CN104825360A - Method for preparing natural hair dye from pumpkin - Google Patents

Method for preparing natural hair dye from pumpkin Download PDF

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Publication number
CN104825360A
CN104825360A CN201510227783.1A CN201510227783A CN104825360A CN 104825360 A CN104825360 A CN 104825360A CN 201510227783 A CN201510227783 A CN 201510227783A CN 104825360 A CN104825360 A CN 104825360A
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CN
China
Prior art keywords
agent
hair dye
pumpkin
pigment
surfactant
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510227783.1A
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Chinese (zh)
Inventor
高海燕
史宏艺
岳娟
徐宇
陈秦君
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Jiangnan University
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Jiangnan University
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Publication date
Application filed by Jiangnan University filed Critical Jiangnan University
Priority to CN201510227783.1A priority Critical patent/CN104825360A/en
Publication of CN104825360A publication Critical patent/CN104825360A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a method for extracting pigments from pumpkin and producing a natural hair dye. The pigment extraction comprises the following steps: adding anhydrous ethanol into pumpkin according to a material/liquid ratio of 1:5 to 1:20, carrying out extraction for 1 to 4 hours at a temperature of 40 to 80 DEG C, filtering the extract, then subjecting filtered extract to centrifugation, and finally distilling and condensing the supernate so as to obtain the pigments. The prepared hair dye comprises an agent A and an agent B, wherein the agent A comprises the following components in percentage by weight: 0.1% to 10% of pumpkin pigment, 10 to 30% of polyol, 1 to 10% of surfactant, 1 to 5% of thickening agent, and the balance being water, the pH value is adjusted to 5-7; the agent B comprises the following components in percentage by weight: 0.5 to 5% of metal mordant, 1 to 10% of surfactant, 1 to 5% of thickening agent, and the balance being water, and the pH value is adjusted to 5-7. The provided method has the following advantages: the raw material resources are wild, the cost is low, the preparation technology is simple, the operation is easy, and the dyeing effect of the produced hair dye can is natural and long-lasting.

Description

A kind of method adopting Fructus Cucurbitae moschatae to prepare natural hair dye
Technical field
The invention belongs to cosmetic field, be specifically related to a kind of method adopting Fructus Cucurbitae moschatae to prepare natural hair dye.
Background technology
Growth in the living standard makes people more pay close attention to the image of self, and hair dye can make on the one hand poliosis contaminate and blackly make up that self is not enough, can change color development to follow the fashion on the other hand, showing personality.Oxidative hair dyes common on market has the advantages such as easy to use, Color good, hold time for a long time, spectral range is wide, but multinomial result of study shows that this kind of hair dye has certain injury to hair, and easily causing allergy, life-time service can cause poisoning, and brings out various cancer.Along with the raising of health of people consciousness, while pursuit hair dyeing effect, more pay close attention to the safety of hair dye.Natural plant pigment abundance, cheap, safety non-toxic, Environmental compatibility are good, tone is natural, and part has the health-care effecies such as antioxidation, sterilization, immunity moderation, is used for preparing the development trend that natural hair dye becomes following hair dye market day by day.
Fructus Cucurbitae moschatae another name Fructus Caricae, pumpkin, hang melon, pumpkin etc., originate in South America, after import China into, all extensively plant on China Heilungkiang, Jiangsu, Henan and other places, being Cucurbitaceae cucurbita plants, is 1 year vegetation that overgrows.Fructus Cucurbitae moschatae has crocus and cyan two kinds, and profile is oblate or irregular gourd shape.Fructus Cucurbitae moschatae contains the compositions such as abundant polysaccharide, carotenoid, mineral element, aminoacid, starch, vitamin, high nutritive value.In addition, in Fructus Cucurbitae moschatae, pigment content is higher, is mainly carotenoid, tone nature and there is the health-care effect such as antioxidation, anticancer appearance.The current research about Fructus Cucurbitae moschatae mainly concentrates on the application in food, beverage, health product, and small part is in the separation and Extraction of medicine, biotechnology and effective ingredient.Consider Fructus Cucurbitae moschatae abundance, safety non-toxic, be of high nutritive value, and pigment content is high, tone nature, therefore can be applied to the preparation of natural botanical hair dye.
Summary of the invention
The object of this invention is to provide a kind of is that raw material extracts pigment and prepares the method for natural hair dye with Fructus Cucurbitae moschatae.
The object of the invention is to be achieved through the following technical solutions.
Fructus Cucurbitae moschatae is cleaned peeling stripping and slicing, blend with juice extractor, take a certain amount of, then add the dehydrated alcohol lixiviate that solid-liquid ratio is 1:5-1:20, the lixiviate 1-6h when temperature is 40-80 DEG C.By lixiviating solution filter and centrifugal, get the supernatant and carry out distillation and concentration, obtain Pigment of the pumpkin.
Using the Pigment of the pumpkin of extraction as hair dye main constituent, prepare a kind of new type natural hair dye.This hair dye forms by two doses, and wherein agent A comprises Pigment of the pumpkin 0.1%-10%, polyhydric alcohol 10%-30%, surfactant 1-10%, thickening agent 1-5%, and all the other are water, and adjustment pH is 5-7; Agent B comprises metal salt mordant 0.5-5%, surfactant 1-10%, thickening agent 1-5%, and all the other are water, and adjustment pH is 5-7.Unit is percetage by weight.
In agent A, polyhydric alcohol is one or more in propylene glycol, butanediol, glycerol.
In agent B, metal salt mordant is in cosmetics the salt allowing any metal ion used, and includes but not limited to iron chloride, ferrous chloride, aluminum chloride, Alumen, copper nitrate.
In agent A mediating recipe B, pH adjusting agent is the one in phosphoric acid, acetic acid or citric acid.
In agent A mediating recipe B, thickening agent comprises one or more in carboxymethyl cellulose, hydroxyethyl-cellulose, hydroxypropyl emthylcellulose, cation guar gum, xanthan gum, sodium alginate.
In agent A mediating recipe B, surfactant comprises one or more in glyceryl monostearate, ceteareth-20, tween 80.
Agent A and agent B is solution, gel, emulsion or cream frost form.
The invention provides and a kind ofly extract pigment by Fructus Cucurbitae moschatae and prepare the method for natural hair dye as main constituent, this hair dye can dye the naturally color such as yellow, maroon, brown.The abundant raw material source of the method and with low cost, preparation technology is simple, be easy to operation, and obtained hair dye Color naturally lastingly.
Detailed description of the invention
Below in conjunction with embodiment, technical scheme of the present invention is described further, but protection scope of the present invention is not limited to this.
Get 50g Fructus Cucurbitae moschatae and clean stripping and slicing, blend with juice extractor, then add 500ml dehydrated alcohol, the heated and stirred 3h when temperature 60 C.By lixiviating solution filter centrifugation, get the supernatant and carry out distillation and concentration, obtain Pigment of the pumpkin.
The Pigment of the pumpkin obtained with extraction is for main constituent preparing natural hair dye.
Agent A: Pigment of the pumpkin 2%, propylene glycol 10%, hydroxypropyl emthylcellulose 3%, adjusts pH to 5 with phosphoric acid, water surplus.
Agent B: iron chloride 1%, propylene glycol 10%, hydroxypropyl emthylcellulose 3%, adjusts pH to 5 with phosphoric acid, water surplus.
Hair colouring methods: cleaned by hair and dry, then by agent A uniform application in hair, have hair dyed 1h at normal temperatures, then by agent B uniform application in hair, cleaned by hair after mordant dyeing 20min and dry up, hair presents naturally brown.

Claims (1)

1. the natural hair dye adopting Fructus Cucurbitae moschatae to prepare, it is characterized in that, technique preparation process of the present invention is: in the clean Fructus Cucurbitae moschatae blended, add the dehydrated alcohol lixiviate that solid-liquid ratio is 1:5-1:20, the lixiviate 1-4h when temperature is 40-80 DEG C, by lixiviating solution filter centrifugation, get supernatant distillation and concentration, obtain Pigment of the pumpkin;
Pigment of the pumpkin extraction obtained, as hair dye main constituent, is prepared a kind of new type natural hair dye, is comprised agent A mediating recipe B, it is characterized in that, agent A comprises Pigment of the pumpkin 0.1%-10%, polyhydric alcohol 10%-30%, surfactant 1-10%, thickening agent 1-5%, all the other are water, and adjustment pH is 5-7; Agent B comprises metal salt mordant 0.5-5%, surfactant 1-10%, thickening agent 1-5%, and all the other are water, and adjustment pH is 5-7; Unit is percetage by weight;
In agent A, polyhydric alcohol is one or more in propylene glycol, butanediol, glycerol;
In agent B, metal salt mordant is in cosmetics the salt allowing any metal ion used, and includes but not limited to iron chloride, ferrous chloride, aluminum chloride, Alumen, copper nitrate;
In agent A mediating recipe B, pH adjusting agent is the one in phosphoric acid, acetic acid or citric acid;
In agent A mediating recipe B, thickening agent comprises one or more in carboxymethyl cellulose, hydroxyethyl-cellulose, hydroxypropyl emthylcellulose, cation guar gum, xanthan gum, sodium alginate;
In agent A mediating recipe B, surfactant comprises one or more in glyceryl monostearate, ceteareth-20, tween 80;
Agent A and agent B is solution, gel, emulsion or cream frost form.
CN201510227783.1A 2015-05-06 2015-05-06 Method for preparing natural hair dye from pumpkin Pending CN104825360A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510227783.1A CN104825360A (en) 2015-05-06 2015-05-06 Method for preparing natural hair dye from pumpkin

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510227783.1A CN104825360A (en) 2015-05-06 2015-05-06 Method for preparing natural hair dye from pumpkin

Publications (1)

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CN104825360A true CN104825360A (en) 2015-08-12

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105754372A (en) * 2016-02-16 2016-07-13 孙小朝 Extraction method of carrot pigment and natural hair dye containing carrot pigment
DE202017004745U1 (en) 2017-09-11 2017-11-02 Botanica Gmbh Natural green extracts
CN114645472A (en) * 2022-03-24 2022-06-21 常州大学 Method for dyeing cotton textile fabric by utilizing pumpkin pigment
TWI781152B (en) * 2017-03-17 2022-10-21 日商資生堂股份有限公司 two-part cosmetic

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006298863A (en) * 2005-04-22 2006-11-02 Hoyu Co Ltd Hair treating agent
CN102423286A (en) * 2011-11-24 2012-04-25 江南大学 Natural hair dye prepared by using phytochrome curcumin and hair dyeing method of natural hair dye
CN104419220A (en) * 2013-09-11 2015-03-18 青岛鹏远康华天然产物有限公司 Method for high-efficiency extraction of pumpkin pigments

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2006298863A (en) * 2005-04-22 2006-11-02 Hoyu Co Ltd Hair treating agent
CN102423286A (en) * 2011-11-24 2012-04-25 江南大学 Natural hair dye prepared by using phytochrome curcumin and hair dyeing method of natural hair dye
CN104419220A (en) * 2013-09-11 2015-03-18 青岛鹏远康华天然产物有限公司 Method for high-efficiency extraction of pumpkin pigments

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
张德华等: "南瓜色素提取及稳定性研究", 《皖西学院学报》 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105754372A (en) * 2016-02-16 2016-07-13 孙小朝 Extraction method of carrot pigment and natural hair dye containing carrot pigment
TWI781152B (en) * 2017-03-17 2022-10-21 日商資生堂股份有限公司 two-part cosmetic
DE202017004745U1 (en) 2017-09-11 2017-11-02 Botanica Gmbh Natural green extracts
CN114645472A (en) * 2022-03-24 2022-06-21 常州大学 Method for dyeing cotton textile fabric by utilizing pumpkin pigment
CN114645472B (en) * 2022-03-24 2024-01-05 常州大学 Method for dyeing cotton textile by using pumpkin pigment

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Application publication date: 20150812