1 |
Embodiment 17 | 1.76 | Embodiment 18 | 1.53 | Embodiment 19 | 2.88 | Embodiment 20 | 3.32 |
Reference examples 17 | 1 | Reference examples 18 | 1 | Reference examples 19 | 1 | Reference examples 20 | 1 |
Embodiment 21 | 2.77 | Embodiment 22 | 2.36 | Embodiment 23 | 3.53 | Embodiment 24 | 1.75 |
Reference examples 21 | 1 | Reference examples 22 | 1 | Reference examples 23 | 1 | Reference examples 24 | 1 |
Embodiment 25 | 2.23 | Embodiment 26 | 1.68 | Embodiment 27 | 2.56 | Embodiment 28 | 2.43 |
Reference examples 25 | 1 | Reference examples 26 | 1 | Reference examples 27 | 1 | Reference examples 28 | 1 |
Embodiment 29 | 2.97 | Embodiment 30 | 1.88 | Embodiment 31 | 3.14 | Embodiment 32 | 3.57 |
Reference examples 29 | 1 | Reference examples 30 | 1 | Reference examples 31 | 1 | Reference examples 32 | 1 |
Embodiment 33 | 2.44 | Embodiment 34 | 2.64 | Embodiment 35 | 2.77 | Embodiment 36 | 3.25 |
Reference examples 33 | 1 | Reference examples 34 | 1 | Reference examples 35 | 1 | Reference examples 36 | 1 |
Embodiment 37 | 2.72 | Embodiment 38 | 1.85 | Embodiment 39 | 2.24 | Embodiment 40 | 2.26 |
Reference examples 37 | 1 | Reference examples 38 | 1 | Reference examples 39 | 1 | Reference examples 40 | 1 |
Embodiment 41 | 1.85 | Embodiment 42 | 2.17 | Embodiment 43 | 1.87 | Embodiment 44 | 2.04 |
Reference examples 41 | 1 | Reference examples 42 | 1 | Reference examples 43 | 1 | Reference examples 44 | 1 |
Embodiment 45 | 1.68 | Embodiment 46 | 2.45 | Embodiment 47 | 1.82 | Embodiment 48 | 1.38 |
Reference examples 45 | 1 | Reference examples 46 | 1 | Reference examples 47 | 1 | Reference examples 48 | 1 |
Claims (10)
1. a kind of effect improve or strengthen (stripping property (/ amount) improvement of in other words, contained (effective) composition in (warm) water or
Strengthen) functional food (or alternative tea), it is (special that the functional food (or alternative tea) contains polysaccharide comprising one (or more)
Starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer with physiologically active (or pharmacological action)
Food grain thing (or powder) I and AAP value (i.e. Absorption Against Pressure value, or claim pressure-bearing expansion (molten
Swollen) value) higher than the food grain thing (or powder) I (it is preferred that high (containing) 1.25 times) one (or more) hydrophilic polymer
(particulate matter (or powder)) II.
2. according to claim 1 to functional food (or alternative tea), it is characterised in that described food grain thing (or powder) I phase
It is AAP for the absorption value under a pressure1, II particle of the hydrophilic polymer is AAP with respect to the absorption value under a pressure2, two
Person's mixture is AAP with respect to the absorption value under a pressure1,2, AAP1,2> (w AAP1+p·AAP2) (more preferably >=1.25
(w·AAP1+p·AAP2)), wherein, w accounts for described food grain thing (or powder) I He for described food grain thing (or powder) I
The percentage of II particle gross weight of the hydrophilic polymer, p for II particle of the hydrophilic polymer account for the food grain thing (or
Powder) I and II particle gross weight of the hydrophilic polymer percentage, and p+w=1, absorption value AAP with respect to pressure
Be in 21.1g/cm2(0.3psi) and 70.3g/cm2(1psi) between, preferably in 35.2g/cm2(0.5psi) and 56.2g/cm2
(0.8psi) measurement under the pressure between, the measure of absorption value AAP is carried out under identical conditions (pressure)).
3. according to claim 1 to functional food (or alternative tea), it is characterised in that the TCC of II particle of the hydrophilic polymer
Value higher than the TCC value of described food grain thing (or powder) I, the AAP value of the mixture of the two be higher than the food grain thing (or
Powder) I and AAP value of any one of II particle of the hydrophilic polymer, the wherein described absorption value with respect to pressure be
21.1g/cm2(0.3psi) and 70.3g/cm2(1psi) between, preferably in 35.2g/cm2(0.5psi) and 56.2g/cm2
(0.8psi) measurement under the pressure between, the measure of absorption value AAP is carried out under identical conditions (pressure)).
4. according to claim 1 to functional food (or alternative tea), it is characterised in that the weight of described particulate matter (or powder) I
Account at least the 10% of the hydrophilic polymer I and II particle gross weight of the hydrophilic polymer.
5. according to claim 1 to functional food (or alternative tea), it is characterised in that described particulate matter (or powder) I is selected from choosing
From living with physiology containing polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer
The edible of property (or pharmacological action) or/and pharmaceutical plant, animal or bacterium algae or its edible or/and pharmaceutical position
Crushed material or powder, or which contains polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based polyphosphazene polymer
The extract powder of compound.
6. according to claim 1 to functional food (or alternative tea), it is characterised in that described particulate matter (or powder) I is selected from down
The crushed material of row Chinese medicine or powder:
1), fruit, kind subclass Chinese medicine
Example is such as, pericarpium zanthoxyli, the seed of feather cockscomb, semen allii tuberosi, fennel seeds, rice sprout, semen armeniacae amarae, fructus polygoni orientalis, waxgourd seed, waxgourd peel, red little
Beans, linseed, the seed of Chinese dodder, tribulus terrestris, puncture vine, the shell of areca nut, in one's early teens, polished rice, Snakegourd Fruit, cassia seed, Psoralea corylifolia, fructus cannabis, cowpea
Beans, tangerine seed, fig, Chinese toona fruit, sandlwood, Kiwi berry, raspberry, Chinese wild pepper, the seed of Oriental arborvitae, evodia rutaecarpa, perilla seed, castor bean,
Longan seed, Chinese honey locust, peanut, frutus cnidii, glutinous rice, franchet groundcherry persistent calyx or fruit, capsicum, tomato, mountain Wu's cornel, fruit Exocarpium Citri Grandis, the seed of cowherb, black nightshade
Son, Chinese torreyanut, semen astragali complanati, plantain seed, the fruit of Rangoon creeper, sword bean, dried orange peel, rascal, Java brucea, dark plum, Chinese prickly ash, balsam pear, granatum, Strychnos nux-vomica
Son, dillseed, Perilla frutescens, Semen Lablab Album, Chinese hawthorn seed, barley, citron, fiveleaf akebia fruit, sea-buckthorn, kaladana, lepidium seed, tung oil tree son, scold
Son, pepper, light wheat, calyx-shaped daphniphyllum fruit, fructus amomi, Oroxylum indicum, trachycarpi,fructus, Amomum cardamomum, malt, fructus alpiniae oxyphyllae, nutmeg, nutmeg
Clothing, coffee senna fruit or seed, fructus gleditsiae, cassia bud, great burdock achene, radish seed, fructus viticis, Gui Ding, gingko, wax gourd, the fruit of Cherokee rose, the fruit of summer cypress,
Fructus meliae toosendan, Momordica grosvenori, the achene of Siberian cocklebur, spina date seed, date, Exocarpium Citri Rubrum, lichee, arillus longan, grape, cherry, coix seed, brush-cherry seed, bar
Beans, the fruit of glossy privet, mulberry fruit, Fructus Aurantii, Gorgon fruit, muskmelon pedicel, peach kernel, semen litchi, the capsule of weeping forsythia, corn stigma, watermelon peel, lotus seeds, walnut kernel, summer are withered
Grass, tsaoko, Chinese anise, semen brassicae, chingma abutilon seed, betel nut, the dried immature fruit of citron orange, the fruit of Chinese magnoliavine, Fructus Corni, cape jasmine, the fruit of Chinese wolfberry, pawpaw, jujube core,
Semen sesami nigrum, the sterculia seed, hawthorn, Buddha's hand, persimmon, Paper mulberry Fruit, mung bean, papaw, gumbo.
2), plant roots, stem class Chinese medicine
Such as, Radix Angelicae Sinensis, radix scrophulariae, Dysosma versipellis, the bighead atractylodes rhizome, rhizoma dioscoreae nipponicae, radix aconiti sinensis, RADIX ACONITI KUSNEZIFFII, rattletop, Longstamen Onion Bulb, fritillaria thunbergii, mountain are kind for example
Mushroom, the root of gansui, cymose buckwheat rhizome, rhizoma arisaematis, fresh rehmannia root, Radix changii, rhizoma typhonii, rhizoma homalonemae, Kaempferia galanga, flea stop, adder-wort, Radix picrorrhizae, asparagus fern,
The rhizoma bolbostemmae, aster, bletilla, the rhizome of davallia, monkshood, saline cistanche, blackberry lily, Cynanchum glaucescens, rhizome of cyrtomium, root of Chinese trichosanthes, felwort, blackfruit greenbrier rhizome and leaf, soil
The root of bidentate achyranthes, Alpinia japonica, RADIX PRZEWALSKIAE TANGUTICAE, the wind-weed, cynomorium songaricum, Jehol Ligusticum Rhizome, corydalis tuber, rhizoma nardostachyos, radix cynanchi atrati, Bulbus Fritillariae Cirrhosae, Morinda officinalis, henry woodbetony root, Rhizoma Sparganii, open country
Pseudo-ginseng, Bi, the tuber of stemona, airpotato yam, adenophora tetraphylla, radix glehniae, hand ginseng, stephanotis, the root of purple-flowered peucedanum, rhizoma zingiberis, Bulbus Allii Fistulosi, pseudo-ginseng, twoleaf platanthera rhizome, ginger
Huang, sealwort, galangal, Rhizoma polygoni vivipari, American Ginseng, water chestnut, radix ranunculi ternati, smilax, fritillary bulb, curcuma zedoary, radix polygonati officinalis, the root of straight ladybell, the root of kudzu vine, remote
Will, the radix paeoniae rubrathe, garlic, thizoma curculiginis, root tuber of aromatic turmeric, the fleece-flower root, decumbent corydalis tuber, rhizoma cyperi, radix ampelopsis, cogongrass rhizome, rhizoma alismatis, the tuber of dwarf lilyturf, bracketplant, rhizoma Gastrodiae, half
Summer, Ligusticum wallichii, Chinese yam, Radix Codonopsis, ginger, radix pseudostellariae, prepared rhizome of rehmannia, rheum officinale, Radix Isatidis, pseudo-ginseng, ginseng, red ginseng, hair arrowhead, method half
Summer.
3), leaves of plants class Chinese medicine
Example such as, holly leaf, thick grass, folium lycii, folium isatidis, Japanses beauty-berry, Pittosporum glabratum Lindl. leaf, leaf mustard, chinaroot greenbrier leaf, Fallopia nervosa, heath
Leaf, Pu'er tea, buzhaye, bluish dogbane, mulberry leaf, folium sennae, coffee senna, Ilex Latifolia Thunb, refute greatly bone, perilla leaf, Chinese holly, knotweed smalt
Leaf, lotus leaf, thin evodia leaf, barrenwort, acute turpinia leaf, lily, peppermint, sanchi leaf, folium panacis japonici cum caule, the bark of eucommia, leek, Herba Andrographitis, tarragon,
Loguat leaf, Chinese tamarisk tops, ginkgo leaf, hairyflower actinidia root and leaf, greater celandine, gumbo.
4), plant flowers class Chinese medicine
Example such as, datlily (day lily), globe artichoke, cauliflower, broccoli, tender flower stalk, sophora flower, pollen pini, peach blossom, camellia,
Lilac daphne, the flower bud of lily magnolia, inular flower, sanchi flower, honeysuckle, Chinese trumpet creeper, plum blossom, Inula britannica chinensis, balsamine, mother chrysanthemum, Flos Albiziae, rose
Flower, flos mume, finger citron flower, Camellia nitidissima, sweet osmanthus, shrub althea flower, flores tiliae, loquat flower, lily, betelnutpalm male flower, FI puerariae, cuckoo
Flower, flower of hyacinth dolichos, stamen nelumbini, cattail pollen, lanatechead saussurea herb with flower, roselle, harlequin glorybower flower, phoenix tree flower, datura flower, gardenia, Flos Magnoliae Officinalis, egg
Flower, jasmine, flower of Panax ginseng, safflower, tussilago, tulip, safflower, wintersweet immature flower, cockscomb, rose, common bombax flower, noisy sheep
Flower, bitter citrus immature flower, globe amaranth, Flos Hibisci Mutabilis, trollflower, China rose, cloves, chrysanthemum, yulan magnolia, Jasmine, fried dough twist.
5), plant entirety Chinese medicine
Example such as, schizonepeta, coriander, bittersweet, black nightshade, Sculellaria barbata, Chinese violet, oriental wormwood, Glabrous Sarcandra Herb, corydlis bungeana, catchweed bedstraw herb, green grass or young crops
Wormwood artemisia, Artemisia japonica, centella, gerbera, Chinese celery, scouring rush, osbeckia chinensis, savatier monochasma herb, elscholtiza, waterplantain ottelia herb, salvia chinensis, Herba lygodii, slowly
Long minister in ancient times, lycopodium calvatum, rooted pellionia herb, water hyacinth, milk thistle, Herba Lycopi, unpleasant swallowwort herb, Pogostemon cablin, rosemary, Xi, potentilla chinensis, great Bai
Medicine, birdsfoot trefoil herb and flower, white dead nettle, Chinese mesona herb, Artemisia anomala, lopseed, little groundcherry herb or fruit, gynostemma pentaphylla, meadow pine, bitter ground courage, wartwort, flaccid knotweed herb,
Involucrate balanophora herb, Common Leafflower Herb, setose thistle, broomrape, david gentian herb, eclipta, Lemongrass, pot marigold, desmodium, Centipeda minima, small stream are yellow
Grass, Sambucus thunbergiana, rhodiola root, sensitive plant, kiss-me, affine cudweed, Common Sage Herb, wolf's milk, Canton love-pea vine, Chinese milkwort herb, pipewort, phoenix
Tail grass, acalypha copperleaf, sealwort, mock-strawberry, bitter leaves, geranium wilfordii, ciliate desert-grass, dandelion, oldenlandia diffusa, Rabdosia rubescens, potentilla discolor, little
Ji, motherwort, cordate houttuynia, ardisia japonica, Mongollian Thyme Herb, Chinese penthorum herb, eupatorium, wrinkled giant hyssop, purslane, hairyvein agrimony, short top top, Chinese lobelia, company
Money grass, Verbena officinalis, concave head amaranth, Asiatic plantain, himalayan creeper herb, field pennycress, witchweed, roxburgh anoectochilus terminal bud.
6), Homonemeae Chinese medicine
Example such as, umbellate pore furgus, glossy ganoderma, Lygodium japonicum, white fungus, tabasheer, fushen, fuling peel, poria cocos, agaric, hickory chick, Chinese gall,
Stone-like omphalia, kelp, rainbow conk, marine alga, Lasiosphaera fenzlii, Cordyceps sinensis, Poria cocos, purple sesame.
7), animal tcm material
Sparrow meat, mutton, pig lung, cow's milk, deer horn glue, deer horn, ground bettle, cornu bubali, sea otter, pearl, tortoise plastron, colla carapacis et plastri testudinis, dog
Meat, mole cricket, rhinoceros horn, mantis egg-case, sea cucumber, toad, goat's horn, pilose antler, turtle shell, jellyfish, Bungarus Parvus, oyster meat, centipede,
Moschus, cuttlebone, cornu cerve degelatinatum, cow-bezoar, dens draconis, jellyfish, dried scallop, antelope's horn, pallas pit viper, bear gall, mother-of-pearl, honeycomb, zaocys dhumnade,
Dragon, snake slough, yellow-swallowtail butterfly larva, deer's sinew, toad skin, black-bone chicken, deer tire, pillworm, garter snake gall, cricket, bird's nest, snail, deer blood, the larva of a silkworm with batrytis,
Dog kidney, aspongopus, hedgehog skin, hippocampus, cockroach, gekko, frog, cicada slough, ant, pork tripe, the membrane of a chicken's gizzard, pork liver, pangolin, deer
Tail, cornu caprae hircus, deer kidney, nutgall, the shell of seaear, Chinese blister beetle, donkey-hide gelatin, honey, silkworm excrement, dung beetle, scorpio, leech, gecko, oyster.
8), other classes contain polysaccharide (particularly starch, viscous polysaccharide) class or/and peptides or protein-based high molecular polymer
Chinese medicine with biologically active (pharmacologically active)
The concentrated dry product of Tabasheer, arisaema cum bile, Divine Comedy, dried human placenta, indigo naturalis, frankincense, aloe leaf juice, catechu be (catechu tree
Dry branch add water pan-fried juice concentration dry extract).
7. according to claim 1 to functional food (or alternative tea), it is characterised in that described particulate matter (or powder) I is selected from down
The crushed material of row integration of drinking and medicinal herbs food or powder:
Cloves, Chinese anise, sword bean, fennel seeds, field thistle, Chinese yam, hawthorn, purslane, zaocys dhumnade, dark plum, pawpaw, fructus cannabis,
Bitter orange flower, radix polygonati officinalis, Radix Glycyrrhizae, the root of Dahurain angelica, gingko, Semen Lablab Album, Flos Semen Lablab Album, arillus longan (longan), cassia seed, lily, nutmeg, meat
Osmanthus, emblic, Buddha's hand, almond (sweet, bitter), sea-buckthorn, oyster, Gorgon fruit, Chinese prickly ash, rde bean, donkey-hide gelatin, the membrane of a chicken's gizzard, malt, kelp,
Jujube (date, wild jujube, dateplum persimmon), Momordica grosvenori, brush-cherry seed, honeysuckle, Chinese olive, cordate houttuynia, ginger (ginger, rhizoma zingiberis), trifoliate orange, matrimony vine
Son, cape jasmine, fructus amomi, the sterculia seed, Poria cocos, citron, elscholtiza, peach kernel, mulberry leaf, mulberry fruit, orange, balloonflower root, fructus alpiniae oxyphyllae, lotus leaf, radish
Son, lotus seeds, galangal, lophatherum gracile, Fermented Soybean, chrysanthemum, witloof, SEMEN SINAPIS ALBAE, sealwort, purple perilla, purple perilla seed, the root of kudzu vine, Semen sesami nigrum, black
Pepper, the sophora bud, sophora flower, dandelion, honey, Chinese torreyanut, spina date seed, fresh Rhizoma Imperatae, fresh Rhizoma Phragmitis, pallas pit viper, orange peel, peppermint, coix seed,
Longstamen Onion Bulb, raspberry, wrinkled giant hyssop, pueraria root powder, Cordyceps militaris.
8. according to claim 1 to functional food (or alternative tea), it is characterised in that described particulate matter (or powder) I is selected from down
The crushed material of row food with health role or powder:
Ginseng, folium panacis japonici cum caule, panax ginseng fruit, pseudo-ginseng, smilax, setose thistle, the fruit of glossy privet, Fructus Corni, radix cyathulae, Bulbus Fritillariae Cirrhosae, Ligusticum wallichii, red deer
Tire, cervus elaphus linnaeus, red deer bone, the red sage root, cortex acanthopanacis, the fruit of Chinese magnoliavine, rattletop, lucid asparagus, rhizoma Gastrodiae, radix pseudostellariae, Morinda officinalis, the banksia rose, scouring rush,
Great burdock achene, radix bardanae, plantain seed, Asiatic plantain, radix glehniae, fritillary bulb, radix scrophulariae, radix rehmanniae recen, Radix Polygoni Multiflori, bletilla, the bighead atractylodes rhizome, white
Chinese herbaceous peony, Amomum cardamomum, the shell of seaear, the stem of noble dendrobium (need to provide can using prove), the root bark of Chinese wolf-berry, Radix Angelicae Sinensis, caulis bambusae in taenian, safflower, rhodiola root, American Ginseng,
Evodia rutaecarpa, radix achyranthis bidentatae, the bark of eucommia, folium cortex eucommiae, semen astragali complanati, moutan bark, aloe, rhizoma atractylodis, Psoralea corylifolia, myrobalan, the radix paeoniae rubrathe, polygala root, Mai Men
Winter, tortoise plastron, eupatorium, cacumen biotae, rhubarb, prepared fleece flower root, wilsonii, rose hip, Herba Lycopi, rhizoma alismatis, rose, roselle, know
Mother, bluish dogbane, Ilex Latifolia Thunb, cymose buckwheat rhizome, the fruit of Cherokee rose, rascal, the bark of official magnolia, Flos Magnoliae Officinalis, turmeric, Fructus Aurantii, the dried immature fruit of citron orange, the seed of Oriental arborvitae, pearl, strand
Stock indigo plant, fenugreek, madder, the Bi roots of grass, semen allii tuberosi, the vine of multiflower knotweed, rhizoma cyperi, the rhizome of davallia, Radix Codonopsis, the root bark of white mulberry, ramulus mori, fritillaria thunbergii, benefit are female
Grass, centella, barrenwort, the seed of Chinese dodder, mother chrysanthemum, ginkgo leaf, the Radix Astragali, Hupeh Fritillary Bulb, folium sennae, gekko, cowberry, Chinese scholartree are real, Pu
Huang, puncture vine, propolis, tamarind, eclipta, prepared RADIX ET RHIZOMA RHEI, prepared rhizome of rehmannia, turtle shell.
9. according to claim 1 to functional food (or alternative tea), it is characterised in that the hydrophilic polymer II is selected from neutralization
Or weakly acidic or weakly alkaline water-swellable and insoluble polymer or the partially pregelatinized starch of part neutralization.
10. according to claim 1 to functional food (or alternative tea), it is characterised in that the hydrophilic polymer II is selected from starch
Grafted propylene acid polymer, cellulose graft acrylate copolymer, humic acid, polycarbophil (Polycarbophil
Polymers), alginic acid, chitin, chitosan, other glycosaminoglycans, poly-aspartate, polyglutamic acid, poly- mixing
Aspartic acid, poly- mixing glutamic acid, poly-asparagine, polyglutamine, polylysine, poly arginine, poly- mixing lysine, poly-
Mixing arginine, and their mixture, weak acid in the hydrophilic polymer II or the degree of neutralization of alkalescent functional group be 5~
100 moles of %.
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