CN110037965A - A kind of pericarpium juglandis hair dye and preparation method thereof - Google Patents
A kind of pericarpium juglandis hair dye and preparation method thereof Download PDFInfo
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- CN110037965A CN110037965A CN201910461169.XA CN201910461169A CN110037965A CN 110037965 A CN110037965 A CN 110037965A CN 201910461169 A CN201910461169 A CN 201910461169A CN 110037965 A CN110037965 A CN 110037965A
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- Prior art keywords
- pericarpium juglandis
- hair
- pericarpium
- dye
- juglandis
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
- A61K2800/4324—Direct dyes in preparations for permanently dyeing the hair
Abstract
The invention discloses a kind of pericarpium juglandis hair dyes and preparation method thereof, including following weight percentage components: pericarpium juglandis dye liquor medicinal extract 5%~7%, walnut oil extract 5%~6%, hydroxyethyl cellulose 0.3%~1%, citric acid 1%~2%, aminomethylpropanol 0.5%~2%, oleyl alcohol ether -20 2%~3%, surplus is deionized water.Pericarpium juglandis hair dye of the invention, using the extract of pure plant pericarpium juglandis as the main component of colorant, have many advantages, such as it is nontoxic, non-stimulated, without allergy, be not easy to fade after coloring.The present invention dyes human hair using natural pigment, pericarpium juglandis dye liquor medicinal extract is made in the natural anthraquinone pigments substance extracted in pericarpium juglandis, dye test is carried out to human hair, effectively improves the problems such as natural pigment hair dye tinctorial property is poor, and synthetic hair dyes are hazardous to the human body.Different metal mordant is added in hair dye, it can be effectively to widen the dyeing range of natural hair dye.
Description
Technical field
The invention belongs to field of hairdye, and in particular to a kind of pericarpium juglandis hair dye and preparation method thereof.
Background technique
21 century China will enter aging society, with silver hair stratum personage gradually increase and today's social life,
Work strain and caused by white hair, depilation phenomenon increase, from aesthetical point, hair-color is provided with huge market.But
Use chemically synthesized oxidative hair dyes on the market at present, carcinogenic probability is big, and harm to the human body is high more.
Summary of the invention
For the prior art, the problem to be solved in the present invention is to provide a kind of pericarpium juglandis hair dye having no toxic side effect and its
Preparation method.
In order to solve the above technical problems, the present invention is achieved by the following technical programs:
A kind of pericarpium juglandis hair dye, including following weight percentage components: pericarpium juglandis dye liquor medicinal extract 5%~7%, walnut oil mentions
Take object 6%~8%, 0 .3%~1% of hydroxyethyl cellulose, citric acid 1%~2%, 0 .5% of aminomethylpropanol~
2%, oleyl alcohol ether -20 2%~3%, surplus is deionized water.
Further, including following weight percentage components: pericarpium juglandis dye liquor medicinal extract 5%, walnut oil extract 7%,
0 .5% of hydroxyethyl cellulose, citric acid 1%, 0 .5% of aminomethylpropanol, oleyl alcohol ether -20 3%, surplus is deionized water.
Further, including following weight percentage components: pericarpium juglandis dye liquor medicinal extract 5%, walnut oil extract 6%,
0 .8% of hydroxyethyl cellulose, 1 .5% of citric acid, aminomethylpropanol 1%, oleyl alcohol ether -20 3%, surplus is deionized water.
Further, including following weight percentage components: pericarpium juglandis dye liquor medicinal extract 6%, walnut oil extract 7%,
0 .5% of hydroxyethyl cellulose, citric acid 1%, aminomethylpropanol 2%, oleyl alcohol ether -20 2%, surplus is deionized water.
A kind of preparation method of pericarpium juglandis hair dye, comprising the following steps: prepare pericarpium juglandis dye liquor medicinal extract first, then will
Pericarpium juglandis dye is added in walnut oil extract, hydroxyethyl cellulose, citric acid, aminomethylpropanol, oleyl alcohol ether -20 and deionized water
It is uniformly mixed in liquid medicinal extract.
Further, the pericarpium juglandis dye liquor medicinal extract is to dry pericarpium juglandis in shady spot, grinding and sieving, according to the Green Dragon
Clothing powder: ethyl alcohol is that ethyl alcohol is added in pericarpium juglandis powder the weight ratio of 1:25~35, concentration of alcohol 60%~80%, constant temperature 50~
8~12h of oscillation treatment at 60 DEG C, centrifugation collect supernatant, the supernatant being collected into are concentrated under reduced pressure at 60~70 DEG C, blueness is made
Imperial clothing dye liquor medicinal extract.
Further, 70 meshes of the screening.
Compared with prior art, the present invention at least has the advantages that, pericarpium juglandis hair dye of the invention, with pure day
The extract of right plant pericarpium juglandis is the main component of colorant, have many advantages, such as it is nontoxic, non-stimulated, without allergy, with chemistry conjunction
At oxidative hair dyes compare, greatly reduce carcinogenic probability, the side effect of human body be substantially reduced, and colour after be not easy
Color.The present invention dyes human hair using natural pigment, the natural anthraquinone pigments substance in pericarpium juglandis is extracted, to people
Chaeta hair carries out dye test, effectively improves that natural pigment hair dye tinctorial property is poor, and synthetic hair dyes have human body
The problems such as endangering.Different metal mordant is added in hair dye, it can be effectively to widen the dyeing range of natural hair dye.
Detailed description of the invention
Fig. 1 is the hair dyeing effect column comparison diagram of different mordant dyeing agent and mordant dyeing method.
Specific embodiment
With reference to the accompanying drawing and specific embodiment, the present invention is made further to explain in detail explanation.
Embodiment 1:
The hair dye preparation of the present embodiment is as follows:
The preparation of pericarpium juglandis dye liquor medicinal extract: pericarpium juglandis dye liquor medicinal extract is to dry pericarpium juglandis in shady spot, smashes it through 70 meshes, presses
Pericarpium juglandis powder: ethyl alcohol is that ethyl alcohol is added in pericarpium juglandis powder the weight ratio of 1:25~35, concentration of alcohol 60%~80%, constant temperature
8~12h of oscillation treatment at 50~60 DEG C, centrifugation collect supernatant, the supernatant being collected into are concentrated under reduced pressure at 60~70 DEG C, make
Obtain pericarpium juglandis dye liquor medicinal extract.
Hair dye preparation: pericarpium juglandis dye liquor medicinal extract 5%, walnut oil extract 7%, hydroxyethyl cellulose 0 is added
.5%, citric acid 1%, 0 .5% of aminomethylpropanol, oleyl alcohol ether -20 3%, surplus is deionized water, and all components are mixed
Uniformly.
Embodiment 2:
The hair dye preparation of the present embodiment is as follows:
The preparation of pericarpium juglandis dye liquor medicinal extract: pericarpium juglandis dye liquor medicinal extract is to dry pericarpium juglandis in shady spot, smashes it through 70 meshes, presses
Pericarpium juglandis powder: ethyl alcohol is that ethyl alcohol is added in pericarpium juglandis powder the weight ratio of 1:25~35, concentration of alcohol 60%~80%, constant temperature
8~12h of oscillation treatment at 50~60 DEG C, centrifugation collect supernatant, the supernatant being collected into are concentrated under reduced pressure at 60~70 DEG C, make
Obtain pericarpium juglandis dye liquor medicinal extract.
Hair dye preparation: pericarpium juglandis dye liquor medicinal extract 5%, walnut oil extract 6%, hydroxyethyl cellulose 0 is added
.8%, 1 .5% of citric acid, aminomethylpropanol 1%, oleyl alcohol ether -20 3%, surplus is deionized water, and all components are mixed
Uniformly.
Embodiment 3:
The hair dye preparation of the present embodiment is as follows:
The preparation of pericarpium juglandis dye liquor medicinal extract: pericarpium juglandis dye liquor medicinal extract is to dry pericarpium juglandis in shady spot, smashes it through 70 meshes, presses
Pericarpium juglandis powder: ethyl alcohol is that ethyl alcohol is added in pericarpium juglandis powder the weight ratio of 1:25~35, concentration of alcohol 60%~80%, constant temperature
8~12h of oscillation treatment at 50~60 DEG C, centrifugation collect supernatant, the supernatant being collected into are concentrated under reduced pressure at 60~70 DEG C, make
Obtain pericarpium juglandis dye liquor medicinal extract.
Hair dye preparation: pericarpium juglandis dye liquor medicinal extract 6%, walnut oil extract 7%, hydroxyethyl cellulose 0 is added
.5%, citric acid 1%, aminomethylpropanol 2%, oleyl alcohol ether -20 2%, surplus is deionized water, all components is mixed equal
It is even.
Embodiment 4:
The hair dye preparation of the present embodiment is as follows:
The preparation of pericarpium juglandis dye liquor medicinal extract: pericarpium juglandis dye liquor medicinal extract is to dry pericarpium juglandis in shady spot, smashes it through 70 meshes, presses
Pericarpium juglandis powder: ethyl alcohol is that ethyl alcohol is added in pericarpium juglandis powder the weight ratio of 1:25~35, concentration of alcohol 60%~80%, constant temperature
8~12h of oscillation treatment at 50~60 DEG C, centrifugation collect supernatant, the supernatant being collected into are concentrated under reduced pressure at 60~70 DEG C, make
Obtain pericarpium juglandis dye liquor medicinal extract.
Hair dye preparation: pericarpium juglandis dye liquor medicinal extract 6%, walnut oil extract 6%, hydroxyethyl cellulose 0 is added
.3%, 1 .5% of citric acid, aminomethylpropanol 1%, -20 2 .5% of oleyl alcohol ether, surplus is deionized water, by all components
It is uniformly mixed.
Embodiment 5:
The hair dye preparation of the present embodiment is as follows:
The preparation of pericarpium juglandis dye liquor medicinal extract: pericarpium juglandis dye liquor medicinal extract is to dry pericarpium juglandis in shady spot, smashes it through 70 meshes, presses
Pericarpium juglandis powder: ethyl alcohol is that ethyl alcohol is added in pericarpium juglandis powder the weight ratio of 1:25~35, concentration of alcohol 60%~80%, constant temperature
8~12h of oscillation treatment at 50~60 DEG C, centrifugation collect supernatant, the supernatant being collected into are concentrated under reduced pressure at 60~70 DEG C, make
Obtain pericarpium juglandis dye liquor medicinal extract.
Hair dye preparation: pericarpium juglandis dye liquor medicinal extract 7%, walnut oil extract 8%, hydroxyethyl cellulose 1%, lemon is added
Lemon acid 2%, aminomethylpropanol 2%, oleyl alcohol ether -20 2%, surplus is deionized water, and all components are uniformly mixed.
Natural plant dye is because of itself dyeing property, and often coloring effect is bad, therefore the Chang Tianjia gold in dyeing course
Belong to mordant to improve rate of dyeing and dyeing effect, common metal salt mordant include Li2+, Fe2+, Cr2+, Al3+, Sn2+,
Na+, Zn2+, K+, Mg2+, Mn2+ etc..In order to effectively widen the dyeing range of pericarpium juglandis natural hair dye, gold is added to hair dye
Belong to ion and carry out mordant dyeing test, specific test situation is as follows:
1, co-bathing dyeing
Equivalent white hair is taken, adjusts 70 DEG C of dyeing temperature, the mordant dyeing of 3g/L metal is added in the 40mL pericarpium juglandis hair rinse of pH=7
Agent, co-bathing dyeing 120min, cooling, washing, dry and colour examining.
Mordant dyeing color before 2,
Equivalent white hair is taken, adjusts 70 DEG C of dyeing temperature, the mordant dyeing 60min in concentration 3g/L metal mordanting bath, then be transferred to
120min, cooling, washing, dry and colour examining are dyed in the 40mL pericarpium juglandis hair rinse of pH=7.
Mordant dyeing color after 3,
Equivalent white hair is taken, 70 DEG C of dyeing temperature is adjusted, is dyed in the 4 0m L pericarpium juglandis hair rinses of pH=7
120min, then it is transferred to mordant dyeing 60min in concentration 3g/L metal salt mordant solution, cooling, washing, dry and colour examining.
The color feature value of dyeing front and back hair is tested using spectrophotometric color measurement instrument, wherein L* represents shading value, and a* represents color
Adjust, b* represents chroma, total color difference △ E=[(△ L*) 2+ (△ a*) 2+ (△ b*) 2], wherein △ L*, △ a* and △ b* be with not
The difference of colored hair L*, a* and b*.△ E indicates the mobile general direction of color difference, and value is bigger to illustrate that color difference is bigger, colours deeper.
For test result as shown in Figure 1, Fig. 1 shows that mordant dyeing color hair dyeing effect is best before carrying out using Fe2+, color is most deep.
Claims (7)
1. a kind of pericarpium juglandis hair dye, which is characterized in that including following weight percentage components: pericarpium juglandis dye liquor medicinal extract 5%
~7%, walnut oil extract 6%~8%, 0 .3%~1% of hydroxyethyl cellulose, citric acid 1%~2%, amino methyl third
0 .5%~2% of alcohol, oleyl alcohol ether -20 2%~3%, surplus is deionized water.
2. a kind of pericarpium juglandis hair dye according to claim 1, which is characterized in that the group including following weight percent
Point: pericarpium juglandis dye liquor medicinal extract 5%, walnut oil extract 7%, 0 .5% of hydroxyethyl cellulose, citric acid 1%, amino methyl third
0 .5% of alcohol, oleyl alcohol ether -20 3%, surplus is deionized water.
3. a kind of pericarpium juglandis hair dye according to claim 1, which is characterized in that the group including following weight percent
Point: pericarpium juglandis dye liquor medicinal extract 5%, walnut oil extract 6%, 0 .8% of hydroxyethyl cellulose, 1 .5% of citric acid, amino first
Base propyl alcohol 1%, oleyl alcohol ether -20 3%, surplus is deionized water.
4. a kind of pericarpium juglandis hair dye according to claim 1, which is characterized in that the group including following weight percent
Point: pericarpium juglandis dye liquor medicinal extract 6%, walnut oil extract 7%, 0 .5% of hydroxyethyl cellulose, citric acid 1%, amino methyl third
Alcohol 2%, oleyl alcohol ether -20 2%, surplus is deionized water.
5. a kind of preparation method of pericarpium juglandis hair dye described in any one according to claim 1~4, which is characterized in that packet
It includes following steps: preparing pericarpium juglandis dye liquor medicinal extract first, then by walnut oil extract, hydroxyethyl cellulose, citric acid, amino
Methylpropanol, oleyl alcohol ether -20 and deionized water are added in pericarpium juglandis dye liquor medicinal extract and are uniformly mixed.
6. preparation method according to claim 5, which is characterized in that the pericarpium juglandis dye liquor medicinal extract is to carry on the back pericarpium juglandis
Negative place is dried, grinding and sieving, according to pericarpium juglandis powder: ethyl alcohol is that pericarpium juglandis powder is added in ethyl alcohol by the weight ratio of 1:25~35
In, concentration of alcohol 60%~80%, 8~12h of oscillation treatment at 50~60 DEG C of constant temperature, supernatant is collected in centrifugation, at 60~70 DEG C
The supernatant being collected into is concentrated under reduced pressure, pericarpium juglandis dye liquor medicinal extract is made.
7. preparation method according to claim 6, which is characterized in that 70 meshes of the screening.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910461169.XA CN110037965A (en) | 2019-05-30 | 2019-05-30 | A kind of pericarpium juglandis hair dye and preparation method thereof |
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| CN201910461169.XA CN110037965A (en) | 2019-05-30 | 2019-05-30 | A kind of pericarpium juglandis hair dye and preparation method thereof |
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| CN110037965A true CN110037965A (en) | 2019-07-23 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110251439A (en) * | 2019-08-05 | 2019-09-20 | 宁夏医科大学 | A kind of pericarpium juglandis flaxseed gum plant hair rinse and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103340770A (en) * | 2013-06-09 | 2013-10-09 | 吕梁学院 | Preparation method for hair dye based on walnut green husk pigment |
| CN104800108A (en) * | 2014-11-20 | 2015-07-29 | 折改梅 | Preparation of constituents of cortex juglandis mandshuricae and manufacturing method of different-colored hair dyes |
| CN109172459A (en) * | 2018-11-01 | 2019-01-11 | 张有林 | A kind of green peel of walnut hair dye and preparation method thereof |
| CN109330950A (en) * | 2018-09-07 | 2019-02-15 | 吕梁学院 | A kind of pericarpium juglandis hair dye and preparation method thereof and application method |
-
2019
- 2019-05-30 CN CN201910461169.XA patent/CN110037965A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103340770A (en) * | 2013-06-09 | 2013-10-09 | 吕梁学院 | Preparation method for hair dye based on walnut green husk pigment |
| CN104800108A (en) * | 2014-11-20 | 2015-07-29 | 折改梅 | Preparation of constituents of cortex juglandis mandshuricae and manufacturing method of different-colored hair dyes |
| CN109330950A (en) * | 2018-09-07 | 2019-02-15 | 吕梁学院 | A kind of pericarpium juglandis hair dye and preparation method thereof and application method |
| CN109172459A (en) * | 2018-11-01 | 2019-01-11 | 张有林 | A kind of green peel of walnut hair dye and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110251439A (en) * | 2019-08-05 | 2019-09-20 | 宁夏医科大学 | A kind of pericarpium juglandis flaxseed gum plant hair rinse and preparation method thereof |
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Application publication date: 20190723 |