CN110393686A - A kind of preparation method and application of bush tealeaves compound botanical hair dye - Google Patents

A kind of preparation method and application of bush tealeaves compound botanical hair dye Download PDF

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CN110393686A
CN110393686A CN201910816725.0A CN201910816725A CN110393686A CN 110393686 A CN110393686 A CN 110393686A CN 201910816725 A CN201910816725 A CN 201910816725A CN 110393686 A CN110393686 A CN 110393686A
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stain
hair
tealeaves
water
bush
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李志英
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Xinzhou Teachers University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00Preparations for care of the hair
    • A61Q5/10Preparations for permanently dyeing the hair
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42Colour properties
    • A61K2800/43Pigments; Dyes
    • A61K2800/432Direct dyes
    • A61K2800/4324Direct dyes in preparations for permanently dyeing the hair

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  • Health & Medical Sciences (AREA)
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  • Cosmetics (AREA)

Abstract

The invention belongs to hair dye technical fields, and in particular to a kind of preparation method and application of bush tealeaves compound botanical hair dye.Present invention mainly solves chemical synthesis class hair dye exists in the prior art toxic to human body, harmful, the big problems of environmental pollution.The present invention includes tri- kinds of A, B, C independent stain compositions, and wherein A stain includes: L-cysteine, sodium carbonate, triethanolamine, sodium carboxymethylcellulose, glycerine and water;B stain includes: iron chloride, sodium carboxymethylcellulose, octyl phenol polyoxyethylene ether and water;C stain includes: hematoxylin, tealeaves pigment, sodium carboxymethylcellulose, citric acid, octyl phenol polyoxyethylene ether and water.Dye component is natural plant pigment hematoxylin and tealeaves pigment, Fe in the present invention3+Mordant is made, H is first used using same bath mordant dyeing2O2Oxidation hair, then softened hair with A stain, it has hair dyed after being mixed with B stain with C stain.

Description

A kind of preparation method and application of bush tealeaves compound botanical hair dye
Technical field
The invention belongs to hair dye technical fields, and in particular to a kind of preparation method of bush tealeaves compound botanical hair dye And application.
Background technique
Hair dye is to a kind of cosmetics of hair-dyeing.By investigation, at home and abroad its sales volume is already at ascendant trend, Hair dyeing has become the fashion selection of people, but the hair dyeing article of international and domestic market prevalence the most is still chemical classes hair dyeing Agent.Chemical synthesis class hair dye hair color is more, and dyeing effect is good, and stability is good, while its raw material is again cheap and easy to get, is had hair dyed Industry is widely used, but due to substances such as the use of a large amount of chemical synthesis substances, especially aromatic amine and amino phenols, makes It can cause great harm human body with extremely strong sensitization and carcinogenicity, such as cause oedema, the bad disease such as headache Shape.
Since reform and opening-up, China's hair color market is influenced by abroad phenyl amines chemistry hair dye, causes chemical hair dyeing Domestic market is impacted in agent.Phenyl amines chemistry hair dye is mainly to be with o-phenylenediamine, m-phenylene diamine (MPD), p-phenylenediamine and its derivative Dye the oxidative hair dyes of intermediate.Although upper color fastness is strong, dyeing time is short and cheap for such hair dye, still Phenylenediamine chemical substance property toxic to human body will lead to human body and many ill symptoms occur, such as if absorbing through human skin Liver damage etc..Therefore in order to reduce damage of the chemical synthesis class hair dye to human body, the research direction of scientist was more in recent years To be explicitly directed to using plant the hair dye for preparing Nantural non-toxic.
Without oxidation dye intermediates such as chemical syntheses in natural botanical hair dye, generally formed by two doses, Yi Jiyou Coloring agent composition, another dose is made of auxiliary agent and metal-chelator.There are two types of its main function mechanism: one is pigment absorption Type;Another kind be active components of plants with it is metal complexed, utilize active constituent in plant and metal salt to form complex compound, infiltration Into hair epidermis or cortex, this mode hair dyeing effect is permanent.The ingredient that botanical hair dye mainly plays a role is vegetable colour. Vegetable colour is nontoxic, quality is natural and highly-safe, and also there is Activities of Some Plants dyestuff certain nutritive value and pharmacology to make With the disadvantages of avoiding carcinogenic chemical synthetic dye, sensitization.At the same time, vegetable colour is easily decomposed and utilizes, and is a kind of Environmentally friendly raw material, substantially pollution-free and available raw material resources are quite abundant.Therefore it has hair dyed for natural plants The development and utilization of agent is imperative.
Bush is a kind of Chinese medicine, and main component is haematoxylin and hematoxylin, has the function of anti-inflammatory and antibacterial.As Raw material extracts pigment, and hair dye obtained, without anaphylaxis and carcinogenicity, and has a good biodegradability to skin, It is environment friendly and pollution-free;Hydroxyl group is rich in hematoxylin molecule, there are also certain antibacterial functions for extracting solution.
China is the native place of tea, and Tea Pigment is a kind of water-soluble phenolic pigment extracted from tealeaves, is contained in Tea Pigment The chemical active ingredients such as a large amount of activity phenolic hydroxyl group, have the function of stronger removing free radical and anti peroxidation of lipid.Catechu Element is the main coloring components of the main soluble pigment and tealeaves pigment in tealeaves pigment.
Summary of the invention
Present invention is generally directed to exist in the prior art, chemical synthesis class hair dye is toxic to human body, harmful, environmental pollution Big problem provides a kind of preparation method and application of bush tealeaves compound botanical hair dye.
In order to achieve the above object, present invention employs following technical proposals:
A kind of bush tealeaves compound botanical hair dye, is made of the stain of tri- independent packagings of A, B, C, under A stain includes State the component of parts by weight: 1 part of L-cysteine, 1 part of sodium carbonate, 0.6 part of triethanolamine, 0.3 part of sodium carboxymethylcellulose, third 0.2 part and 7 parts of water of triol;B stain includes the component of following portions by weight: 0.7 part of iron chloride, 1.5 parts of sodium carboxymethylcellulose, 0.3 part and 8 parts of water of octyl phenol polyoxyethylene ether;C stain includes the component of following portions by weight: 0.2 part of hematoxylin, Tea color 0.2 part of element, 0.4 part of sodium carboxymethylcellulose, 0.4 part of citric acid, 0.4 part of octyl phenol polyoxyethylene ether and 12 parts of water.
A kind of preparation method of bush tealeaves compound botanical hair dye, comprising the following steps:
(1) it takes stem tea several, cleans, dry 30min at 110 DEG C, be ground into 60 mesh powders, using 40% second Alcohol extracts 10min as extractant, and Extracting temperature is 80 DEG C, and the tea-leaf power of crushing is mixed in mass ratio for 1:40 with distilled water It closes, filtering dries after filtrate is concentrated, tealeaves pigment is made;
(2) it takes bush several, cleans, dry 30min at 110 DEG C, be ground into 60 mesh powders, under room temperature, will crush Sappan wood and distilled water be in mass ratio 1:25 proportion, adjust pH=9, keep solution boiling temperature extract 50min, obtain To hematoxylin extracting solution, filter paper is placed on Buchner funnel, using vacuum pump to the reddish yellow hematoxylin extracting solution into Row filters, and after collecting filtrate and being concentrated, is placed in drying in baking oven, hematoxylin is made;
(3) tealeaves pigment, hematoxylin and other components made of taking, according to the stain by tri- independent packagings of A, B, C Composition, A stain includes the component of following portions by weight: 1 part of L-cysteine, 1 part of sodium carbonate, 0.6 part of triethanolamine, carboxymethyl 0.3 part of sodium cellulosate, 0.2 part of glycerine and 7 parts of water;B stain includes the component of following portions by weight: 0.7 part of iron chloride, carboxylic first 1.5 parts of base sodium cellulosate, 0.3 part of octyl phenol polyoxyethylene ether and 8 parts of water;C stain includes the component of following portions by weight: bush 0.2 part of pigment, 0.2 part of tealeaves pigment, 0.4 part of sodium carboxymethylcellulose, 0.4 part of citric acid, 0.4 part of octyl phenol polyoxyethylene ether With 12 parts of water;It is uniformly mixed and bush tealeaves compound botanical hair dye is made.
A kind of bush tealeaves compound botanical hair dye application is used for hair-dyeing.
A kind of application method of bush tealeaves compound botanical hair dye, comprising the following steps:
(1) hair to be dyed is cleaned, and with 6% H now prepared2O2Solution is applied to the oxidation of hair position 10min;
(2) A stain is applied to the hair position aoxidized to soften, the softening time is 30-40min, softening temperature It is 35-40 DEG C, then water is cleaned up and dried;
(3) it takes B stain and C stain to be mixed with the ratio of 1:1, B stain and C stain intermixture is applied to hair portion Position keeps 50-60min, and temperature is 40-45 DEG C, then rinses well, conventionally by hair dryer.
Compared with prior art the invention has the following advantages that the present invention selects natural plant pigment bush and tealeaves to replace Chemical synthetic dye, without oxidation dye intermediates such as chemical syntheses, without the examination for having potential hazard to human body in entire preparation Agent does not generate any pair of poisonous and hazardous substance of human body in hair dye yet, and hair colouring methods are easily understood, after hair dyeing quality from So, highly-safe, and vegetable colour is easily decomposed and utilizes, and is a kind of environmentally friendly raw material, it is substantially pollution-free and can Material resources are also very abundant.Simple production process is easy to extract and prepare, at low cost.
Detailed description of the invention
Fig. 1 is blank group and iron chloride is added to the comparison diagram of tea extract color change;
Fig. 2 is blank group and iron chloride is added to the comparison diagram of bush extracting solution color change;
Fig. 3 is blank group and iron chloride is added to the comparison diagram of mixed extract color change;
Fig. 4 is the different hair dyeing effect figure of temperature of having hair dyed;
Fig. 5 is the different hair dyeing effect figure of dyeing time.
Specific embodiment
The following examples are further illustrations of the invention, rather than limiting the invention.
Embodiment 1:
A kind of bush tealeaves compound botanical hair dye, is made of the stain of tri- independent packagings of A, B, C:
A stain includes the component of following portions by weight: L-cysteine 1.0g, sodium carbonate 1.0g, triethanolamine 0.6g, carboxylic Sodium carboxymethylcellulose pyce 0.3g, glycerine 0.2g and water 7.0g;
B stain includes the component of following portions by weight: iron chloride 0.7g, sodium carboxymethylcellulose 1.5g, octyl phenol polyoxy Vinethene 0.3g and water 8.0g;
C stain includes the component of following portions by weight: hematoxylin 0.2g, tealeaves pigment 0.2g, sodium carboxymethylcellulose 0.4g, citric acid 0.4g, octyl phenol polyoxyethylene ether 0.4g and water 12.0g.
A kind of preparation method of bush tealeaves compound botanical hair dye, comprising the following steps:
(1) it takes stem tea several, cleans, dry 30min at 110 DEG C, be ground into 60 mesh powders, using 40% second Alcohol extracts 10min as extractant, and Extracting temperature is 80 DEG C, and the tea-leaf power of crushing is mixed in mass ratio for 1:40 with distilled water It closes, filtering dries after filtrate is concentrated, tealeaves pigment is made;See that Fig. 1 is blank group and iron chloride is added to tea extract face The comparison diagram of color change, is blank group in the test tube of the figure left side, and the right test tube is that tea extract color change after iron chloride is added Situation obviously observes that iron chloride can make tea extract colour developing more obvious by comparing;
(2) it takes bush several, cleans, dry 30min at 110 DEG C, be ground into 60 mesh powders, under room temperature, will crush Sappan wood and distilled water be in mass ratio 1:25 proportion, adjust pH=9, keep solution boiling temperature extract 50min, obtain To hematoxylin extracting solution, filter paper is placed on Buchner funnel, using vacuum pump to the reddish yellow hematoxylin extracting solution into Row filters, and after collecting filtrate and being concentrated, is placed in drying in baking oven, hematoxylin is made;See that Fig. 2 is blank group and addition iron chloride It is blank group in the test tube of the figure left side to the comparison diagram of bush extracting solution color change, the right test tube is that bush after iron chloride is added Extracting solution color change situation obviously observes that iron chloride can make the colour developing of bush extracting solution more obvious by comparing;
(3) tealeaves pigment, hematoxylin and other components made of taking, according to the stain by tri- independent packagings of A, B, C, A stain includes the component of following portions by weight: 1 part of L-cysteine, 1 part of sodium carbonate, 0.6 part of triethanolamine, carboxymethyl cellulose 0.3 part of plain sodium, 0.2 part of glycerine and 7 parts of water;B stain includes the component of following portions by weight: 0.7 part of iron chloride, carboxymethyl are fine Plain 1.5 parts of the sodium of dimension, 0.3 part of octyl phenol polyoxyethylene ether and 8 parts of water;C stain includes the component of following portions by weight: hematoxylin 0.2 part, 0.2 part of tealeaves pigment, 0.4 part of sodium carboxymethylcellulose, 0.4 part of citric acid, 0.4 part of octyl phenol polyoxyethylene ether and water 12 parts;It is uniformly mixed and bush tealeaves compound botanical hair dye is made.
A kind of application method of bush tealeaves compound botanical hair dye, it is characterized in that the following steps are included:
(1) hair to be dyed is cleaned, and with 6% H now prepared2O2Solution is applied to the oxidation of hair position 10min;
(2) A stain is applied to the hair position aoxidized to soften, the softening time is 30min, softening temperature 35 DEG C, then water is cleaned up and is dried;
(3) it takes B stain and C stain to be mixed with the ratio of 1:1, B stain and C stain intermixture is applied to hair portion Position keeps 50min, and temperature is 40 DEG C, then rinses well, conventionally by hair dryer.See that Fig. 3 is blank group and adds Enter iron chloride to the comparison diagram of mixed extract color change, be blank group in the test tube of the figure left side, the right test tube is that chlorination is added Mixed extract color change situation after iron obviously observes that iron chloride can make mixed extract colour developing brighter by comparing It is aobvious.
Embodiment 2:
A kind of bush tealeaves compound botanical hair dye, is made of the stain of tri- independent packagings of A, B, C:
A stain includes the component of following portions by weight: L-cysteine 1.0g, sodium carbonate 1.0g, triethanolamine 0.6g, carboxylic Sodium carboxymethylcellulose pyce 0.3g, glycerine 0.2g and water 7.0g;
B stain includes the component of following portions by weight: iron chloride 0.7g, sodium carboxymethylcellulose 1.5g, octyl phenol polyoxy Vinethene 0.3g and water 8.0g;
C stain includes the component of following portions by weight: hematoxylin 0.2g, tealeaves pigment 0.2g, sodium carboxymethylcellulose 0.4g, citric acid 0.4g, octyl phenol polyoxyethylene ether 0.4g and water 12.0g.
A kind of preparation method of bush tealeaves compound botanical hair dye, comprising the following steps:
(1) it takes stem tea several, cleans, dry 30min at 110 DEG C, be ground into 60 mesh powders, using 40% second Alcohol extracts 10min as extractant, and Extracting temperature is 80 DEG C, and the tea-leaf power of crushing is mixed in mass ratio for 1:40 with distilled water It closes, filtering dries after filtrate is concentrated, tealeaves pigment is made;
(2) it takes bush several, cleans, dry 30min at 110 DEG C, be ground into 60 mesh powders, under room temperature, will crush Sappan wood and distilled water be in mass ratio 1:25 proportion, adjust pH=9, keep solution boiling temperature extract 50min, obtain To hematoxylin extracting solution, filter paper is placed on Buchner funnel, using vacuum pump to the reddish yellow hematoxylin extracting solution into Row filters, and after collecting filtrate and being concentrated, is placed in drying in baking oven, hematoxylin is made;
(3) tealeaves pigment, hematoxylin and other components made of taking, according to the stain by tri- independent packagings of A, B, C, A stain includes the component of following portions by weight: 1 part of L-cysteine, 1 part of sodium carbonate, 0.6 part of triethanolamine, carboxymethyl cellulose 0.3 part of plain sodium, 0.2 part of glycerine and 7 parts of water;B stain includes the component of following portions by weight: 0.7 part of iron chloride, carboxymethyl are fine Plain 1.5 parts of the sodium of dimension, 0.3 part of octyl phenol polyoxyethylene ether and 8 parts of water;C stain includes the component of following portions by weight: hematoxylin 0.2 part, 0.2 part of tealeaves pigment, 0.4 part of sodium carboxymethylcellulose, 0.4 part of citric acid, 0.4 part of octyl phenol polyoxyethylene ether and water 12 parts;It is uniformly mixed and bush tealeaves compound botanical hair dye is made.
A kind of application method of bush tealeaves compound botanical hair dye, it is characterized in that the following steps are included:
(1) hair to be dyed is cleaned, and with 6% H now prepared2O2Solution is applied to the oxidation of hair position 10min;
(2) A stain is applied to the hair position aoxidized to soften, the softening time is 40min, softening temperature 40 DEG C, then water is cleaned up and is dried;
(3) it takes B stain and C stain to be mixed with the ratio of 1:1, B stain and C stain intermixture is applied to hair portion Position keeps 60min, and temperature is 45 DEG C, then rinses well, conventionally by hair dryer.
Embodiment 3:
A kind of bush tealeaves compound botanical hair dye, is made of the stain of tri- independent packagings of A, B, C:
A stain includes the component of following portions by weight: L-cysteine 1.0g, sodium carbonate 1.0g, triethanolamine 0.6g, carboxylic Sodium carboxymethylcellulose pyce 0.3g, glycerine 0.2g and water 7.0g;
B stain includes the component of following portions by weight: iron chloride 0.7g, sodium carboxymethylcellulose 1.5g, octyl phenol polyoxy Vinethene 0.3g and water 8.0g;
C stain includes the component of following portions by weight: hematoxylin 0.2g, tealeaves pigment 0.2g, sodium carboxymethylcellulose 0.4g, citric acid 0.4g, octyl phenol polyoxyethylene ether 0.4g and water 12.0g.
A kind of preparation method of bush tealeaves compound botanical hair dye, comprising the following steps:
(1) it takes stem tea several, cleans, dry 30min at 110 DEG C, be ground into 60 mesh powders, using 40% second Alcohol extracts 10min as extractant, and Extracting temperature is 80 DEG C, and the tea-leaf power of crushing is mixed in mass ratio for 1:40 with distilled water It closes, filtering dries after filtrate is concentrated, tealeaves pigment is made;
(2) it takes bush several, cleans, dry 30min at 110 DEG C, be ground into 60 mesh powders, under room temperature, will crush Sappan wood and distilled water be in mass ratio 1:25 proportion, adjust pH=9, keep solution boiling temperature extract 50min, obtain To hematoxylin extracting solution, filter paper is placed on Buchner funnel, using vacuum pump to the reddish yellow hematoxylin extracting solution into Row filters, and after collecting filtrate and being concentrated, is placed in drying in baking oven, hematoxylin is made;
(3) tealeaves pigment, hematoxylin and other components made of taking, according to the stain by tri- independent packagings of A, B, C, A stain includes the component of following portions by weight: 1 part of L-cysteine, 1 part of sodium carbonate, 0.6 part of triethanolamine, carboxymethyl cellulose 0.3 part of plain sodium, 0.2 part of glycerine and 7 parts of water;B stain includes the component of following portions by weight: 0.7 part of iron chloride, carboxymethyl are fine Plain 1.5 parts of the sodium of dimension, 0.3 part of octyl phenol polyoxyethylene ether and 8 parts of water;C stain includes the component of following portions by weight: hematoxylin 0.2 part, 0.2 part of tealeaves pigment, 0.4 part of sodium carboxymethylcellulose, 0.4 part of citric acid, 0.4 part of octyl phenol polyoxyethylene ether and water 12 parts;It is uniformly mixed and bush tealeaves compound botanical hair dye is made.
A kind of application method of bush tealeaves compound botanical hair dye, it is characterized in that the following steps are included:
(1) hair to be dyed is cleaned, and with 6% H now prepared2O2Solution is applied to the oxidation of hair position 10min;
(2) A stain is applied to the hair position aoxidized to soften, the softening time is 35min, softening temperature 37 DEG C, then water is cleaned up and is dried;
(3) it takes B stain and C stain to be mixed with the ratio of 1:1, B stain and C stain intermixture is applied to hair portion Position keeps 55min, and temperature is 42 DEG C, then rinses well, conventionally by hair dryer.
See Fig. 4, is the different hair dyeing effect figure of temperature of having hair dyed, is followed successively by 25 DEG C, 30 DEG C, 35 DEG C, 40 from left to right in figure DEG C, 45 DEG C, selective staining is good and to convenient 40-45 DEG C of temperature of human body;See Fig. 5, is the different hair dyeing effect of dyeing time Scheme, hair color variation degree when being followed successively by 0min, 20min, 30min, 40min, 50min and 60min from left to right in figure, 50-60min hair-dyeing degree is good.

Claims (4)

1. a kind of bush tealeaves compound botanical hair dye, it is characterized in that being made of the stain of tri- independent packagings of A, B, C, A stain Component including following portions by weight: 1 part of L-cysteine, 1 part of sodium carbonate, 0.6 part of triethanolamine, sodium carboxymethylcellulose 0.3 part, 0.2 part of glycerine and 7 parts of water;B stain includes the component of following portions by weight: 0.7 part of iron chloride, carboxymethyl cellulose 1.5 parts of sodium, 0.3 part of octyl phenol polyoxyethylene ether and 8 parts of water;C stain includes the component of following portions by weight: hematoxylin 0.2 Part, 0.2 part of tealeaves pigment, 0.4 part of sodium carboxymethylcellulose, 0.4 part of citric acid, 0.4 part of octyl phenol polyoxyethylene ether and water 12 Part.
2. a kind of preparation method of bush tealeaves compound botanical hair dye, it is characterized in that the following steps are included:
(1) it takes stem tea several, cleans, dry 30min at 110 DEG C, be ground into 60 mesh powders, made using 40% ethyl alcohol 10min is extracted for extractant, it with distilled water is that 1:40 is mixed by the tea-leaf power of crushing that Extracting temperature is 80 DEG C in mass ratio, Filtering, dries after filtrate is concentrated, tealeaves pigment is made;
(2) it takes bush several, cleans, dry 30min at 110 DEG C, be ground into 60 mesh powders, under room temperature, by the Soviet Union of crushing Wood powder and distilled water are 1:25 proportion in mass ratio, adjust pH=9, keep the boiling temperature of solution to extract 50min, are revived The wooden pigment extract, filter paper is placed on Buchner funnel, is taken out using vacuum pump to the reddish yellow hematoxylin extracting solution Filter after collecting filtrate and being concentrated, is placed in drying in baking oven, hematoxylin is made;
(3) tealeaves pigment, hematoxylin and other components made of taking, according to tri- independent packaging stains of A, B, C, A stain packet Include the component of following portions by weight: 1 part of L-cysteine, 1 part of sodium carbonate, 0.6 part of triethanolamine, sodium carboxymethylcellulose 0.3 Part, 0.2 part of glycerine and 7 parts of water;B stain includes the component of following portions by weight: 0.7 part of iron chloride, sodium carboxymethylcellulose 1.5 parts, 0.3 part of octyl phenol polyoxyethylene ether and 8 parts of water;C stain includes the component of following portions by weight: 0.2 part of hematoxylin, 0.2 part of tealeaves pigment, 0.4 part of sodium carboxymethylcellulose, 0.4 part of citric acid, 0.4 part of octyl phenol polyoxyethylene ether and 12 parts of water; It is uniformly mixed and bush tealeaves compound botanical hair dye is made.
3. a kind of bush tealeaves compound botanical hair dye application, it is characterized in that: being used for hair-dyeing.
4. a kind of application method of bush tealeaves compound botanical hair dye, it is characterized in that the following steps are included:
(1) hair to be dyed is cleaned, and with 6% H now prepared2O2Solution is applied to hair position oxidation 10min;
(2) A stain is applied to the hair position aoxidized to soften, the softening time is 30-40min, softening temperature 35- 40 DEG C, then water is cleaned up and is dried;
(3) it takes B stain and C stain to be mixed with the ratio of 1:1, B and C intermixture is applied to hair position, keep 50- 60min, temperature are 40-45 DEG C, are then rinsed well, conventionally by hair dryer.
CN201910816725.0A 2019-08-30 2019-08-30 A kind of preparation method and application of bush tealeaves compound botanical hair dye Pending CN110393686A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110887719A (en) * 2019-12-20 2020-03-17 云南中医药大学 Method for processing tissue sample of histopathology
CN114699351A (en) * 2022-04-15 2022-07-05 南京斯拜科生物科技股份有限公司 Natural hair dye using tea leaf extract as raw material and preparation method thereof
CN115517991A (en) * 2022-01-25 2022-12-27 西南医科大学 Three-agent type safe and nontoxic hair dye and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101164528A (en) * 2007-10-19 2008-04-23 江南大学 Natural hair dyeing agent prepared by plant pigment catechu and hair dyeing method thereof
CN102824283A (en) * 2012-09-17 2012-12-19 山西大学 Environment-friendly hair-care hair dye and preparation method thereof
CN109806176A (en) * 2019-03-22 2019-05-28 广州韩金靓化妆品有限公司 A kind of botanical hair dye and preparation method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101164528A (en) * 2007-10-19 2008-04-23 江南大学 Natural hair dyeing agent prepared by plant pigment catechu and hair dyeing method thereof
CN102824283A (en) * 2012-09-17 2012-12-19 山西大学 Environment-friendly hair-care hair dye and preparation method thereof
CN109806176A (en) * 2019-03-22 2019-05-28 广州韩金靓化妆品有限公司 A kind of botanical hair dye and preparation method

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110887719A (en) * 2019-12-20 2020-03-17 云南中医药大学 Method for processing tissue sample of histopathology
CN115517991A (en) * 2022-01-25 2022-12-27 西南医科大学 Three-agent type safe and nontoxic hair dye and preparation method thereof
CN115517991B (en) * 2022-01-25 2024-03-22 西南医科大学 Three-agent type safe and nontoxic hair dye and preparation method thereof
CN114699351A (en) * 2022-04-15 2022-07-05 南京斯拜科生物科技股份有限公司 Natural hair dye using tea leaf extract as raw material and preparation method thereof

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Application publication date: 20191101