CN104059381A - Natural textile dye and preparation method thereof - Google Patents
Natural textile dye and preparation method thereof Download PDFInfo
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- CN104059381A CN104059381A CN201410292506.4A CN201410292506A CN104059381A CN 104059381 A CN104059381 A CN 104059381A CN 201410292506 A CN201410292506 A CN 201410292506A CN 104059381 A CN104059381 A CN 104059381A
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- camphortree
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Abstract
The invention relates to a natural textile dye and a preparation method thereof. The natural textile dye comprises the following raw materials in parts by mass: 20-30 parts of impatiens balsamina extracts, 6-8 parts of camphor tree leaf extracting solution, 6-8 parts of ephedra and 6-8 parts of tea leaves. The preparation method comprises the following steps of (1) smashing ephedra and tea leaves; (2) heating ephedra and tea leaves, stirring, absorbing and filtering; (3) extracting the filtrate by using ethyl acetate, adding impatiens balsamina extracts and camphor tree leaf extracting solution, heating and stirring to obtain a red brown paste, namely, the natural textile dye. The natural textile dye is safe, environment-friendly, capable of taking mildew-proof and anti-bacterial effects, favorable in pigment stability as well as simple and easy in preparation method.
Description
Technical field
The present invention relates to a kind of textile dyestuff and preparation method thereof, particularly a kind of natural textile dyestuff and preparation method thereof.
Background technology
The fast development of modern social economy, improves constantly human living standard, and quality of life is improved greatly, the healthy topic that has become current people's relation.Existing dyestuff mostly is the organic dye of chemosynthesis, and HUMAN HEALTH is existed to certain potential safety hazard, and the contaminated wastewater that synthetic dyestuff machine intermediate causes is troubling especially.Natural dyestuff one is loved by the people, but its extraction inconvenience and price are compared with organic dye costliness, therefore its development is always slower.
Summary of the invention
The object of the invention is provides a kind of natural textile dyestuff and preparation method thereof in order to overcome above deficiency, and safety and environmental protection of the present invention, also has the effect of fungus-resistant, and pigment stability is good, and preparation method is simple.
Technical scheme of the present invention comprises: a kind of natural textile dyestuff, and natural textile dyestuff comprises the raw material of following mass fraction: Extracts from Flowers of Impatiens balsamina L 20-30 part, Leaf of Camphortree extraction liquid 6-8 part, Chinese ephedra 6-8 part, tealeaves 6-8 part;
The preparation method of natural textile dyestuff comprises the following steps:
A, according to above-mentioned massfraction, will after Chinese ephedra and tealeaves cleaning, drying, smash with machinery:
B, the Chinese ephedra after smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50-60 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate;
C, in gained filtrate, add ethyl acetate to extract, organic phase is separated, in organic phase, add Extracts from Flowers of Impatiens balsamina L and Leaf of Camphortree extraction liquid, intensification 60-70
oc, stirs 25min, obtains sorrel paste and is natural textile dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods:
A, will after fresh Flower of Garden Balsam cleaning, drying, smash with machinery;
B, get Flower of Garden Balsam particle and add in the reactor that aqueous ethanolic solution is housed, feed liquid mass ratio is 1:20-40, at 30-50
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate;
C, by filtrate distillation and concentration, in 40-60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Leaf of Camphortree extraction liquid is prepared by following methods:
A, will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered;
B, get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:11-13, and microwave power is 400W-500W, 70
ounder C condition, extract 15-20min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
Aqueous ethanolic solution available volume is than the aqueous ethanolic solution for 40%-80%.
Beneficial effect of the present invention:
1, the present invention adopts natural plant, environmentally friendly and to human body without any toxic action,, and make fabric with delicate fragrance, environmental protection, can widespread use and fabric printing field;
2, coloring matter of the present invention has good stability and has good fungus-resistant performance, can effectively protect fabric corruption aging, and can effectively suppress the phenomenon of damaging by worms;
3, preparation method of the present invention is simple, and raw material is extensive, and cost cheapness can wide popularization and application.
embodiment:
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and this embodiment only, for explaining the present invention, does not form limiting the scope of the present invention.
Embodiment 1
A kind of natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: 20 parts of Extracts from Flowers of Impatiens balsamina Ls, 6 parts of Leaf of Camphortree extraction liquids, 6 parts, Chinese ephedra, 6 parts of tealeaves; According to massfraction, will after Chinese ephedra and tealeaves cleaning, drying, smash with machinery: the Chinese ephedra after smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate; In gained filtrate, add ethyl acetate to extract, organic phase is separated, in described organic phase, add Extracts from Flowers of Impatiens balsamina L and Leaf of Camphortree extraction liquid, heat up 70
oc, stirs 25min, obtains sorrel paste and is natural textile dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods: will after fresh Flower of Garden Balsam cleaning, drying, smash with machinery; Get Flower of Garden Balsam particle and add that volume ratio is housed is that in 50% the reactor of aqueous ethanolic solution, feed liquid mass ratio is 1:25,40
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate; By filtrate distillation and concentration, in 60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Leaf of Camphortree extraction liquid is prepared by following methods: will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered; Get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:12, and microwave power is 400W, 70
ounder C condition, extract 15min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record and use the fabric of the present invention's dyeing to be respectively 99.80%, 99.50% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 2
A kind of natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: 30 parts of Extracts from Flowers of Impatiens balsamina Ls, 8 parts of Leaf of Camphortree extraction liquids, 8 parts, Chinese ephedra, 8 parts of tealeaves; According to massfraction, will after Chinese ephedra and tealeaves cleaning, drying, smash with machinery: the Chinese ephedra after smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate; In gained filtrate, add ethyl acetate to extract, organic phase is separated, in described organic phase, add Extracts from Flowers of Impatiens balsamina L and Leaf of Camphortree extraction liquid, heat up 70
oc, stirs 25min, obtains sorrel paste and is natural textile dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods: will after fresh Flower of Garden Balsam cleaning, drying, smash with machinery; Get Flower of Garden Balsam particle and add that volume ratio is housed is that in 50% the reactor of aqueous ethanolic solution, feed liquid mass ratio is 1:30,40
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate; By filtrate distillation and concentration, in 60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Leaf of Camphortree extraction liquid is prepared by following methods: will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered; Get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:12, and microwave power is 500W, 70
ounder C condition, extract 15min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record and use the fabric of the present invention's dyeing to be respectively 99.90%, 99.80% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 3
A kind of natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: 25 parts of Extracts from Flowers of Impatiens balsamina Ls, 7 parts of Leaf of Camphortree extraction liquids, 7 parts, Chinese ephedra, 7 parts of tealeaves; According to massfraction, will after Chinese ephedra and tealeaves cleaning, drying, smash with machinery: the Chinese ephedra after smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate; In gained filtrate, add ethyl acetate to extract, organic phase is separated, in described organic phase, add Extracts from Flowers of Impatiens balsamina L and Leaf of Camphortree extraction liquid, heat up 70
oc, stirs 25min, obtains sorrel paste and is natural textile dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods: will after fresh Flower of Garden Balsam cleaning, drying, smash with machinery; Get Flower of Garden Balsam particle and add that volume ratio is housed is that in 50% the reactor of aqueous ethanolic solution, feed liquid mass ratio is 1:25,40
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate; By filtrate distillation and concentration, in 60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Leaf of Camphortree extraction liquid is prepared by following methods: will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered; Get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:12, and microwave power is 400W, 70
ounder C condition, extract 15min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record and use the fabric of the present invention's dyeing to be respectively 99.80%, 99.71% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 4
A kind of natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: 25 parts of Extracts from Flowers of Impatiens balsamina Ls, 8 parts of Leaf of Camphortree extraction liquids, 6 parts, Chinese ephedra, 6 parts of tealeaves; According to massfraction, will after Chinese ephedra and tealeaves cleaning, drying, smash with machinery: the Chinese ephedra after smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate; In gained filtrate, add ethyl acetate to extract, organic phase is separated, in described organic phase, add Extracts from Flowers of Impatiens balsamina L and Leaf of Camphortree extraction liquid, heat up 70
oc, stirs 25min, obtains sorrel paste and is natural textile dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods: will after fresh Flower of Garden Balsam cleaning, drying, smash with machinery; Get Flower of Garden Balsam particle and add that volume ratio is housed is that in 50% the reactor of aqueous ethanolic solution, feed liquid mass ratio is 1:30,40
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate; By filtrate distillation and concentration, in 60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Leaf of Camphortree extraction liquid is prepared by following methods: will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered; Get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:13, and microwave power is 400W, 70
ounder C condition, extract 15min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record and use the fabric of the present invention's dyeing to be respectively 99.78%, 99.75% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 5
A kind of natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: 20 parts of Extracts from Flowers of Impatiens balsamina Ls, 8 parts of Leaf of Camphortree extraction liquids, 8 parts, Chinese ephedra, 7 parts of tealeaves; According to massfraction, will after Chinese ephedra and tealeaves cleaning, drying, smash with machinery: the Chinese ephedra after smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate; In gained filtrate, add ethyl acetate to extract, organic phase is separated, in described organic phase, add Extracts from Flowers of Impatiens balsamina L and Leaf of Camphortree extraction liquid, heat up 70
oc, stirs 25min, obtains sorrel paste and is natural textile dyestuff.
Extracts from Flowers of Impatiens balsamina L is prepared by following methods: will after fresh Flower of Garden Balsam cleaning, drying, smash with machinery; Get Flower of Garden Balsam particle and add that volume ratio is housed is that in 50% the reactor of aqueous ethanolic solution, feed liquid mass ratio is 1:30,40
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate; By filtrate distillation and concentration, in 60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
Leaf of Camphortree extraction liquid is prepared by following methods: will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered; Get Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:11, and microwave power is 400W, 70
ounder C condition, extract 15min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record and use the fabric of the present invention's dyeing to be respectively 99.87%, 99.80% to streptococcus aureus, colibacillary bacteriostasis rate.
Mothproof effect to dyestuff of the present invention is tested: get the wool product of embodiment 1-embodiment 5 made dyeings each 20 parts be not placed under environment of the same race with 20 parts of the wool products of the same race of this dyeing, after 3 months, both contrast, with the wool product of this dyeing to damage by worms phenomenon lighter than the wool product of the same race of not using this dyeing.
Even with dyestuff gained DYED FABRICS color and luster of the present invention, colour fastness is high, and has significant fungus-resistant effect.
Claims (4)
1. a natural textile dyestuff, is characterized in that: described natural textile dyestuff comprises the raw material of following mass fraction: Extracts from Flowers of Impatiens balsamina L 20-30 part, Leaf of Camphortree extraction liquid 6-8 part, Chinese ephedra 6-8 part, tealeaves 6-8 part;
The preparation method of described natural textile dyestuff comprises the following steps:
A, according to described massfraction, will after Chinese ephedra and tealeaves cleaning, drying, smash with machinery:
B, the Chinese ephedra after described smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50-60 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate;
C, in described filtrate, add ethyl acetate to extract, organic phase is separated, in described organic phase, add Extracts from Flowers of Impatiens balsamina L and Leaf of Camphortree extraction liquid, intensification 60-70
oc, stirs 25min, obtains sorrel paste and is natural textile dyestuff.
2. a kind of natural textile dyestuff and preparation method thereof according to claim 1, is characterized in that
:described Extracts from Flowers of Impatiens balsamina L is prepared by following methods:
A, will after fresh Flower of Garden Balsam cleaning, drying, smash with machinery;
B, get described Flower of Garden Balsam particle and add in the reactor that aqueous ethanolic solution is housed, feed liquid mass ratio is 1:20-40, at 30-50
ounder C condition, stir 3h, after having stirred in 50
ounder C, constant temperature soaks 24h, is cooled to 25
oc, filters to get filtrate;
C, by described filtrate distillation and concentration, in 40-60
oc is dried, and obtains red-purple paste and is Extracts from Flowers of Impatiens balsamina L.
3. a kind of natural textile dyestuff and preparation method thereof according to claim 1, is characterized in that
:described Leaf of Camphortree extraction liquid is prepared by following methods:
A, will after fresh Leaf of Camphortree cleaning, drying, use mechanical mill powdered;
B, get described Leaf of Camphortree powder and add in the container that water is housed, feed liquid mass ratio is 1:11-13, and microwave power is 400W-500W, 70
ounder C condition, extract 15-20min, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
4. aqueous ethanolic solution according to claim 2, is characterized in that
:described aqueous ethanolic solution available volume is than the aqueous ethanolic solution for 40%-80%.
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Cited By (5)
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| CN104559307A (en) * | 2015-01-22 | 2015-04-29 | 南通顺阳化工有限公司 | Natural textile dye |
| CN105602281A (en) * | 2015-12-18 | 2016-05-25 | 安徽宜民服饰有限公司 | Plant dye |
| CN105754375A (en) * | 2016-05-18 | 2016-07-13 | 新世嘉纺织品（南通）有限公司 | Plant dye for textile and preparation method of plant dye |
| CN105908533A (en) * | 2016-05-22 | 2016-08-31 | 南通富之岛寝具发展有限公司 | Texture reactive dye containing garden balsam extract |
| CN109098013A (en) * | 2018-08-28 | 2018-12-28 | 苏州典传创意科技有限公司 | A kind of natural dye for Nature Fibre Textile product |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104559307A (en) * | 2015-01-22 | 2015-04-29 | 南通顺阳化工有限公司 | Natural textile dye |
| CN105602281A (en) * | 2015-12-18 | 2016-05-25 | 安徽宜民服饰有限公司 | Plant dye |
| CN105754375A (en) * | 2016-05-18 | 2016-07-13 | 新世嘉纺织品（南通）有限公司 | Plant dye for textile and preparation method of plant dye |
| CN105908533A (en) * | 2016-05-22 | 2016-08-31 | 南通富之岛寝具发展有限公司 | Texture reactive dye containing garden balsam extract |
| CN109098013A (en) * | 2018-08-28 | 2018-12-28 | 苏州典传创意科技有限公司 | A kind of natural dye for Nature Fibre Textile product |
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Application publication date: 20140924 |