CN101416930A - Face mask containing pullulan - Google Patents
Face mask containing pullulan Download PDFInfo
- Publication number
- CN101416930A CN101416930A CNA2008101872810A CN200810187281A CN101416930A CN 101416930 A CN101416930 A CN 101416930A CN A2008101872810 A CNA2008101872810 A CN A2008101872810A CN 200810187281 A CN200810187281 A CN 200810187281A CN 101416930 A CN101416930 A CN 101416930A
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- pulullan polysaccharide
- facial film
- skin
- polyglutamic acid
- facial
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Abstract
The invention provides a mask containing Pullulan polysaccharide, and a preparation method thereof. The mask consists of efficient water-retention oxygen-resistant components such as the Pullulan polysaccharide, polyglutamic acid and the like, and contains nutrients such as epidermal growth factors, vitamin C, tea polyphenol and the like. The mask is characterized by strong adhesion, strong oxygen resistance, effective water retention, easy removal and the like. When a covering membrane is formed on the skin, the skin can be tightened and wrinkles stretch temporarily, thus being beneficial to the absorption of nutrients such as the epidermal growth factors, the vitamin C and the like.
Description
Technical field
The invention belongs to cosmetic field, relate to a kind of facial film that contains pulullan polysaccharide.
Background technology
Facial film is a kind of cosmetics and skincare product that applies on the face, through 20～30 minutes, just can form the tight thin film on the face of one deck, so be called facial film after applying.The principle of facial film is to utilize the dressing of a thick layer of not same-action and composition to apply in face, and the obstruct skin contacts with air.When this one deck dressing is attached on the skin tightly, can the skin temperature be risen; After the skin temperature rises, just can blood circulation promoting, the nutrient that infiltrates skin is spread apart in that iuntercellular is darker widelyr.Those can't moisture evaporated then can be deposited in epidermal area skin surface, and the moisture of epidermal area is full, and it is will smoother tight that skin seems, it is light that microgroove also can become; In addition, temperature and warm meeting make cutin softening, the pore expansion; Pore one expansion, the sweat mixed with dirt that is deposited in the inside just can be seized the opportunity eliminating, this also just why facial film possess the reason of thorough cleaning skin function
The present invention utilizes pulullan polysaccharide resistance oxygen good, soluble in water, and easy film forming and the good characteristics of polyglutamic acid water conservation are as the main composition of facial film film former.This facial film can make skin-tightening, and wrinkle of skin is temporarily unfolded, and helps the absorption of nutritional labelings such as epidermal growth factor, vitamin C.Clean skin, pore refining, wrinkle-chasing arranged, brighten, effect such as skin care.It is single that this facial film has solved present most of facial film nutritional labeling, and the shortcoming that nutrition can not effectively absorb has really solved the wrinkle removal of facial film, crease-resistant and to speckle dispelling, eliminates skin sore, the unconspicuous shortcoming of blackhead effect.But its effective synergism skin that comprises multiple nutritional components and pulullan polysaccharide and polyglutamic acid obtains prescribing adequate nutrition, and skin is had health care and regeneration function.
Summary of the invention
The purpose of this invention is to provide a kind of can efficient clean skin, pore refining, wrinkle-chasing, brighten, the facial film manufacturing technology of effect such as skin care, the technological core of this facial film is to use pulullan polysaccharide and polyglutamic acid as the facial film film former.
The present invention makees facial film, and it is composed as follows:
Fruit acid 1%～5%, g/mL
Sorbitol 1%～5%, g/mL
Tea polyphenols 0.002%～0.015%, g/mL
Polyvinyl alcohol 5%～15%, g/mL
Carboxymethyl cellulose 3%～6%, g/mL
Glycerol 2%～6%, g/mL
Vitamin C 0.05%～0.5%, g/mL
Epidermal growth factor 0.0000001%～0.0005%, g/mL
Pulullan polysaccharide 2%～10%, g/mL
Polyglutamic acid 2%～10%, g/mL
Sodium benzoate 0.1%～0.5%, g/mL
Essence 0.01%～0.05%, g/mL
Other fruit juice 10%～20%, g/mL
Sterilized water adds to 100%, g/mL
The mean molecule quantity of the pulullan polysaccharide that the present invention is used is 5～2,200,000 dalton, and the mean molecule quantity of polyglutamic acid is 10～1,000,000 dalton.
The preparation method of facial film of the present invention, form by following steps:
(1) pulullan polysaccharide powder and polyglutamic acid powder is soluble in water, abundant mixing;
(2) polyvinyl alcohol, sorbitol are added the water stirring and evenly mixing, add sodium benzoate, be heated to 60 ℃;
(3) with carboxymethyl cellulose and other fruit juice constituents mix homogeneously and add essence;
(4) with above-mentioned various composition mix homogeneously, other compositions of polishing.
Facial film of the present invention its to have adhesion strength strong, characteristics such as hinder oxygen, highly effective water-keeping by force and easily remove when forming coverlay on skin, can make skin-tightening, wrinkle of skin is temporarily unfolded.
The specific embodiment
Embodiment 1
(1) gets pulullan polysaccharide powder 3kg and be dissolved in distilled water, get polyglutamic acid 2kg and be dissolved in distilled water, mix homogeneously;
(2) get 10kg polyvinyl alcohol and 3kg sorbitol, add water and stir, add the 0.2kg sodium benzoate, be heated to 60 ℃;
(3) with carboxymethyl cellulose 5kg and other fruit juice constituents 15kg mix homogeneously and add essence 0.02kg;
(4) with above-mentioned each component mix homogeneously, add fruit acid 3kg, tea polyphenols 0.005kg, glycerol 5kg, Vc0.2kg, epidermal growth factor 0.00002kg adds water to 100kg.
Embodiment 2
(1) gets pulullan polysaccharide powder 5kg and be dissolved in distilled water, get polyglutamic acid 3kg and be dissolved in distilled water, mix homogeneously;
(2) get 8kg polyvinyl alcohol and 2kg sorbitol, add water and stir, add the 0.2kg sodium benzoate, be heated to 60 ℃;
(3) with carboxymethyl cellulose 6kg and other fruit juice constituents 14kg mix homogeneously and add essence 0.03kg;
(4) with above-mentioned each component mix homogeneously, add fruit acid 5kg, tea polyphenols 0.005kg, glycerol 5kg, Vc0.2kg, epidermal growth factor 0.00002kg adds water to 100kg.
Embodiment 3
(1) gets pulullan polysaccharide powder 4kg and be dissolved in distilled water, get polyglutamic acid 3kg and be dissolved in distilled water, mix homogeneously;
(2) get 13kg polyvinyl alcohol and 3kg sorbitol, add water and stir, add the 0.2kg sodium benzoate, be heated to 60 ℃;
(3) with carboxymethyl cellulose 5kg and other fruit juice constituents 15kg mix homogeneously and add essence 0.02kg;
(4) with above-mentioned each component mix homogeneously, add fruit acid 3kg, tea polyphenols 0.005kg, glycerol 5kg, Vc0.2kg, epidermal growth factor 0.00002kg adds water to 100kg.
Experimental study: the result of use of investigating facial film
Select female volunteers 80 people.
Symptom before using: facial heavy wool, corse sweat pore has blackhead that wrinkle, speckle are arranged, and the skin obfuscation is matt.
Using method: above-mentioned volunteer is divided into two groups at random: a group is used this facial film, and the b group is used common facial film.Clean face, facial film is spread on the face, take facial film off after 20～40 minutes, clean.Once a day, use a week.
Criterion of therapeutical effect:
(1) effective: skin exquisiteness, flexible, facial pore diminishes, no blackhead, wrinkle and speckle reduce.
(2) invalid: blackhead tails off to some extent, and pore diminishes, and the skin obfuscation is matt, and wrinkle and speckle are not seen obvious minimizing.
Result's (seeing Table 1)
The comparative study of table 1 facial film result of use
By the result as seen, because this facial film highly effective water-keeping and have strong resistance oxygen, the facial film nutritional labeling can at utmost be absorbed by skin, can improve skin in a short time, and more common facial film has better result of use.
Claims (4)
1, a kind of facial film that contains pulullan polysaccharide is characterized in that: the film former of this facial film is pulullan polysaccharide and polyglutamic acid.
2, a kind of facial film that contains pulullan polysaccharide, it is characterized in that: this facial film is made up of following composition:
Fruit acid 1%～5%, g/mL
Sorbitol 1%～5%, g/mL
Tea polyphenols 0.002%～0.015%, g/mL
Polyvinyl alcohol 5%～15%, g/mL
Carboxymethyl cellulose 3%～6%, g/mL
Glycerol 2%～6%, g/mL
Vitamin C 0.05%～0.5%, g/mL
Epidermal growth factor 0.0000001%～0.0005%, g/mL
Pulullan polysaccharide 2%～10%, g/mL
Polyglutamic acid 2%～10%, g/mL
Sodium benzoate 0.1%～0.5%, g/mL
Essence 0.01%～0.05%, g/mL
Other fruit juice 10%～20%, g/mL
Sterilized water adds to 100%, g/mL
3, the preparation method of claim 1 or 2 described facial films, it is characterized in that: this method may further comprise the steps:
(1) pulullan polysaccharide powder and polyglutamic acid powder is soluble in water, abundant mixing;
(2) polyvinyl alcohol, sorbitol are added the water stirring and evenly mixing, add sodium benzoate, be heated to 60 ℃;
(3) with carboxymethyl cellulose and other fruit juice constituents mix homogeneously and add essence;
(4) with above-mentioned various composition mix homogeneously, other compositions of polishing.
4, claims 1 or 2 described facial films is characterized in that: the mean molecule quantity of pulullan polysaccharide is 5～2,200,000 dalton, and the mean molecule quantity of polyglutamic acid is 10～1,000,000 dalton.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008101872810A CN101416930B (en) | 2008-12-22 | 2008-12-22 | Face mask containing pullulan |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2008101872810A CN101416930B (en) | 2008-12-22 | 2008-12-22 | Face mask containing pullulan |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN101416930A true CN101416930A (en) | 2009-04-29 |
| CN101416930B CN101416930B (en) | 2011-03-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2008101872810A Active CN101416930B (en) | 2008-12-22 | 2008-12-22 | Face mask containing pullulan |
Country Status (1)
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| CN103622872A (en) * | 2013-11-30 | 2014-03-12 | 苏州市洋海电子有限公司 | Chinese herbal medicine mask |
| CN103690396A (en) * | 2013-12-25 | 2014-04-02 | 天津北洋百川生物技术有限公司 | Mask containing high-molecular polyglutamic acid and preparation method of mask |
| CN104725652A (en) * | 2015-04-02 | 2015-06-24 | 陈洁 | Preparation method of degradable composite pullulan film |
| CN105193655A (en) * | 2015-09-25 | 2015-12-30 | 斐丝肌(上海)商贸有限公司 | Composite with efficacies of water locking and moisturizing, face mask and face mask preparation method |
| CN105213252A (en) * | 2015-09-25 | 2016-01-06 | 斐丝肌(上海)商贸有限公司 | A kind ofly lock essence of water moisture-keeping efficacy and preparation method thereof |
| CN105233263A (en) * | 2015-11-18 | 2016-01-13 | 桂林华诺威基因药业有限公司 | Wrinkle-removing and anti-ageing composition |
| CN105233264A (en) * | 2015-11-18 | 2016-01-13 | 桂林华诺威基因药业有限公司 | Composition for treating yellowish skin |
| CN106176327A (en) * | 2016-09-18 | 2016-12-07 | 天津北洋百川生物技术有限公司 | A kind of shampoo containing polyglutamic acid and preparation method thereof |
| CN106214514A (en) * | 2016-09-18 | 2016-12-14 | 天津北洋百川生物技术有限公司 | A kind of bath gel containing γ polyglutamic acid and preparation method thereof |
| CN106265098A (en) * | 2016-09-18 | 2017-01-04 | 天津北洋百川生物技术有限公司 | A kind of perfume patch of health environment-friendly and preparation method thereof |
| CN106966047A (en) * | 2017-03-23 | 2017-07-21 | 浙江工业大学 | A kind of preparation method of edible nanofiber preservative film |
| CN107157911A (en) * | 2017-07-06 | 2017-09-15 | 天津杞源堂生物工程有限公司 | A kind of after-sun fermentation Chinese wolfberry fruit liquid level film and preparation method thereof |
| CN107233275A (en) * | 2017-07-06 | 2017-10-10 | 天津杞源堂生物工程有限公司 | A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film and preparation method thereof |
| CN107296784A (en) * | 2017-07-06 | 2017-10-27 | 天津杞源堂生物工程有限公司 | A kind of skin whitening, moisturizing fermentation Chinese wolfberry fruit liquid level film and preparation method thereof |
| CN107308094A (en) * | 2017-07-06 | 2017-11-03 | 天津杞源堂生物工程有限公司 | A kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film and preparation method thereof |
| CN107308071A (en) * | 2017-05-23 | 2017-11-03 | 天津杞源堂生物工程有限公司 | It is a kind of to add matrimony vine facial mask of polyglutamic acid and preparation method thereof |
| CN107308070A (en) * | 2017-05-23 | 2017-11-03 | 天津杞源堂生物工程有限公司 | It is a kind of to add lactobacillus-fermented matrimony vine facial mask of polyglutamic acid and preparation method thereof |
| CN109010130A (en) * | 2018-09-12 | 2018-12-18 | 华南理工大学 | A kind of polyethylene glycol oxide skin care mask carriers substrate and preparation method thereof |
| CN109310590A (en) * | 2015-12-31 | 2019-02-05 | 莱雅公司 | Firm composition |
| CN110269813A (en) * | 2019-02-18 | 2019-09-24 | 广州暨大美塑生物科技有限公司 | A kind of composite reactive polypeptide biological micro crystal freeze-dried powder preparation |
| US10568839B2 (en) | 2011-01-11 | 2020-02-25 | Capsugel Belgium Nv | Hard capsules |
| US11319566B2 (en) | 2017-04-14 | 2022-05-03 | Capsugel Belgium Nv | Process for making pullulan |
| US11576870B2 (en) | 2017-04-14 | 2023-02-14 | Capsugel Belgium Nv | Pullulan capsules |
-
2008
- 2008-12-22 CN CN2008101872810A patent/CN101416930B/en active Active
Cited By (25)
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| US10568839B2 (en) | 2011-01-11 | 2020-02-25 | Capsugel Belgium Nv | Hard capsules |
| CN103622872A (en) * | 2013-11-30 | 2014-03-12 | 苏州市洋海电子有限公司 | Chinese herbal medicine mask |
| CN103690396A (en) * | 2013-12-25 | 2014-04-02 | 天津北洋百川生物技术有限公司 | Mask containing high-molecular polyglutamic acid and preparation method of mask |
| CN103690396B (en) * | 2013-12-25 | 2015-08-26 | 天津北洋百川生物技术有限公司 | Facial film of pbz polymer polyglutamic acid and preparation method thereof |
| CN104725652A (en) * | 2015-04-02 | 2015-06-24 | 陈洁 | Preparation method of degradable composite pullulan film |
| CN105193655A (en) * | 2015-09-25 | 2015-12-30 | 斐丝肌(上海)商贸有限公司 | Composite with efficacies of water locking and moisturizing, face mask and face mask preparation method |
| CN105213252A (en) * | 2015-09-25 | 2016-01-06 | 斐丝肌(上海)商贸有限公司 | A kind ofly lock essence of water moisture-keeping efficacy and preparation method thereof |
| CN105233264A (en) * | 2015-11-18 | 2016-01-13 | 桂林华诺威基因药业有限公司 | Composition for treating yellowish skin |
| CN105233263A (en) * | 2015-11-18 | 2016-01-13 | 桂林华诺威基因药业有限公司 | Wrinkle-removing and anti-ageing composition |
| CN109310590A (en) * | 2015-12-31 | 2019-02-05 | 莱雅公司 | Firm composition |
| CN106265098A (en) * | 2016-09-18 | 2017-01-04 | 天津北洋百川生物技术有限公司 | A kind of perfume patch of health environment-friendly and preparation method thereof |
| CN106214514A (en) * | 2016-09-18 | 2016-12-14 | 天津北洋百川生物技术有限公司 | A kind of bath gel containing γ polyglutamic acid and preparation method thereof |
| CN106176327A (en) * | 2016-09-18 | 2016-12-07 | 天津北洋百川生物技术有限公司 | A kind of shampoo containing polyglutamic acid and preparation method thereof |
| CN106966047A (en) * | 2017-03-23 | 2017-07-21 | 浙江工业大学 | A kind of preparation method of edible nanofiber preservative film |
| CN106966047B (en) * | 2017-03-23 | 2019-04-09 | 浙江工业大学 | A kind of preparation method of edible nanofiber preservative film |
| US11576870B2 (en) | 2017-04-14 | 2023-02-14 | Capsugel Belgium Nv | Pullulan capsules |
| US11319566B2 (en) | 2017-04-14 | 2022-05-03 | Capsugel Belgium Nv | Process for making pullulan |
| CN107308071A (en) * | 2017-05-23 | 2017-11-03 | 天津杞源堂生物工程有限公司 | It is a kind of to add matrimony vine facial mask of polyglutamic acid and preparation method thereof |
| CN107308070A (en) * | 2017-05-23 | 2017-11-03 | 天津杞源堂生物工程有限公司 | It is a kind of to add lactobacillus-fermented matrimony vine facial mask of polyglutamic acid and preparation method thereof |
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| CN107296784A (en) * | 2017-07-06 | 2017-10-27 | 天津杞源堂生物工程有限公司 | A kind of skin whitening, moisturizing fermentation Chinese wolfberry fruit liquid level film and preparation method thereof |
| CN107233275A (en) * | 2017-07-06 | 2017-10-10 | 天津杞源堂生物工程有限公司 | A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film and preparation method thereof |
| CN109010130A (en) * | 2018-09-12 | 2018-12-18 | 华南理工大学 | A kind of polyethylene glycol oxide skin care mask carriers substrate and preparation method thereof |
| CN110269813A (en) * | 2019-02-18 | 2019-09-24 | 广州暨大美塑生物科技有限公司 | A kind of composite reactive polypeptide biological micro crystal freeze-dried powder preparation |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101416930B (en) | 2011-03-16 |
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| EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Shandong Freda Bioengineering Co., Ltd. Assignor: Shandong Biological Pharmaceutical Academy Contract record no.: 2012370000112 Denomination of invention: Face mask containing pullulan Granted publication date: 20110316 License type: Exclusive License Open date: 20090429 Record date: 20120426 |