CN105213238A - The preparation method of the sub-non-water hand cleanser of Suaeda salsa - Google Patents

The preparation method of the sub-non-water hand cleanser of Suaeda salsa Download PDF

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Publication number
CN105213238A
CN105213238A CN201410238421.8A CN201410238421A CN105213238A CN 105213238 A CN105213238 A CN 105213238A CN 201410238421 A CN201410238421 A CN 201410238421A CN 105213238 A CN105213238 A CN 105213238A
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Prior art keywords
suaeda salsa
sub
water
stock solution
preparation
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CN201410238421.8A
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Chinese (zh)
Inventor
马玉心
王志红
崔大练
邓一兵
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Zhejiang Ocean University ZJOU
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Zhejiang Ocean University ZJOU
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Abstract

A preparation method for the sub-non-water hand cleanser of Suaeda salsa, is characterized in that step: prepare the sub-stock solution of Suaeda salsa; Bottle with a lid put into by the sodium hypochlorite solid taking 1.8 ~ 2.2g, 60 ~ 70 DEG C of fusings in thermostat water bath; Add 18 ~ 22ml mass concentration be the ethanol water of 73 ~ 77% and continue heating, at 60 ~ 70 DEG C, be incubated 4 ~ 6 minutes; Above-mentioned solution is cooled to 9 ~ 11 DEG C, and the mass concentration then adding 7 ~ 9mL is the glycerine water solution mix homogeneously of 0.9 ~ 1.1%; Add the sub-stock solution 9 ~ 11ml of Suaeda salsa of preparation; Finally slowly add 0.9 ~ 1.1g sodium chloride, and to be constantly stirred to liquid be thick.Formula of the present invention is unique, preparation technology is simple, easy to operate, and raw material is natural, and cost is low, and obtained non-water hand cleanser has good dirt-removing power, action temperature and, can not only degerming decontamination, and do not hinder hands, and to skin, there is moistening and protective effect.

Description

The preparation method of the sub-non-water hand cleanser of Suaeda salsa
Technical field
The invention belongs to daily washing product technical field, relate to a kind of non-water hand cleanser, specifically the preparation method of the sub-non-water hand cleanser of a kind of Suaeda salsa.
Background technology
The handwashing liquid great majority that market is sold need washing in use, are therefore inconvenient to use in some special places.For this reason, also investigated some non-water hand cleansers at present, as the Chinese invention patent " a kind of non-water hand cleanser " that the patent No. is CN201210338547.3, its formula comprises following component: stearic acid 20-25 part, glycerol 10-14 part, liquid paraffin 5-10 part, lanoline 4-6 part, vaseline 5-8 part, hydroxyethyl-cellulose 1-3 part, triethanolamine 5-10 part.It is also the Chinese invention patent " a kind of natural non-water hand cleanser " of CN201010620794.3 just like the patent No., with parts by weight, be made up of following material: lanoline: 3 ~ 10, glycerol: 20 ~ 30, tetraoxygen lauryl alcohol ether: 10 ~ 20, polyvinyl alcohol: 20 ~ 30, triethanolamine: 10 ~ 20, Borneolum Syntheticum: 3 ~ 8, vaseline: 2 ~ 5, essence: 0.1 ~ 0.3.Although the non-water hand cleanser using above-mentioned two formula to make just can wash without water, containing chemical substance in their composition, not only cost is high, may cause damage in addition to skin.
Suaeda salsa belongs to Chenopodiaceae, Suaeda, has another name called Suaeda salsa, is folk tradition wild herbs, is Chenopodiaceae Suaeda annual herb plant, wild in Coastal beach and salt-soda soil, is the euhalophyte that salt resistance ability is very strong.Along with deepening continuously to wild plant resource developmental research, it is found that, it is a kind of quality vegetables, industrial crops and the plant resources [Sun Yumei with value medical health care, Zhao Jin, Zhou Wei. Current Situation & Future [J] Beijing Technology and Business University journal (natural science edition) 2005,23 (1): 1-3 of China's halophytes Herba suadeae glaucae exploitation].
Research proves, common seepweed seeds oil Linoleic acid content is high, the conjugated linoleic acid of economic worth can be had more in order to preparation, conjugated linoleic acid after refining is a kind of high-class healthy product, have and prevent the effect such as thrombosis, antitumor, atherosclerosis, antioxidation, reduction body fat, increase muscle, fast-selling in international market in the last few years; Two kinds of extracts of Herba suadeae glaucae seedling and seed have the effect of antioxidant activity, antitumor enhancing non-specific immunity function, obvious inhibitory action [Zheng Weifa is had to acute inflammation, Chen Caifa, Li Wei. the chemical composition of Suaeda salsa seedling and seed chloroform/methanol extract and antiinflammatory action [J] thereof. Chinese patent medicine, 2003,25 (12): 9971002.], especially have a significant effect to escherichia coli, to preventing disease, slow down aging has great importance; In addition, Herba suadeae glaucae is again natural food coloring source, in comprehensive process Herba suadeae glaucae product process, the filtrate of Herba suadeae glaucae juice can be utilized to produce chlorophyll (1kg Herba suadeae glaucae leaf can obtain 1g chlorophyll), Herba suadeae glaucae marennin is used as the complementary color agent of condensed food, in the Suaeda salsa red autumnal leaves phase, can process and produce Herba suadeae glaucae red pigment (Herba suadeae glaucae is red), red pigment belongs to the higher pigment additive of value in the food industry, and Herba suadeae glaucae is red will fill a hole in the market.
The characteristic that above-mentioned Suaeda salsa has, makes it can be applied in the field of articles for washing, prepares non-water hand cleanser at present have not been reported at home using Suaeda salsa as raw material.
Summary of the invention
Technical problem to be solved by this invention is to provide the preparation method of the sub-non-water hand cleanser of a kind of Suaeda salsa, technique is simple, raw material is natural, cost is low, and not only dirt-removing power is strong for obtained handwashing liquid, environmental protection, but also has the effects such as degerming, crease-resistant, aging resistance.
The present invention solves the problems of the technologies described above adopted technical scheme: the preparation method of the sub-non-water hand cleanser of a kind of Suaeda salsa, is characterized in that comprising the following steps:
1) gather fresh Suaeda salsa and prepare the sub-stock solution of Suaeda salsa as raw material;
2) bottle with a lid put into by the sodium hypochlorite solid taking 1.8 ~ 2.2g, and in thermostat water bath, 60 ~ 70 DEG C slowly melt;
3) toward step 2) add 18 ~ 22ml mass concentration in the sodium hypochlorite that melted and be the ethanol water of 73 ~ 77% and continue heating, at thermostat temperature is 60-70 DEG C, be incubated 4 ~ 6 minutes;
4), after insulation terminates, above-mentioned solution is cooled to 9 ~ 11 DEG C, and the mass concentration then adding 7 ~ 9mL is the glycerine water solution of 0.9 ~ 1.1% and is uniformly mixed;
5) then step 1 is added) the sub-stock solution 9 ~ 11ml of Suaeda salsa for preparing;
6) finally slowly add 0.9 ~ 1.1g sodium chloride, and to be constantly stirred to liquid be thick.
As improvement, described fresh Suaeda salsa refers to green, do not take on a red color, and water content is high, not shrivelled Suaeda salsa.
As improvement, described step 1) detailed process of preparing the sub-stock solution of Suaeda salsa is:
A, fresh Suaeda salsa peeled off lower green leaves collect and clean with running water after, put into the beaker of cleaning;
B, clean blade is put into the ethanol water sterilization 4 ~ 6 minutes of mass concentration 73 ~ 77%, then to immerse in distilled water cleaning 2 ~ 3 times, wash away ethanol;
C, the leaf after sterilization is put into juice extractor and squeezed the juice for 9 ~ 11 seconds, obtain green liquid, be the sub-stock solution of Suaeda salsa;
D, to contain with clean beaker and get the sub-stock solution of the Suaeda salsa squeezed, and wrap with plastic bag, seal, be placed on 9 ~ 10 DEG C of refrigerator cold-storages for subsequent use.
Compared with prior art, the invention has the advantages that: formula is unique, Suaeda salsa is adopted to be prepared as raw material, the extract contained in the sub-stock solution of Suaeda salsa not only has antioxidation, also have bacteriostasis effect especially to have a significant effect to escherichia coli, the stearic acid contained can be used as surfactant, while clean hands, also reach antibacterial, whitening, crease-resistant and slow down aging effect, and Herba suadeae glaucae marennin is just as natural pigment.Preparation technology of the present invention is simple, easy to operate, and raw material is natural, cost is low, and obtained non-water hand cleanser has good dirt-removing power, action temperature and, can not only degerming decontamination, and do not hinder hands, and to skin, there is moistening and protective effect,
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
Embodiment 1
1, fresh Suaeda salsa is gathered
Collect fresh Suaeda salsa in the place that Suaeda salsa grows densely, the standard of fresh Suaeda salsa is: green, do not take on a red color, and water content is high, not shrivelled.
2, the sub-stock solution of Suaeda salsa is made
Squeeze the sub-stock solution of Suaeda salsa in accordance with the following steps:
A, fresh Suaeda salsa peeled off lower green leaves collect and clean with running water after, put into the beaker of cleaning;
B, clean blade is put into the ethanol water sterilization 5 minutes of mass concentration 75%, then to immerse in distilled water cleaning 2 times, wash away ethanol;
C, the leaf after sterilization is put into juice extractor and squeezed the juice for 10 seconds, obtain green liquid, be the sub-stock solution of Suaeda salsa;
D, to contain with clean beaker and get the sub-stock solution of the Suaeda salsa squeezed, and wrap with plastic bag, seal, be placed on 10 DEG C of refrigerator cold-storages for subsequent use.
3, the sub-non-water hand cleanser of Suaeda salsa is made
1) bottle with a lid put into by the sodium hypochlorite solid taking 2g, and in thermostat water bath, 65 DEG C slowly melt;
2) in the above-mentioned sodium hypochlorite melted, add 20ml mass concentration be the ethanol water of 75% and continue heating, at 65 DEG C, be incubated 5 minutes;
3), after insulation terminates, above-mentioned solution is cooled to 10 DEG C, and the mass concentration then adding 8mL is the glycerine water solution of 1% and is uniformly mixed;
4) the sub-stock solution 10ml of Suaeda salsa walking and prepare then is added;
5) finally slowly add 1g sodium chloride, and to be constantly stirred to liquid be thick;
6) the non-water hand cleanser bottling will prepared, namely obtains the sub-non-water hand cleanser finished product of Suaeda salsa.
Embodiment 2
1, fresh Suaeda salsa is gathered
Collect fresh Suaeda salsa in the place that Suaeda salsa grows densely, the standard of fresh Suaeda salsa is: green, do not take on a red color, and water content is high, not shrivelled.
2, the sub-stock solution of Suaeda salsa is made
Squeeze the sub-stock solution of Suaeda salsa in accordance with the following steps:
A, fresh Suaeda salsa peeled off lower green leaves collect and clean with running water after, put into the beaker of cleaning;
B, clean blade is put into the ethanol water sterilization 6 minutes of mass concentration 73%, then to immerse in distilled water cleaning 3 times, wash away ethanol;
C, the leaf after sterilization is put into juice extractor and squeezed the juice for 9 seconds, obtain green liquid, be the sub-stock solution of Suaeda salsa;
D, to contain with clean beaker and get the sub-stock solution of the Suaeda salsa squeezed, and wrap with plastic bag, seal, be placed on 9 DEG C of refrigerator cold-storages for subsequent use.
3, the sub-non-water hand cleanser of Suaeda salsa is made
1) bottle with a lid put into by the sodium hypochlorite solid taking 2g, and in thermostat water bath, 60 DEG C slowly melt;
2) in the above-mentioned sodium hypochlorite melted, add 22ml mass concentration be the ethanol water of 73% and continue heating, at 60 DEG C, be incubated 6 minutes;
3), after insulation terminates, above-mentioned solution is cooled to 9 DEG C, and the mass concentration then adding 7mL is the glycerine water solution of 1.1% and is uniformly mixed;
4) the sub-stock solution 9ml of Suaeda salsa walking and prepare then is added;
5) finally slowly add 0.9g sodium chloride, and to be constantly stirred to liquid be thick;
6) the non-water hand cleanser bottling will prepared, namely obtains the sub-non-water hand cleanser finished product of Suaeda salsa.
Embodiment 3
1, fresh Suaeda salsa is gathered
Collect fresh Suaeda salsa in the place that Suaeda salsa grows densely, the standard of fresh Suaeda salsa is: green, do not take on a red color, and water content is high, not shrivelled.
2, the sub-stock solution of Suaeda salsa is made
Squeeze the sub-stock solution of Suaeda salsa in accordance with the following steps:
A, fresh Suaeda salsa peeled off lower green leaves collect and clean with running water after, put into the beaker of cleaning;
B, clean blade is put into the ethanol water sterilization 4 minutes of mass concentration 77%, then to immerse in distilled water cleaning 2 times, wash away ethanol;
C, the leaf after sterilization is put into juice extractor and squeezed the juice for 11 seconds, obtain green liquid, be the sub-stock solution of Suaeda salsa;
D, to contain with clean beaker and get the sub-stock solution of the Suaeda salsa squeezed, and wrap with plastic bag, seal, be placed on 11 DEG C of refrigerator cold-storages for subsequent use.
3, the sub-non-water hand cleanser of Suaeda salsa is made
1) bottle with a lid put into by the sodium hypochlorite solid taking 2g, and in thermostat water bath, 70 DEG C slowly melt;
2) in the above-mentioned sodium hypochlorite melted, add 18ml mass concentration be the ethanol water of 77% and continue heating, at 70 DEG C, be incubated 4 minutes;
3), after insulation terminates, above-mentioned solution is cooled to 11 DEG C, and the mass concentration then adding 9mL is the glycerine water solution of 0.9% and is uniformly mixed;
4) the sub-stock solution 11ml of Suaeda salsa walking and prepare then is added;
5) finally slowly add 1.1g sodium chloride, and to be constantly stirred to liquid be thick;
6) the non-water hand cleanser bottling will prepared, namely obtains the sub-non-water hand cleanser finished product of Suaeda salsa.
Obtained finished product handwashing liquid is green viscous liquid, and the shelf-life is 3 ~ 4 years at normal temperatures.
After practical application, non-water hand cleanser of the present invention has good dirt-removing power, action temperature and, can not only degerming decontamination, and do not hinder hands, and to skin, there is moistening and protective effect, and there is the distinctive draft abnormal smells from the patient of Suaeda salsa.

Claims (3)

1. a preparation method for the sub-non-water hand cleanser of Suaeda salsa, is characterized in that comprising the following steps:
1) gather fresh Suaeda salsa and prepare the sub-stock solution of Suaeda salsa as raw material;
2) bottle with a lid put into by the sodium hypochlorite solid taking 1.8 ~ 2.2g, and in thermostat water bath, 60 ~ 70 DEG C slowly melt;
3) toward step 2) add 18 ~ 22ml mass concentration in the sodium hypochlorite that melted and be the ethanol water of 73 ~ 77% and continue heating, at thermostat temperature is 60-70 DEG C, be incubated 4 ~ 6 minutes;
4), after insulation terminates, above-mentioned solution is cooled to 9 ~ 11 DEG C, and the mass concentration then adding 7 ~ 9mL is the glycerine water solution of 0.9 ~ 1.1% and is uniformly mixed;
5) then step 1 is added) the sub-stock solution 9 ~ 11ml of Suaeda salsa for preparing;
6) finally slowly add 0.9 ~ 1.1g sodium chloride, and to be constantly stirred to liquid be thick.
2. preparation method according to claim 1, is characterized in that: described fresh Suaeda salsa refers to green, do not take on a red color, and water content is high, not shrivelled Suaeda salsa.
3. preparation method according to claim 1, is characterized in that: described step 1) detailed process of preparing the sub-stock solution of Suaeda salsa is:
A, fresh Suaeda salsa peeled off lower green leaves collect and clean with running water after, put into the beaker of cleaning;
B, clean blade is put into the ethanol water sterilization 4 ~ 6 minutes of mass concentration 73 ~ 77%, then to immerse in distilled water cleaning 2 ~ 3 times, wash away ethanol;
C, the leaf after sterilization is put into juice extractor and squeezed the juice for 9 ~ 11 seconds, obtain green liquid, be the sub-stock solution of Suaeda salsa;
D, to contain with clean beaker and get the sub-stock solution of the Suaeda salsa squeezed, and wrap with plastic bag, seal, be placed on 9 ~ 10 DEG C of refrigerator cold-storages for subsequent use.
CN201410238421.8A 2014-05-29 2014-05-29 The preparation method of the sub-non-water hand cleanser of Suaeda salsa Pending CN105213238A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112237558A (en) * 2019-07-17 2021-01-19 辽宁泓新科技成果转化服务有限公司 Facial mask and preparation method thereof
CN113952261A (en) * 2020-07-16 2022-01-21 盘锦大工碱蓬生物科技有限公司 Suaeda salsa bath plant salt, preparation process and use method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102178620A (en) * 2010-12-24 2011-09-14 徐美仙 Antiseptic hand-washing solution without water washing

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102178620A (en) * 2010-12-24 2011-09-14 徐美仙 Antiseptic hand-washing solution without water washing

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
高健: "盐地碱蓬中黄酮类物质的提取及抗氧化性研究", 《盐城工学院学报》 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112237558A (en) * 2019-07-17 2021-01-19 辽宁泓新科技成果转化服务有限公司 Facial mask and preparation method thereof
CN113952261A (en) * 2020-07-16 2022-01-21 盘锦大工碱蓬生物科技有限公司 Suaeda salsa bath plant salt, preparation process and use method thereof

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Application publication date: 20160106