CN104825359A - Method for preparing natural hair dye from black plum peels - Google Patents
Method for preparing natural hair dye from black plum peels Download PDFInfo
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- CN104825359A CN104825359A CN201510227322.4A CN201510227322A CN104825359A CN 104825359 A CN104825359 A CN 104825359A CN 201510227322 A CN201510227322 A CN 201510227322A CN 104825359 A CN104825359 A CN 104825359A
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Abstract
The invention relates to a method for extracting pigments from black plum peels and preparing a natural hair dye. The pigment extraction comprises the following steps: adding an ethanol solution (20-80%) into black plum peels according to a material/liquid ratio of 1:10-1:100, carrying out extraction at a temperature of 20-80 DEG C for 0.5 to 3 hours, filtering the extract, then subjected filtered extract to centrifugation, and condensing the supernate so as to obtain the pigment. The prepared hair dye comprises an agent A and an agent B, wherein the agent A is composed of the following components in percentage by weight: 0.1 to 10% of black plum peel pigment, 10 to 30% of polyol, 1 to 10% of surfactant, 1 to 5% of thickening agent, and the balance being water, the pH value of agent A is adjusted to the range of 5-7; the agent B comprises the following components in percentage by weight: 0.5 to 5% of metal mordant, 1 to 10% of surfactant, 1 to 5% of thickening agent, and the balance being water, and the pH value of the agent B is adjusted to the range of 5-7. The provided method can comprehensively utilize the resources, moreover, the preparation technology is simple, the operation is easy, and the prepared hair dye is safe, and nontoxic, and the dyeing effect is natural.
Description
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of method adopting black cloth woods peel to prepare natural hair dye.
Background technology
Hair dye is a kind of for changing color development, reaches the cosmetics of hair caring object.Hair dye can make on the one hand poliosis contaminate the black poliosis shortcoming made up because disease and heredity etc. cause, and can meet that youngster is followed the fashion, the needs of showing personality on the other hand by changing color development.Oxidative hair dyes, because having the advantages such as easy to use, Color good, hold time for a long time, spectral range is wide, is most popular in all hair dyeing cosmetics.But multinomial result of study shows that this kind of hair dye has certain injury to hair, and easily causes allergy, and life-time service can cause poisoning, and brings out various cancer.Along with the raising of health of people consciousness, while pursuit hair dyeing effect, more pay close attention to the safety of hair dye.Natural plant pigment abundance, cheap, safety non-toxic, tone nature, and part has the health-care effecies such as antioxidation, sterilization, immunity moderation.The natural hair dye prepared with it does not produce constitutional to hair to stimulate, and also can not cause skin allergy.In addition, natural pigment is bio-renewables, can natural degradation, and this makes natural hair dye day by day become the development trend in following hair dye market.
Black cloth woods belongs to the one of Fructus Pruni salicinae, and the black Fructus Pruni salicinae that has another name called, black cloth are bright, black rose Lee etc.Because this kind introduces from the U.S., the color of fruit is atropurpureus, is called again American Black Lee, U.S. Lee.Black cloth woods contains the nutritional labelings such as vitamin, fruit acid, sugar, several amino acids, protein, cellulose, calcium, phosphorus, ferrum, carotene, has good health care and nutritive value.In addition, the peel of black cloth woods is aubergine, and pigment content enriches, and is good natural pigment source.The pigment of black cloth woods peel is mainly anthocyanidin, is a kind of strong antioxidant, has the important physiological function such as slow down aging, opposing tumor.
Consider that black cloth woods sarcocarp is mainly used to processing beverage, fruit wine etc., and the peel of black cloth woods is generally dropped as waste material, therefore black cloth woods peel is extracted pigment as raw material and is used for preparing the comprehensive utilization that natural hair dye can realize resource.
The present invention adopts the pigment in ethanol extraction black cloth woods peel, and the pigment obtained by extraction and isolation dyes as the main constituent of hair dye to hair.
Summary of the invention
The object of this invention is to provide and a kind ofly extract pigment with black cloth woods peel for raw material and prepare the method for natural hair dye.
The object of the invention is to be achieved through the following technical solutions.
Cleaned by black cloth woods and peel, peel is smashed to pieces, takes a certain amount of, adds the lixiviate of 20%-80% alcoholic solution by solid-liquid ratio 1:10-1:100, the lixiviate 0.5-3h when temperature is 20-80 DEG C.By lixiviating solution filter centrifugation, get the supernatant and carry out distillation and concentration, obtain black cloth woods pericarp pigment.
Using the pigment of extraction as hair dye main constituent, prepare a kind of new type natural hair dye.This hair dye forms by two doses, and wherein agent A comprises black cloth woods pericarp pigment 0.1%-10%, polyhydric alcohol 10%-30%, surfactant 1-10%, thickening agent 1-5%, and all the other are water, and adjustment pH is 5-7; Agent B comprises metal salt mordant 0.5-5%, surfactant 1-10%, thickening agent 1-5%, and all the other are water, and adjustment pH is 5-7.Unit is percetage by weight.
In agent A, polyhydric alcohol is one or more in propylene glycol, butanediol, glycerol.
In agent B, metal salt mordant is in cosmetics the salt allowing any metal ion used, and includes but not limited to iron chloride, ferrous chloride, aluminum chloride, Alumen, copper nitrate.
In agent A mediating recipe B, pH adjusting agent is the one in phosphoric acid, acetic acid or citric acid.
In agent A mediating recipe B, thickening agent comprises one or more in carboxymethyl cellulose, hydroxyethyl-cellulose, hydroxypropyl emthylcellulose, cation guar gum, xanthan gum, sodium alginate.
In agent A mediating recipe B, surfactant comprises one or more in glyceryl monostearate, ceteareth-20, tween 80.
Agent A and agent B is solution, gel, emulsion or cream frost form.
The invention provides and a kind ofly extract pigment by black cloth woods peel and prepare the method for natural hair dye as main constituent, this hair dye can dye the naturally color such as yellow, purple, maroon.The method achieve the comprehensive utilization of resource, and prepare hair dye technique simple, be easy to operation, obtained hair dye safety non-toxic, Color are naturally lastingly.
Detailed description of the invention
Below in conjunction with embodiment, technical scheme of the present invention is described further, but protection scope of the present invention is not limited to this.
Get 30g black cloth woods peel and blend, then adding 600ml, 40% alcoholic solution, the heated and stirred 1h when temperature 80 DEG C.By lixiviating solution filter centrifugation, get the supernatant and carry out distillation and concentration, obtain black cloth woods pericarp pigment.
The pigment obtained with extraction is for main constituent preparing natural hair dye.
Agent A: black cloth woods skin pigment 2%, propylene glycol 10%, hydroxypropyl emthylcellulose 3%, adjusts pH to 5 with phosphoric acid, water surplus.
Agent B: iron chloride 1%, propylene glycol 10%, hydroxypropyl emthylcellulose 3%, adjusts pH to 5 with phosphoric acid, water surplus.
Hair colouring methods: cleaned by hair and dry, then by agent A uniform application in hair, have hair dyed 1h at normal temperatures, then by agent B uniform application in hair, cleaned by hair after mordant dyeing 20min and dry up, hair presents naturally brown.
Claims (1)
1. the natural hair dye adopting black cloth woods peel to prepare, it is characterized in that, technique preparation process of the present invention is: in the clean black cloth woods peel blended, add the lixiviate of 20%-80% alcoholic solution by solid-liquid ratio 1:10-1:100, the lixiviate 0.5-3h when temperature is 20-80 DEG C, by lixiviating solution filter centrifugation, get supernatant distillation and concentration, obtain black cloth woods pericarp pigment;
Black cloth woods pericarp pigment extraction obtained is as hair dye main constituent, prepare a kind of new type natural hair dye, comprise agent A mediating recipe B, it is characterized in that, agent A comprises black cloth woods pericarp pigment 0.1%-10%, polyhydric alcohol 10%-30%, surfactant 1-10%, thickening agent 1-5%, all the other are water, and adjustment pH is 5-7; Agent B comprises metal salt mordant 0.5-5%, surfactant 1-10%, thickening agent 1-5%, and all the other are water, and adjustment pH is 5-7; Unit is percetage by weight;
In agent A, polyhydric alcohol is one or more in propylene glycol, butanediol, glycerol;
In agent B, metal salt mordant is in cosmetics the salt allowing any metal ion used, and includes but not limited to iron chloride, ferrous chloride, aluminum chloride, Alumen, copper nitrate;
In agent A mediating recipe B, pH adjusting agent is the one in phosphoric acid, acetic acid or citric acid;
In agent A mediating recipe B, thickening agent comprises one or more in carboxymethyl cellulose, hydroxyethyl-cellulose, hydroxypropyl emthylcellulose, cation guar gum, xanthan gum, sodium alginate;
In agent A mediating recipe B, surfactant comprises one or more in glyceryl monostearate, ceteareth-20, tween 80;
Agent A and agent B is solution, gel, emulsion or cream frost form.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510227322.4A CN104825359A (en) | 2015-05-06 | 2015-05-06 | Method for preparing natural hair dye from black plum peels |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510227322.4A CN104825359A (en) | 2015-05-06 | 2015-05-06 | Method for preparing natural hair dye from black plum peels |
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| Publication Number | Publication Date |
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| CN104825359A true CN104825359A (en) | 2015-08-12 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510227322.4A Pending CN104825359A (en) | 2015-05-06 | 2015-05-06 | Method for preparing natural hair dye from black plum peels |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105754372A (en) * | 2016-02-16 | 2016-07-13 | 孙小朝 | Extraction method of carrot pigment and natural hair dye containing carrot pigment |
| CN108451838A (en) * | 2018-07-01 | 2018-08-28 | 佛山市芊茹化妆品有限公司 | A kind of fermentation composition and preparation method thereof with black hair |
| CN109172459A (en) * | 2018-11-01 | 2019-01-11 | 张有林 | A kind of green peel of walnut hair dye and preparation method thereof |
| CN109589331A (en) * | 2019-02-19 | 2019-04-09 | 刘晓双 | A kind of external drug and application thereof inhibiting Postoperative Intravenous thrombosis |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102423286A (en) * | 2011-11-24 | 2012-04-25 | 江南大学 | Natural hair dye prepared by using phytochrome curcumin and hair dyeing method of natural hair dye |
| CN103027856A (en) * | 2012-12-24 | 2013-04-10 | 江南大学 | Mordant used for curcumin hair dye |
-
2015
- 2015-05-06 CN CN201510227322.4A patent/CN104825359A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102423286A (en) * | 2011-11-24 | 2012-04-25 | 江南大学 | Natural hair dye prepared by using phytochrome curcumin and hair dyeing method of natural hair dye |
| CN103027856A (en) * | 2012-12-24 | 2013-04-10 | 江南大学 | Mordant used for curcumin hair dye |
Non-Patent Citations (1)
| Title |
|---|
| 詹嘉红等: "黑布林李子皮色素的提取及稳定性", 《食品研究与开发》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105754372A (en) * | 2016-02-16 | 2016-07-13 | 孙小朝 | Extraction method of carrot pigment and natural hair dye containing carrot pigment |
| CN108451838A (en) * | 2018-07-01 | 2018-08-28 | 佛山市芊茹化妆品有限公司 | A kind of fermentation composition and preparation method thereof with black hair |
| CN109172459A (en) * | 2018-11-01 | 2019-01-11 | 张有林 | A kind of green peel of walnut hair dye and preparation method thereof |
| CN109589331A (en) * | 2019-02-19 | 2019-04-09 | 刘晓双 | A kind of external drug and application thereof inhibiting Postoperative Intravenous thrombosis |
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| RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20150812 |