CN109172459A - A kind of green peel of walnut hair dye and preparation method thereof - Google Patents
A kind of green peel of walnut hair dye and preparation method thereof Download PDFInfo
- Publication number
- CN109172459A CN109172459A CN201811297252.XA CN201811297252A CN109172459A CN 109172459 A CN109172459 A CN 109172459A CN 201811297252 A CN201811297252 A CN 201811297252A CN 109172459 A CN109172459 A CN 109172459A
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- walnut
- green peel
- medicinal extract
- dye
- hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
Abstract
The invention discloses a kind of green peel of walnut hair dyes and preparation method thereof, including following weight percentage components: green peel of walnut dye liquor medicinal extract 5%~7%, lauryl amide EDA6%~8%, hydroxyethyl cellulose 0.3%~1%, citric acid 1%~2%, aminomethylpropanol 0.5%~2%, oleyl alcohol ether -20 2%~3%, surplus is deionized water.Green peel of walnut hair dye of the invention, with the extract (green peel of walnut dye liquor medicinal extract) of pure plant green peel of walnut be colorant main component, have many advantages, such as it is nontoxic, non-stimulated, without allergy, be not easy to fade after coloring.The present invention dyes human hair using natural pigment, extract the natural anthraquinone pigments substance in green peel of walnut, dye test is carried out to human hair, effectively improves the problems such as natural pigment hair dye tinctorial property is poor, and synthetic hair dyes are hazardous to the human body.Different metal mordant is added in hair dye, it can be effectively to widen the dyeing range of natural hair dye.
Description
Technical field
The invention belongs to field of hairdye, and in particular to a kind of green peel of walnut hair dye and preparation method thereof.
Background technique
21 century China will enter aging society, with silver hair stratum personage gradually increase and today's social life,
Work strain and caused by white hair, depilation phenomenon increase, from aesthetical point, hair-color is provided with huge market.But
Use chemically synthesized oxidative hair dyes on the market at present, carcinogenic probability is big, and harm to the human body is high more.
Summary of the invention
For the prior art, the problem to be solved in the present invention is to provide a kind of green peel of walnut hair dye having no toxic side effect and
Preparation method.
In order to solve the above technical problems, the present invention is achieved by the following technical programs:
A kind of green peel of walnut hair dye, including following weight percentage components: green peel of walnut dye liquor medicinal extract 5%~7%,
Lauryl amide EDA 6%~8%, hydroxyethyl cellulose 0.3%~1%, citric acid 1%~2%, aminomethylpropanol
0.5%~2%, oleyl alcohol ether -20 2%~3%, surplus is deionized water.
Further, including following weight percentage components: green peel of walnut dye liquor medicinal extract 5%, lauryl amide EDA
7%, hydroxyethyl cellulose 0.5%, citric acid 1%, aminomethylpropanol 0.5%, oleyl alcohol ether -20 3%, surplus is deionization
Water.
Further, including following weight percentage components: green peel of walnut dye liquor medicinal extract 5%, lauryl amide EDA
6%, hydroxyethyl cellulose 0.8%, citric acid 1.5%, aminomethylpropanol 1%, oleyl alcohol ether -20 3%, surplus is deionization
Water.
Further, including following weight percentage components: green peel of walnut dye liquor medicinal extract 6%, lauryl amide EDA
7%, hydroxyethyl cellulose 0.5%, citric acid 1%, aminomethylpropanol 2%, oleyl alcohol ether -20 2%, surplus is deionized water.
A kind of preparation method of green peel of walnut hair dye, comprising the following steps: prepare green peel of walnut dye liquor medicinal extract first, so
Core is added in lauryl amide EDA, hydroxyethyl cellulose, citric acid, aminomethylpropanol, oleyl alcohol ether -20 and deionized water afterwards
It is uniformly mixed in peach green peel dye liquor medicinal extract.
Further, the green peel of walnut dye liquor medicinal extract is to dry green peel of walnut in shady spot, grinding and sieving, according to
Green peel of walnut powder: ethyl alcohol is that ethyl alcohol is added in green peel of walnut powder the weight ratio of 1:25~35, concentration of alcohol 60%~80%,
8~12h of oscillation treatment at 50~60 DEG C of constant temperature, centrifugation collect supernatant, the supernatant being collected into are concentrated under reduced pressure at 60~70 DEG C
Green peel of walnut dye liquor medicinal extract is made in liquid.
Further, 70 meshes of the screening.
Compared with prior art, the present invention at least has the advantages that, green peel of walnut hair dye of the invention, with pure
The extract of natural plants green peel of walnut be colorant main component, have many advantages, such as it is nontoxic, non-stimulated, without allergy, with change
The oxidative hair dyes for learning synthesis are compared, and are greatly reduced carcinogenic probability, are substantially reduced to the side effect of human body, and after coloring not
Easily fade.The present invention dyes human hair using natural pigment, extracts the natural anthraquinone pigments object in green peel of walnut
Matter carries out dye test to human hair, and it is poor to effectively improve natural pigment hair dye tinctorial property, synthetic hair dyes pair
The problems such as human body is harmful.Different metal mordant is added in hair dye, can also effectively widen the dyeing of natural hair dye
Range.
Detailed description of the invention
Fig. 1 is the hair dyeing effect column comparison diagram of different mordant dyeing agent and mordant dyeing method.
Specific embodiment
With reference to the accompanying drawing and specific embodiment, the present invention is made further to explain in detail explanation.
Embodiment 1:
The hair dye preparation of the present embodiment is as follows:
The preparation of green peel of walnut dye liquor medicinal extract: green peel of walnut dye liquor medicinal extract is to dry green peel of walnut in shady spot, after crushing
70 meshes are crossed, by green peel of walnut powder: ethyl alcohol is that ethyl alcohol is added in green peel of walnut powder the weight ratio of 1:25~35, concentration of alcohol
60%~80%, 8~12h of oscillation treatment at 50~60 DEG C of constant temperature, centrifugation collect supernatant, are concentrated under reduced pressure and receive at 60~70 DEG C
Green peel of walnut dye liquor medicinal extract is made in the supernatant collected.
Hair dye preparation: green peel of walnut dye liquor medicinal extract 5%, lauryl amide EDA 7%, hydroxyethyl cellulose is added
0.5%, citric acid 1%, aminomethylpropanol 0.5%, oleyl alcohol ether -20 3%, surplus is deionized water, and all components are mixed
Uniformly.
Embodiment 2:
The hair dye preparation of the present embodiment is as follows:
The preparation of green peel of walnut dye liquor medicinal extract: green peel of walnut dye liquor medicinal extract is to dry green peel of walnut in shady spot, after crushing
70 meshes are crossed, by green peel of walnut powder: ethyl alcohol is that ethyl alcohol is added in green peel of walnut powder the weight ratio of 1:25~35, concentration of alcohol
60%~80%, 8~12h of oscillation treatment at 50~60 DEG C of constant temperature, centrifugation collect supernatant, are concentrated under reduced pressure and receive at 60~70 DEG C
Green peel of walnut dye liquor medicinal extract is made in the supernatant collected.
Hair dye preparation: green peel of walnut dye liquor medicinal extract 5%, lauryl amide EDA 6%, hydroxyethyl cellulose is added
0.8%, citric acid 1.5%, aminomethylpropanol 1%, oleyl alcohol ether -20 3%, surplus is deionized water, and all components are mixed
Uniformly.
Embodiment 3:
The hair dye preparation of the present embodiment is as follows:
The preparation of green peel of walnut dye liquor medicinal extract: green peel of walnut dye liquor medicinal extract is to dry green peel of walnut in shady spot, after crushing
70 meshes are crossed, by green peel of walnut powder: ethyl alcohol is that ethyl alcohol is added in green peel of walnut powder the weight ratio of 1:25~35, concentration of alcohol
60%~80%, 8~12h of oscillation treatment at 50~60 DEG C of constant temperature, centrifugation collect supernatant, are concentrated under reduced pressure and receive at 60~70 DEG C
Green peel of walnut dye liquor medicinal extract is made in the supernatant collected.
Hair dye preparation: green peel of walnut dye liquor medicinal extract 6%, lauryl amide EDA 7%, hydroxyethyl cellulose is added
0.5%, citric acid 1%, aminomethylpropanol 2%, oleyl alcohol ether -20 2%, surplus is deionized water, all components is mixed equal
It is even.
Embodiment 4:
The hair dye preparation of the present embodiment is as follows:
The preparation of green peel of walnut dye liquor medicinal extract: green peel of walnut dye liquor medicinal extract is to dry green peel of walnut in shady spot, after crushing
70 meshes are crossed, by green peel of walnut powder: ethyl alcohol is that ethyl alcohol is added in green peel of walnut powder the weight ratio of 1:25~35, concentration of alcohol
60%~80%, 8~12h of oscillation treatment at 50~60 DEG C of constant temperature, centrifugation collect supernatant, are concentrated under reduced pressure and receive at 60~70 DEG C
Green peel of walnut dye liquor medicinal extract is made in the supernatant collected.
Hair dye preparation: green peel of walnut dye liquor medicinal extract 6%, lauryl amide EDA 6%, hydroxyethyl cellulose is added
0.3%, citric acid 1.5%, aminomethylpropanol 1%, oleyl alcohol ether -20 2.5%, surplus is deionized water, and all components are mixed
It closes uniform.
Embodiment 5:
The hair dye preparation of the present embodiment is as follows:
The preparation of green peel of walnut dye liquor medicinal extract: green peel of walnut dye liquor medicinal extract is to dry green peel of walnut in shady spot, after crushing
70 meshes are crossed, by green peel of walnut powder: ethyl alcohol is that ethyl alcohol is added in green peel of walnut powder the weight ratio of 1:25~35, concentration of alcohol
60%~80%, 8~12h of oscillation treatment at 50~60 DEG C of constant temperature, centrifugation collect supernatant, are concentrated under reduced pressure and receive at 60~70 DEG C
Green peel of walnut dye liquor medicinal extract is made in the supernatant collected.
Hair dye preparation: addition green peel of walnut dye liquor medicinal extract 7%, lauryl amide EDA 8%, hydroxyethyl cellulose 1%,
Citric acid 2%, aminomethylpropanol 2%, oleyl alcohol ether -20 2%, surplus is deionized water, and all components are uniformly mixed.
Natural plant dye is because of itself dyeing property, and often coloring effect is bad, therefore the often addition gold in dyeing course
Belong to mordant to improve rate of dyeing and dyeing effect, common metal salt mordant includes Li2+、Fe2+、Cr2+、Al3+、Sn2+、Na+、
Zn2+、K+、Mg2+、Mn2+Deng.In order to effectively widen the dyeing range of green peel of walnut natural hair dye, to hair dye addition metal from
Son carries out mordant dyeing test, and specific test situation is as follows:
1. co-bathing dyeing
Equivalent white hair is taken, adjusts 70 DEG C of dyeing temperature, 3g/L gold is added in the 40mL green peel of walnut hair rinse of pH=7
Belong to mordant, co-bathing dyeing 120min, cooling, washing, dry and colour examining.
Mordant dyeing color before 2.
Take equivalent white hair, adjust 70 DEG C of dyeing temperature, the mordant dyeing 60min in concentration 3g/L metal mordanting bath, then by its
It is transferred in the 40mL green peel of walnut hair rinse of pH=7 and dyes 120min, cooling, washing, dry and colour examining.
Mordant dyeing color after 3.
Equivalent white hair is taken, 70 DEG C of dyeing temperature is adjusted, is dyed in the 40mL green peel of walnut hair rinse of pH=7
120min, then it is transferred to mordant dyeing 60min in concentration 3g/L metal salt mordant solution, cooling, washing, dry and colour examining.
The color feature value of dyeing front and back hair is tested using spectrophotometric color measurement instrument, wherein L* represents shading value, and a* represents color
It adjusts, b* represents chroma, total color difference △ E=[(△ L*)2+(△a*)2+(△b*)2], wherein △ L*, △ a* and △ b* are and do not contaminate
The difference of color hair L*, a* and b*.△ E indicates the mobile general direction of color difference, and value is bigger to illustrate that color difference is bigger, colours deeper.Examination
Result is tested as shown in Figure 1, Fig. 1 shows using Fe2+Mordant dyeing color hair dyeing effect is best before carrying out, and color is most deep.
Claims (7)
1. a kind of green peel of walnut hair dye, which is characterized in that including following weight percentage components: green peel of walnut dye liquor medicinal extract
5%~7%, lauryl amide EDA 6%~8%, hydroxyethyl cellulose 0.3%~1%, citric acid 1%~2%, amino first
Base propyl alcohol 0.5%~2%, oleyl alcohol ether -20 2%~3%, surplus is deionized water.
2. a kind of green peel of walnut hair dye according to claim 1, which is characterized in that the group including following weight percent
Point: green peel of walnut dye liquor medicinal extract 5%, lauryl amide EDA 7%, hydroxyethyl cellulose 0.5%, citric acid 1%, amino methyl
Propyl alcohol 0.5%, oleyl alcohol ether -20 3%, surplus is deionized water.
3. a kind of green peel of walnut hair dye according to claim 1, which is characterized in that the group including following weight percent
Point: green peel of walnut dye liquor medicinal extract 5%, lauryl amide EDA 6%, hydroxyethyl cellulose 0.8%, citric acid 1.5%, amino first
Base propyl alcohol 1%, oleyl alcohol ether -20 3%, surplus is deionized water.
4. a kind of green peel of walnut hair dye according to claim 1, which is characterized in that the group including following weight percent
Point: green peel of walnut dye liquor medicinal extract 6%, lauryl amide EDA7%, hydroxyethyl cellulose 0.5%, citric acid 1%, amino methyl
Propyl alcohol 2%, oleyl alcohol ether -20 2%, surplus is deionized water.
5. a kind of preparation method of green peel of walnut hair dye described in any one according to claim 1~4, which is characterized in that
The following steps are included: green peel of walnut dye liquor medicinal extract is prepared first, then by lauryl amide EDA, hydroxyethyl cellulose, lemon
Acid, aminomethylpropanol, oleyl alcohol ether -20 and deionized water are added in green peel of walnut dye liquor medicinal extract and are uniformly mixed.
6. preparation method according to claim 5, which is characterized in that the green peel of walnut dye liquor medicinal extract is by green peel of walnut
It is dried in shady spot, grinding and sieving, according to green peel of walnut powder: ethyl alcohol is that walnut is added in ethyl alcohol by the weight ratio of 1:25~35
In green peel powder, concentration of alcohol 60%~80%, 8~12h of oscillation treatment at 50~60 DEG C of constant temperature, centrifugation collects supernatant, 60~
The supernatant being collected into is concentrated under reduced pressure at 70 DEG C, green peel of walnut dye liquor medicinal extract is made.
7. preparation method according to claim 6, which is characterized in that 70 meshes of the screening.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811297252.XA CN109172459A (en) | 2018-11-01 | 2018-11-01 | A kind of green peel of walnut hair dye and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811297252.XA CN109172459A (en) | 2018-11-01 | 2018-11-01 | A kind of green peel of walnut hair dye and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110037965A (en) * | 2019-05-30 | 2019-07-23 | 西藏圣雪生物科技有限公司 | A kind of pericarpium juglandis hair dye and preparation method thereof |
| CN114134728A (en) * | 2021-11-16 | 2022-03-04 | 西北农林科技大学 | Preparation method for dyeing first-layer cow leather on walnut green husk dye liquor |
| CN114796040A (en) * | 2022-03-04 | 2022-07-29 | 广东药科大学 | Black dragon clothes composite hair dye and preparation method thereof |
| CN115501152A (en) * | 2022-11-08 | 2022-12-23 | 苏州中纺学面料产业研究院 | Preparation method of natural hair dye and natural hair dye |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110037965A (en) * | 2019-05-30 | 2019-07-23 | 西藏圣雪生物科技有限公司 | A kind of pericarpium juglandis hair dye and preparation method thereof |
| CN114134728A (en) * | 2021-11-16 | 2022-03-04 | 西北农林科技大学 | Preparation method for dyeing first-layer cow leather on walnut green husk dye liquor |
| CN114134728B (en) * | 2021-11-16 | 2023-08-18 | 西北农林科技大学 | Preparation method of ox leather with dyeing head layer on walnut green seedcase dye liquor |
| CN114796040A (en) * | 2022-03-04 | 2022-07-29 | 广东药科大学 | Black dragon clothes composite hair dye and preparation method thereof |
| CN115501152A (en) * | 2022-11-08 | 2022-12-23 | 苏州中纺学面料产业研究院 | Preparation method of natural hair dye and natural hair dye |
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