CN106518653A - Membrane extraction process for hydroxycitric acid - Google Patents
Membrane extraction process for hydroxycitric acid Download PDFInfo
- Publication number
- CN106518653A CN106518653A CN201610845298.5A CN201610845298A CN106518653A CN 106518653 A CN106518653 A CN 106518653A CN 201610845298 A CN201610845298 A CN 201610845298A CN 106518653 A CN106518653 A CN 106518653A
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- Prior art keywords
- membrane
- carrying
- film
- permeate
- concentration
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
Abstract
The invention discloses a membrane extraction process for hydroxycitric acid. The process comprises a series of steps, i.e., carrying out raw material crushing, carrying out lixiviating filtration, carrying out separation, carrying out membrane filtration, carrying out membrane thickening and carrying out drying. The process comprises the following concrete operation steps: (1) crushing garcinia cambogia in a crusher; (2) adding water into the crushed garcinia cambogia, carrying out heating to carry out boiling, and carrying out filtration with gauze; (3) carrying out separation treatment with a separation membrane, and collecting separation membrane permeate; (4) carrying out treatment with a ceramic membrane, and collecting ceramic membrane permeate; (5) subjecting the separation membrane permeate to thickening treatment through a thickening membrane, and collecting thickening membrane permeate; and (6) carrying out low-temperature vacuum drying on a thickened solution of the thickening membrane, and taking out powder until the thickened solution is dried into the powder, thereby obtaining the finished product hydroxycitric acid. According to the membrane extraction process for the hydroxycitric acid, disclosed by the invention, the process is simple, the design is reasonable, the purity of extraction of the hydroxycitric acid is high, the treatment effect is stable, and the process is low in energy consumption and is pollution-free.
Description
Technical field
The invention belongs to technical field of membrane separation, and in particular to a kind of hydroxycitrate sorrel extraction process.
Background technology
Hydroxycitric acid (HCA) is a kind of derivant of citric acid, is widely present in the torrid zones such as Fructus Resina garciniae, Calyx Hibisci Sabdariffae
In rain forest plant.HCA has the ability for adjusting organism lipid metabolism level, and therefore HCA becomes part diet products and nutrition
One of composition of health product.The extracting method complex operation of traditional hydroxycitric acid, needs substantial amounts of chemical reagent, equipment to hold high
Expensive, DNA purity is not high, and yield is relatively low.
The content of the invention
It is an object of the invention to provide a kind of simple to operate, reasonable in design, DNA purity is high, effect stability, yield
High hydroxycitrate sorrel extraction process.
The technical scheme is that a kind of hydroxycitrate sorrel extraction process, blend including raw material, extract filtration, separation,
Membrane filtration, membrance concentration and series of steps is dried, concrete operation step is as follows：
Step one, Fructus Resina garciniae is put in pulper blends；
Step 2, the broken shape Fructus Resina garciniae for obtaining step one add water, heated and boiled, and with filtered through gauze, filtering residue washes two with water
It is secondary；
Step 3, separating treatment is carried out by seperation film, obtain seperation film permeate and seperation film dope, collected seperation film and pass through
Liquid；
Step 4, under the high temperature conditions with ceramic film process seperation film permeate, obtain ceramic membrane permeate and ceramic membrane dope
Collect ceramic membrane permeate；
Step 5, by ceramic membrane permeate by concentrate film carry out concentration, obtain concentrate membrance concentration liquid and concentration film pass through
Liquid, collects concentration membrance concentration liquid；
Step 6, concentration film dope is carried out into low-temperature vacuum drying, be dried to powder and take out, obtain finished product hydroxycitric acid.
Preferably, the step 3 seperation film is hollow fiber ultrafiltration membrane, and the seperation film dope is macromole pectin.
Preferably, the ceramic membrane in the step 4 is tubular ceramic membrane.
Preferably, it is rolling organic membrane to concentrate film described in the step 5.
The present invention is a kind of hydroxycitrate sorrel extraction process, by a series of membrane separation technique and to Fructus Resina garciniae
A little simple process, can extract highly purified hydroxycitric acid.
Beneficial effects of the present invention：
Invention is a kind of berberine film extraction process, process is simple, reasonable in design, and hydroxycitric acid DNA purity is high, process effect
Fruit is stable, and energy consumption is low, pollution-free.The hydroxycitric acid of extraction comes from natural extract, while and having Western medicine raw material clear and definite
Chemical composition and anti-obesity mechanism, its synthesis by suppression fat, the burning of promotion fatty acid, the intake of reduction food, three
Integrally, the effect of slimming is reached, is a kind of rare, most preferable, the most healthy Weight-reducing health of current fat-reducing effect
Raw material.
Description of the drawings
Fig. 1 is a kind of flow chart of hydroxycitrate sorrel extraction process of the invention.
Specific embodiment
For ease of skilled artisan understands that the present invention program, in conjunction with specific embodiment to technical solution of the present invention
It is further described in detail.
As shown in figure 1, a kind of hydroxycitrate sorrel extraction process of the present invention, blends including raw material, extracts filtration, divides
From, membrane filtration, membrance concentration and be dried series of steps, concrete operation step is as follows：
Step one, Fructus Resina garciniae is put in pulper blends；
Step 2, the broken shape Fructus Resina garciniae for obtaining step one add water, heated and boiled, and with filtered through gauze, filtering residue washes two with water
It is secondary；
Step 3, separating treatment is carried out by seperation film, obtain seperation film permeate and seperation film dope, collected seperation film and pass through
Liquid；
Step 4, under the high temperature conditions with ceramic film process seperation film permeate, obtain ceramic membrane permeate and ceramic membrane dope
Collect ceramic membrane permeate；
Step 5, by ceramic membrane permeate by concentrate film carry out concentration, obtain concentrate membrance concentration liquid and concentration film pass through
Liquid, collects concentration membrance concentration liquid；
Step 6, concentration film dope is carried out into low-temperature vacuum drying, be dried to powder and take out, obtain finished product hydroxycitric acid.
The step 3 seperation film be hollow fiber ultrafiltration membrane, the seperation film dope be macromole pectin, the pottery in the step 4
Porcelain film is tubular ceramic membrane, and it is rolling organic membrane to concentrate film described in the step 5.
The present invention is a kind of hydroxycitrate sorrel extraction process, is blended by raw material, extracts filtration, separation, membrane filtration, film
Concentration and dried finally give highly purified hydroxycitric acid finished product, carry out sealing stored under refrigeration, the hydroxyl of extraction
Citric acid promotes the burning of fatty acid by suppressing fatty synthesis, reduces the intake of food, and the Trinity reaches weight reducing and subtracts
The effect of fertilizer, is a kind of holy product of fat-reducing.
The present invention program is exemplarily described above, it is clear that the present invention is implemented and do not limited by aforesaid way
System, as long as the various unsubstantialities for employing method of the present invention design and technical scheme and carrying out are improved, or not improved will send out
Bright design and technical scheme directly apply to other occasions, within protection scope of the present invention.
Claims (4)
1. a kind of hydroxycitrate sorrel extraction process, blends including raw material, extracts filtration, separation, membrane filtration, membrance concentration and drying
Series of steps, concrete operation step are as follows：
Step one, Fructus Resina garciniae is put in pulper blends；
Step 2, the broken shape Fructus Resina garciniae for obtaining step one add water, heated and boiled, and with filtered through gauze, filtering residue washes two with water
It is secondary；
Step 3, separating treatment is carried out by seperation film, obtain seperation film permeate and seperation film dope, collected seperation film and pass through
Liquid；
Step 4, under the high temperature conditions with ceramic film process seperation film permeate, obtain ceramic membrane permeate and ceramic membrane dope
Collect ceramic membrane permeate；
Step 5, by ceramic membrane permeate by concentrate film carry out concentration, obtain concentrate membrance concentration liquid and concentration film pass through
Liquid, collects concentration membrance concentration liquid；
Step 6, concentration film dope is carried out into low-temperature vacuum drying, be dried to powder and take out, obtain finished product hydroxycitric acid.
2. a kind of hydroxycitrate sorrel extraction process according to claim 1, it is characterised in that the step 3 seperation film
For hollow fiber ultrafiltration membrane, the seperation film dope is macromole pectin.
3. a kind of berberine film extraction process according to claim 1, it is characterised in that the ceramic membrane in the step 4
For tubular ceramic membrane.
4. a kind of berberine film extraction process according to claim 1, it is characterised in that concentrate described in the step 5
Film is rolling organic membrane.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610845298.5A CN106518653A (en) | 2016-09-24 | 2016-09-24 | Membrane extraction process for hydroxycitric acid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610845298.5A CN106518653A (en) | 2016-09-24 | 2016-09-24 | Membrane extraction process for hydroxycitric acid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106518653A true CN106518653A (en) | 2017-03-22 |
Family
ID=58344073
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610845298.5A Pending CN106518653A (en) | 2016-09-24 | 2016-09-24 | Membrane extraction process for hydroxycitric acid |
Country Status (1)
| Country | Link |
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| CN (1) | CN106518653A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107473958A (en) * | 2017-08-20 | 2017-12-15 | 合肥信达膜科技有限公司 | A kind of method that hydroxycitric acid is extracted from HCA |
| CN108047029A (en) * | 2017-12-20 | 2018-05-18 | 南京慧博生物科技有限公司 | A kind of preparation method of the extraction purification hydroxycitric acid from Garcinia Cambogia |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104084047A (en) * | 2014-07-17 | 2014-10-08 | 新疆鹏弘生物科技有限公司 | Glycyrrhiza extracting solution clarification and concentration membrane system |
| CN104610049A (en) * | 2015-02-12 | 2015-05-13 | 白心亮 | Method for extracting hydroxyl citric acid from garcinia cambogia |
| CN104844447A (en) * | 2015-04-15 | 2015-08-19 | 义乌章舸生物工程有限公司 | Method for preparing high-purity hydroxycitric acid with garcinia cambogia as raw material |
-
2016
- 2016-09-24 CN CN201610845298.5A patent/CN106518653A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104084047A (en) * | 2014-07-17 | 2014-10-08 | 新疆鹏弘生物科技有限公司 | Glycyrrhiza extracting solution clarification and concentration membrane system |
| CN104610049A (en) * | 2015-02-12 | 2015-05-13 | 白心亮 | Method for extracting hydroxyl citric acid from garcinia cambogia |
| CN104844447A (en) * | 2015-04-15 | 2015-08-19 | 义乌章舸生物工程有限公司 | Method for preparing high-purity hydroxycitric acid with garcinia cambogia as raw material |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107473958A (en) * | 2017-08-20 | 2017-12-15 | 合肥信达膜科技有限公司 | A kind of method that hydroxycitric acid is extracted from HCA |
| CN108047029A (en) * | 2017-12-20 | 2018-05-18 | 南京慧博生物科技有限公司 | A kind of preparation method of the extraction purification hydroxycitric acid from Garcinia Cambogia |
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Application publication date: 20170322 |