CN107157827A - One-pack type hair-care hair dye and its preparation and application based on walnut green husk pigment - Google Patents
One-pack type hair-care hair dye and its preparation and application based on walnut green husk pigment Download PDFInfo
- Publication number
- CN107157827A CN107157827A CN201710336105.8A CN201710336105A CN107157827A CN 107157827 A CN107157827 A CN 107157827A CN 201710336105 A CN201710336105 A CN 201710336105A CN 107157827 A CN107157827 A CN 107157827A
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- China
- Prior art keywords
- hair
- green husk
- pack type
- polyquaternium
- walnut green
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000000118 hair dye Substances 0.000 title claims abstract description 39
- 235000009496 Juglans regia Nutrition 0.000 title claims abstract description 31
- 235000020234 walnut Nutrition 0.000 title claims abstract description 31
- 239000000049 pigment Substances 0.000 title claims abstract description 29
- 239000010903 husk Substances 0.000 title claims abstract description 28
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 240000007049 Juglans regia Species 0.000 title 1
- 241000758789 Juglans Species 0.000 claims abstract description 30
- 229920000289 Polyquaternium Polymers 0.000 claims abstract description 20
- 238000003756 stirring Methods 0.000 claims abstract description 16
- 229910052751 metal Inorganic materials 0.000 claims abstract description 10
- 239000002184 metal Substances 0.000 claims abstract description 10
- 150000003839 salts Chemical class 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 claims abstract description 8
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 8
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 8
- 229940101267 panthenol Drugs 0.000 claims abstract description 8
- 235000020957 pantothenol Nutrition 0.000 claims abstract description 8
- 239000011619 pantothenol Substances 0.000 claims abstract description 8
- 150000005846 sugar alcohols Polymers 0.000 claims abstract description 8
- 239000002562 thickening agent Substances 0.000 claims abstract description 8
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 7
- 239000003093 cationic surfactant Substances 0.000 claims abstract description 7
- 239000004519 grease Substances 0.000 claims abstract description 7
- 238000013019 agitation Methods 0.000 claims abstract description 5
- 239000002537 cosmetic Substances 0.000 claims abstract description 5
- 230000003020 moisturizing effect Effects 0.000 claims abstract description 5
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical group C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 12
- 239000000975 dye Substances 0.000 claims description 10
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 8
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 claims description 7
- 238000000034 method Methods 0.000 claims description 6
- 235000006708 antioxidants Nutrition 0.000 claims description 5
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims description 4
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims description 4
- 229930003427 Vitamin E Natural products 0.000 claims description 4
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims description 4
- 150000001768 cations Chemical class 0.000 claims description 4
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims description 4
- 235000011187 glycerol Nutrition 0.000 claims description 4
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims description 4
- 235000019165 vitamin E Nutrition 0.000 claims description 4
- 229940046009 vitamin E Drugs 0.000 claims description 4
- 239000011709 vitamin E Substances 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 3
- 229940037003 alum Drugs 0.000 claims description 3
- 229940082500 cetostearyl alcohol Drugs 0.000 claims description 3
- OULAJFUGPPVRBK-UHFFFAOYSA-N tetratriacontyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO OULAJFUGPPVRBK-UHFFFAOYSA-N 0.000 claims description 3
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims description 2
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 2
- 229920002907 Guar gum Polymers 0.000 claims description 2
- -1 INCROQUAT TMC-80 Chemical compound 0.000 claims description 2
- 229920000688 Poly[(2-ethyldimethylammonioethyl methacrylate ethyl sulfate)-co-(1-vinylpyrrolidone)] Polymers 0.000 claims description 2
- 235000021355 Stearic acid Nutrition 0.000 claims description 2
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 2
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 2
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 2
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 2
- 229960000541 cetyl alcohol Drugs 0.000 claims description 2
- WOWHHFRSBJGXCM-UHFFFAOYSA-M cetyltrimethylammonium chloride Chemical compound [Cl-].CCCCCCCCCCCCCCCC[N+](C)(C)C WOWHHFRSBJGXCM-UHFFFAOYSA-M 0.000 claims description 2
- XTVVROIMIGLXTD-UHFFFAOYSA-N copper(II) nitrate Chemical compound [Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O XTVVROIMIGLXTD-UHFFFAOYSA-N 0.000 claims description 2
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- NOPFSRXAKWQILS-UHFFFAOYSA-N docosan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCO NOPFSRXAKWQILS-UHFFFAOYSA-N 0.000 claims description 2
- 229960000735 docosanol Drugs 0.000 claims description 2
- DDXLVDQZPFLQMZ-UHFFFAOYSA-M dodecyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+](C)(C)C DDXLVDQZPFLQMZ-UHFFFAOYSA-M 0.000 claims description 2
- 239000000665 guar gum Substances 0.000 claims description 2
- 235000010417 guar gum Nutrition 0.000 claims description 2
- 229960002154 guar gum Drugs 0.000 claims description 2
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 2
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical group [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 claims description 2
- 229910021645 metal ion Inorganic materials 0.000 claims description 2
- GOQYKNQRPGWPLP-UHFFFAOYSA-N n-heptadecyl alcohol Natural products CCCCCCCCCCCCCCCCCO GOQYKNQRPGWPLP-UHFFFAOYSA-N 0.000 claims description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 2
- 239000003755 preservative agent Substances 0.000 claims description 2
- 230000002335 preservative effect Effects 0.000 claims description 2
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical class CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims description 2
- 229920005573 silicon-containing polymer Polymers 0.000 claims description 2
- 235000010413 sodium alginate Nutrition 0.000 claims description 2
- 239000000661 sodium alginate Substances 0.000 claims description 2
- 229940005550 sodium alginate Drugs 0.000 claims description 2
- 239000008117 stearic acid Substances 0.000 claims description 2
- 229960004274 stearic acid Drugs 0.000 claims description 2
- 229940012831 stearyl alcohol Drugs 0.000 claims description 2
- 229920001285 xanthan gum Polymers 0.000 claims description 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 claims 2
- LYRFLYHAGKPMFH-UHFFFAOYSA-N octadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(N)=O LYRFLYHAGKPMFH-UHFFFAOYSA-N 0.000 claims 2
- YFVKHKCZBSGZPE-UHFFFAOYSA-N 1-(1,3-benzodioxol-5-yl)-2-(propylamino)propan-1-one Chemical compound CCCNC(C)C(=O)C1=CC=C2OCOC2=C1 YFVKHKCZBSGZPE-UHFFFAOYSA-N 0.000 claims 1
- LZZYPRNAOMGNLH-UHFFFAOYSA-M Cetrimonium bromide Chemical compound [Br-].CCCCCCCCCCCCCCCC[N+](C)(C)C LZZYPRNAOMGNLH-UHFFFAOYSA-M 0.000 claims 1
- 150000003863 ammonium salts Chemical class 0.000 claims 1
- PLMFYJJFUUUCRZ-UHFFFAOYSA-M decyltrimethylammonium bromide Chemical compound [Br-].CCCCCCCCCC[N+](C)(C)C PLMFYJJFUUUCRZ-UHFFFAOYSA-M 0.000 claims 1
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims 1
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims 1
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims 1
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims 1
- 229940037312 stearamide Drugs 0.000 claims 1
- 239000004094 surface-active agent Substances 0.000 claims 1
- 238000004043 dyeing Methods 0.000 abstract description 25
- 239000000443 aerosol Substances 0.000 abstract description 8
- 238000007789 sealing Methods 0.000 abstract description 2
- 150000002632 lipids Chemical class 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 7
- 239000000203 mixture Substances 0.000 description 4
- 241001080929 Zeugopterus punctatus Species 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 230000037308 hair color Effects 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 239000001024 permanent hair color Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 210000004761 scalp Anatomy 0.000 description 3
- 230000003213 activating effect Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000005923 long-lasting effect Effects 0.000 description 2
- 230000000474 nursing effect Effects 0.000 description 2
- RZJRJXONCZWCBN-UHFFFAOYSA-N octadecane Chemical compound CCCCCCCCCCCCCCCCCC RZJRJXONCZWCBN-UHFFFAOYSA-N 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- GEYOCULIXLDCMW-UHFFFAOYSA-N 1,2-phenylenediamine Chemical compound NC1=CC=CC=C1N GEYOCULIXLDCMW-UHFFFAOYSA-N 0.000 description 1
- CBCKQZAAMUWICA-UHFFFAOYSA-N 1,4-phenylenediamine Chemical compound NC1=CC=C(N)C=C1 CBCKQZAAMUWICA-UHFFFAOYSA-N 0.000 description 1
- MPNXSZJPSVBLHP-UHFFFAOYSA-N 2-chloro-n-phenylpyridine-3-carboxamide Chemical compound ClC1=NC=CC=C1C(=O)NC1=CC=CC=C1 MPNXSZJPSVBLHP-UHFFFAOYSA-N 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 206010002198 Anaphylactic reaction Diseases 0.000 description 1
- 206010012434 Dermatitis allergic Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 125000005211 alkyl trimethyl ammonium group Chemical group 0.000 description 1
- 150000001412 amines Chemical group 0.000 description 1
- AJXBTRZGLDTSST-UHFFFAOYSA-N amino 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)ON AJXBTRZGLDTSST-UHFFFAOYSA-N 0.000 description 1
- 230000036783 anaphylactic response Effects 0.000 description 1
- 208000003455 anaphylaxis Diseases 0.000 description 1
- 201000008937 atopic dermatitis Diseases 0.000 description 1
- 208000010668 atopic eczema Diseases 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000007822 coupling agent Substances 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 230000008595 infiltration Effects 0.000 description 1
- 238000001764 infiltration Methods 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 206010023332 keratitis Diseases 0.000 description 1
- 208000032839 leukemia Diseases 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229940049292 n-(3-(dimethylamino)propyl)octadecanamide Drugs 0.000 description 1
- WWVIUVHFPSALDO-UHFFFAOYSA-N n-[3-(dimethylamino)propyl]octadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(=O)NCCCN(C)C WWVIUVHFPSALDO-UHFFFAOYSA-N 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 229940038384 octadecane Drugs 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 150000008442 polyphenolic compounds Chemical class 0.000 description 1
- 235000013824 polyphenols Nutrition 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 150000004053 quinones Chemical class 0.000 description 1
- 239000001026 semi permanent hair color Substances 0.000 description 1
- 239000002453 shampoo Substances 0.000 description 1
- 230000003637 steroidlike Effects 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- BKEOXUSOEGMVTL-UHFFFAOYSA-N trimethyl-$l^{3}-bromane Chemical compound CBr(C)C BKEOXUSOEGMVTL-UHFFFAOYSA-N 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/10—Preparations for permanently dyeing the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
- A61K2800/4324—Direct dyes in preparations for permanently dyeing the hair
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Inorganic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to special cosmetics field, for one-pack type hair-care hair dye and its preparation and application based on walnut green husk pigment, hair dye is made up of walnut green husk pigment, polyalcohol, panthenol, cationic surfactant, thickener, polyquaternium, grease, metal salt mordant, acidizer, antioxidant, deionized water, and preparation process is：(1) a certain amount of deionized water is weighed, 70~80 DEG C are heated to, lipid, polyalcohol, cationic surfactant is added, waits to be completely dissolved, 20~30min of mechanical agitation；(2) 40~55 DEG C are cooled the temperature to, antioxidant, panthenol, acidizer, polyquaternium is added, 20~30min is stirred；(3) add walnut green husk pigment to stir after 10~15min, add mordant and stir 5~10min；(4) mixing speed is improved, adds thickener, 20~30min is stirred after moisturizing and is produced；Preparation process of the present invention is simple, and easy to operate, gained aerosol type one-pack type hair dye stability is good, and normal temperature sealing can be preserved 3 years, and dyeing time is short, and hair dyeing temperature is low.
Description
Technical field
The invention belongs to special cosmetics technical field, more particularly to a kind of one-pack type hair care based on walnut green husk pigment
The method of preparation and use of hair dye.
Background technology
Hair dye refers to change hair color, the cosmetics with specific use.People use at most for a long time
Hair dye is permanent and semi-permanent hairdye.But as the oxidation dye of oxide hair dye main component, tradition is permanent
Hair dye is also named oxidative coloration of hair agent.The specific dyeing mechanism of this hair dye is made in the oxidation dye of low relative molecular mass
Mesosome and other compositions are penetrated into the middle of hair, and oxidation polymerization generation macromolecular dyestuff is carried out in hair and hair is latched in
It is interior.Oxide hair dye is nearly all by dyestuff intermediate, 3 kinds of reactive compounds institutes of colour coupler (being also coupling agent) and oxidant
Composition particularly p-phenylenediamine has found it is that anaphylaxis material can cause allergic dermatitis, is disabled by some European countries.Closely
For scientific research it is also shown that phenylenediamine and some of derivative have cumulative bad, rust denaturation, mutability, can trigger eye keratitis,
Ephritis and leukaemia etc..Permanent hairdye in the market is generally 2-part hair dyeing agents simultaneously, and it will be adjusted before having hair dyed
Match somebody with somebody, cause hair dye cumbersome.
There are some researches show, green peel of walnut contain abundant various trace elements, flavonoids, Polyphenols, quinones, polysaccharide,
Diarylheptanoids, and the composition such as steroidal, aliphatic acid, terpene, vitamin.Walnut husk (green peel of walnut) pigment
It is a kind of water colo(u)r, there is preferable dyeability to hair.The principal component of current walnut green husk pigment hair dyeing, it is existing
Problem is that dye uptake is low, and color is too shallow.The present invention forms coloured network and thing using the active component in plant and metallic salt, oozes
Its dye uptake can be improved by penetrating into hair epidermis or entering hair cortex, then increase infiltration by cationic surfactant.
It is unstable for the research generally existing dye cream of aerosol type one-pack type hair dye at present, the problems such as preparation process is easily affected by the external environment,
Therefore it is urgently to be resolved hurrily for the aerosol type one-pack type hair dye of preparation stability height, safety non-toxic.
The content of the invention
In order to overcome the shortcoming of above-mentioned prior art, it is an object of the invention to provide a kind of based on walnut green husk pigment
The method of preparation and use of one-pack type hair-care hair dye, it is by walnut green husk pigment and metal mordant dyeing and cationic surfactant
With reference to easy to use, nursing scalp and hair, dyeing more longlasting and hair dyeing hair color effect more preferably dyeing properties.
To achieve these goals, the technical solution adopted by the present invention is：
One-pack type hair-care hair dye based on walnut green husk pigment, is made up of the composition of following percentage by weight：
Walnut green husk pigment 1%~30%, polyalcohol 1%~30%, panthenol 0.01%~3%, cation surface activating
Agent 1%~10%, thickener 0.01%~1.5%, polyquaternium 0.01%~10%, grease 0.01%~15%, metal matchmaker
Stain 0.5%~5%, acidizer 0~5%, antioxidant 0.1~0.6%, deionized water surplus.
The cationic surfactant is OTAC, hexadecyltrimethylammonium chloride, 18
Alkyl trimethyl ammonium bromide, INCROQUAT TMC-80, DTAC, trimethyl bromine
Change the one or more in ammonium, stearamidopropyl dimethylamine.
The grease be saualane, dimethyl silicone polymer, GTCC, cetostearyl alcohol, stearyl alcohol, cetanol, stearic acid,
One or more in docosyl alcohol, the polyalcohol is the one or more in propane diols, butanediol, glycerine, described anti-oxidant
Agent is vitamin E, and the acidizer is citric acid, and the thickener is carboxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl first
One or more in base cellulose, cation guar gum, xanthans, sodium alginate.
The polyquaternium is polyquaternium -7, Polyquaternium-10, polyquaternium -33, polyquaternium -39, polyquaternary amine
One or more in salt -47, polyquaternium -11, polyquaternium -6, polyquaternium -28, Merquat 280.
The metal salt mordant is the salt of any metal ion for allowing in cosmetics to use.
The metal salt mordant is iron chloride, frerrous chloride, aluminium chloride, alum or copper nitrate.
Present invention also offers the preparation method of the one-pack type hair-care hair dye based on walnut green husk pigment, including such as
Lower step：
(1) a certain amount of deionized water is weighed, 70~80 DEG C are heated to, grease, polyalcohol, cation surface activating is added
Agent, waits to be completely dissolved, 20~30min of mechanical agitation；
(2) and then cool the temperature to 40~55 DEG C, sequentially add antioxidant, panthenol, acidizer, polyquaternium, stirring
20~30min；
(3) add walnut green husk pigment to stir after 10~15min, add metal salt mordant and stir 5~10min；
(4) mixing speed is improved, adds thickener, and system carries out stirring 20~30min after moisturizing, produces one-pack type
Hair dye.
Speed of agitator is 300~800 revs/min in the step (1) (2), the mixing speed in step (3) for 1000~
1500 revs/min.
Described preparation process is carried out under air-proof condition.
The application method of one-pack type hair-care hair dye of the present invention based on walnut green husk pigment, takes quantitative hair dye
Uniformly it is applied on hair, is then sealed with preservative film, has hair dyed 20~30min at a temperature of 35~40 DEG C.
Compared with prior art, preparation process of the present invention is simple, easy to operate, the aerosol type one-pack type hair dye stability prepared
Good, sealing can be preserved 3 years under normal temperature, while dyeing time is shorter, hair dyeing temperature is low.
Brief description of the drawings
Fig. 1 is the hair dye of the invention hair dyeing effect figure at a temperature of different hair dyeings.
Fig. 2 is the hair dye of the invention hair dyeing effect figure under different dyeing times.
Embodiment
The following detailed description of the specific implementation of the present invention, it is necessary to it is pointed out here that, implement to be only intended to this hair below
Bright further illustrates, it is impossible to be interpreted as the limitation to invention protection domain, and the art skilled person is according to above-mentioned hair
Some nonessential modifications and adaptations that bright content is made to the present invention, still fall within protection scope of the present invention.
First, preparation process
Embodiment 1
A certain amount of deionized water is weighed, 80 DEG C are heated to, 5% cetostearyl alcohol, 5% glycerine, 2.5% octadecane is added
Base trimethyl ammonium chloride, waits to be completely dissolved, mechanical agitation 30min, and rotating speed is 500 turns/min；Then 45 DEG C are cooled the temperature to, according to
After 0.1% vitamin E of secondary addition, 0.5% panthenol, 0.02% citric acid, 1.0% polyquaternium -7 stirring 25min, 20% is added
Walnut green husk pigment, stirs 5min；Add 2.5% frerrous chloride stirring 10min；Mixing speed is improved to 1200 turns/min,
30min is stirred after adding 0.3% hydroxyethyl cellulose, and system progress moisturizing, aerosol type one-pack type hair dye is produced.
Embodiment 2
A certain amount of deionized water is weighed, 80 DEG C are heated to, 6% saualane, 5% glycerine, 2.5% cetyl three is added
Ammonio methacrylate, waits to be completely dissolved, mechanical agitation 30min, and rotating speed is 300 turns/min；Then 45 DEG C are cooled the temperature to, is added successively
Enter after 0.1% vitamin E, 0.5% panthenol, 0.02% citric acid, 1.5% polyquaternium -7 stirring 30min, add 25% walnut
Rascal pigment, stirs 10min；Add 1.5% alum stirring 10min；Mixing speed is improved to 800 turns/min, 1.0% is added
30min is stirred after hydroxyethyl cellulose, and system progress moisturizing, aerosol type one-pack type hair dye is produced.
2nd, hair dyeing temperature comparative test
It is prepared as described above the aerosol type one-pack type hair dye of method preparation, reference picture 1, to white topknot at a temperature of temperature is 40 DEG C
Dyed, after 30min, hair dyeing effect has reached most preferably, therefore the hair dyeing temperature in practical operation typically from 35~40 DEG C
Degree.
3rd, dyeing time comparative test
It is prepared as described above the aerosol type one-pack type hair dye of method preparation, reference picture 2, to white topknot at a temperature of temperature is 40 DEG C
Dyed, when dyeing time reaches 30min, hair dyeing effect has reached most preferably, therefore according to different topknots in practical operation
Situation, the general dyeing time from 20~30min.
4th, checking test
The basic condition for contaminating originator is as shown in the table：
Test result is as shown in the table：
Per being cleaned with conventional shampoo within 2-3 days after subject's hair dyeing, start to decolourize after 4-5 times；Sun-proof number is more than 10 days；
Very well, correct leatherware has good logic to hair dyeing effect, and non-stimulated to scalp.It can be seen that, hair dye of the invention has
Easy to use, nursing scalp and hair, dye more longlasting and hair dyeing hair color effect more preferably dyeing properties.
To disclosed in this invention the description of embodiment be not intended to limit the scope of the present invention, but for describing
The present invention.Correspondingly, the scope of the present invention is not limited by embodiment of above, but is carried out by claim or its equivalent
Limit.
Claims (10)
1. the one-pack type hair-care hair dye based on walnut green husk pigment, it is characterised in that by following percentage by weight into packet
Into：
Walnut green husk pigment 1%~30%, polyalcohol 1%~30%, panthenol 0.01%~3%, cationic surfactant 1%
~10%, thickener 0.01%~1.5%, polyquaternium 0.01%~10%, grease 0.01%~15%, metal salt mordant
0.5%~5%, acidizer 0~5%, antioxidant 0.1~0.6%, deionized water surplus.
2. the one-pack type hair-care hair dye based on walnut green husk pigment according to claim 1, it is characterised in that the sun from
Sub- surfactant be OTAC, hexadecyltrimethylammonium chloride, Cetyltrimethylammonium bromide,
INCROQUAT TMC-80, DTAC, DTAB, stearamide propyl
One or more in dimethylamine.
3. the one-pack type hair-care hair dye based on walnut green husk pigment according to claim 1, it is characterised in that the grease
For one kind in saualane, dimethyl silicone polymer, GTCC, cetostearyl alcohol, stearyl alcohol, cetanol, stearic acid, docosyl alcohol or
A variety of, the polyalcohol is the one or more in propane diols, butanediol, glycerine, and the antioxidant is vitamin E, described
Acidizer is citric acid, and the thickener is carboxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl methyl cellulose, cation
One or more in guar gum, xanthans, sodium alginate.
4. the one-pack type hair-care hair dye based on walnut green husk pigment according to claim 1, it is characterised in that the poly- season
Ammonium salt be polyquaternium -7, Polyquaternium-10, polyquaternium -33, polyquaternium -39, polyquaternium -47, polyquaternium -11,
One or more in polyquaternium -6, polyquaternium -28, Merquat 280.
5. the one-pack type hair-care hair dye based on walnut green husk pigment according to claim 1, it is characterised in that the metal
Mordant is the salt of any metal ion for allowing in cosmetics to use.
6. the one-pack type hair-care hair dye based on walnut green husk pigment according to claim 1, it is characterised in that the metal
Mordant is iron chloride, frerrous chloride, aluminium chloride, alum or copper nitrate.
7. the preparation method of the one-pack type hair-care hair dye based on walnut green husk pigment described in claim 1, it is characterised in that bag
Include following steps：
(1) a certain amount of deionized water is weighed, 70~80 DEG C are heated to, grease, polyalcohol, cationic surfactant is added,
Wait to be completely dissolved, 20~30min of mechanical agitation；
(2) and then cool the temperature to 40~55 DEG C, sequentially add antioxidant, panthenol, acidizer, polyquaternium, stirring 20~
30min；
(3) add walnut green husk pigment to stir after 10~15min, add metal salt mordant and stir 5~10min；
(4) mixing speed is improved, adds thickener, and system carries out stirring 20~30min after moisturizing, produces one-pack type hair dyeing
Agent.
8. the preparation method of the one-pack type hair-care hair dye based on walnut green husk pigment according to claim 7, its feature exists
In, speed of agitator is 300~800 revs/min in the step (1) (2), the mixing speed in step (3) for 1000~1500 turns/
Point.
9. the preparation method of the one-pack type hair-care hair dye based on walnut green husk pigment according to claim 7, its feature exists
In described preparation process is carried out under air-proof condition.
10. the application method of the one-pack type hair-care hair dye based on walnut green husk pigment described in claim 1, it is characterised in that
Take quantitative hair dye to be uniformly applied on hair, then sealed with preservative film, at a temperature of 35~40 DEG C have hair dyed 20~
30min。
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| CN201710336105.8A CN107157827B (en) | 2017-05-12 | 2017-05-12 | Single-agent hair care hair dye based on walnut green husk pigment and preparation and use methods thereof |
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Cited By (7)
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| CN107789241A (en) * | 2017-09-22 | 2018-03-13 | 拉芳家化股份有限公司 | Hair film composition with hair care colour fixation and preparation method thereof |
| CN107938389A (en) * | 2017-12-28 | 2018-04-20 | 张永成 | A kind of soft solid agent of antibacterial dyed suitable for natural dye to textile |
| CN108143643A (en) * | 2018-01-10 | 2018-06-12 | 郑州拓洋生物工程有限公司 | Hair dye and preparation method and application |
| CN109172459A (en) * | 2018-11-01 | 2019-01-11 | 张有林 | A kind of green peel of walnut hair dye and preparation method thereof |
| CN109674680A (en) * | 2019-01-30 | 2019-04-26 | 苏州妮优雅化妆品有限公司 | A kind of hair coloring preparation composition |
| CN114796040A (en) * | 2022-03-04 | 2022-07-29 | 广东药科大学 | Black dragon clothes composite hair dye and preparation method thereof |
| CN115581648A (en) * | 2022-10-21 | 2023-01-10 | 浙江章华保健美发实业有限公司 | Dry fruit hair dye and using method thereof |
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| CN104800108A (en) * | 2014-11-20 | 2015-07-29 | 折改梅 | Preparation of constituents of cortex juglandis mandshuricae and manufacturing method of different-colored hair dyes |
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| US20070251024A1 (en) * | 2006-05-01 | 2007-11-01 | Erjeana Greaves | Composition for dyeing keratin fibers and a method of dyeing hair using same |
| CN103340770A (en) * | 2013-06-09 | 2013-10-09 | 吕梁学院 | Preparation method for hair dye based on walnut green husk pigment |
| CN104800108A (en) * | 2014-11-20 | 2015-07-29 | 折改梅 | Preparation of constituents of cortex juglandis mandshuricae and manufacturing method of different-colored hair dyes |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107789241A (en) * | 2017-09-22 | 2018-03-13 | 拉芳家化股份有限公司 | Hair film composition with hair care colour fixation and preparation method thereof |
| CN107938389A (en) * | 2017-12-28 | 2018-04-20 | 张永成 | A kind of soft solid agent of antibacterial dyed suitable for natural dye to textile |
| CN108143643A (en) * | 2018-01-10 | 2018-06-12 | 郑州拓洋生物工程有限公司 | Hair dye and preparation method and application |
| CN109172459A (en) * | 2018-11-01 | 2019-01-11 | 张有林 | A kind of green peel of walnut hair dye and preparation method thereof |
| CN109674680A (en) * | 2019-01-30 | 2019-04-26 | 苏州妮优雅化妆品有限公司 | A kind of hair coloring preparation composition |
| CN114796040A (en) * | 2022-03-04 | 2022-07-29 | 广东药科大学 | Black dragon clothes composite hair dye and preparation method thereof |
| CN115581648A (en) * | 2022-10-21 | 2023-01-10 | 浙江章华保健美发实业有限公司 | Dry fruit hair dye and using method thereof |
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