CN104432075B - A kind of leaf of Moringa oral liquid and preparation method thereof - Google Patents

A kind of leaf of Moringa oral liquid and preparation method thereof Download PDF

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Publication number
CN104432075B
CN104432075B CN201410819012.7A CN201410819012A CN104432075B CN 104432075 B CN104432075 B CN 104432075B CN 201410819012 A CN201410819012 A CN 201410819012A CN 104432075 B CN104432075 B CN 104432075B
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China
Prior art keywords
moringa
leaf
extract
extracting solution
reflux
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CN104432075A (en
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邱彬
黄建凡
李想
王文斌
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FUZHOU JIAYOU CHEMICAL TECHNOLOGY Co Ltd
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FUZHOU JIAYOU CHEMICAL TECHNOLOGY Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention discloses a kind of leaf of Moringa oral liquid and preparation method thereof.With leaf of Moringa as primary raw material, stevioside, Mentholum, sorbic acid are adjuvant.Its core is to be pulverized by leaf of Moringa as superfine powder, it is crushed to breaking cellular wall, extracted by alcohol heating reflux, reflux, extract, is added again with distilled water, united extraction liquid, is evaporated under reduced pressure and concentrates, obtain Moringa extract, guarantee that the nutritional labeling in the natural leaf of Moringa of ecosystem and biological activity are not destroyed by high temperature and chemical solvent, and make the dosage form being prone to preserve transport use.The present invention is effectively improved the bioavailability of leaf of Moringa complete nutrition ingredients, provides a kind of extra-nutrition to people, improves the environmental protective hygienic product of human body sub-health status.

Description

A kind of leaf of Moringa oral liquid and preparation method thereof
Technical field
The present invention relates to health food processing and fabricating field, particularly to a kind of leaf of Moringa oral liquid and preparation method thereof.
Background technology
Leaf of Moringa is the leaves of perennial torrid zone deciduous tree Moringa tree (being also called drumstick tree) originating in India, edible.Containing profuse nutritional labeling in leaf of Moringa, calcium content is more than 4 times of milk, containing trace element such as the highest potassium, ferrum, zinc, possibly together with abundant vitamin and aminoacid etc., including 5 kinds in eight kinds of essential amino acids, especially lysine and threonine, is a kind of functional food containing fully nutrient.As long as a people is able to eat about the 25 grams nutritional needs that can meet different crowd every day.In addition, it has been investigated that, Moringa extract also treats the biological functions such as ulcer, antiinflammatory be antibacterial, blood sugar lowering, blood fat reducing, blood pressure lowering, antitumor.
In China, the research and development of Moringa tree was applied also in the starting stage at present, be also formed without preparing with Moringa for raw material the large-scale application of health product.On the other hand, nutritious due to Moringa tree, various its secondary metabolites contents are high, and processing technique is more complicated, it is desirable to fully obtain nutritional labeling and be not destroyed, to be prone to preserve transport, salable leaf of Moringa health product the most increasingly difficult.The present invention is after fully analyzing the nutritional labeling of leaf of Moringa, it was found that for extracting leaf of Moringa nutritional labeling for preparing a kind of new method of oral liquid.
Summary of the invention
Present invention aims to the deficiencies in the prior art, it is provided that a kind of leaf of Moringa oral liquid and preparation method thereof.This oral liquid can supplement the nutrients, improve human body sub-health status.
In order to realize foregoing invention purpose, the present invention adopts the following technical scheme that
The preparation method of a kind of leaf of Moringa oral liquid, comprises the following steps:
1) leaf of Moringa is crushed to breaking cellular wall;
2) then extract with alcohol heating reflux, it is thus achieved that the first extracting solution;Then adding distilled water in filtering residue, heating and refluxing extraction obtains the second extracting solution;
3) merge the first extracting solution and the second extracting solution, be evaporated under reduced pressure and be concentrated into paste, add 50~100 times of distilled water allotments are uniform, add adjuvant, mix homogeneously, fill, low temperature discontinuous sterilization, prepare leaf of Moringa oral liquid.
In step 1), leaf of Moringa is ground into 500 mesh to 1500 mesh superfine powder by super micron mill.
Step 2) in the preparation method of the first extracting solution be: leaf of Moringa powder is put in reflux, extract, device, adds the ethanol of 8-10 times amount 60-70%, adjust the temperature to 60-65 DEG C, reflux, extract, 60 minutes, filter to obtain ethanol extract;Repeat to extract 3 times, merge ethanol extract, obtain the first extracting solution.
Step 2) in the preparation method of the second extracting solution be: the residue after ethanol extraction is put into reflux, extract, device, adds 10-12 times amount distilled water, be heated to 60-70 DEG C, reflux, extract, 90 minutes, filter, obtain aqueous extract;Repeat to extract 3 times, merge aqueous extract, obtain the second extracting solution.
Adjuvant described in step 3) includes stevioside, Mentholum, sorbic acid;In prepared leaf of Moringa oral liquid, containing 0.05-0.07 wt% stevioside, 0.8-1.2wt% Mentholum, 0.04-0.05 wt% sorbic acid.
The beneficial effects of the present invention is:
The present invention is fully extracted the effective nutritional labeling in leaf of Moringa, prepares leaf of Moringa oral liquid;This oral liquid can improve the efficiency that absorption of human body utilizes, and mouthfeel is improved, it is easy to carries use, is a kind of extra-nutrition, improves the environmental protective hygienic food of health sub-health state.
Detailed description of the invention
Present invention the following example further illustrates the present invention, but protection scope of the present invention is not limited to the following example.
Embodiment 1
The concrete preparation process of a kind of Moringa oral liquid is as follows:
1) by clean, decontamination, dry leaf of Moringa, it is crushed to breaking cellular wall with super micron mill, crosses the superfine powder of 500 mesh;
2) leaf of Moringa powder is put in reflux, extract, device, add the ethanol of 10 times amount 60 wt%, adjust the temperature to 60 DEG C, reflux, extract, 60 minutes, filters to obtain ethanol extract, repeats above operation totally 3 times, merge ethanol extract, obtain the first extracting solution;
3) reclaim residue, residue is put into reflux, extract, device, adds 10 times amount distilled water, be heated to 70 DEG C, reflux, extract, 90 minutes, filters, obtains aqueous extract, repeat above operation totally 3 times, merge aqueous extract, obtain the second extracting solution;
4) merging first and second extracting solution, be evaporated under reduced pressure by leaf of Moringa extracting solution and be concentrated into paste, the distilled water allotment adding 50 times of quality is 2wt% to the concentration of leaf of Moringa, adds stevioside, Mentholum, sorbic acid, then fill, low temperature discontinuous sterilization.
Leaf of Moringa oral liquid prepared by the present embodiment, stevioside content is 0.05 wt%, Determination of menthol is 1.0 wt%, Determination of sorbic is 0.04 wt%, it is extracted the nutritional labeling in raw material leaf of Moringa greatly, and is avoided destruction and the loss of effective nutritional labeling by effective processing technology;Make nutritional labeling abundant in leaf of Moringa, it is easier to allow human digestive organ absorb, meet people's demand to needed by human nutrition, human body sub-health status can be improved well.
Embodiment 2
The concrete preparation process of a kind of Moringa oral liquid is as follows:
1) by clean, decontamination, dry leaf of Moringa, it is crushed to breaking cellular wall with super micron mill, crosses the superfine powder of 1000 mesh;
2) leaf of Moringa powder is put in reflux, extract, device, add the ethanol of 8 times amount 70 wt%, adjust the temperature to 65 DEG C, reflux, extract, 60 minutes, filters to obtain ethanol extract, repeats above operation totally 3 times, merge ethanol extract, obtain the first extracting solution;
3) reclaim residue, residue is put into reflux, extract, device, adds 12 times amount distilled water, be heated to 65 DEG C, reflux, extract, 90 minutes, filters, obtains aqueous extract, repeat above operation totally 3 times, merge aqueous extract, obtain the second extracting solution;
4) merging first and second extracting solution, be evaporated under reduced pressure by leaf of Moringa extracting solution and be concentrated into paste, the distilled water allotment adding 100 times of quality is 1wt% to the concentration of leaf of Moringa, adds stevioside, Mentholum, sorbic acid, then fill, low temperature discontinuous sterilization.
Leaf of Moringa oral liquid prepared by the present embodiment, stevioside content is 0.07 wt%, Determination of menthol is 0.8 wt%, Determination of sorbic is 0.04 wt%, it is extracted the nutritional labeling in raw material leaf of Moringa greatly, and is avoided destruction and the loss of effective nutritional labeling by effective processing technology;Make nutritional labeling abundant in leaf of Moringa, it is easier to allow human digestive organ absorb, meet people's demand to needed by human nutrition, human body sub-health status can be improved well.
Embodiment 3
The concrete preparation process of a kind of Moringa oral liquid is as follows:
1) by clean, decontamination, dry leaf of Moringa, it is crushed to breaking cellular wall with super micron mill, crosses the superfine powder of 500 mesh;
2) leaf of Moringa powder is put in reflux, extract, device, add the ethanol of 9 times amount 65 wt%, adjust the temperature to 62 DEG C, reflux, extract, 60 minutes, filters to obtain ethanol extract, repeats above operation totally 3 times, merge ethanol extract, obtain the first extracting solution;
3) reclaim residue, residue is put into reflux, extract, device, adds 11 times amount distilled water, be heated to 60 DEG C, reflux, extract, 90 minutes, filters, obtains aqueous extract, repeat above operation totally 3 times, merge aqueous extract, obtain the second extracting solution;
4) merging first and second extracting solution, be evaporated under reduced pressure by leaf of Moringa extracting solution and be concentrated into paste, the distilled water allotment adding 75 times of quality is 1.5wt% to the concentration of leaf of Moringa, adds stevioside, Mentholum, sorbic acid, then fill, low temperature discontinuous sterilization.
Leaf of Moringa oral liquid prepared by the present embodiment, stevioside content is 0.06 wt%, Determination of menthol is 1.2 wt%, Determination of sorbic is 0.05 wt%, it is extracted the nutritional labeling in raw material leaf of Moringa greatly, and is avoided destruction and the loss of effective nutritional labeling by effective processing technology;Make nutritional labeling abundant in leaf of Moringa, it is easier to allow human digestive organ absorb, meet people's demand to needed by human nutrition, human body sub-health status can be improved well.
The above; being only the present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto, any those familiar with the art is in the technical scope of present disclosure; the change that can readily occur in or replacement, all should contain within protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain of claims.

Claims (1)

1. the preparation method of a leaf of Moringa oral liquid, it is characterised in that: concretely comprise the following steps:
1) leaf of Moringa is crushed to breaking cellular wall;
2) then extract with alcohol heating reflux, it is thus achieved that the first extracting solution;Then adding distilled water in filtering residue, heating and refluxing extraction obtains the second extracting solution;
3) merge the first extracting solution and the second extracting solution, be evaporated under reduced pressure and be concentrated into paste, add 50~100 times of distilled water allotments are uniform, add adjuvant, mix homogeneously, fill, low temperature discontinuous sterilization, prepare leaf of Moringa oral liquid;
Step 2) in the preparation method of the first extracting solution be: leaf of Moringa powder is put in reflux, extract, device, adds the ethanol of 8-10 times amount 60-70%, adjust the temperature to 60-65 DEG C, reflux, extract, 60 minutes, filter to obtain ethanol extract;Repeat to extract 3 times, merge ethanol extract, obtain the first extracting solution;
Step 2) in the preparation method of the second extracting solution be: the residue after ethanol extraction is put into reflux, extract, device, adds 10-12 times amount distilled water, be heated to 60-70 DEG C, reflux, extract, 90 minutes, filter, obtain aqueous extract;Repeat to extract 3 times, merge aqueous extract, obtain the second extracting solution;In step 1), leaf of Moringa is ground into 500 mesh to 1500 mesh superfine powder by super micron mill;Adjuvant described in step 3) includes stevioside, Mentholum, sorbic acid;In prepared leaf of Moringa oral liquid, containing 0.05-0.07 wt% stevioside, 0.8-1.2wt% Mentholum, 0.04-0.05 wt% sorbic acid.
CN201410819012.7A 2014-12-25 2014-12-25 A kind of leaf of Moringa oral liquid and preparation method thereof Expired - Fee Related CN104432075B (en)

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Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105685620A (en) * 2015-07-08 2016-06-22 海南木辣达生物科技有限公司 Moringa oleifera oral liquid and preparation method thereof
CN105054067B (en) * 2015-08-27 2017-12-15 大闽食品(漳州)有限公司 A kind of preparation method of water-soluble moringa oleifera leaf extractive
CN105166912B (en) * 2015-10-22 2018-06-22 李佳忠 A kind of compound Moringa stem of noble dendrobium oral liquid and preparation method thereof
CN105192832A (en) * 2015-11-07 2015-12-30 三株福尔制药有限公司 Composition of probiotic fermented horseradish tree leaves as well as preparation method and application of composition
CN106107339A (en) * 2016-06-25 2016-11-16 韶关绿之源包装食品有限公司 Moringa method for preparing beverage
CN107348289A (en) * 2017-08-23 2017-11-17 尹飞 Moringa oleifera beverage and preparation method thereof
CN108420074A (en) * 2018-04-09 2018-08-21 江西牧威利元生物科技有限公司 A kind of tyrosinase activity inhibitor and its application

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CN1745664A (en) * 2004-09-09 2006-03-15 林保村 Moringaceae beverage and production thereof
CN103652930A (en) * 2013-12-31 2014-03-26 广州天来宝生物科技有限公司 Moringa calcium total nutrient and preparation method thereof
CN103704806A (en) * 2013-12-10 2014-04-09 马鞍山市安康菌业有限公司 Moringa oleifera leaf nutritional beverage and preparation method thereof
CN103750440A (en) * 2013-12-16 2014-04-30 马鞍山市安康菌业有限公司 Horseradish tree leaf nutritious drink and preparation method thereof
CN103989174A (en) * 2014-06-10 2014-08-20 陈宗进 Moringa oleifera composite all-nutrition nutrient

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1745664A (en) * 2004-09-09 2006-03-15 林保村 Moringaceae beverage and production thereof
CN103704806A (en) * 2013-12-10 2014-04-09 马鞍山市安康菌业有限公司 Moringa oleifera leaf nutritional beverage and preparation method thereof
CN103750440A (en) * 2013-12-16 2014-04-30 马鞍山市安康菌业有限公司 Horseradish tree leaf nutritious drink and preparation method thereof
CN103652930A (en) * 2013-12-31 2014-03-26 广州天来宝生物科技有限公司 Moringa calcium total nutrient and preparation method thereof
CN103989174A (en) * 2014-06-10 2014-08-20 陈宗进 Moringa oleifera composite all-nutrition nutrient

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