CN104031404B - A kind of natural textile dye well its preparation method - Google Patents
A kind of natural textile dye well its preparation method Download PDFInfo
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- CN104031404B CN104031404B CN201410293928.3A CN201410293928A CN104031404B CN 104031404 B CN104031404 B CN 104031404B CN 201410293928 A CN201410293928 A CN 201410293928A CN 104031404 B CN104031404 B CN 104031404B
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- camphortree
- leaf
- extraction liquid
- dyestuff
- natural textile
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- 239000004753 textile Substances 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000007788 liquid Substances 0.000 claims abstract description 51
- 241000723346 Cinnamomum camphora Species 0.000 claims abstract description 44
- 239000000975 dye Substances 0.000 claims abstract description 44
- 239000000284 extract Substances 0.000 claims abstract description 38
- 238000000605 extraction Methods 0.000 claims abstract description 37
- 239000000706 filtrate Substances 0.000 claims abstract description 29
- 241001465251 Ephedra sinica Species 0.000 claims abstract description 24
- 235000001018 Hibiscus sabdariffa Nutrition 0.000 claims abstract description 11
- 235000005291 Rumex acetosa Nutrition 0.000 claims abstract description 11
- 240000007001 Rumex acetosella Species 0.000 claims abstract description 11
- 235000003513 sheep sorrel Nutrition 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 241000283690 Bos taurus Species 0.000 claims description 21
- 241000219991 Lythraceae Species 0.000 claims description 21
- 235000014360 Punica granatum Nutrition 0.000 claims description 21
- 238000004140 cleaning Methods 0.000 claims description 21
- 238000001035 drying Methods 0.000 claims description 21
- 238000003756 stirring Methods 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 14
- 239000012074 organic phase Substances 0.000 claims description 14
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 7
- 235000011089 carbon dioxide Nutrition 0.000 claims description 7
- 238000004821 distillation Methods 0.000 claims description 7
- 239000002024 ethyl acetate extract Substances 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 7
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 7
- 238000010792 warming Methods 0.000 claims description 7
- 238000009736 wetting Methods 0.000 claims description 7
- 230000000694 effects Effects 0.000 abstract description 9
- 241000233866 Fungi Species 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 abstract description 4
- 239000000049 pigment Substances 0.000 abstract description 2
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 1
- 238000004043 dyeing Methods 0.000 description 9
- 239000004744 fabric Substances 0.000 description 9
- 241000191967 Staphylococcus aureus Species 0.000 description 5
- 230000000844 anti-bacterial effect Effects 0.000 description 5
- 230000002882 anti-plaque Effects 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 5
- 238000007655 standard test method Methods 0.000 description 5
- 239000000047 product Substances 0.000 description 4
- 210000002268 wool Anatomy 0.000 description 4
- 230000018109 developmental process Effects 0.000 description 2
- 230000032683 aging Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Landscapes
- Coloring (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The present invention relates to a kind of natural textile dye well its preparation method, natural textile dyestuff comprises the raw material of following mass fraction: Pericarpium Granati extract 20-30 part, Leaf of Camphortree extraction liquid 6-8 part, Chinese ephedra 6-8 part; Its preparation method comprises the following steps: Chinese ephedra is smashed by (1); (2) by Chinese ephedra heated and stirred absorbing and filtering; (3) filtrate being extracted with ethyl acetate adds Pericarpium Granati extract and Leaf of Camphortree extraction liquid, and heated and stirred obtains sorrel paste; (4) sorrel paste dyestuff is cured, pulverizes, obtain Powdered natural dyestuff.Environmental protection of the present invention, also has the effect of fungus-resistant, and pigment stability is good, and preparation method is simple.
Description
Technical field
The present invention relates to a kind of textile dyestuff and preparation method thereof, particularly a kind of natural textile dye well its preparation method.
Background technology
Along with the fast development of economy, people's living standard improves constantly, and quality of life is improved greatly, environmental protection, health, the green topic having become current people's relation.Existing dyestuff mostly is the organic dye of chemosynthesis, certain potential safety hazard is existed to HUMAN HEALTH, and the contaminated wastewater that synthetic dyestuff machine intermediate causes is troubling especially, natural dyestuff is subject to people likes because has good consistency to environment, but it extracts inconvenience and price comparatively organic dye costliness, therefore its development is always slower.
Summary of the invention
The object of the invention is to provide a kind of natural textile dye well its preparation method, safety and environmental protection of the present invention to overcome above deficiency, also having the effect of fungus-resistant, and pigment stability is good, preparation method is simple.
Technical scheme of the present invention comprises: a kind of natural textile dyestuff, and natural textile dyestuff comprises the raw material of following mass fraction: Pericarpium Granati extract 20-30 part, Leaf of Camphortree extraction liquid 6-8 part, Chinese ephedra 6-8 part;
The preparation method of natural textile dyestuff comprises the following steps:
A, according to massfraction, to smash after Chinese ephedra cleaning, drying with machinery:
B, the Chinese ephedra after smashing is added in the reactor that 60 parts of water are housed, in 50-60
ounder C condition, constant temperature stirs 3h, filters to get filtrate;
C, in filtrate, add ethyl acetate extract, organic phase is separated, in organic phase, adds Pericarpium Granati extract and Leaf of Camphortree extraction liquid, intensification 60-70
oc, stirs 25min, obtains sorrel paste dyestuff;
D, sorrel paste dyestuff is cured, pulverizes, obtain Powdered natural dyestuff.
Pericarpium Granati extract is prepared by following methods:
A, to smash after pomegranate rind cleaning, drying with machinery;
B, get pomegranate rind particle and add and be equipped with in the reactor of water, feed liquid mass ratio is 1:10-15, makes pomegranate rind fully wetting, and adding sodium carbonate adjust ph is 9, is warming up to 80-90
oc, continue logical carbonic acid gas and constantly stir, the time is 1-2h, filters to get filtrate;
C, by filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods:
A, use mechanical mill powdered by after fresh Leaf of Camphortree cleaning, drying;
B, get Leaf of Camphortree powder and add and be equipped with in the container of water, feed liquid mass ratio is 1:11-13, and microwave power is 400W-500W, 70
oextract 15-20min under C condition, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
Beneficial effect of the present invention:
1, raw material of the present invention is natural, environmentally friendly and to human body without any toxic action, and make fabric with delicate fragrance, environmental protection, can widespread use and fabric printing field;
2, coloring matter of the present invention has good stability and has good fungus-resistant performance, fabric corruption effectively can be protected aging, and effectively can suppress phenomenon of damaging by worms;
3, preparation method of the present invention is simple, and raw material is easy to get, inexpensive, can wide popularization and application.
embodiment:
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and this embodiment only for explaining the present invention, does not form limiting the scope of the present invention.
Embodiment 1
A kind of natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: Pericarpium Granati extract 20 parts, Leaf of Camphortree extraction liquid 6 parts, 6 parts, Chinese ephedra; According to massfraction, smash after Chinese ephedra cleaning, drying with machinery: the Chinese ephedra after smashing is added in the reactor that 60 parts of water are housed, in 50
ounder C condition, constant temperature stirs 3h, filters to get filtrate; In gained filtrate, add ethyl acetate extract, organic phase is separated, in described organic phase, adds Pericarpium Granati extract and Leaf of Camphortree extraction liquid, heat up 70
oc, stirs 25min, obtains sorrel paste and be natural textile dyestuff.
Pericarpium Granati extract is prepared by following methods: smash after pomegranate rind cleaning, drying with machinery; Get pomegranate rind particle to add and be equipped with in the reactor of water, feed liquid mass ratio is 1:10, makes pomegranate rind fully wetting, and adding sodium carbonate adjust ph is 9, is warming up to 85
oc, continue logical carbonic acid gas and constantly stir, the time is 2h, filters to get filtrate; By filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods: use mechanical mill powdered by after fresh Leaf of Camphortree cleaning, drying; Get Leaf of Camphortree powder to add and be equipped with in the container of water, feed liquid mass ratio is 1:12, and microwave power is 400W, 70
oextract 15min under C condition, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record and use the fabric of the present invention's dyeing to be respectively 99.50%, 99.30% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 2
A kind of natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: Pericarpium Granati extract 30 parts, Leaf of Camphortree extraction liquid 8 parts, 8 parts, Chinese ephedra; According to massfraction, smash after Chinese ephedra and tealeaves cleaning, drying with machinery: the Chinese ephedra after smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate; In gained filtrate, add ethyl acetate extract, organic phase is separated, in described organic phase, adds Pericarpium Granati extract and Leaf of Camphortree extraction liquid, heat up 70
oc, stirs 25min, obtains sorrel paste and be natural textile dyestuff.
Pericarpium Granati extract is prepared by following methods: smash after pomegranate rind cleaning, drying with machinery; Get pomegranate rind particle to add and be equipped with in the reactor of water, feed liquid mass ratio is 1:12, makes pomegranate rind fully wetting, and adding sodium carbonate adjust ph is 9, is warming up to 85
oc, continue logical carbonic acid gas and constantly stir, the time is 2h, filters to get filtrate; By filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods: use mechanical mill powdered by after fresh Leaf of Camphortree cleaning, drying; Get Leaf of Camphortree powder to add and be equipped with in the container of water, feed liquid mass ratio is 1:12, and microwave power is 500W, 70
oextract 15min under C condition, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record and use the fabric of the present invention's dyeing to be respectively 99.80%, 99.70% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 3
A kind of natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: Pericarpium Granati extract 25 parts, Leaf of Camphortree extraction liquid 7 parts, 7 parts, Chinese ephedra; According to massfraction, smash after Chinese ephedra and tealeaves cleaning, drying with machinery: the Chinese ephedra after smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate; In gained filtrate, add ethyl acetate extract, organic phase is separated, in described organic phase, adds Pericarpium Granati extract and Leaf of Camphortree extraction liquid, heat up 70
oc, stirs 25min, obtains sorrel paste and be natural textile dyestuff.
Pericarpium Granati extract is prepared by following methods: smash after pomegranate rind cleaning, drying with machinery; Get pomegranate rind particle to add and be equipped with in the reactor of water, feed liquid mass ratio is 1:15, makes pomegranate rind fully wetting, and adding sodium carbonate adjust ph is 9, is warming up to 85
oc, continue logical carbonic acid gas and constantly stir, the time is 2h, filters to get filtrate; By filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods: use mechanical mill powdered by after fresh Leaf of Camphortree cleaning, drying; Get Leaf of Camphortree powder to add and be equipped with in the container of water, feed liquid mass ratio is 1:12, and microwave power is 400W, 70
oextract 15min under C condition, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record and use the fabric of the present invention's dyeing to be respectively 99.50%, 99.50% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 4
A kind of natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: Pericarpium Granati extract 20 parts, Leaf of Camphortree extraction liquid 8 parts, 8 parts, Chinese ephedra; According to massfraction, smash after Chinese ephedra and tealeaves cleaning, drying with machinery: the Chinese ephedra after smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate; In gained filtrate, add ethyl acetate extract, organic phase is separated, in described organic phase, adds Pericarpium Granati extract and Leaf of Camphortree extraction liquid, heat up 70
oc, stirs 25min, obtains sorrel paste and be natural textile dyestuff.
Pericarpium Granati extract is prepared by following methods: smash after pomegranate rind cleaning, drying with machinery; Get pomegranate rind particle to add and be equipped with in the reactor of water, feed liquid mass ratio is 1:12, makes pomegranate rind fully wetting, and adding sodium carbonate adjust ph is 9, is warming up to 85
oc, continue logical carbonic acid gas and constantly stir, the time is 2h, filters to get filtrate; By filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods: use mechanical mill powdered by after fresh Leaf of Camphortree cleaning, drying; Get Leaf of Camphortree powder to add and be equipped with in the container of water, feed liquid mass ratio is 1:12, and microwave power is 400W, 70
oextract 15min under C condition, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record and use the fabric of the present invention's dyeing to be respectively 99.55%, 99.52% to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 5
A kind of natural textile dyestuff, natural textile dyestuff comprises the raw material of following mass fraction: Pericarpium Granati extract 30 parts, Leaf of Camphortree extraction liquid 6 parts, 6 parts, Chinese ephedra; According to massfraction, smash after Chinese ephedra and tealeaves cleaning, drying with machinery: the Chinese ephedra after smashing and tealeaves are added in the reactor that 60 parts of water are housed, in 50 successively
ounder C condition, constant temperature stirs 3h, filters to get filtrate; In gained filtrate, add ethyl acetate extract, organic phase is separated, in described organic phase, adds Pericarpium Granati extract and Leaf of Camphortree extraction liquid, heat up 70
oc, stirs 25min, obtains sorrel paste and be natural textile dyestuff.
Pericarpium Granati extract is prepared by following methods: smash after pomegranate rind cleaning, drying with machinery; Get pomegranate rind particle to add and be equipped with in the reactor of water, feed liquid mass ratio is 1:12, makes pomegranate rind fully wetting, and adding sodium carbonate adjust ph is 9, is warming up to 85
oc, continue logical carbonic acid gas and constantly stir, the time is 2h, filters to get filtrate; By filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
Leaf of Camphortree extraction liquid is prepared by following methods: use mechanical mill powdered by after fresh Leaf of Camphortree cleaning, drying; Get Leaf of Camphortree powder to add and be equipped with in the container of water, feed liquid mass ratio is 1:12, and microwave power is 400W, 70
oextract 15min under C condition, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
With reference to E2149-2010 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record and use the fabric of the present invention's dyeing to be respectively 99.62%, 99.60% to streptococcus aureus, colibacillary bacteriostasis rate.
The mothproof effect of dyestuff of the present invention is tested: the wool product of the made dyeing of Example 1-embodiment 5 each 20 parts be placed in environment of the same race with the wool product of the same race 20 parts not with this dyeing under, after 3 months, both contrast, lighter with the wool product of the same race of this dyeing than not by the phenomenon of damaging by worms of the wool product of this dyeing.
By dyestuff gained DYED FABRICS uniform color of the present invention, colour fastness is high, and has significant fungus-resistant effect.
Claims (3)
1. a natural textile dyestuff, is characterized in that: described natural textile dyestuff comprises the raw material of following mass fraction: Pericarpium Granati extract 20-30 part, Leaf of Camphortree extraction liquid 6-8 part, Chinese ephedra 6-8 part;
The preparation method of described natural textile dyestuff comprises the following steps:
A, according to described massfraction, to smash after Chinese ephedra cleaning, drying with machinery:
B, the Chinese ephedra after described smashing added 60 parts of water are housed reactor in, in 50-60
ounder C condition, constant temperature stirs 3h, filters to get filtrate;
C, in described filtrate, add ethyl acetate extract, organic phase is separated, in described organic phase, adds Pericarpium Granati extract and Leaf of Camphortree extraction liquid, intensification 60-70
oc, stirs 25min, obtains sorrel paste dyestuff;
D, described sorrel paste dyestuff is cured, pulverizes, obtain Powdered natural dyestuff.
2. a kind of natural textile dyestuff according to claim 1, is characterized in that
:described Pericarpium Granati extract is prepared by following methods:
A, to smash after pomegranate rind cleaning, drying with machinery;
B, get described pomegranate rind particle and add and be equipped with in the reactor of water, feed liquid mass ratio is 1:10-15, makes pomegranate rind fully wetting, and adding sodium carbonate adjust ph is 9, is warming up to 80-90
oc, continue logical carbonic acid gas and constantly stir, the time is 1-2h, filters to get filtrate;
C, by described filtrate distillation and concentration, obtain red-purple paste and be Pericarpium Granati extract.
3. a kind of natural textile dyestuff according to claim 1, is characterized in that
:described Leaf of Camphortree extraction liquid is prepared by following methods:
A, use mechanical mill powdered by after fresh Leaf of Camphortree cleaning, drying;
B, get described Leaf of Camphortree powder and add and be equipped with in the container of water, feed liquid mass ratio is 1:11-13, and microwave power is 400W-500W, 70
oextract 15-20min under C condition, obtain sticky shape extraction liquid and be Leaf of Camphortree extraction liquid.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410293928.3A CN104031404B (en) | 2014-06-26 | 2014-06-26 | A kind of natural textile dye well its preparation method |
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| CN104031404A CN104031404A (en) | 2014-09-10 |
| CN104031404B true CN104031404B (en) | 2016-04-27 |
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| CN106192461A (en) * | 2016-07-20 | 2016-12-07 | 珠海无用文化创意有限公司 | Natural Camphor Tree Seeds is applied to the method on Nature Fibre Textile product as vegetable colour |
Citations (6)
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|---|---|---|---|---|
| CN101353485A (en) * | 2007-07-23 | 2009-01-28 | 重庆谭木匠工艺品有限公司 | Vegetable dye and preparation thereof |
| KR20090030739A (en) * | 2007-09-21 | 2009-03-25 | 전남대학교산학협력단 | The natural safflower powder dye which it extracts from safflower and its preparation method |
| CN101559030A (en) * | 2008-04-18 | 2009-10-21 | 闫征 | Plant hair dye by taking ginger extract as penetrating agent |
| CN102051063A (en) * | 2010-11-29 | 2011-05-11 | 南通职业大学 | Camphor tree dye, extracting method thereof and use thereof |
| CN103265823A (en) * | 2013-05-04 | 2013-08-28 | 江门职业技术学院 | Pomegranate rind nature dye preparation and application of pomegranate rind nature dye in fabric |
| CN103554960A (en) * | 2013-11-08 | 2014-02-05 | 哈尔滨市工艺美术有限责任公司 | Formula and production method for preparing red brown wheat straw dye |
-
2014
- 2014-06-26 CN CN201410293928.3A patent/CN104031404B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101353485A (en) * | 2007-07-23 | 2009-01-28 | 重庆谭木匠工艺品有限公司 | Vegetable dye and preparation thereof |
| KR20090030739A (en) * | 2007-09-21 | 2009-03-25 | 전남대학교산학협력단 | The natural safflower powder dye which it extracts from safflower and its preparation method |
| CN101559030A (en) * | 2008-04-18 | 2009-10-21 | 闫征 | Plant hair dye by taking ginger extract as penetrating agent |
| CN102051063A (en) * | 2010-11-29 | 2011-05-11 | 南通职业大学 | Camphor tree dye, extracting method thereof and use thereof |
| CN103265823A (en) * | 2013-05-04 | 2013-08-28 | 江门职业技术学院 | Pomegranate rind nature dye preparation and application of pomegranate rind nature dye in fabric |
| CN103554960A (en) * | 2013-11-08 | 2014-02-05 | 哈尔滨市工艺美术有限责任公司 | Formula and production method for preparing red brown wheat straw dye |
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Effective date of registration: 20200630 Address after: Room 407, building 6, Shengze textile science and Technology Creative Park, 1188 West Second Ring Road, Shengze Town, Wujiang District, Suzhou City, Jiangsu Province Patentee after: SUZHOU GANNZ EIECTRONIC TECHNOLOGY Co.,Ltd. Address before: 215200 Group 9, Xingqiao Village, Shengze Town, Wujiang District, Suzhou City, Jiangsu Province Patentee before: Suzhou Yongdyeing Textile Finishing Co.,Ltd. |
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| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160427 |