CN107308070A - It is a kind of to add lactobacillus-fermented matrimony vine facial mask of polyglutamic acid and preparation method thereof - Google Patents
It is a kind of to add lactobacillus-fermented matrimony vine facial mask of polyglutamic acid and preparation method thereof Download PDFInfo
- Publication number
- CN107308070A CN107308070A CN201710366905.4A CN201710366905A CN107308070A CN 107308070 A CN107308070 A CN 107308070A CN 201710366905 A CN201710366905 A CN 201710366905A CN 107308070 A CN107308070 A CN 107308070A
- Authority
- CN
- China
- Prior art keywords
- facial mask
- matrimony vine
- polyglutamic acid
- fermented
- liquid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/88—Polyamides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention belongs to cosmetic skin field, and in particular to a kind of to add lactobacillus-fermented matrimony vine facial mask of polyglutamic acid and preparation method thereof.The matrimony vine facial mask of the present invention includes the facial mask stoste of spunlace non-woven cloth Face film towel and infiltration on spunlace non-woven cloth；Facial mask stoste includes the component of following parts by weight：Pure water, fermentation Chinese wolfberry fruit liquid, polyglutamic acid, vitamin C, asparagus juice, pearl powder, propane diols and pulullan polysaccharide.The matrimony vine facial mask of the present invention prepares fermentation Chinese wolfberry fruit liquid using lactobacillus-fermented, prepared by compounding natural moisture preserving whitening composition polyglutamic acid.The present invention prepares zymotic fluid to the storage rate of active ingredient apparently higher than the storage rate of alcoholic fermentation using lactobacillus-fermented matrimony vine, the nutritional ingredient of matrimony vine is more fully utilized and is discharged.This composition of the polyglutamic acid that the present invention is used not only there is extremely strong moisture retention can also effectively control the dissolution of Chinese-wolfberry nutritive composition, with slow release effect, make the using effect of matrimony vine facial mask more preferable.
Description
Technical field
The invention belongs to cosmetic skin field, and in particular to a kind of lactobacillus-fermented matrimony vine face for adding polyglutamic acid
Film and preparation method thereof.
Background technology
With the improvement of living standards, people also increasingly pursue beautiful pursuit inherent and natural.Therefore to skin
Health care consciousness is also being improved.Concept to cosmetics also progressively changes.In the past using beauty as main purpose, turning now to
Beauty is laid equal stress on nursing, especially in the conceptive of facial mask, is more the nursing skin of promotion science, and in the market majorityization
The complex manufacturing technology of cosmetic and mostly contain artificial synthesized chemicals, easily stimulate to skin, especially some skins it is quick
Touching group and the crowd of particular time, cause allergy, people is produced query to the composition of cosmetics.
Matrimony vine, the also known as fruit of Chinese wolfberry, are Solanaceae deciduous plant (Lycium chintnse) or lycium barbarum (Lycium
Barbarum ripening fruits), is famous nourishing Chinese medicine, is included in by health ministry《It is both food and the article of medicine
List》.Modern pharmacological research result shows that matrimony vine is except having reducing blood lipid known to people, decompression, hypoglycemic, enhancing body to exempt from
Epidemic disease function etc. is acted on, moreover it is possible to make erythrocyte sod activity rise.Its polysaccharide Wheat Protein, to safeguarding the normal of human body cell
Develop, improve DNA repair ability and promote senile cell to be reversed to young direction and all play beneficial effect.The chemistry of matrimony vine
Composition mainly contains LBP-X (LBP), glycine betaine, carotenoid and carotenoid ester, vitamin C, several amino acids and
Various trace elements.Because of place of production difference, component content slightly has difference to matrimony vine.By the fermentation process of saccharomycete, Chinese holly can be lifted
The absorbability of the nutriment of Qi, converts some compositions to skin sensitivity, reduces allergic reaction.
The application for preparing facial mask using matrimony vine is existing a lot, such as refer in patent CN201610219829.X a kind of black
Matrimony vine facial mask, it uses lycium ruthenicum to take its extract solution after grinding, then constitutes the raw materials such as itself and cucumber, its process be not related to by
Fermentation Chinese wolfberry fruit prepares facial mask technique.A kind of preparation side of fermentation Chinese wolfberry fruit liquid level film is relate in patent CN201610830191.3
Method, is formed by fermentation Chinese wolfberry fruit liquid, collagen, vitamin C, asparagus juice pearl powder and propane diols simply compounding.The above method
Advantage is, as facial mask stoste, to add fermentation Chinese wolfberry fruit liquid, do not destroy based on active ingredient as far as possible using pure natural raw material, is retained
Active ingredient in fermentation Chinese wolfberry fruit liquid, obtained facial mask has moisturizing, whitening, effect of anti-aging, but uses saccharomycete
During fermentation, the storage rate of active ingredient is slightly lower in fermentation Chinese wolfberry fruit liquid, thus the matrimony vine facial mask finally prepared its to different crowd
Using effect need to be improved.
Therefore, the using effect for how further improving matrimony vine facial mask is the current technical issues that need to address.
The content of the invention
The purpose of the present invention is that there is provided a kind of lactobacillus-fermented Chinese holly for adding polyglutamic acid in view of the shortcomings of the prior art
Qi facial mask and preparation method thereof.The matrimony vine facial mask of the present invention prepares fermentation Chinese wolfberry fruit liquid using lactobacillus-fermented, compounds natural moisture preserving
It is prepared by whitening composition polyglutamic acid.The present invention using lactobacillus-fermented matrimony vine prepare the glycine betaine after zymotic fluid, lactobacillus-fermented,
The storage rate of carrotene and LBP-X is respectively 67.7%, 32.3% and 88.4%, hence it is evident that higher than alcoholic fermentation (saccharomycete
Fermentation) to the storage rate of wolfberry, the nutritional ingredient of matrimony vine is more fully utilized and is discharged.The present invention is used
Polyglutamic acid this composition not only there is extremely strong moisture retention can also effectively control the dissolution of Chinese-wolfberry nutritive composition, with slow
Effect is released, makes the using effect of matrimony vine facial mask more preferable.
To achieve the above object, the present invention is adopted the following technical scheme that：
A kind of lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid, the matrimony vine facial mask includes spunlace non-woven cloth facial mask
The facial mask stoste of towel and infiltration on spunlace non-woven cloth；The facial mask stoste includes the component of following parts by weight：
The lactic acid bacteria used during the fermentation Chinese wolfberry fruit liquid fermentation is CGMCC NO.1.1 lactic acid bacteria；
The molecular weight of the polyglutamic acid is 90-100 ten thousand.
It is used as preferred technical scheme：
It is preferred that, the particle diameter of the pearl powder is 100-200nm.
It is preferred that, the pulullan polysaccharide is 20-30 ten thousand for molecular weight.Increase pulullan polysaccharide composition, the composition and
Polyglutamic acid is compounded, and can be beneficial to the film-formation result of facial mask, moisturizing and slow release effect are more preferable.
The present invention also provides the preparation method for the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid, including following step
Suddenly：
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, become thick liquid；It is poly-
Glutamic acid solution viscosity is larger, can be very good suspension pearl powder, helps to be well mixed；
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit
Liquid is stirred and evenly mixed, and obtains facial mask stoste；
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked in facial mask stoste, then vacuum seal
Dress, is made matrimony vine facial mask.
It is preferred that, the preparation method of the fermentation Chinese wolfberry fruit liquid is：By dry wolfberry and water in mass ratio 1:8-15 mixing is abundant
Mashing, based on liquid, following percentage by weight material is added into basal liquid：Yeast extract 0.1-0.4%, phosphoric acid hydrogen two
Potassium 0.03-0.2%, magnesium sulfate 0.01-0.2%, Triammonium citrate 0.1-0.2%, manganese sulfate 0.001-0.005%, it is fully mixed
Sterilized after even, inoculating lactic acid bacterium is placed in 180rpm on shaking table, 30 DEG C, cultivates 48h, obtain fermentation Chinese wolfberry fruit stoste；By the proferment
Liquid filtration sterilization, retains supernatant and the pH value of supernatant is adjusted into neutrality, obtain fermentation Chinese wolfberry fruit liquid.
It is preferred that, when being stirred in step (1), the speed of stirring is 80-100r/min.
It is preferred that, when being stirred in step (2), it need to stir at ambient temperature, the speed of stirring is 80-100r/min.
It is preferred that, the time of immersion is 30-40min in step (3).
Inventive principle：
Due to, containing the ultrahydrophilic group (- COOH) of more than 1000, can fully keep water in polyglutamic acid molecule
Point, can be in skin table for improving voidage in matrimony vine facial mask between nutritional ingredient, being absorbed beneficial to the effective nutritional ingredient of matrimony vine
Face forms thin film protection skin and absorbed, and is the optimal transport platform of nutrient, moisture and Touch skin familiarity in matrimony vine facial mask,
Effectively increase dissolving, storage, conveying and the absorption in matrimony vine facial mask active ingredient.In addition, polyglutamic acid has hydrophilic radical,
Carboxyl, ionizable negatively charged, the adsorbable nutritional ingredient of negative electrical charge, because its powerful group attribute can slowly discharge matrimony vine battalion
Form point, during face mask film, moisture and the uniform dissolution of nutrition can be made so that skin slow-absorbing.
The present invention prepares glycine betaine, carrotene and matrimony vine after zymotic fluid, lactobacillus-fermented using lactobacillus-fermented matrimony vine
The storage rate of polysaccharide is respectively 67.7%, 32.3% and 88.4%, hence it is evident that had higher than alcoholic fermentation (saccharomycetes to make fermentation) to matrimony vine
The storage rate of composition is imitated, after lactic fermentation, pH declines, and oxidation-reduction potential rises, environment is in reduction-state, ascorbic acid, thiamines
Element, riboflavin etc. is preferably preserved.Therefore, using lactobacillus-fermented matrimony vine, enable the nutritional ingredient of matrimony vine more abundant
Utilization and release.The storage rate of glycine betaine, carrotene and LBP-X wherein in fermentation Chinese wolfberry fruit liquid is measured by HPLC
's.Beneficial effect：
Polyglutamic acid has extremely strong moisture retention, can form layer protecting film on skin to prevent the steaming of skin moisture
Hair, it can penetrate into skin deep layer, self moisture-keeping system of recovery skin.With advancing age with the aggravation of physical fatigue,
The function of profit certainly of skin can gradually weaken, or even disappear, and the facial mask that with the addition of polyglutamic acid can repair the profit work(certainly of skin
Energy.Therefore polyglutamic acid has good beauty protecting effect for the skin of the mankind.
The present invention is substituted original using moisturizing whitening composition of the pure natural polymer substance polyglutamic acid as facial mask stoste
Component collagen albumen, add fermentation Chinese wolfberry fruit liquid, using lactobacillus-fermented, some skins of farthest degrading be not easy absorb and
The material of easy sensitization, retains the active ingredient in fermentation Chinese wolfberry fruit liquid, and the facial mask of preparation has moisturizing, whitening, the work(of anti-aging
Effect, has certain effect to different crowd.This composition of polyglutamic acid not only there is extremely strong moisture retention can also effectively control
The dissolution of Chinese-wolfberry nutritive composition, with slow release effect.Therefore, polyglutamic acid of the invention this be not merely that instead of collagen egg
In vain, this moisturizing ingredient of hyaluronic acid, glycerine etc., moreover it is possible to acted synergistically with fermentation Chinese wolfberry fruit liquid, imitate the use of matrimony vine facial mask
Fruit is more preferably.
Polyglutamic acid is a kind of water solubility, biodegradable, without toxicity, is used biological high made from microbe fermentation method
Molecule.It is a kind of high-end product to the nutritious effect of skin, is completely suitable for all skins, and provide better than hyalomitome
The lasting moistening effect of acid and collagen, it is only necessary to very low concentration, it is possible to reach good effect, therefore cost is very
It is low.Available in skin care item, shampoo, hair-cream, shaving cream and lipstick.Therefore, matrimony vine preparation method of the invention is easy, feasible
Property it is high, it is easy to promote production, and cost is not high.
The present invention prepares zymotic fluid using lactobacillus-fermented matrimony vine, and prior art prepares fermentation Chinese wolfberry fruit using alcoholic fermentation
The storage rate of glycine betaine, carrotene and LBP-X after liquid, lactobacillus-fermented is respectively 67.7%, 32.3% and 88.4%,
Apparently higher than storage rate of the alcoholic fermentation (saccharomycetes to make fermentation) to wolfberry, after lactic fermentation, pH declines, redox
Current potential rises, and environment is in reduction-state, and ascorbic acid, thiamine, riboflavin etc. are preferably preserved.Therefore, using lactic acid bacteria
Fermentation matrimony vine, enables the nutritional ingredient of matrimony vine more fully to utilize and discharge, the using effect being applied in facial mask is more preferable.
Embodiment
The invention will be further elucidated with reference to specific embodiments.It should be understood that these embodiments are merely to illustrate this hair
Bright rather than limitation the scope of the present invention.In addition, it is to be understood that after the content of the invention lectured has been read, art technology
Personnel can make various changes or modifications to the present invention, and these equivalent form of values equally fall within the application appended claims and limited
Fixed scope.
Embodiment 1
The present invention the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid, by weight, including composition it is as follows：
25 parts of pure water；
20 parts of fermentation Chinese wolfberry fruit liquid；
2 parts of polyglutamic acid；Molecular weight is 930,000；
0.1 part of vitamin C；
15 parts of asparagus juice；
10 parts of pearl powder；The particle diameter of pearl powder is 100nm；
0.3 part of propane diols；
2 parts of pulullan polysaccharide；Molecular weight is 200,000；
The preparation method of the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid of the present invention, comprises the following steps：Chinese holly
The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask in prepared by Qi facial mask；
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 80r/min, make its into
For thick liquid；
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit
Mixing is stirred at room temperature in liquid, and stir speed (S.S.) is 80r/min, obtains facial mask stoste；The lactic acid that fermentation Chinese wolfberry fruit liquid is used when fermenting
Bacterium is CGMCC NO.1.1 lactic acid bacterias；
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 30min, Ran Houzhen in facial mask stoste
Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows：By dry wolfberry and water in mass ratio 1:8 mixing fully mashing, is used as base
Plinth liquid, following percentage by weight material is added into basal liquid：Yeast extract 0.1%, dipotassium hydrogen phosphate 0.03%, magnesium sulfate
0.01%, Triammonium citrate 0.1%, manganese sulfate 0.001% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing
180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C；By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant
The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.
Embodiment 2
The present invention the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid, by weight, including composition it is as follows：
30 parts of pure water；
22 parts of fermentation Chinese wolfberry fruit liquid；
5 parts of polyglutamic acid；Molecular weight is 1,000,000；
0.2 part of vitamin C；
16 parts of asparagus juice；
12 parts of pearl powder；The particle diameter of pearl powder is 150nm；
0.4 part of propane diols；
3 parts of pulullan polysaccharide；Molecular weight is 250,000；
The preparation method of the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid of the present invention, comprises the following steps：Chinese holly
The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask in prepared by Qi facial mask；
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 90r/min, make its into
For thick liquid；
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit
Mixing is stirred at room temperature in liquid, and stir speed (S.S.) is 90r/min, obtains facial mask stoste；The lactic acid that fermentation Chinese wolfberry fruit liquid is used when fermenting
Bacterium is CGMCC NO.1.1 lactic acid bacterias；
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 35min, Ran Houzhen in facial mask stoste
Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows：By dry wolfberry and water in mass ratio 1:15 mixing fully mashing, as
Basal liquid, following percentage by weight material is added into basal liquid：Yeast extract 0.4%, dipotassium hydrogen phosphate 0.2%, sulfuric acid
Magnesium 0.2%, Triammonium citrate 0.2%, manganese sulfate 0.005% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing
180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C；By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant
The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.
Embodiment 3
The present invention the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid, by weight, including composition it is as follows：
The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask in prepared by matrimony vine facial mask；
30 parts of pure water；
25 parts of fermentation Chinese wolfberry fruit liquid；
5 parts of polyglutamic acid；Molecular weight is 900,000；
0.4 part of vitamin C；
17 parts of asparagus juice；
15 parts of pearl powder；The particle diameter of pearl powder is 200nm；
0.8 part of propane diols；
4 parts of pulullan polysaccharide；Molecular weight is 280,000；
The preparation method of the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid of the present invention, comprises the following steps：Chinese holly
The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask in prepared by Qi facial mask；
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 95r/min, make its into
For thick liquid；
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit
Mixing is stirred at room temperature in liquid, and stir speed (S.S.) is 95r/min, obtains facial mask stoste；The lactic acid that fermentation Chinese wolfberry fruit liquid is used when fermenting
Bacterium is CGMCC NO.1.1 lactic acid bacterias；
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 40min, Ran Houzhen in facial mask stoste
Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows：By dry wolfberry and water in mass ratio 1:12 mixing fully mashing, as
Basal liquid, following percentage by weight material is added into basal liquid：Yeast extract 0.3%, dipotassium hydrogen phosphate 0.1%, sulfuric acid
Magnesium 0.05%, Triammonium citrate 0.12%, manganese sulfate 0.004% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing
180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C；By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant
The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.
The fermentation Chinese wolfberry fruit liquid level film that embodiment 3 is prepared is given different age group crowd and used, each age bracket 100
People, obtained result such as table 1.
Table 1 is the preparation effect of matrimony vine facial mask prepared by embodiment 3
Found by table 1, the moisturizing of such fermentation Chinese wolfberry fruit liquid level film, whitening, effect of anti-aging, to different crowd
There is good effect.
Embodiment 4
The present invention the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid, by weight, including composition it is as follows：
40 parts of pure water；
35 parts of fermentation Chinese wolfberry fruit liquid；
3 parts of polyglutamic acid；Molecular weight is 950,000；
0.5 part of vitamin C；
20 parts of asparagus juice；
15 parts of pearl powder；The particle diameter of pearl powder is 100nm；
0.8 part of propane diols；
5 parts of pulullan polysaccharide；Molecular weight is 300,000；
The preparation method of the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid of the present invention, comprises the following steps：Chinese holly
The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask in prepared by Qi facial mask；
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 100r/min, makes it
As thick liquid；
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit
Mixing is stirred at room temperature in liquid, and stir speed (S.S.) is 100r/min, obtains facial mask stoste；The lactic acid that fermentation Chinese wolfberry fruit liquid is used when fermenting
Bacterium is CGMCC NO.1.1 lactic acid bacterias；
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 33min, Ran Houzhen in facial mask stoste
Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows：By dry wolfberry and water in mass ratio 1:13 mixing fully mashing, as
Basal liquid, following percentage by weight material is added into basal liquid：Yeast extract 0.3%, dipotassium hydrogen phosphate 0.15%, sulfuric acid
Magnesium 0.12%, Triammonium citrate 0.16%, manganese sulfate 0.004% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing
180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C；By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant
The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.
Embodiment 5
The present invention the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid, by weight, including composition it is as follows：
30 parts of pure water；
30 parts of fermentation Chinese wolfberry fruit liquid；
4 parts of polyglutamic acid；Molecular weight is 900,000；
0.4 part of vitamin C；
18 parts of asparagus juice；
13 parts of pearl powder；The particle diameter of pearl powder is 100nm；
0.6 part of propane diols；
7 parts of pulullan polysaccharide；Molecular weight is 300,000；
The preparation method of the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid of the present invention, comprises the following steps：Chinese holly
The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask in prepared by Qi facial mask；
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 100r/min, makes it
As thick liquid；
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit
Mixing is stirred at room temperature in liquid, and stir speed (S.S.) is 100r/min, obtains facial mask stoste；The lactic acid that fermentation Chinese wolfberry fruit liquid is used when fermenting
Bacterium is CGMCC NO.1.1 lactic acid bacterias；
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 38min, Ran Houzhen in facial mask stoste
Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows：By dry wolfberry and water in mass ratio 1:12 mixing fully mashing, as
Basal liquid, following percentage by weight material is added into basal liquid：Yeast extract 0.3%, dipotassium hydrogen phosphate 0.09%, sulfuric acid
Magnesium 0.15%, Triammonium citrate 0.15%, manganese sulfate 0.003% sterilizes, inoculating lactic acid bacterium is placed on shaking table after fully mixing
180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C；By the fermenation raw liquid filtration sterilization, retain supernatant and by supernatant
The pH value of liquid is adjusted to neutrality, obtains fermentation Chinese wolfberry fruit liquid.
Claims (8)
1. a kind of lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid, it is characterized in that：The matrimony vine facial mask include spun lacing without
Spin the facial mask stoste of cloth Face film towel and infiltration on spunlace non-woven cloth；The facial mask stoste includes the component of following parts by weight：
25-40 parts of pure water；
20-35 parts of fermentation Chinese wolfberry fruit liquid；
2-5 parts of polyglutamic acid；
0.1-0.5 parts of vitamin C；
15-20 parts of asparagus juice；
10-15 parts of pearl powder；
0.3-0.8 parts of propane diols；
2-7 parts of pulullan polysaccharide；
The lactic acid bacteria used during the fermentation Chinese wolfberry fruit liquid fermentation is CGMCC NO.1.1 lactic acid bacteria；
The molecular weight of the polyglutamic acid is 90-100 ten thousand.
2. the lactobacillus-fermented matrimony vine facial mask according to claim 1 for adding polyglutamic acid, it is characterised in that the treasure
The particle diameter of pearl powder is 100-200nm.
3. the lactobacillus-fermented matrimony vine facial mask according to claim 1 for adding polyglutamic acid, it is characterised in that described general
Shandong orchid polysaccharide is 20-30 ten thousand for molecular weight.
4. the preparation method of the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid as described in claim 1-3 is any, its
It is characterized in comprise the following steps：
（1）Polyglutamic acid and pearl powder are dissolved in pure water, and stirred, thick liquid is become；
（2）Asparagus juice is added in aforesaid liquid, vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit liquid is added and stirs
Mixing is mixed, facial mask stoste is obtained；
（3）Soaked after the sterilizing of facial mask stoste, then by spunlace non-woven cloth Face film towel in facial mask stoste, then Vacuum Package, system
Obtain matrimony vine facial mask.
5. the preparation method for the lactobacillus-fermented matrimony vine facial mask for adding polyglutamic acid stated according to claim 4, its feature exists
In：The preparation method of the fermentation Chinese wolfberry fruit liquid is：By dry wolfberry and water in mass ratio 1:The abundant mashing of 8-15 mixing, based on
Liquid, following percentage by weight material is added into basal liquid：Yeast extract 0.1-0.4%, dipotassium hydrogen phosphate 0.03-0.2%, sulphur
Sour magnesium 0.01-0.2%, Triammonium citrate 0.1-0.2%, manganese sulfate 0.001-0.005%, sterilize after fully mixing, inoculating lactic acid
Bacterium, is placed in 180rpm on shaking table, 30 DEG C, cultivates 48h, obtain fermentation Chinese wolfberry fruit stoste；By the fermenation raw liquid filtration sterilization, in reservation
The pH value of supernatant is simultaneously adjusted to neutrality by clear liquid, obtains fermentation Chinese wolfberry fruit liquid.
6. the preparation method of the lactobacillus-fermented matrimony vine facial mask according to claim 4 for adding polyglutamic acid, its feature
It is：Step（1）During middle stirring, the speed of stirring is 80-100r/min.
7. the preparation method of the lactobacillus-fermented matrimony vine facial mask according to claim 4 for adding polyglutamic acid, its feature
It is：Step（2）During middle stirring, it need to stir at ambient temperature, the speed of stirring is 80-100r/min.
8. the preparation method of the lactobacillus-fermented matrimony vine facial mask according to claim 4 for adding polyglutamic acid, its feature
It is：Step（3）The time of middle immersion is 30-40min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710366905.4A CN107308070A (en) | 2017-05-23 | 2017-05-23 | It is a kind of to add lactobacillus-fermented matrimony vine facial mask of polyglutamic acid and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710366905.4A CN107308070A (en) | 2017-05-23 | 2017-05-23 | It is a kind of to add lactobacillus-fermented matrimony vine facial mask of polyglutamic acid and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107308070A true CN107308070A (en) | 2017-11-03 |
Family
ID=60183828
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710366905.4A Pending CN107308070A (en) | 2017-05-23 | 2017-05-23 | It is a kind of to add lactobacillus-fermented matrimony vine facial mask of polyglutamic acid and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107308070A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108165583A (en) * | 2017-12-26 | 2018-06-15 | 银川凤仪堂生物工程有限公司 | Matrimony vine enzymatic hydrolysis and fermentation liquid and preparation process and the application in cosmetics |
| CN109504396A (en) * | 2018-12-27 | 2019-03-22 | 天津艾孚森科技发展有限公司 | A kind of saline-alkali land soil conditioner and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2573651A1 (en) * | 1984-11-23 | 1986-05-30 | Allorant Solange | Formula for the regeneration of human or animal dermis |
| JP2003210133A (en) * | 2002-01-18 | 2003-07-29 | Oubiken:Kk | Production and use of fermentation product |
| CN101416930A (en) * | 2008-12-22 | 2009-04-29 | 山东省生物药物研究院 | Face mask containing pullulan |
| CN106265447A (en) * | 2016-09-18 | 2017-01-04 | 天津北洋百川生物技术有限公司 | A kind of preparation method of fermentation Chinese wolfberry fruit liquid level film |
-
2017
- 2017-05-23 CN CN201710366905.4A patent/CN107308070A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2573651A1 (en) * | 1984-11-23 | 1986-05-30 | Allorant Solange | Formula for the regeneration of human or animal dermis |
| JP2003210133A (en) * | 2002-01-18 | 2003-07-29 | Oubiken:Kk | Production and use of fermentation product |
| CN101416930A (en) * | 2008-12-22 | 2009-04-29 | 山东省生物药物研究院 | Face mask containing pullulan |
| CN106265447A (en) * | 2016-09-18 | 2017-01-04 | 天津北洋百川生物技术有限公司 | A kind of preparation method of fermentation Chinese wolfberry fruit liquid level film |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108165583A (en) * | 2017-12-26 | 2018-06-15 | 银川凤仪堂生物工程有限公司 | Matrimony vine enzymatic hydrolysis and fermentation liquid and preparation process and the application in cosmetics |
| CN109504396A (en) * | 2018-12-27 | 2019-03-22 | 天津艾孚森科技发展有限公司 | A kind of saline-alkali land soil conditioner and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109170469A (en) | A kind of Isin glue collagen peptide solid beverage and preparation method thereof | |
| CN105078875B (en) | A kind of cosmetics and preparation method thereof containing peony extract | |
| CN107296784A (en) | A kind of skin whitening, moisturizing fermentation Chinese wolfberry fruit liquid level film and preparation method thereof | |
| CN107281082A (en) | A kind of nutrient solution containing small-molecular peptides and the facial mask and preparation method including it | |
| CN102424625B (en) | Edible and medical fungi blackening agent, its preparation method and application | |
| CN107157911A (en) | A kind of after-sun fermentation Chinese wolfberry fruit liquid level film and preparation method thereof | |
| CN108815072A (en) | A kind of plant composition fermentation magma and its preparation method and application | |
| CN104757560A (en) | Glutathione yeast enzymolysis solution composition and preparation method thereof | |
| CN105663021A (en) | Glutathione fermented mask and preparation method thereof | |
| CN107308070A (en) | It is a kind of to add lactobacillus-fermented matrimony vine facial mask of polyglutamic acid and preparation method thereof | |
| CN107233275A (en) | A kind of light spot is dispelled yellow fermentation Chinese wolfberry fruit liquid level film and preparation method thereof | |
| CN107308071A (en) | It is a kind of to add matrimony vine facial mask of polyglutamic acid and preparation method thereof | |
| CN108850758A (en) | A kind of preparation method of the fructus lycii enzyme beverage with anti-fatigue effect | |
| CN106307532A (en) | Rosa roxburghii tratt composite enzyme and preparation method thereof | |
| CN108201136A (en) | Chromium-rich nutrition fortifier and preparation method thereof | |
| CN112516018B (en) | Selenium-rich mung bean fermentation liquor with whitening, anti-aging, moisturizing and toxin expelling effects and mask composition thereof | |
| CN107836514A (en) | A kind of winter jujube tailored version efficient fresh-keeping agent and preparation method thereof | |
| CN107648585A (en) | A kind of anti-ageing anti-wrinkle Essence containing white fungus, aurantiamarin and soluble protein | |
| CN114028291B (en) | Composition for improving dark eye circles and preparation method and application thereof | |
| CN103122294B (en) | Wine containing SOD (Superoxide Dismutase) component and preparation method thereof | |
| CN1271576A (en) | Beautifying active substance prepared from distillers' grains | |
| CN107802516A (en) | A kind of long-acting preserving moisture and protecting skin Essence | |
| CN107648153A (en) | A kind of Essence of the zymotic fluid containing chrysanthemum and its preparation method and application | |
| CN110013460A (en) | Plant enzyme shampoo paste and preparation method thereof | |
| KR20170095702A (en) | Manufacturing method of cosmetic composition containing nano particle natural materials and cosmetic composition manufactured by the same |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171103 |