CN111671714B - Plant hair dye for nourishing and protecting hair and hair dyeing method thereof - Google Patents
Plant hair dye for nourishing and protecting hair and hair dyeing method thereof Download PDFInfo
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Abstract
The invention discloses a plant hair dye for nourishing and protecting hair and a hair dyeing method thereof, and the plant hair dye comprises an agent A and an agent B, wherein the agent A comprises 1 to 4 percent of water-soluble metal salt, 2 to 4 percent of thickening agent, 0.01 to 0.05 percent of vitamin C, 2 to 4 percent of humectant, 0.05 to 0.2 percent of surfactant and the balance of water; the agent B comprises 2 to 5 percent of glossy privet fruit powder, 1 to 3 percent of prepared fleece-flower root powder, 0.5 to 3 percent of Chinese gall extract, 0.5 to 2 percent of myrobalan pigment, 0.5 to 3 percent of grape pigment, 0.5 to 2 percent of madder pigment, 1 to 2 percent of thickening agent, 2 to 4 percent of humectant, 0.1 to 0.2 percent of surfactant and the balance of water; the hair dye has stable hair dyeing effect and less fading in hair washing process; the plant hair dye does not contain toxic and harmful components of phenol and aniline, such as an oxidant, an alkali agent and an oxidation type hair dye, does not cause harm to human bodies, and is safe and healthy and has the effects of nourishing and protecting hair.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to a plant hair dye for nourishing and protecting hair and a hair dyeing method thereof.
Background
At present, the most popular hair coloring products in the international and domestic markets are oxidative hair dyes. Oxidative hair dyes usually contain harmful components such as p-phenylenediamine, toluene-2, 5-diamine, resorcinol, m-aminophenol, p-aminophenol, etc., which are simple in structure and small in molecule, and can be absorbed through the skin to cause rash and damage the liver. The oxidation type hair dye contains an oxidizing agent and an alkaline agent, so that the original pigment and a scale layer of hair are damaged during dyeing, the hair is dyed more thoroughly, but harmful components can also enter the scalp through a medulla layer to be harmful to the health of a human body, and the hair dye can also cause hair loss after long-term use. There is a proposal by experts that the frequency of hair dyeing using an oxidative hair dye should not exceed 3 times/year, which is far from satisfying the requirement of covering white hair. At present, safe and healthy hair dyes are urgently needed in the market to meet the requirements of consumers.
Disclosure of Invention
The plant hair dye does not contain an oxidant, does not use an alkaline agent, does not add phenol and aniline toxic and harmful components of an oxidation type hair dye, does not cause harm to a human body, does not stimulate scalp and allergy, does not cause alopecia, does not damage a scale layer structure on the surface of hair, is safe and healthy, and can play a role in nourishing scalp and hair while dyeing hair.
In order to achieve the purpose, the invention adopts the following technical scheme:
a plant hair dye for nourishing and caring hair comprises agent A and agent B,
the agent A comprises 1 to 4 percent of water-soluble metal salt, 2 to 4 percent of thickening agent, 0.01 to 0.05 percent of vitamin C, 2 to 4 percent of humectant, 0.05 to 0.2 percent of surfactant and the balance of water; the unit is mass percentage;
the agent B comprises 2 to 5 percent of glossy privet fruit powder, 1 to 3 percent of prepared fleece-flower root powder, 0.5 to 3 percent of Chinese gall extract, 0.5 to 2 percent of myrobalan pigment, 0.5 to 3 percent of grape pigment, 0.5 to 2 percent of madder pigment, 1 to 2 percent of thickening agent, 2 to 4 percent of humectant, 0.1 to 0.2 percent of surfactant and the balance of water; the unit is mass percent.
Further, the water-soluble metal salt in the agent A is one or more of ferrous sulfate and zinc sulfate.
Further, the thickening agent is one or more of carboxymethyl cellulose, methyl cellulose, hydroxyethyl cellulose, Arabic gum, hydroxypropyl cellulose and hydroxypropyl methyl cellulose.
Further, the surfactant is one or more of non-toxic and nonirritating fatty alcohol polyoxyethylene ether nonionic surfactants and betaine amphoteric surfactants.
Further, the humectant is compounded by glycerin and one or more of polyethylene glycol 600, polyethylene glycol 800 and polyethylene glycol 1000.
Further, the glossy privet fruit in the preparation B is used after being crushed by a traditional Chinese medicine crusher and sieved by a 100-mesh sieve, and the prepared fleece-flower root is used after being crushed by the traditional Chinese medicine crusher and sieved by a 150-mesh sieve.
Further, the preparation method of the gallnut extract in the preparation B comprises the following steps: pulverizing Galla chinensis, sieving, extracting with 70% ethanol solution, vacuum filtering, purifying, extracting to remove harmful heavy metals, concentrating, drying, and recovering solvent.
Furthermore, pigment molecules with the molecular weight less than 350 are separated during the purification of myrobalan pigment, grape pigment and madder pigment in the agent B, and are used for preparing the hair dye after harmful heavy metals are removed by extraction.
The preparation method of the plant hair dye for nourishing and protecting hair of the invention comprises the following steps: the preparation method of the agent A comprises the following steps: adding the thickener into water, stirring while adding, continuously stirring to be transparent paste after adding, preparing 6-10% of thickener paste, and adding the humectant and the surfactant into the thickener paste; dissolving water-soluble metal salt and vitamin C in water, adding into thickener paste containing humectant and surfactant, adding the rest water, and stirring;
the preparation method of the agent B is as follows: weighing the glossy privet fruit powder and the prepared fleece-flower root powder according to the required amount, adding 75-85 ℃ hot water which is 5 times of the total mass of the glossy privet fruit powder and the prepared fleece-flower root powder, stirring and stirring uniformly while adding, and cooling to room temperature to obtain glossy privet fruit and prepared fleece-flower root paste for later use; the thickener paste is prepared by adding humectant and surfactant into thickener paste, stirring, adding fructus Ligustri Lucidi, radix Polygoni Multiflori Preparata paste, Galla chinensis extract, fructus Chebulae pigment, grape pigment, Rubia cordifolia pigment and water, and stirring.
The hair dyeing method of the plant hair dye for nourishing and protecting hair of the invention comprises the following steps: uniformly coating the agent A on hair, keeping at 45-55 deg.C for 20-40min, and washing hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 45-55 ℃ for 40-70 min; and finally, washing the hair.
Fructus Ligustri Lucidi has effects in nourishing liver and kidney, improving eyesight, blackening hair, delaying aging, regulating immunity, resisting tumor, resisting cancer, inhibiting bacteria, and resisting virus.
Radix Polygoni Multiflori Preparata has effects of nourishing essence and blood, and can be used for treating diseases due to essence and blood deficiency, such as premature gray hair, asthenia after illness, giddiness, tinnitus, neurasthenia, etc.
The Galla chinensis extract mainly contains Galla chinensis tannin and gallic acid, and has antibacterial, antiviral, mutation inhibiting, antioxidant, free radical scavenging, and antitumor effects.
The fructus Chebulae pigment is a natural plant pigment extracted from fructus Chebulae or fructus Chebulae (Terminalia chebula L.) of Combretaceae, and has antibacterial, free radical scavenging, antitumor, and ultraviolet resisting effects.
The grape pigment is widely present in the wastes of wine and grape beverage production and processing, and has wide sources. The grape pigment belongs to anthocyanin pigment, and has effects of resisting ultraviolet, inhibiting bacteria, resisting oxidation, scavenging free radicals, etc.
The madder pigment is a red yellow pigment extracted from roots of madder plants, and has the effects of cooling blood, stopping bleeding, clearing away heat and toxic materials, relieving swelling and pain, and promoting blood circulation to remove blood stasis.
The six components are matched for use, so that the hair dyeing agent has a broad-spectrum antibacterial effect, does not need a preservative, has natural hair dyeing color, little fading in the hair washing process and a lasting hair dyeing effect.
The invention has the beneficial effects that: the combination of fructus Ligustri Lucidi and radix Polygoni Multiflori Preparata can fully exert its health promotion function, and has effects of nourishing and caring hair, and can reduce the amount of thickener in hair dye. The hair surface is a scale layer, the structure is compact, plant pigment with larger molecular weight is used for dyeing, the dyeing is difficult, the pigment with the molecular weight less than 350, which is separated during the purification of the myrobalan pigment, the grape pigment and the madder pigment, is used for dyeing the hair, and the separated pigment with larger molecular weight can be used for dyeing textiles, so that natural resources can be fully utilized.
Uniformly coating the agent A on hair, keeping at 45-55 deg.C for 20-40min, forming coordination bond between metal ions in the agent A and hair, or forming ionic bond with carboxyl negative ions in hair, washing off other substances in the agent A with clear water, uniformly coating the agent B on hair, and keeping at 45-55 deg.C for 40-70 min; under the action of damp heat, the hair scale layer is expanded, the plant pigment dyes the hair, and forms coordinate bond combination with metal ions on the hair, so that the color fastness is improved, and the nutrient components in the agent B can play a role in hair nourishing and protecting.
The hair dye prepared from plant components such as glossy privet fruit, radix polygoni multiflori preparata, Chinese gall extract, myrobalan pigment, grape pigment, madder pigment and the like can play a broad-spectrum antibacterial role, does not need preservatives, has stable hair dyeing effect and less fading in the hair washing process, and can play the roles of nourishing and protecting hair and scalp while dyeing hair.
Drawings
FIG. 1 shows the color fastness after dyeing in examples 5 and 6.
FIG. 2 is a view showing the surface appearance of hair observed by a Quanta 250 scanning electron microscope, wherein (a) the surface appearance of white hair before dyeing, (b) the surface appearance of hair after dyeing using the plant hair dye for hair care and hair care of the present invention, and (c) the surface appearance of hair after dyeing using a certain brand of oxidative hair dye.
Detailed Description
The present invention will be further described with reference to the following examples. It is to be understood that the following examples are illustrative only and are not intended to limit the scope of the invention, which is to be given numerous insubstantial modifications and adaptations by those skilled in the art based on the teachings set forth above.
Example 1
The plant hair dye for nourishing and caring hair of the embodiment comprises a preparation A and a preparation B, wherein the preparation A comprises 4% of ferrous sulfate, 2% of methyl cellulose, 0.05% of vitamin C, 1% of glycerol, 6001% of polyethylene glycol, 0.2% of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The preparation B comprises fructus Ligustri Lucidi powder 5%, radix Polygoni Multiflori Preparata powder 3%, Galla chinensis extract 3%, fructus Chebulae pigment 2%, grape pigment 2%, Rubia cordifolia pigment 0.5%, hydroxypropyl methylcellulose 1%, glycerol 1%, polyethylene glycol 8003%, betaine amphoteric surfactant 0.2%, and water in balance; the unit is mass percent.
The application method of the plant hair dye for nourishing and caring hair in the embodiment comprises the following steps: uniformly coating the agent A on hair, keeping the temperature at 45 ℃ for 40min, and washing the hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 45 ℃ for 70 min; and finally, washing the hair.
Example 2
The plant hair dye for nourishing and caring hair of the embodiment comprises a preparation A and a preparation B, wherein the preparation A comprises 2% of zinc sulfate, 4% of hydroxyethyl cellulose, 0.01% of vitamin C, 0.5% of glycerol, 8003.5% of polyethylene glycol, 0.1% of fatty alcohol polyoxyethylene ether nonionic surfactant, 0.05% of betaine amphoteric surfactant and the balance of water; the unit is mass percent. The preparation B comprises 2% of glossy privet fruit powder, 1% of prepared fleece-flower root powder, 1% of Chinese gall extract, 0.5% of myrobalan pigment, 3% of grape pigment, 1.5% of madder pigment, 2% of Arabic gum, 0.5% of glycerol, 6002.5% of polyethylene glycol, 0.1% of betaine amphoteric surfactant and the balance of water; the unit is mass percent.
The application method of the plant hair dye for nourishing and caring hair in the embodiment comprises the following steps: uniformly coating the agent A on hair, keeping the temperature at 55 ℃ for 20min, and washing the hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 55 ℃ for 40 min; and finally, washing the hair.
Example 3
The plant hair dye for nourishing and caring hair of the embodiment comprises a preparation A and a preparation B, wherein the preparation A comprises 1% of ferrous sulfate, 1% of Arabic gum, 2% of hydroxypropyl cellulose, 0.03% of vitamin C, 1% of glycerol, 6000.5% of polyethylene glycol, 10001% of polyethylene glycol, 0.05% of fatty alcohol polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The preparation B comprises glossy privet fruit powder 3%, radix polygoni multiflori preparata powder 2%, gallnut extract 2%, myrobalan pigment 1%, grape pigment 0.5%, madder pigment 2%, hydroxyethyl cellulose 1%, hydroxypropyl cellulose 1%, glycerol 1%, polyethylene glycol 10001%, fatty alcohol polyoxyethylene ether nonionic surfactant 0.2% and the balance of water; the unit is mass percent.
The application method of the plant hair dye for nourishing and caring hair in the embodiment comprises the following steps: uniformly coating the agent A on hair, keeping the temperature at 50 ℃ for 30min, and washing the hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 50 ℃ for 50 min; and finally, washing the hair.
Example 4
The plant hair dye for nourishing and caring hair of the embodiment comprises an agent A and an agent B, wherein the agent A comprises 2% of ferrous sulfate, 1% of zinc sulfate, 1% of carboxymethyl cellulose, 3% of hydroxypropyl methyl cellulose, 0.04% of vitamin C, 1.5% of glycerol, 6000.5% of polyethylene glycol, 0.05% of betaine amphoteric surfactant and the balance of water; the unit is mass percent. The preparation B comprises glossy privet fruit powder 4%, radix polygoni multiflori preparata powder 3%, gallnut extract 0.5%, myrobalan pigment 1.5%, grape pigment 1%, madder pigment 1%, carboxymethyl cellulose 2%, glycerol 1.5%, polyethylene glycol 6001.5%, fatty alcohol polyoxyethylene ether nonionic surfactant 0.1%, betaine amphoteric surfactant 0.1%, and the balance of water; the unit is mass percent.
The application method of the plant hair dye for nourishing and caring hair in the embodiment comprises the following steps: uniformly coating the agent A on hair, keeping the temperature at 45 ℃ for 30min, and washing the hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 55 ℃ for 60 min; and finally, washing the hair.
Example 5
The plant hair dye for nourishing and caring hair of the embodiment comprises an agent A and an agent B, wherein the agent A comprises 2.5% of ferrous sulfate, 1% of zinc sulfate, 2% of hydroxyethyl cellulose, 1% of methyl cellulose, 0.02% of vitamin C, 2% of glycerol, 8002% of polyethylene glycol, 0.1% of fatty alcohol polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The preparation B comprises fructus Ligustri Lucidi powder 2%, radix Polygoni Multiflori Preparata powder 2%, Galla chinensis extract 1%, fructus Chebulae pigment 1%, grape pigment 3%, Rubia cordifolia pigment 2%, hydroxypropyl cellulose 2%, glycerol 2%, polyethylene glycol 8002%, fatty alcohol polyoxyethylene ether nonionic surfactant 0.1%, and water in balance; the unit is mass percent.
The application method of the plant hair dye for nourishing and caring hair in the embodiment comprises the following steps: uniformly coating the agent A on hair, keeping the temperature at 50 ℃ for 40min, and washing the hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 55 ℃ for 50 min; and finally, washing the hair.
Example 6
The plant hair dye for nourishing and caring hair of the embodiment comprises a preparation A and a preparation B, wherein the preparation A comprises 3% of ferrous sulfate, 2.5% of hydroxypropyl methylcellulose, 0.03% of vitamin C, 2% of glycerol, 10001% of polyethylene glycol, 0.1% of betaine amphoteric surfactant and the balance of water; the unit is mass percent. The preparation B comprises 5 percent of glossy privet fruit powder, 1 percent of prepared fleece-flower root powder, 2 percent of nutgall extract, 2 percent of myrobalan pigment, 1 percent of grape pigment, 1 percent of madder pigment, 1 percent of methyl cellulose, 3 percent of glycerol, 10000.5 percent of polyethylene glycol, 0.05 percent of fatty alcohol polyoxyethylene ether nonionic surfactant, 0.15 percent of betaine amphoteric surfactant and the balance of water; the unit is mass percent.
The application method of the plant hair dye for nourishing and caring hair in the embodiment comprises the following steps: uniformly coating the agent A on hair, keeping the temperature at 55 ℃ for 30min, and washing the hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 45 ℃ for 70 min; and finally, washing the hair.
Example 7
The plant hair dye for nourishing and caring hair of the embodiment comprises a preparation A and a preparation B, wherein the preparation A comprises 4% of zinc sulfate, 3% of hydroxypropyl cellulose, 0.02% of vitamin C, 3% of glycerol, 10001% of polyethylene glycol, 0.2% of betaine amphoteric surfactant and the balance of water; the unit is mass percent. Agent B comprises fructus Ligustri Lucidi powder 4%, radix Polygoni Multiflori Preparata powder 2%, Galla chinensis extract 2.5%, fructus Chebulae pigment 0.5%, grape pigment 1.5%, Rubia cordifolia pigment 0.5%, hydroxyethyl cellulose 2%, glycerol 3.5%, polyethylene glycol 6000.5%, fatty alcohol polyoxyethylene ether nonionic surfactant 0.05%, betaine amphoteric surfactant 0.05%, and water in balance; the unit is mass percent.
The application method of the plant hair dye for nourishing and caring hair in the embodiment comprises the following steps: uniformly coating the agent A on hair, keeping the temperature at 50 ℃ for 20min, and washing the hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 50 ℃ for 70 min; and finally, washing the hair.
Example 8
The plant hair dye for nourishing and caring hair comprises an agent A and an agent B, wherein the agent A comprises 3% of zinc sulfate, 4% of carboxymethyl cellulose, 0.01% of vitamin C, 3.5% of glycerol, 10000.5% of polyethylene glycol, 0.15% of fatty alcohol polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The preparation B comprises glossy privet fruit powder 3%, prepared fleece-flower root powder 1%, Chinese gall extract 3%, myrobalan pigment 2%, grape pigment 1%, madder pigment 0.5%, carboxymethyl cellulose 0.5%, methyl cellulose 0.5%, hydroxyethyl cellulose 0.5%, arabic gum 0.5%, glycerin 0.5%, polyethylene glycol 10001.5%, fatty alcohol polyoxyethylene ether nonionic surfactant 0.15%, and the balance of water; the unit is mass percent.
The application method of the plant hair dye for nourishing and caring hair in the embodiment comprises the following steps: uniformly coating the agent A on hair, keeping the temperature at 45 ℃ for 20min, and washing the hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 55 ℃ for 70 min; and finally, washing the hair.
Example 9
The plant hair dye for nourishing and caring hair of the embodiment comprises a preparation A and a preparation B, wherein the preparation A comprises 1% of ferrous sulfate, 3% of zinc sulfate, 1% of hydroxyethyl cellulose, 1% of Arabic gum, 1% of hydroxypropyl cellulose, 1% of hydroxypropyl methyl cellulose, 0.02% of vitamin C, 0.5% of glycerol, 6001.5% of polyethylene glycol, 0.15% of betaine amphoteric surfactant and the balance of water; the unit is mass percent. The preparation B comprises fructus Ligustri Lucidi powder 2%, radix Polygoni Multiflori Preparata powder 3%, Galla chinensis extract 0.5%, fructus Chebulae pigment 1%, grape pigment 0.5%, Rubia cordifolia pigment 2%, hydroxypropyl cellulose 1%, glycerol 0.5%, polyethylene glycol 8002.5%, betaine amphoteric surfactant 0.15%, and water in balance; the unit is mass percent.
The application method of the plant hair dye for nourishing and caring hair in the embodiment comprises the following steps: uniformly coating the agent A on hair, keeping the temperature at 55 ℃ for 40min, and washing the hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 45 ℃ for 40 min; and finally, washing the hair.
Example 10
The plant hair dye for nourishing and caring hair of the embodiment comprises a preparation A and a preparation B, wherein the preparation A comprises 2% of ferrous sulfate, 4% of Arabic gum, 0.05% of vitamin C, 0.5% of glycerol, 10003.5% of polyethylene glycol, 0.15% of fatty alcohol-polyoxyethylene ether nonionic surfactant, 0.05% of betaine amphoteric surfactant and the balance of water; the unit is mass percent. The preparation B comprises glossy privet fruit powder 4%, radix polygoni multiflori preparata powder 2%, gallnut extract 1%, myrobalan pigment 0.5%, grape pigment 3%, madder pigment 1%, carboxymethyl cellulose 1%, glycerol 0.5%, polyethylene glycol 6003.5%, fatty alcohol polyoxyethylene ether nonionic surfactant 0.15%, betaine amphoteric surfactant 0.05% and the balance of water; the unit is mass percent.
The application method of the plant hair dye for nourishing and caring hair in the embodiment comprises the following steps: uniformly coating the agent A on hair, keeping the temperature at 50 ℃ for 35min, and washing the hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 50 ℃ for 40 min; and finally, washing the hair.
Testing of color characteristic values: the measurements were carried out 4 times per sample using a SCT textile color measuring and matching instrument model CE7000A, using a D65 illuminant and an observation angle of 10 ℃ and averaged.
Color fastness: rubbing the dyed hair with shampoo for 1min, washing for 1min, rubbing with towel, drying with blower, and combing for 1 time. The hair was washed several times, and the values of L, a, and b before and after washing were measured with a color measuring instrument, and each sample was measured 4 times using a D65 light source and an observation angle of 10 degrees, and the average value was taken. The color difference (. DELTA.E) before and after washing was calculated by the following equation (1).
ΔE＝[(Ln*-L0*)2+(an*-a0*)2+(bn*-b0*)2]1/2 (1)
Wherein L is0*、a0*、b0Color characteristic values before washing, Ln*、an*、bnEach is a color feature value after n washes.
TABLE 1 examples 1-10 color characteristics and shine of hair after dyeing
| K/S value | a* | b* | Hair shine | |
| Example 1 | 16.685 | 2.762 | 0.575 | Good taste |
| Example 2 | 13.728 | 7.255 | 7.609 | Good taste |
| Example 3 | 12.539 | 5.354 | 1.762 | Good taste |
| Example 4 | 14.776 | 5.783 | 3.695 | Good taste |
| Example 5 | 16.878 | 5.843 | 1.013 | Good taste |
| Example 6 | 15.239 | 3.001 | 0.515 | Good taste |
| Example 7 | 12.736 | 7.486 | 4.823 | Good taste |
| Example 8 | 13.282 | 6.357 | 4.176 | Good taste |
| Example 9 | 13.625 | 5.628 | 2.465 | Good taste |
| Example 10 | 14.791 | 3.672 | 1.453 | Good taste |
The K/S value represents the apparent color depth, K is an absorption coefficient, S is a scattering coefficient, and the larger the K/S value is, the more light is absorbed, the thicker the color is; a represents red and green colorimetric values of the color, and the a value is positive and represents the color deviation of red; the a is negative and indicates that the color light is green. b represents a yellow-blue colorimetric value of the color, and the b value is positive and represents the color deviation yellow; the b-value is negative and indicates that the color light is blue.
The results of the color fastness tests after dyeing of example 5, example 6 are shown in FIG. 1.
As can be seen from fig. 1, the difference in color increases with the number of washing times, and the difference in color does not change much with the number of washing times after the number of washing times exceeds 14. After 12 times of washing, the color difference of example 5 is less than 5, and the color difference of example 6 is less than 4, which indicates that the color fastness is better.
20 allergic constitution volunteers were selected and each person was dyed 10 times with the hair dye and the dyeing method of example 5, and the safety of the hair dye was evaluated, and the results are shown in Table 2.
TABLE 2 evaluation results of safety
| Irritation property | Anaphylaxis (itching, red swelling, burning pain, eruption, etc. of scalp) | Alopecia (baldness) |
| Is free of | Is free of | Is free of |
Comparative example 1 (based on example 5, the plant components in agent B are all glossy privet fruit powder)
The agent A comprises 2.5 percent of ferrous sulfate, 1 percent of zinc sulfate, 2 percent of hydroxyethyl cellulose, 1 percent of methyl cellulose, 0.02 percent of vitamin C, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The agent B comprises 11 percent of glossy privet fruit powder, 2 percent of hydroxypropyl cellulose, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent.
The hair dyeing method was the same as in example 5.
Comparative example 2 (based on example 5, the plant components in agent B are all prepared fleece-flower root powder)
The agent A comprises 2.5 percent of ferrous sulfate, 1 percent of zinc sulfate, 2 percent of hydroxyethyl cellulose, 1 percent of methyl cellulose, 0.02 percent of vitamin C, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The preparation B comprises 11% of prepared fleece-flower root powder, 2% of hydroxypropyl cellulose, 2% of glycerol, 8002% of polyethylene glycol, 0.1% of fatty alcohol polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent.
The hair dyeing method was the same as in example 5.
Comparative example 3 (on the basis of example 5, the plant components in agent B were all gallnut extract)
The agent A comprises 2.5 percent of ferrous sulfate, 1 percent of zinc sulfate, 2 percent of hydroxyethyl cellulose, 1 percent of methyl cellulose, 0.02 percent of vitamin C, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The agent B comprises 11% of nutgall extract, 2% of hydroxypropyl cellulose, 2% of glycerol, 8002% of polyethylene glycol, 0.1% of fatty alcohol polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent.
The hair dyeing method was the same as in example 5.
Comparative example 4 (in example 5, all the plant components in agent B were myrobalan pigment)
The agent A comprises 2.5 percent of ferrous sulfate, 1 percent of zinc sulfate, 2 percent of hydroxyethyl cellulose, 1 percent of methyl cellulose, 0.02 percent of vitamin C, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The agent B comprises 11% of myrobalan pigment, 2% of hydroxypropyl cellulose, 2% of glycerol, 8002% of polyethylene glycol, 0.1% of fatty alcohol polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent.
The hair dyeing method was the same as in example 5.
Comparative example 5 (in example 5, all the plant components in agent B were grape pigment)
The agent A comprises 2.5 percent of ferrous sulfate, 1 percent of zinc sulfate, 2 percent of hydroxyethyl cellulose, 1 percent of methyl cellulose, 0.02 percent of vitamin C, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The agent B comprises 11% of grape pigment, 2% of hydroxypropyl cellulose, 2% of glycerol, 8002% of polyethylene glycol, 0.1% of fatty alcohol polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent.
The hair dyeing method was the same as in example 5.
Comparative example 6 (based on example 5, all of the plant components in agent B were alizarin)
The agent A comprises 2.5 percent of ferrous sulfate, 1 percent of zinc sulfate, 2 percent of hydroxyethyl cellulose, 1 percent of methyl cellulose, 0.02 percent of vitamin C, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The agent B comprises 11% of madder pigment, 2% of hydroxypropyl cellulose, 2% of glycerol, 8002% of polyethylene glycol, 0.1% of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent.
The hair dyeing method was the same as in example 5.
TABLE 3 Hair dyeing Effect of comparative examples 1 to 6
As shown in Table 3, the poor storage stability of the formulation B containing only fructus Ligustri Lucidi and radix Polygoni Multiflori Preparata is mainly caused by the fact that radix Polygoni Multiflori Preparata contains more starch and fructus Ligustri Lucidi contains more cellulose and protein. None of the 6 comparative examples in table 3 had a sufficiently dark hair color. In contrast, comparative examples 4, 5 and 6 have higher hair dyeing color yield.
Comparative example 7 (myrobalan pigment + grape pigment + madder pigment)
The agent A comprises 2.5 percent of ferrous sulfate, 1 percent of zinc sulfate, 2 percent of hydroxyethyl cellulose, 1 percent of methyl cellulose, 0.02 percent of vitamin C, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The agent B comprises myrobalan pigment 6%, grape pigment 3%, madder pigment 2%, hydroxypropyl cellulose 2%, glycerol 2%, polyethylene glycol 8002%, fatty alcohol polyoxyethylene ether nonionic surfactant 0.1%, and the balance of water; the unit is mass percent.
The hair dyeing method was the same as in example 5.
Comparative example 8 (Galla chinensis extract + Terminalia chebula pigment + grape pigment + madder pigment)
The agent A comprises 2.5 percent of ferrous sulfate, 1 percent of zinc sulfate, 2 percent of hydroxyethyl cellulose, 1 percent of methyl cellulose, 0.02 percent of vitamin C, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The preparation B comprises 5% of nutgall extract, 1% of myrobalan pigment, 3% of grape pigment, 2% of madder pigment, 2% of hydroxypropyl cellulose, 2% of glycerol, 8002% of polyethylene glycol, 0.1% of fatty alcohol polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent.
The hair dyeing method was the same as in example 5.
Comparative example 9 (glossy privet fruit powder + gallnut extract + myrobalan pigment + grape pigment + madder pigment)
The agent A comprises 2.5 percent of ferrous sulfate, 1 percent of zinc sulfate, 2 percent of hydroxyethyl cellulose, 1 percent of methyl cellulose, 0.02 percent of vitamin C, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. Agent B comprises fructus Ligustri Lucidi powder 4%, Galla chinensis extract 1%, fructus Chebulae pigment 1%, grape pigment 3%, alizarin pigment 2%, hydroxypropyl cellulose 2%, glycerol 2%, polyethylene glycol 8002%, fatty alcohol polyoxyethylene ether nonionic surfactant 0.1%, and water in balance; the unit is mass percent.
The hair dyeing method was the same as in example 5.
Comparative example 10 (radix Polygoni Multiflori Preparata powder + Galla chinensis extract + Terminalia chebula pigment + grape pigment + Rubia cordifolia pigment)
The agent A comprises 2.5 percent of ferrous sulfate, 1 percent of zinc sulfate, 2 percent of hydroxyethyl cellulose, 1 percent of methyl cellulose, 0.02 percent of vitamin C, 2 percent of glycerol, 8002 percent of polyethylene glycol, 0.1 percent of fatty alcohol-polyoxyethylene ether nonionic surfactant and the balance of water; the unit is mass percent. The preparation B comprises radix Polygoni Multiflori Preparata powder 4%, Galla chinensis extract 1%, fructus Chebulae pigment 1%, grape pigment 3%, Rubia cordifolia pigment 2%, hydroxypropyl cellulose 2%, glycerol 2%, polyethylene glycol 8002%, fatty alcohol polyoxyethylene ether nonionic surfactant 0.1%, and water in balance; the unit is mass percent.
The hair dyeing method was the same as in example 5.
TABLE 4 hair dyeing effect of comparative examples 7 to 10 and example 5
As can be seen from the comparison of tables 3 and 4, the myrobalan pigment, the grape pigment and the madder pigment are used independently, so that the hair dyeing color is lighter, and the hair dyeing color depth can be improved after the hair dyeing pigment is mixed and used. As shown in Table 4, both the glossy privet fruit and the radix polygoni multiflori preparata have certain hair nourishing and protecting effects, and the hair nourishing and protecting effects are better when the glossy privet fruit and the radix polygoni multiflori preparata are mixed. The deterioration of hair dye containing fructus Ligustri Lucidi powder and radix Polygoni Multiflori Preparata powder can be prevented by adding Galla chinensis extract, fructus Chebulae pigment, grape pigment, and Rubia cordifolia pigment.
Comparative example 11
The formula and the hair dyeing method of the hair dye are the same as those in example 5, and the difference from example 5 is that the pigments with different molecular weights are not separated during the purification of the myrobalan pigment, the grape pigment and the madder pigment.
As a result: comparative example 11 the hair dyed was slightly lighter than example 5, significantly poorer in color fastness than example 5, and was severely faded upon shampooing. The main reason is that the dye with large molecular weight can not dye the hair fully, and part of the pigment can only be absorbed on the outer surface of the scale layer of the hair, so that the hair is easy to fade when being washed.
Fig. 2 is a view of the surface appearance of hair observed by a Quanta 250 scanning electron microscope, and it can be seen from fig. 2 that after the plant hair dye for nourishing and caring hair of the present invention is used for dyeing hair, the scales on the surface of hair are not damaged, and after a certain brand of oxidation type hair dye is used for dyeing hair, the scales on the surface of hair are shortened and obviously damaged.
The foregoing shows and describes the general principles and features of the present invention, together with the advantages thereof. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (9)
1. A plant hair dye for nourishing and caring hair is characterized in that: comprises an agent A and an agent B,
the agent A comprises 1 to 4 percent of water-soluble metal salt, 2 to 4 percent of thickening agent, 0.01 to 0.05 percent of vitamin C, 2 to 4 percent of humectant, 0.05 to 0.2 percent of surfactant and the balance of water; the unit is mass percentage;
the agent B comprises 2 to 5 percent of glossy privet fruit powder, 1 to 3 percent of prepared fleece-flower root powder, 0.5 to 3 percent of Chinese gall extract, 0.5 to 2 percent of myrobalan pigment, 0.5 to 3 percent of grape pigment, 0.5 to 2 percent of madder pigment, 1 to 2 percent of thickening agent, 2 to 4 percent of humectant, 0.1 to 0.2 percent of surfactant and the balance of water; the unit is mass percentage;
the myrobalan pigment, the grape pigment and the madder pigment in the agent B are separated to obtain pigment molecules with the molecular weight less than 350 during purification, and the pigment molecules are extracted to remove harmful heavy metals and then are used for preparing the hair dye.
2. The plant hair dye for nourishing and caring hair according to claim 1, wherein: the water-soluble metal salt in the agent A is one or more of ferrous sulfate and zinc sulfate.
3. The plant hair dye for nourishing and caring hair according to claim 1, wherein: the thickener is one or more of carboxymethyl cellulose, methyl cellulose, hydroxyethyl cellulose, acacia, hydroxypropyl cellulose and hydroxypropyl methyl cellulose.
4. The plant hair dye for nourishing and caring hair according to claim 1, wherein: the surfactant is one or more of nontoxic and nonirritating fatty alcohol polyoxyethylene ether nonionic surfactant and betaine amphoteric surfactant.
5. The plant hair dye for nourishing and caring hair according to claim 1, wherein: the humectant is one or more of glycerin and polyethylene glycol 600, polyethylene glycol 800 and polyethylene glycol 1000.
6. The plant hair dye for nourishing and caring hair according to claim 1, wherein: the glossy privet fruit in the preparation B is used after being crushed by a traditional Chinese medicine crusher and sieved by a 100-mesh sieve, and the prepared fleece-flower root is used after being crushed by a traditional Chinese medicine crusher and sieved by a 150-mesh sieve.
7. The plant hair dye for nourishing and caring hair according to claim 1, wherein: the preparation method of the gallnut extract in the preparation B comprises the following steps: pulverizing Galla chinensis, sieving, extracting with 70% ethanol solution, vacuum filtering, purifying, extracting to remove harmful heavy metals, concentrating, drying, and recovering solvent.
8. The method for preparing a plant hair dye for nourishing and caring hair according to any one of claims 1 to 7, wherein: the preparation method of the agent A comprises the following steps: adding the thickener into water, stirring while adding, continuously stirring to form a transparent paste after adding, preparing 6-10% of thickener paste, and adding the humectant and the surfactant into the thickener paste; dissolving water-soluble metal salt and vitamin C in water, adding into thickener paste containing humectant and surfactant, adding the rest water, and stirring;
the preparation method of the agent B is as follows: weighing the glossy privet fruit powder and the prepared fleece-flower root powder according to the required amount, adding 75-85 ℃ hot water which is 5 times of the total mass of the glossy privet fruit powder and the prepared fleece-flower root powder, stirring and stirring uniformly while adding, and cooling to room temperature to obtain glossy privet fruit and prepared fleece-flower root paste for later use; the thickener paste is prepared by adding humectant and surfactant into thickener paste, stirring, adding fructus Ligustri Lucidi, radix Polygoni Multiflori Preparata paste, Galla chinensis extract, fructus Chebulae pigment, grape pigment, Rubia cordifolia pigment and water, and stirring.
9. A method for dyeing hair by using the plant hair dye for hair care according to any one of claims 1 to 7, characterized in that: uniformly coating the agent A on hair, keeping at 45-55 deg.C for 20-40min, and washing hair with clear water; then, uniformly coating the agent B on hair, and keeping the temperature at 45-55 ℃ for 40-70 min; and finally, washing the hair.
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| CN113599287A (en) * | 2021-09-17 | 2021-11-05 | 广州御采堂化妆品有限公司 | Two-agent type clear water hair dyeing composition and hair dyeing method thereof |
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