CN105193655A - Composite with efficacies of water locking and moisturizing, face mask and face mask preparation method - Google Patents
Composite with efficacies of water locking and moisturizing, face mask and face mask preparation method Download PDFInfo
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Abstract
The invention relates to the technical field of cosmetics, in particular to a composite with efficacies of water locking and moisturizing, a face mask and a face mask preparation method. The composite with the efficacies of water locking and moisturizing is prepared from, by weight, 4-8 parts of glycine betaine, 2-4 parts of trehalose, 1-2 parts of glycine soja seed extract, 5-10 parts of chamomilla recutita flower extract, 5-10 parts of carbamide, 0.5-1 part of allantoin, 0.1-0.5 part of hyaluronan, 0.2-0.5 part of sodium hyaluronate, 0.2-0.5 part of hydrolyzed sclerotium gum, 0.2-0.5 part of pullulan, 0.1-0.5 part of carbomer, 20-30 parts of glycerin and 40-70 parts of water. The composite with the efficacies of water locking and moisturizing is specially designed for water locking and moisturizing of skin and has the advantages of safety, effectiveness, easiness in absorption and applicability to addition to general cosmetics.
Description
Technical field
The present invention relates to cosmetic technical field, particularly relate to a kind of containing this lock water moisture-keeping efficacy compositions, mask and preparation method thereof.
Background technology
As everyone knows, skin hydropenia is almost the root of all skin problems, and skin hydropenia can reduce metabolism and the cell viability of Skin Cell, thus causes skin to occur microgroove, wrinkle, obscure, the problem such as mottle, desquamation; Skin hydropenia can allow skin be in a kind of sub-health state always, thus causes skin-tolerant to be deteriorated, and easily causes the problem such as sensitivity, red blood streak by environmental stimuli; Skin hydropenia easily causes skin beauty water oil unbalance, and skin can cause skin fuel-displaced too much because of hydropenia, forms skin quality dry in outer oil, thus easily forms small pox skin, bring very large puzzlement to the life of the personage that likes to be beautiful.In a word, skin hydropenia can bring a series of problem to skin, and the moisturizing of such skin, moisturizing and lock water just seem particularly important.
Replenishing water and preserving moisture product is a lot of on the market at present, but most of replenishing water and preserving moisture product can only bring moment moisturizing by some replenishing water and preserving moisture agent, do not consider deisgn product from skin texture and moisturizing, lock water, the triple solid space of moisturizing, such product replenishing water and preserving moisture effect is just difficult to accomplish lastingly, to be also difficult to the series of problems accomplishing to prevent skin hydropenia to bring.Replenishing water and preserving moisture is carried out exactly in addition on the market by wetting agent, the effect of lock water is reached by the closure of oils and fats, such product is all generally cream frost, emulsion quality, and inside product, need more emulsifying agent to carry out stable profit system, substantially can not apply inside water-based product, moreover emulsifying agent generally all can bring the zest of skin, some dry especially and responsive skin just can not use.
How in conjunction with skin texture, skin moisturizing, lock water, moisturizing mechanism, design and develop out gentleness, safety, effectively and can lasting moisturizing, lock water, moisturizing skin care item, be a technical barrier of current skin protection research field existence.
Summary of the invention
Object of the present invention, exactly in order to solve and prevent skin hydropenia to provide a kind of lock water moisture-keeping efficacy compositions.
Another object of the present invention also there are provided a kind of mask containing above-mentioned lock water moisture-keeping efficacy compositions and preparation method thereof.
The common manifestation that the present invention causes according to skin hydropenia, in conjunction with being closely connected of skin layers structure and water, by betanin, trehalose, Wild soybean seed extract, Flos Chrysanthemi extract (Matricaria recutita), carbamide, allantoin, hyaluronic acid, hyaluronate sodium, hydrolysis Scleroglucan, sprout short stalk enzyme polysaccharide, carbomer, glycerol, 13 kinds of different efficacies active matters such as water are combined, form compound recipe lock water moisture-keeping efficacy compositions, and it can be used as primary efficacy additive, make the salubrious mask easily absorbed, make it have moment moisturizing, lock water, lasting moisturizing, to releive the effects such as skin, thus effectively prevent and alleviate the skin problem that skin hydropenia is brought, new solution is brought to the skin replenishing water and preserving moisture of the personage that likes to be beautiful.
The object of the present invention is achieved like this:
One has lock water moisture-keeping efficacy compositions, is made up of the Effect raw material of following weight portion:
Betanin 4-8 part, trehalose 2-4 part, Wild soybean seed extract 1-2 part, Flos Chrysanthemi extract 5-10, carbamide 5-10 part, allantoin 0.5-1 part, hyaluronic acid 0.1-0.5 part, hyaluronate sodium 0.2-0.5 part, hydrolysis Scleroglucan 0.2-0.5 part, sprout short stalk enzyme polysaccharide 0.2-0.5 part, carbomer 0.1-0.5 part, glycerol 20-30 part, water 40-70 part.
Said components, dewaters as outside company's preparation, is marketable material.
Described lock water moisture-keeping efficacy compositions, described hyaluronate sodium comprises the hyaluronate sodium of three kinds of molecular weight, its molecule strength be respectively 20-40 ten thousand, 500,000,130-180 ten thousand, and the preferred 1:1:2 of its proportioning.
Described lock water moisture-keeping efficacy compositions, described betanin and the preferred 2:1 of the proportioning of trehalose, in order to reach optimum moistening effect, wherein betanin preferably 6%, trehalose preferably 3%.
Described lock water moisture-keeping efficacy compositions, described hydrolysis Scleroglucan with sprout the preferred 1:1 of proportioning of short stalk enzyme polysaccharide, in order to reach optimum moisture retention water film-strength, be wherein hydrolyzed Scleroglucan and the short stalk enzyme polysaccharide preferably 0.4% that sprouts.
The preparation method of described lock water moisture-keeping efficacy compositions, comprises the following steps:
In advance by hyaluronate sodium, be hydrolyzed Scleroglucan, sprout short stalk enzyme polysaccharide and glycerol dispersion moistening complete, water is added again in preformulation pot, by carbomer moistening 5 minutes in water, open stirring 35 revs/min, add premix material, hyaluronic acid successively, after being heated to 40-45 DEG C, then add betanin, trehalose, allantoin, carbamide, Flos Chrysanthemi extract, Wild soybean seed extract successively, insulated and stirred 30min, dissolves completely stand-by.
On the other hand, present invention also offers a kind of facial film with lock water moisture-keeping efficacy, comprise A phase and B phase, described A phase is made up of the raw material of following weight percentage ratio:
A phase:
Described B phase is made up of the raw material of following weight percentage ratio:
B phase:
Present invention also offers a kind of preparation method of above-mentioned mask, comprise the following steps:
(1) raw material is prepared according to following component and weight wt% thereof: deionized water 60.0-80.0wt%, butanediol 3.0-5.0wt%, glycyrrhizic acid dipotassium 0.2-0.5wt%, lock water moisture-keeping efficacy compositions 20.0-30.0wt%, phenoxyethanol 0.1-0.3wt%, 1,2-hexanediol 0.2-0.5wt%, orange blossom water 0.1-0.5wt%;
(2) use butanediol dispersion moistening xanthan gum to evenly for subsequent use in advance, deionized water is joined in main preparation pot, open and stir (35 revs/min) and open heating, drop into xanthan gum premix material, drop into glycyrrhizic acid dipotassium again, after being heated to 80-85 DEG C, insulated and stirred 30 minutes, opens cooling water temperature subsequently;
(3) after being cooled to 45 DEG C, add lock water moisture-keeping efficacy compositions, phenoxyethanol, ethylene glycol, orange blossom water successively, open homogenizing (1000-1500 rev/min), homogenizing 5 minutes is to evenly, stir (35 revs/min) 20 minutes, detect the pH value of material body after mix homogeneously, pH value, within the scope of 5.0.0-7.0, crosses 200 eye mesh screen dischargings.
Have a facial film for lock water moisture-keeping efficacy, described mask is prepared by said method.
Mask recommendation method of the present invention is: after clean of every day, by facial film coating with on face skin, after 15-20 minute, after opening facial mask cloth, is massaged into absorption completely.The gentle water profit of facial film of the present invention easily absorbs, and uses 2-4 time weekly.
Lock water moisture-keeping efficacy compositions selected by the present invention, there is triple three-dimensional hydrodynamic force system, first is heavily moment moisturizing dynamical system, mainly contain betanin, trehalose, carbamide, glycerol forms, they all belong to micromolecule wetting agent, be easy to be absorbed by hydropenia skin, and their water absorption are all very strong, be easy to accomplish instantaneously to skin moisturizing, wherein betanin another name trimethyl glycine, hygroscopicity is strong and good with skin-friendliness, trehalose, plant origin, there is the effect of stabilizing cell membrane and protein structure and resist drying, carbamide and glycerol are all skin epidermis nature moisturizing factor active component, there is good moisturizing effects instantaneously.
Second is heavily lock hydrodynamic force system, mainly contain hyaluronic acid, the hyaluronate sodium of three kinds of molecular weight, carbomer, hyaluronate sodium is as star's moisturizing active component, and its water suction lock outlet capacity is 500 times-1000 times of own wt, lock waterwall can be formed when acting on skin, reduce moisture loss.Hyaluronic acid is micromolecule moisturizing active matter, it is the precursor of macromole hyaluronate sodium, because molecular weight is very little, slowly can be absorbed by keratodermatitis, be embedded into skin epidermis, carbomer is high molecular polymer, there are powerful suspension and the attribute of stabilising system, when it together with multiple hyaluronate sodium hydration time, its energy and hyaluronate sodium form a space structure, waterishlogged hyaluronate sodium and hyaluronic acid is filled with inside this space structure, it is a lock water treasure-house, when acting on skin, they endurable formation lock waterwall.
The triple be moisturizing dynamical system; mainly contain hydrolysis Scleroglucan, the short stalk enzyme polysaccharide that sprouts composition; they are the fabulous macromolecule wetting agent of film property; particularly sprout short stalk enzyme polysaccharide, and common name is pulullan polysaccharide, can form the ventilative protecting film of one deck at skin surface; when it uses together with hydrolysis Scleroglucan time; staggered and the moisture retention ventilated membrane closely of one deck can be formed, moisture can be stoped to walk from skin volatilization, the intrusion of alien bacteria, dust can be intercepted again.
Lock water moisture-keeping efficacy compositions selected by the present invention, except having triple three-dimensional hydrodynamic force system, with the addition of Wild soybean seed extract, Flos Chrysanthemi extract, allantoin especially.Add allantoin in the present composition, mainly by allantoin energy horny layer softening albumen, contribute to the impact that alleviation skin barrier absorbs active matter; Add anthemidis flos water in the present composition, mainly, antiallergic calm to the Shu Min of skin by Flos Matricariae chamomillae is used for improving skin to the toleration of external active substance, contributes to the absorption improving active matter; The present composition adds Wild soybean seed extract, its chief active thing is the enzymolysis lecithin in Wild soybean source, there is the fabulous compatibility in itself and skin and epidermis cell gap, the passage of a Transdermal absorption can be formed at intercellular substance, make moisturizing small molecule active thing of the present invention can be absorbed by the skin the effect reaching multilamellar moisturizing endlessly, they and triple three-dimensional hydrodynamic force system complement each other simultaneously, jointly reach moment moisturizing, lock the effect of water, long-acting moisturizing lastingly.
Lock water moisture-keeping efficacy composition material in the present invention is conveniently easy to get, and facial mask liquid preparation method of the present invention is easy, and safe and effective, has and well experiences sensation and result of use, be with a wide range of applications and market prospect.
Accompanying drawing explanation
Fig. 1 is different embodiment skin moisture content test result design sketchs;
Fig. 2 is the design sketch trying out test result for a long time.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1-4 raw material and proportioning (mass percent), in table 1:
Table 1
Raw material sources in above-described embodiment are in table 2:
Table 2
Embodiment 1-4 is prepared by following steps:
(1) use butanediol dispersion moistening xanthan gum to evenly for subsequent use in advance, deionized water is joined in main preparation pot, open and stir (35 revs/min) and open heating, drop into xanthan gum premix material, drop into glycyrrhizic acid dipotassium again, after being heated to 80-85 DEG C, insulated and stirred 30 minutes, opens cooling water temperature subsequently;
(2) after being cooled to 45 DEG C, add lock water moisture-keeping efficacy compositions, phenoxyethanol, ethylene glycol, orange blossom water successively, open homogenizing (1000-1500 rev/min), homogenizing 5 minutes is to evenly, stir (35 revs/min) 20 minutes, detect the pH value of material body after mix homogeneously, pH value, within the scope of 5.0.0-7.0, crosses 200 eye mesh screen dischargings.
Carry out high/low temperature accelerated test (at-15 DEG C, under 5 DEG C and 49 DEG C and cold cycling, testing 30 days respectively, 60 days and 90 days) to embodiment 1 to 4, test result is in table 3:
Table 3
Result shows: facial mask liquid of the present invention, when higher than having excellent stability when GB, can meet the demand of listing.
Efficacy experiments of the present invention
One, replenishing water and preserving moisture effect
1. moisture of skin test
1) experimental apparatus: select German CK company Multi-functional skin tester MPA9 and moisture content test probe CorneometerCM825;
2) experimental principle: what moisture measurement adopted is universally acknowledged CORNEOMETER-capacitance method, the test philosophy of moisture content is quite large based on dielectric constant (<7) change of water (81) and other material, according to the difference of water content, the measuring capacitor of suitable shape can change along with the change of the capacitance of skin, and the capacitance of skin is in the scope measured, the water content of skin so just can be measured.Its result is represented by the humidity measurements (MoistureMeasurementValue, MMV) of setting.MMV is the numerical value of 0 ~ 150.The measuring method of capacitance is more superior than additive method, because tested skin and test probe do not have factitious contact, does not almost have electric current by tested skin, and therefore in fact test result is not subject to the impact of polarity effect and ionic conductivity.There is no inertia in moisture equilibrium establishment process in instrument probe and skin, can Quick Measurement be realized, also eliminate the impact of viable skin on measurement result so simultaneously.
3) test condition: the measuring process of skin hydration rate MMV is larger by ambient temperature, humidity effect.Measure under selecting 20 DEG C and 50% relative humidity conditions.
4) test method: tested object is 10 20-55 year female volunteers, and testing first three sky need not any skin care item.An embodiment of the present invention 1-4 and commercially available replenishing water and preserving moisture mask product is selected in test.Before test, experimenter needs unification clean water both hands inner forearm.Measurement markers is carried out at experimenter's both hands inner forearm after cleaning.The each labelling of right-hand man's forearm 5 pilot regions in this experiment, the corresponding commercially available prod of numbering CS01-CS05, CS01-04 corresponding embodiment 1-4, CS05.A kind of tested material is smeared in each region, interregional every 1cm.Often locating pilot region is 5 × 5cm2, and test specimen amount is 0.2g.After experimenter sits quietly 30 minutes in constant environment, use Corneometer to carry out the measurement of recipient site blank value, each region, according to a definite sequence fixation measuring 5 points, draws its meansigma methods.Then be responsible for smearing sample by special messenger, and start timing.The change of MMV value is measured according to the time period of 30min, 1h, 4h, 24h, 48h.The meansigma methods at every turn detected is deducted the change that blank value is this period MMV value, namely draws the rate of increase of MMV value at removing blank value.
Skin moisture content Growth Rate Calculation formula is as follows:
Skin moisture content rate of increase %=(MMVt-MMV0)/MMV0 × 100%
In formula: MMV0---smear front skin MMV
MMVt---smear rear t period skin MMV
Test result is as shown in table 4 and Fig. 2:
Table 4
| Time/h | 0.5h | 1h | 4h | 24h | 48h |
| Embodiment 1 | 75.2 | 80.5 | 55.6 | 38.6 | 35.8 |
| Embodiment 2 | 78.3 | 81.2 | 58.1 | 40.5 | 39.6 |
| Embodiment 3 | 79.8 | 81.6 | 59.6 | 41.8 | 45.6 |
| Embodiment 4 | 80.5 | 82.6 | 60.5 | 42.3 | 40.8 |
| Commercial samples | 60.2 | 55.3 | 45.6 | 18.1 | 9.2 |
Test result shows, the embodiment of the present invention has good moment moisturizing effect and lasting moistening effect, and particularly lasting moistening effect is better than commercially available prod.
2, product beta test measure of merit
Experimental technique
Embodiment 1-4 and commercially available product for resolving poxes are tried out for a long time.Test number is 50 people, is divided into 5 groups, often organizes 10 people, respectively trial edition inventive embodiments 1-4 and commercially available prod, and test period is 28 days, uses test products after clean of tester, within every two days, uses once.Tester carried out self assessment skin replenishing water and preserving moisture effect in the 0th day, the 7th day, the 14th day, the 28th day, resilient flexible effect, glossy minimizing effect, the colour of skin highlight effect and microgroove reduces the use senses such as effect and is subject to.Test result is as shown in table 5 and Fig. 2:
Table 5
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Commercial samples | |
| Replenishing water and preserving moisture effect | 8.8 | 8.9 | 9.0 | 9.0 | 7.8 |
| Resilient flexible effect | 8.3 | 8.6 | 8.7 | 8.8 | 7.0 |
| Glossy minimizing effect | 8.1 | 8.3 | 8.6 | 8.6 | 3.6 |
| The colour of skin highlights effect | 8.2 | 8.3 | 8.3 | 8.4 | 7.5 |
| Microgroove reduces effect | 8.2 | 8.5 | 8.4 | 8.6 | 5.0 |
test result shows: the present invention is all better than commercially available product for resolving poxes, long-term a series of skin problems that can effectively prevent or alleviate skin hydropenia to bring on probation simultaneously containing the facial film locking the combination of water moisture-keeping efficacy in replenishing water and preserving moisture, soft skin, the effect controlled in water oil balance, bright color and minimizing microgroove etc.
Above embodiment is used for illustrative purposes only, but not limitation of the present invention, person skilled in the relevant technique, without departing from the spirit and scope of the present invention, various conversion or modification can also be made, therefore all equivalent technical schemes also should belong to category of the present invention, should be limited by each claim.
Claims (8)
1. have a compositions for lock water moisture-keeping efficacy, it is characterized in that, described compositions is made up of the Effect raw material of following weight portion:
Betanin 4-8 part, trehalose 2-4 part, Wild soybean seed extract 1-2 part, Flos Chrysanthemi extract 5-10, carbamide 5-10 part, allantoin 0.5-1 part, hyaluronic acid 0.1-0.5 part, hyaluronate sodium 0.2-0.5 part, hydrolysis Scleroglucan 0.2-0.5 part, sprout short stalk enzyme polysaccharide 0.2-0.5 part, carbomer 0.1-0.5 part, glycerol 20-30 part, water 40-70 part.
2. lock water moisture-keeping efficacy compositions as claimed in claim 1, it is characterized in that, described hyaluronate sodium comprises the hyaluronate sodium of three kinds of molecular weight, its molecule strength be respectively 20-40 ten thousand, 500,000,130-180 ten thousand, and its proportioning is 1:1:2.
3. lock water moisture-keeping efficacy compositions as claimed in claim 1, it is characterized in that, described betanin and the weight proportion of trehalose are the lock water moisture-keeping efficacy compositions described in this right of 2:1., it is characterized in that, described beet alkali content is 6 parts of gross weight, and content of trehalose is 3 parts of gross weight.
4. lock water moisture-keeping efficacy compositions as claimed in claim 1, it is characterized in that, described hydrolysis Scleroglucan is 1:1 with the weight proportion of the short stalk enzyme polysaccharide that sprouts.
5. lock water moisture-keeping efficacy compositions as claimed in claim 4, it is characterized in that, described hydrolysis Scleroglucan is 0.4 part with the short stalk enzyme polysaccharide that sprouts.
6. the preparation method of the lock water moisture-keeping efficacy compositions as described in claim 1-5 any one, is characterized in that: comprise the following steps:
In advance by hyaluronate sodium, be hydrolyzed Scleroglucan, sprout short stalk enzyme polysaccharide and glycerol dispersion moistening complete, water is added again in preformulation pot, by carbomer moistening 5 minutes in water, open stirring 35 revs/min, add premix material, hyaluronic acid successively, after being heated to 40-45 DEG C, add betanin, trehalose, allantoin, carbamide, Flos Chrysanthemi extract more successively, Wild soybean seed extract, insulated and stirred 30min, dissolves completely stand-by.
7. have a mask for lock water moisture-keeping efficacy, it is characterized in that, described mask comprises A phase and B phase, and described A phase is made up of the raw material of following weight percentage ratio:
A phase:
Deionized water 60.0-80.0wt%
Butanediol 3.0-5.0wt%
Xanthan gum 0.05-0.1wt%
Glycyrrhizic acid dipotassium 0.2-0.5wt%
Described B phase is made up of the raw material of following weight percentage ratio:
B phase:
Lock water moisture-keeping efficacy compositions 20.0-30.0wt%
Phenoxyethanol 0.1-0.3wt%
1,2-hexanediol 0.2-0.5wt%
Orange blossom water 0.1-0.5wt%.
8. the preparation method of mask as claimed in claim 7, is characterized in that, comprise the following steps:
(1) raw material is prepared according to following component and weight wt% thereof: deionized water 60.0-80.0wt%, butanediol 3.0-5.0wt%, glycyrrhizic acid dipotassium 0.2-0.5wt%, lock water moisture-keeping efficacy compositions 20.0-30.0wt%, phenoxyethanol 0.1-0.3wt%, 1,2-hexanediol 0.2-0.5wt%, orange blossom water 0.1-0.5wt%;
(2) use butanediol dispersion moistening xanthan gum to evenly for subsequent use in advance, deionized water is joined in main preparation pot, open and stir, 35 revs/min and open heating, drop into xanthan gum premix material, then drop into glycyrrhizic acid dipotassium, after being heated to 80-85 DEG C, insulated and stirred 30 minutes, opens cooling water temperature subsequently;
(3) after being cooled to 45 DEG C, add lock water moisture-keeping efficacy compositions, phenoxyethanol, ethylene glycol, orange blossom water successively, open homogenizing, 1000-1500 rev/min, homogenizing stirs 35 revs/min to evenly in 5 minutes, 20 minutes, detect the pH value of material body after mix homogeneously, pH value, within the scope of 5.0.0-7.0, crosses 200 eye mesh screen dischargings.
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