CN104059382A - Natural textile dye and preparation method thereof - Google Patents
Natural textile dye and preparation method thereof Download PDFInfo
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- CN104059382A CN104059382A CN201410294061.3A CN201410294061A CN104059382A CN 104059382 A CN104059382 A CN 104059382A CN 201410294061 A CN201410294061 A CN 201410294061A CN 104059382 A CN104059382 A CN 104059382A
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Abstract
The invention relates to a natural textile dye and a preparation method thereof. The natural textile dye comprises the following raw materials in parts by mass: 10-15 parts of impatiens balsamina extracts, 10-15 parts of pomegranate bark extracts and 6-8 parts of camphor tree leaf extracting solution. The preparation method comprises the following steps of sequentially adding impatiens balsamina extracts, pomegranate bark extracts and camphor tree leaf extracting solution into a reactor with 50 parts of water according to the mass fraction, stirring, heating to 60-70 DEG C after all the components are dissolved, and stirring for 25min to obtain a red brown paste dye; curing the red brown paste dye and smashing to obtain a powdery natural dye. The natural textile dye is safe, environment-friendly, capable of taking mildew-proof, anti-bacterial and mothproof effects, favorable in pigment stability as well as simple and easy in preparation method.
Description
Technical field
The present invention relates to a kind of textile dyestuff and preparation method thereof, particularly a kind of natural textile dyestuff and preparation method thereof.
Background technology
Along with economic fast development, people's living standard improves constantly, and quality of life is improved greatly, and green health has become the focus that current people are concerned about.Existing dyestuff mostly is the organic dye of chemosynthesis, be there is to certain potential safety hazard in HUMAN HEALTH, and the contaminated wastewater that synthetic dyestuff machine intermediate causes is troubling especially, natural dyestuff is loved by the people because of its environmental protection, but its extraction inconvenience and price are expensive compared with organic dye, therefore its development is always slower.
Summary of the invention
The object of the invention is provides a kind of natural textile dyestuff and preparation method thereof in order to overcome above deficiency, and safety and environmental protection of the present invention, also has the mothproof effect of fungus-resistant, and pigment stability is good, and preparation method is simple.
Technical scheme of the present invention comprises: a kind of natural textile dyestuff, and natural textile dyestuff comprises the raw material of following mass fraction: Extracts from Flowers of Impatiens balsamina L 10-15 part, Pericarpium Granati extract 10-15 part, Leaf of Camphortree extraction liquid 6-8 part;
The preparation method of natural textile dyestuff comprises the following steps:
A, according to massfraction, Extracts from Flowers of Impatiens balsamina L, Pericarpium Granati extract and Leaf of Camphortree extraction liquid are added in the reactor that 50 parts of water are housed successively, stir, after all dissolving, be warming up to 60-70
oc, stirs 25min, obtains sorrel paste dyestuff;
B, sorrel paste dyestuff is cured, is pulverized, obtain Powdered natural dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods:
A, will after fresh Flower of Garden Balsam cleaning, drying, with machinery, smash;
B, get Flower of Garden Balsam particle and add in the reactor that aqueous ethanolic solution is housed, feed liquid mass ratio is 1:20-40, at 30-50
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate;
C, by filtrate distillation and concentration, in 40-60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Pericarpium Granati extract is prepared by following methods:
A, will after pomegranate rind cleaning, drying, with machinery, smash;
B, get pomegranate rind particle and add in the reactor that water is housed, feed liquid mass ratio is 1:10-15, makes pomegranate rind fully wetting, and adding sodium carbonate to regulate pH value is 9, is warming up to 80-90
oc, continues logical carbonic acid gas and constantly stirs, and the time is 1-2h, filters to get filtrate;
C, by filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods:
A, will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered;
B, get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:11-13, and microwave power is 400W-500W, 70
ounder C condition, extract 15-20min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
Aqueous ethanolic solution available volume is than being the aqueous ethanolic solution of 40%-80%.
Beneficial effect of the present invention:
1, raw material of the present invention is natural, environmentally friendly and to human body without any toxic action,, and make fabric with delicate fragrance, environmental protection, can widespread use and fabric printing field;
2, coloring matter of the present invention has good stability and has good fungus-resistant performance, can effectively protect fabric corruption aging, and can effectively suppress the phenomenon of damaging by worms;
3, preparation method of the present invention is simple, and raw material is easy to get, and cost is cheap, can wide popularization and application.
embodiment:
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and this embodiment only, for explaining the present invention, does not form limiting the scope of the present invention.
Embodiment 1
A natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: 10 parts of Extracts from Flowers of Impatiens balsamina Ls, 10 parts of Pericarpium Granati extracts, 6 parts of Leaf of Camphortree extraction liquids; According to massfraction, Extracts from Flowers of Impatiens balsamina L, Pericarpium Granati extract and Leaf of Camphortree extraction liquid are added in the reactor that 50 parts of water are housed successively, stir, after all dissolving, be warming up to 70
oc, stirs 25min, obtains sorrel paste dyestuff; Sorrel paste dyestuff is cured, is pulverized, obtain Powdered natural dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods: will after fresh Flower of Garden Balsam cleaning, drying, with machinery, smash; Get Flower of Garden Balsam particle and add and be equipped with in the reactor that volume ratio is 50% aqueous ethanolic solution, feed liquid mass ratio is 1:25,40
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate; By filtrate distillation and concentration, in 60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Pericarpium Granati extract is prepared by following methods: will after pomegranate rind cleaning, drying, with machinery, smash; Get pomegranate rind particle and add in the reactor that water is housed, feed liquid mass ratio is 1:10, makes pomegranate rind fully wetting, and adding sodium carbonate to regulate pH value is 9, is warming up to 85
oc, continues logical carbonic acid gas and constantly stirs, and the time is 2h, filters to get filtrate; By filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods: will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered; Get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:12, and microwave power is 400W, 70
ounder C condition, extract 15min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 < < fixing standard test methods > > of antibacterial antiplaque agent determination of activity under dynamic Contact condition, record and use the fabric of the present invention's dyeing to be respectively 99.50%, 99.30% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 2
A natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: 15 parts of Extracts from Flowers of Impatiens balsamina Ls, 15 parts of Pericarpium Granati extracts, 8 parts of Leaf of Camphortree extraction liquids; According to massfraction, Extracts from Flowers of Impatiens balsamina L, Pericarpium Granati extract and Leaf of Camphortree extraction liquid are added in the reactor that 50 parts of water are housed successively, stir, after all dissolving, be warming up to 70
oc, stirs 25min, obtains sorrel paste dyestuff; Sorrel paste dyestuff is cured, is pulverized, obtain Powdered natural dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods: will after fresh Flower of Garden Balsam cleaning, drying, with machinery, smash; Get Flower of Garden Balsam particle and add and be equipped with in the reactor that volume ratio is 50% aqueous ethanolic solution, feed liquid mass ratio is 1:30,40
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate; By filtrate distillation and concentration, in 60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Pericarpium Granati extract is prepared by following methods: will after pomegranate rind cleaning, drying, with machinery, smash; Get pomegranate rind particle and add in the reactor that water is housed, feed liquid mass ratio is 1:12, makes pomegranate rind fully wetting, and adding sodium carbonate to regulate pH value is 9, is warming up to 85
oc, continues logical carbonic acid gas and constantly stirs, and the time is 2h, filters to get filtrate; By filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods: will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered; Get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:12, and microwave power is 500W, 70
ounder C condition, extract 15min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 < < fixing standard test methods > > of antibacterial antiplaque agent determination of activity under dynamic Contact condition, record and use the fabric of the present invention's dyeing to be respectively 99.70%, 99.40% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 3
A natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: 12 parts of Extracts from Flowers of Impatiens balsamina Ls, 12 parts of Pericarpium Granati extracts, 7 parts of Leaf of Camphortree extraction liquids; According to massfraction, Extracts from Flowers of Impatiens balsamina L, Pericarpium Granati extract and Leaf of Camphortree extraction liquid are added in the reactor that 50 parts of water are housed successively, stir, after all dissolving, be warming up to 70
oc, stirs 25min, obtains sorrel paste dyestuff; Sorrel paste dyestuff is cured, is pulverized, obtain Powdered natural dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods: will after fresh Flower of Garden Balsam cleaning, drying, with machinery, smash; Get Flower of Garden Balsam particle and add and be equipped with in the reactor that volume ratio is 50% aqueous ethanolic solution, feed liquid mass ratio is 1:25,40
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate; By filtrate distillation and concentration, in 60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Pericarpium Granati extract is prepared by following methods: will after pomegranate rind cleaning, drying, with machinery, smash; Get pomegranate rind particle and add in the reactor that water is housed, feed liquid mass ratio is 1:15, makes pomegranate rind fully wetting, and adding sodium carbonate to regulate pH value is 9, is warming up to 85
oc, continues logical carbonic acid gas and constantly stirs, and the time is 2h, filters to get filtrate; By filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods: will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered; Get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:12, and microwave power is 400W, 70
ounder C condition, extract 15min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 < < fixing standard test methods > > of antibacterial antiplaque agent determination of activity under dynamic Contact condition, record and use the fabric of the present invention's dyeing to be respectively 99.60%, 99.45% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 4
A natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: 10 parts of Extracts from Flowers of Impatiens balsamina Ls, 15 parts of Pericarpium Granati extracts, 8 parts of Leaf of Camphortree extraction liquids; According to massfraction, Extracts from Flowers of Impatiens balsamina L, Pericarpium Granati extract and Leaf of Camphortree extraction liquid are added in the reactor that 50 parts of water are housed successively, stir, after all dissolving, be warming up to 70
oc, stirs 25min, obtains sorrel paste dyestuff; Sorrel paste dyestuff is cured, is pulverized, obtain Powdered natural dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods: will after fresh Flower of Garden Balsam cleaning, drying, with machinery, smash; Get Flower of Garden Balsam particle and add and be equipped with in the reactor that volume ratio is 50% aqueous ethanolic solution, feed liquid mass ratio is 1:25,40
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate; By filtrate distillation and concentration, in 60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Pericarpium Granati extract is prepared by following methods: will after pomegranate rind cleaning, drying, with machinery, smash; Get pomegranate rind particle and add in the reactor that water is housed, feed liquid mass ratio is 1:12, makes pomegranate rind fully wetting, and adding sodium carbonate to regulate pH value is 9, is warming up to 85
oc, continues logical carbonic acid gas and constantly stirs, and the time is 2h, filters to get filtrate; By filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods: will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered; Get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:12, and microwave power is 400W, 70
ounder C condition, extract 15min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 < < fixing standard test methods > > of antibacterial antiplaque agent determination of activity under dynamic Contact condition, record and use the fabric of the present invention's dyeing to be respectively 99.68%, 99.52% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 5
A natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: 15 parts of Extracts from Flowers of Impatiens balsamina Ls, 10 parts of Pericarpium Granati extracts, 8 parts of Leaf of Camphortree extraction liquids; According to massfraction, Extracts from Flowers of Impatiens balsamina L, Pericarpium Granati extract and Leaf of Camphortree extraction liquid are added in the reactor that 50 parts of water are housed successively, stir, after all dissolving, be warming up to 70
oc, stirs 25min, obtains sorrel paste dyestuff; Sorrel paste dyestuff is cured, is pulverized, obtain Powdered natural dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods: will after fresh Flower of Garden Balsam cleaning, drying, with machinery, smash; Get Flower of Garden Balsam particle and add and be equipped with in the reactor that volume ratio is 50% aqueous ethanolic solution, feed liquid mass ratio is 1:25,40
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate; By filtrate distillation and concentration, in 60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Pericarpium Granati extract is prepared by following methods: will after pomegranate rind cleaning, drying, with machinery, smash; Get pomegranate rind particle and add in the reactor that water is housed, feed liquid mass ratio is 1:13, makes pomegranate rind fully wetting, and adding sodium carbonate to regulate pH value is 9, is warming up to 85
oc, continues logical carbonic acid gas and constantly stirs, and the time is 2h, filters to get filtrate; By filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods: will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered; Get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:12, and microwave power is 400W, 70
ounder C condition, extract 15min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 < < fixing standard test methods > > of antibacterial antiplaque agent determination of activity under dynamic Contact condition, record and use the fabric of the present invention's dyeing to be respectively 99.66%, 99.62% to streptococcus aureus, colibacillary bacteriostasis rate.
Mothproof effect to dyestuff of the present invention is tested: each 20 parts of wool products getting embodiment 1-embodiment 5 made dyeings with 20 parts of the wool products of the same race of this dyeing, be not placed under environment of the same race, after 3 months, both contrast, with the wool product of this dyeing to damage by worms phenomenon lighter than the wool product of the same race of not using this dyeing.
Even with dyestuff gained DYED FABRICS color and luster of the present invention, colour fastness is high, and has significant fungus-resistant effect.
Claims (5)
1. a natural textile dyestuff, is characterized in that: described natural textile dyestuff comprises the raw material of following mass fraction: Extracts from Flowers of Impatiens balsamina L 10-15 part, Pericarpium Granati extract 10-15 part, Leaf of Camphortree extraction liquid 6-8 part;
The preparation method of described natural textile dyestuff comprises the following steps:
A, according to described massfraction, Extracts from Flowers of Impatiens balsamina L, Pericarpium Granati extract and Leaf of Camphortree extraction liquid are added in the reactor that 50 parts of water are housed successively, stir, after all dissolving, be warming up to 60-70
oc, stirs 25min, obtains sorrel paste dyestuff;
B, described sorrel paste dyestuff is cured, is pulverized, obtain Powdered natural dyestuff.
2. a kind of natural textile dyestuff and preparation method thereof according to claim 1, is characterized in that
:described Extracts from Flowers of Impatiens balsamina L is prepared by following methods:
A, will after fresh Flower of Garden Balsam cleaning, drying, with machinery, smash;
B, get described Flower of Garden Balsam particle and add in the reactor that aqueous ethanolic solution is housed, feed liquid mass ratio is 1:20-40, at 30-50
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate;
C, by described filtrate distillation and concentration, in 40-60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
3. a kind of natural textile dyestuff and preparation method thereof according to claim 1, is characterized in that
:described Pericarpium Granati extract is prepared by following methods:
A, will after pomegranate rind cleaning, drying, with machinery, smash;
B, get described pomegranate rind particle and add in the reactor that water is housed, feed liquid mass ratio is 1:10-15, makes pomegranate rind fully wetting, and adding sodium carbonate to regulate pH value is 9, is warming up to 80-90
oc, continues logical carbonic acid gas and constantly stirs, and the time is 1-2h, filters to get filtrate;
C, by described filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
4. a kind of natural textile dyestuff and preparation method thereof according to claim 1, is characterized in that
:described Leaf of Camphortree extraction liquid is prepared by following methods:
A, will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered;
B, get described Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:11-13, and microwave power is 400W-500W, 70
ounder C condition, extract 15-20min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
5. aqueous ethanolic solution according to claim 2, is characterized in that
:described aqueous ethanolic solution available volume is than being the aqueous ethanolic solution of 40%-80%.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104559307A (en) * | 2015-01-22 | 2015-04-29 | 南通顺阳化工有限公司 | Natural textile dye |
| CN105602281A (en) * | 2015-12-18 | 2016-05-25 | 安徽宜民服饰有限公司 | Plant dye |
| CN106120383A (en) * | 2016-07-18 | 2016-11-16 | 南通富之岛寝具发展有限公司 | A kind of high-temperature resistant antibacterial dyestuff |
| CN108299845A (en) * | 2017-12-29 | 2018-07-20 | 罗莱生活科技股份有限公司 | A kind of pomegranate husk pigment extracting solution as well as preparation method and application thereof |
| CN109487590A (en) * | 2018-11-20 | 2019-03-19 | 广东精英纺织服饰科技有限公司 | A kind of textile dyestuff and preparation method thereof with the anti-function that fades |
| CN111636217A (en) * | 2020-06-23 | 2020-09-08 | 广东精英纺织服饰科技有限公司 | Textile dye with flame retardant function and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104559307A (en) * | 2015-01-22 | 2015-04-29 | 南通顺阳化工有限公司 | Natural textile dye |
| CN105602281A (en) * | 2015-12-18 | 2016-05-25 | 安徽宜民服饰有限公司 | Plant dye |
| CN106120383A (en) * | 2016-07-18 | 2016-11-16 | 南通富之岛寝具发展有限公司 | A kind of high-temperature resistant antibacterial dyestuff |
| CN108299845A (en) * | 2017-12-29 | 2018-07-20 | 罗莱生活科技股份有限公司 | A kind of pomegranate husk pigment extracting solution as well as preparation method and application thereof |
| CN109487590A (en) * | 2018-11-20 | 2019-03-19 | 广东精英纺织服饰科技有限公司 | A kind of textile dyestuff and preparation method thereof with the anti-function that fades |
| CN111636217A (en) * | 2020-06-23 | 2020-09-08 | 广东精英纺织服饰科技有限公司 | Textile dye with flame retardant function and preparation method thereof |
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Application publication date: 20140924 |