CN110946812A

CN110946812A - Anti-hair loss and hair-nourishing essence and preparation method thereof

Info

Publication number: CN110946812A
Application number: CN201911326084.7A
Authority: CN
Inventors: 莫贤东; 林泽森; 萧少仪; 黄勇
Original assignee: Guangzhou Yuxin Cosmetics Co Ltd
Current assignee: Guangzhou Yuxin Cosmetics Co Ltd
Priority date: 2019-12-20
Filing date: 2019-12-20
Publication date: 2020-04-03

Abstract

The invention discloses an anti-hair loss and hair-nourishing essence and a preparation method thereof, wherein the preparation method comprises the following steps: weighing the raw materials of dimethyl sulfone and adenosine, and uniformly dispersing with water; weighing the preservative, and heating and dispersing; weighing 1, 3-propanediol, butanediol, EDTA-2NA and water, stirring and heating, and naturally cooling; weighing Polygoni Multiflori radix extract, Ginseng radix extract, folium Platycladi extract, rhizoma anemarrhenae extract, rhizoma Zingiberis recens extract, and radix Angelicae sinensis extract, stirring well, adding processed dimethyl sulfone, adenosine and antiseptic, stirring well, inspecting, filtering, discharging, and filling to obtain the final product. The preparation method disclosed by the invention has the advantages of simple process, low cost, increase of the residual quantity of the active ingredients in the finished product, shortening of the effective time and enhancement of the effect.

Description

Anti-hair loss and hair-nourishing essence and preparation method thereof

Technical Field

The invention relates to the technical field of cosmetics, in particular to anti-hair loss and hair-nourishing essence and a preparation method thereof.

Background

Alopecia refers to the phenomenon of hair loss. The normal hair loss is the hair in the catagen and telogen phases, and the normal amount of hair can be maintained because the hair entering the catagen phase and the hair newly entering the anagen phase are constantly in dynamic balance. Pathological alopecia refers to abnormal or excessive hair loss, the symptoms of alopecia are gradually younger, and the physiological troubles of alopecia patients are gradually changed into psychological troubles. The reasons for alopecia are numerous, and the pressure of life, high-intensity work, bad living habits and the like all lead the alopecia of young people to become an increasingly serious social phenomenon.

At present, most of anti-hair loss and hair growth products on the market are of a washing type, the residual quantity of the anti-hair loss and hair growth effective components contained in the products is very little, and the anti-hair loss and hair growth effects are not ideal. Long service period and slow effect.

Therefore, in combination with the above problems, it is an urgent need to solve the problems of the art to provide an anti-hair loss and hair growth essence with strong effect and fast effect by adopting a reasonable combination of various traditional Chinese medicine extracts and solvents, and a preparation method thereof.

Disclosure of Invention

In view of the above, the invention provides an anti-hair loss and hair-nourishing essence and a preparation method thereof, the preparation method disclosed by the invention has the advantages of simple process and low cost, different forms and effectiveness of hair care products can be developed by adopting reasonable compounding of various traditional Chinese medicine extracts and solvents, the residual quantity of effective substances is increased, the effective time is shortened, the effect is enhanced, the anti-hair loss and hair-nourishing essence is suitable for large-scale industrial production, and the requirements of markets and consumers are met.

In order to achieve the purpose, the technical scheme adopted by the invention is as follows:

a preparation method of an anti-hair loss and hair-nourishing essence comprises the following specific steps:

s1, weighing dimethyl sulfone as a raw material, adding water, placing in a stainless steel pot at room temperature, stirring for 1-2min, and uniformly dispersing until the mixture is transparent and has no particles; weighing adenosine, adding water, and uniformly dispersing by the same method until the adenosine is transparent and has no particles; weighing the preservative, heating and stirring, dispersing until the preservative is transparent and has no particles, and keeping the temperature and stirring at 55 ℃;

s2, weighing 1, 3-propylene glycol, butanediol, EDTA-2NA and water, placing in an emulsifying pot, heating while stirring, stirring for 30-60min, and naturally cooling to 40-45 ℃;

s3, weighing the polygonum multiflorum extract, the ginseng root extract, the cacumen biotae extract, the rhizoma anemarrhenae root extract, the ginger root extract and the angelica root extract, putting the materials into an emulsifying pot, uniformly stirring the materials in a sterile environment, adding the dimethyl sulfone, the adenosine and the preservative which are processed in the step S1, stirring the materials until the materials are uniformly dispersed without particles, filtering the materials after the materials are inspected to be qualified, discharging the materials, and filling the materials to obtain the finished product.

Preferably, in the step S1, the stirring speed of the dimethyl sulfone, the adenosine and the preservative is 50-200 r/min.

Preferably, in the step S1, the temperature is raised to 55-60 ℃, and the mixture is stirred for 30min under the condition of heat preservation.

Preferably, in step S1, the preservative includes, but is not limited to, 1, 2-hexanediol, p-hydroxyacetophenone.

By adopting the preferable scheme, the invention has the beneficial effects that: the preservative selects 1, 2-hexanediol and p-hydroxyacetophenone, so that the product can be protected from microbial contamination, the shelf life and the service life of the product can be prolonged, the safety of the product can be ensured, and the infection of a consumer caused by the contaminated product can be prevented.

Preferably, in the step S2, the temperature is raised to 80-85 ℃ and the stirring speed is 50-200 r/min.

Preferably, in the step S3, the stirring speed is 500-1500 r/min.

An anti-hair loss and hair-nourishing essence comprises the following components in percentage by weight: 6-11.0% of polygonum multiflorum extract, 3.0-6.0% of dimethyl sulfone, 0.5-1.0% of adenosine, 1, 3-propylene glycol, 1-5% of preservative, 0.5-1.2% of butanediol, 15.0-30.0% of butanediol, 3.0-6.0% of ginseng root extract, 0.6-3.0% of rhizoma anemarrhenae root extract, 0.1-1.0% of cacumen biotae extract, 3.0-6.0% of ginger root extract, 0.1-1.0% of angelica root extract, EDTA-2 NA: 0.1-0.2% and the balance of water.

Further, the raw material of the polygonum multiflorum extract is preferably from Xiang-De Qing city of polygonum multiflorum of China.

Further, the ginseng root extract raw material is preferably selected from Jilin Changbai mountain.

Further, the angelica root extract raw material is preferably selected from village-Gansu province Min county of Chinese angelica.

Further, the ginger root extract is preferably selected from the group consisting of Yuxiang-Laiwu of Zingiber officinale Rosc.

The traditional Chinese medicinal materials used in the traditional Chinese medicine extract disclosed by the invention are screened according to scientific basis, organically combined and combined according to the traditional Chinese medicine theory, rather than simply superposed according to the single traditional Chinese medicine efficacy, and the specific efficacy of the traditional Chinese medicinal materials is as follows:

the polygonum multiflorum contains various trace elements such as zinc, manganese, copper, iron, calcium, barium, nickel, strontium, boron and the like, has the effects of blackening hair and beautifying, and can directly permeate into hair follicles in the formula to increase the nutrition of the hair follicles.

The ginseng is sweet and slightly bitter in taste, warm and mild in nature, has the effects of tonifying blood and qi, and removing stagnation by qi depression, can open a channel to ensure that the nutrition supply of hair follicles is smoother and hair mother cells are activated when being used together with the angelica.

The angelica is rich in 106 volatile and water-soluble substances, wherein the volatile oil contains 41 components, 18 water-soluble substances mainly comprising polysaccharide, 19 amino acids (comprising 8 amino acids which can not be synthesized by human bodies) and 15 trace elements, has the effects of strengthening the muscles and the bodies, and is an ideal health-care product for enriching the blood, invigorating the circulation of blood and nourishing; chinese angelica is sweet and pungent in flavor, warm in nature and capable of enriching blood; promoting blood circulation; the composition has effects of replenishing blood, invigorating qi, and resolving stagnation, and can open channel to supply nutrition to hair follicle smoothly.

The ginger root is rich in multiple vitamins, and can stimulate scalp blood circulation, provide more nutrition for hair growth, and strengthen hair root.

The cacumen Platycladi and rhizoma anemarrhenae have effects of inhibiting androgen generation, and preventing and inhibiting seborrheic alopecia.

In addition, dimethyl sulfone has effects of promoting blood circulation and promoting hair. Keratin is the main protein forming the skin of the hide, the hair follicle of the fur skin, and the keratin has higher cysteine and disulfide bond content. The dimethyl sulfone can provide organic sulfur for keratin, promote hair growth, and has effects of strengthening and consolidating hair. Adenosine has effects of stimulating hair growth, coordinating with dimethyl sulfone, and promoting hair growth.

Through the technical scheme, compared with the prior art, the invention has the following beneficial effects:

the invention overcomes the problem of singleness of the form and the using method of the existing hair care product, adopts a plurality of traditional Chinese medicine extracts and adenosine and dimethyl sulfone, the traditional Chinese medicine extracts have the effect of emphasizing on the efficacy, the ginger root extract promotes the blood circulation, the ginseng root extract activates hair mother cells, the ginseng root extract, the polygonum multiflorum extract and the angelica root extract provide nutritional factors, the cacumen biotae extract and the rhizoma anemarrhenae root extract inhibit the secretion of male hormones and improve seborrheic alopecia, and the dimethyl sulfone and the adenosine provide organic sulfur and other nutrients for hair. According to the invention, the hair care essence product with an obvious effect is developed through scientific and reasonable raw material component matching, the multi-target effect is achieved, the residual quantity of active substances is increased, the effect is obvious after 2 months of use, the effect taking time is shortened, and the optimal effect is achieved.

Detailed Description

The technical solutions in the embodiments of the present invention are clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

Example 1:

the embodiment 1 of the invention discloses an anti-hair loss and hair-nourishing essence and a preparation method thereof, and the adopted technical scheme is as follows:

s1, weighing dimethyl sulfone as a raw material, adding water, placing in a stainless steel pot at room temperature, stirring for 1-2min, and uniformly dispersing until the mixture is transparent and has no particles; weighing adenosine, adding water, and uniformly dispersing by the same method until the adenosine is transparent and has no particles; weighing 1, 2-hexanediol and p-hydroxyacetophenone, heating to 55 ℃, stirring, keeping the temperature at 55 ℃, stirring for 30min, and dispersing until the mixture is transparent and has no particles; wherein the stirring speed of the dimethyl sulfone, the adenosine and the preservative is 50 r/min;

s2, weighing 1, 3-propylene glycol, butanediol, EDTA-2NA and water, placing in an emulsifying pot, heating while stirring, heating to 80 ℃, stirring at a speed of 50r/min for 60min, and naturally cooling to 40 ℃;

s3, weighing the polygonum multiflorum extract, the ginseng root extract, the cacumen biotae extract, the rhizoma anemarrhenae root extract, the ginger root extract and the angelica root extract, putting the polygonum multiflorum extract, the ginseng root extract, the cacumen biotae extract, the rhizoma anemarrhenae root extract, the rhizoma zingiberis recens root extract and the angelica root extract into an emulsifying pot, uniformly stirring the mixture in a sterile environment at the stirring speed of 500r/min, adding the dimethyl sulfone, the adenosine and the preservative processed in the step S1, stirring the mixture at the stirring speed of 500r/min until all the materials are uniformly dispersed and have no particles.

An anti-hair loss and hair-nourishing essence comprises the following components in percentage by weight: 1, 3-propylene glycol, 30% of butanediol, 0.1% of EDTA-2NA, 0.3% of 1, 2-hexanediol, 0.2% of p-hydroxyacetophenone, 3% of dimethyl sulfone, 0.5% of adenosine, 6% of a polygonum multiflorum extract, 0.1% of a angelica root extract, 0.1% of a cacumen biotae extract, 3% of a ginger root extract, 3% of a rhizoma anemarrhenae root extract, 3% of a ginseng root extract and the balance of deionized water.

Example 2:

the embodiment 2 of the invention discloses an anti-hair loss and hair-nourishing essence and a preparation method thereof, and the adopted technical scheme is as follows:

s1, weighing dimethyl sulfone as a raw material, adding water, placing in a stainless steel pot at room temperature, stirring for 1-2min, and uniformly dispersing until the mixture is transparent and has no particles; weighing adenosine, adding water, and uniformly dispersing by the same method until the adenosine is transparent and has no particles; weighing 1, 2-hexanediol and p-hydroxyacetophenone, heating to 57 ℃, stirring, keeping the temperature at 55 ℃, stirring for 30min, and dispersing until the mixture is transparent and has no particles; wherein the stirring speed of the dimethyl sulfone, the adenosine and the preservative is 100 r/min;

s2, weighing 1, 3-propylene glycol, butanediol, EDTA-2NA and water, placing in an emulsifying pot, heating while stirring, heating to 82 ℃, stirring at a speed of 100r/min for 40min, and naturally cooling to 43 ℃;

s3, weighing the polygonum multiflorum extract, the ginseng root extract, the cacumen biotae extract, the rhizoma anemarrhenae root extract, the ginger root extract and the angelica root extract, putting the materials into an emulsifying pot, uniformly stirring the materials in a sterile environment at the stirring speed of 1000r/min, adding the dimethyl sulfone, the adenosine and the preservative processed in the step S1, stirring the materials at the stirring speed of 1000r/min until the materials are uniformly dispersed and have no particles, filtering the materials after the materials are inspected to be qualified, discharging the materials, and filling the materials to obtain the finished product.

An anti-hair loss and hair-nourishing essence comprises the following components in percentage by weight: 5% of 1, 3-propylene glycol, 15% of butanediol, 0.2% of EDTA-2NA, 0.7% of 1, 2-hexanediol, 0.5% of p-hydroxyacetophenone, 6% of dimethyl sulfone, 0.7% of adenosine, 9% of a polygonum multiflorum extract, 0.7% of a angelica root extract, 0.7% of a cacumen biotae extract, 6% of a ginger root extract, 0.6% of a rhizoma anemarrhenae root extract, 5% of a ginseng root extract and the balance of deionized water.

Example 3:

the embodiment 3 of the invention discloses an anti-hair loss and hair-nourishing essence and a preparation method thereof, and the adopted technical scheme is as follows:

s1, weighing dimethyl sulfone as a raw material, adding water, placing in a stainless steel pot at room temperature, stirring for 1-2min, and uniformly dispersing until the mixture is transparent and has no particles; weighing adenosine, adding water, and uniformly dispersing by the same method until the adenosine is transparent and has no particles; weighing 1, 2-hexanediol and p-hydroxyacetophenone, heating to 60 ℃, stirring, keeping the temperature at 55 ℃, stirring for 30min, and dispersing until the mixture is transparent and has no particles; wherein the stirring speeds of the dimethyl sulfone, the adenosine and the preservative are all 200 r/min;

s2, weighing 1, 3-propylene glycol, butanediol, EDTA-2NA and water, placing in an emulsifying pot, heating while stirring, heating to 85 ℃, stirring at a speed of 200r/min for 30min, and naturally cooling to 45 ℃;

s3, weighing the polygonum multiflorum extract, the ginseng root extract, the cacumen biotae extract, the rhizoma anemarrhenae root extract, the ginger root extract and the angelica root extract, putting the materials into an emulsifying pot, uniformly stirring the materials in a sterile environment at the stirring speed of 1500r/min, adding the dimethyl sulfone, the adenosine and the preservative processed in the step S1, stirring the materials at the stirring speed of 1500r/min until the materials are uniformly dispersed and have no particles, filtering the materials after the materials are inspected to be qualified, discharging the materials, and filling the materials to obtain the finished product.

An anti-hair loss and hair-nourishing essence comprises the following components in percentage by weight: 3% of 1, 3-propylene glycol, 5% of butanediol, 0.1% of EDTA-2NA, 0.4% of 1, 2-hexanediol, 0.4% of p-hydroxyacetophenone, 5% of dimethyl sulfone, 1% of adenosine, 11% of a polygonum multiflorum extract, 1% of a angelica root extract, 1% of a cacumen biotae extract, 5% of a ginger root extract, 1% of a rhizoma anemarrhenae root extract, 6% of a ginseng root extract and the balance of deionized water.

Example 4:

to further illustrate the benefits of the present invention, the test subjects were tested according to the samples obtained in examples 1-3.

Selecting 30 specially trained volunteers, spraying the samples on scalp, massaging for 5-10 minutes, using for 2 times a day for two months continuously, observing the thick hair condition of half month, one month and two months before and after use, sequentially evaluating the effect of the samples in different time periods and scoring; the evaluation criteria (effective rate%) were: very good (80-100), good (60-80), general (40-60), poor (20-40), invalid (0-20), the highest score of each performance is 100, the lowest score is 0, the higher score represents the better performance of the product, the higher the comprehensive average value is, the better the effect is, the average result is recorded, and the experimental data are shown in table 1:

TABLE 1

From the test results in table 1, the comprehensive use evaluation of example 3 was most preferable, followed by example 2 and example 1. According to the data, the embodiment 3 has the best effect and the optimal raw material matching proportion.

The embodiments in the present description are described in a progressive manner, each embodiment focuses on differences from other embodiments, and the same and similar parts among the embodiments are referred to each other.

The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims

1. The preparation method of the anti-hair loss and hair-nourishing essence is characterized by comprising the following specific steps of:

2. The method for preparing the anti-hair-loss and hair-nourishing essence according to claim 1, wherein in the step S1, the stirring speeds of the dimethyl sulfone, the adenosine and the preservative are all 50-200 r/min.

3. The method for preparing the anti-hair-loss and hair-nourishing essence according to claim 1, wherein in the step S1, the temperature is raised to 55-60 ℃, and the mixture is stirred for 30 min.

4. The method for preparing the anti-hair-loss and hair-nourishing essence according to claim 1, wherein in the step S1, the preservative includes but is not limited to 1, 2-hexanediol and p-hydroxyacetophenone.

5. The method for preparing the anti-hair-loss and hair-nourishing essence according to claim 1, wherein in the step S2, the temperature is raised to 80-85 ℃ and the stirring speed is 50-200 r/min.

6. The method as claimed in claim 1, wherein the stirring speed in step S3 is 500-1500 r/min.

7. The anti-hair loss and hair-nourishing essence prepared according to the method of any one of claims 1 to 5, which is characterized by comprising the following components in percentage by weight: 6-11.0% of polygonum multiflorum extract, 3.0-6.0% of dimethyl sulfone, 0.5-1.0% of adenosine, 1, 3-propylene glycol, 1-5% of preservative, 0.5-1.2% of butanediol, 15.0-30.0% of butanediol, 3.0-6.0% of ginseng root extract, 0.6-3.0% of rhizoma anemarrhenae root extract, 0.1-1.0% of cacumen biotae extract, 3.0-6.0% of ginger root extract, 0.1-1.0% of angelica root extract, EDTA-2 NA: 0.1-0.2% and the balance of water.