CN107308094A - A kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film and preparation method thereof - Google Patents

A kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film and preparation method thereof Download PDF

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CN107308094A
CN107308094A CN201710547637.6A CN201710547637A CN107308094A CN 107308094 A CN107308094 A CN 107308094A CN 201710547637 A CN201710547637 A CN 201710547637A CN 107308094 A CN107308094 A CN 107308094A
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chinese wolfberry
wolfberry fruit
extract
fermentation chinese
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刘建军
乔长晟
严婷婷
张飞扬
牛思思
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Tianjin Qi Yuan Tang Biological Engineering Co Ltd
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Tianjin Qi Yuan Tang Biological Engineering Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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    • A61K8/73Polysaccharides
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    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/736Chitin; Chitosan; Derivatives thereof
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K8/88Polyamides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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    • A61Q17/04Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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Abstract

The invention belongs to cosmetic skin field, and in particular to a kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film and preparation method thereof.The facial mask of the present invention includes spunlace non-woven cloth Face film towel and infiltration in facial mask stoste thereon;Facial mask stoste includes following components:Pure water, fermentation Chinese wolfberry fruit liquid, polyglutamic acid, vitamin C, asparagus juice, pearl powder, propane diols, chitosan oligomer, coptis extract, Flos Pelargonii Hortori, Herba Patriniae extract, hippophae rhamnoides, angelica extract, aminoglucose hydrochloride and pulullan polysaccharide.The Deacne pack of the present invention is when laying, chitosan oligomer and aminoglucose hydrochloride, which can take the lead in entering in Skin Cell, carries out bactericidal antiphlogistic, then the slow of the nutritional ingredient of coptis extract, fish pelargonium etc. is extracted into skin, salubrious oil-control and the reparation and cytothesis for carrying out cell.The sun-proof reparation facial mask of the present invention effectively controls each nutritional ingredient into the order of Skin Cell, by mutually being cooperateed between each component, collective effect, quick repair cell.

Description

A kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film and preparation method thereof
Technical field
The invention belongs to cosmetic skin field, and in particular to a kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film and its preparation side Method.
Background technology
Acne is commonly called as " whelk ", is called " pimples " " acne " " acne " " dark sore " etc., is most common pilosebaceous follicle Chronic inflammatory skin.Because of the blocking of sebaceous gland duct and pore, caused by sebum outflow is not smooth.It is several from after adolescence Everyone can be on the face or acne was given birth at other positions, and simply some people's quantity are few, and the time is short, typically after 25 years old from So tend to recovery from illness, so need not be present to the mind;Somebody's quantity is more, shows as papule, blackhead, warts, abscess, tubercle, tumour, Even scar, often hinders attractive in appearance.Somebody is sought medical advice carelessly or oneself is disorderly controlled, so that sb.'s illness took a turn for the worse, produces more scars, eternal regret Throughout one's life.
Acne is a kind of multifactor caused disease, and under conditions of having inherent cause, 3male hormone secretion increases (especially That protona in skin histology increases) and the effect of the microorganism such as bacillus acnes in follicular orifice be pathogenesis of acne Two principal elements.The development of human sebaceous glands is directly dominated with sebum secretion by male sex hormone, and puberty is swashed due to male Plain level is significantly improved, and stimulates sebaceous glands, enlivens sebum secretion dysfunction, sebum is largely secreted, and makes skin glossy shinny, Follicular orifice also expands therewith, and because the angling of pilosebaceous duct or follicular orifice is blocked, excessive sebum can not be discharged in time, Stasis of blood product forms fat bolt in hair follicle, i.e., so-called acne.Dissolved lipase, protease and hyalomitome produced by bacillus acnes Triglyceride in sour enzyme decomposable asymmetric choice net sebum, as free fatty, it can destroy follicular wall, make hair follicle inclusion enter and Corium and perifollicolar tissue are stimulated, causes inflammatory reaction around pilosebaceous follicle, causes a series of acne symptoms.A part of purulence Blister is due to the scabies secondary infection of demodex folliculorum parasitism or staphylococcus albus.
The method of existing anti-acne has a many kinds, and 1, such as laser therapy whelk method, it can rapid damage propionic acid whelk Bacillus, effectively suppresses bacterial reproduction, eliminates its stimulation and destruction to tissue, but the effect of laser therapy is too strong, and And simply physical method destroys acne, it is impossible to fundamentally anti-acne;2nd, using aloe, chamomile, tea tree etc., some are natural Plant component, Chinese medicinal ingredients or Chinese medicine and plant mixing composition anti-acne, existing this anti-acne method safety, can play regulation Skin oil and fat is so as to the effect of fundamentally anti-acne, but when using this natral plant ingredients anti-acne after time length, anti-acne The marking is difficult complete removal, and formula is needed to be improved;3rd, using salicylic acid, Bo Nisong, dexamethasone etc., some Western medicine remove acne, west The side effect of medicine is strong, and cost is high.Cleaning is the first step of skin care, is also the first step of anti-acne, if be ignored as from the first step or The wrong face cleaning product of person's choosing, the skin problem such as fuel-displaced, pore is thick, small pox only can be more serious, and skin can also become more and more crisp Weak, anti-acne can also become relatively difficult, because the blocking of pore can also hinder the absorption of product for resolving poxes.
Therefore, it is necessary to research and develop a kind of effective oil-control Chinese herbal medicine facial mask, produced with salubrious oil-control prevention small pox, slowly The purpose that the internal environment of slow conditioning skin is finally reached anti-acne is the current technical issues that need to address.
The content of the invention
The purpose of the present invention is that there is provided a kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film and its system in view of the shortcomings of the prior art Preparation Method.In the salubrious oil-control fermentation Chinese wolfberry fruit liquid level film of the present invention, the active component in coptis extract can effectively remove epidermis It is damp and hot, detoxicating, relieving inflammation;Active component in Herba Patriniae extract and sea-buckthorn can be effectively clearing heat and detoxicating, salubrious oil-control, removal acne print, With cool blood, eliminating dampness, antipruritic effect;The active component that angelica extract, fermentation Chinese wolfberry fruit liquid and fish pelargonium contain can effectively promote Enter cytothesis;Chitosan oligomer and aminoglucose hydrochloride have good inhibiting bacteria and diminishing inflammation effect.It is poly- that the present invention is used This composition of glutamic acid, due to its larger strand and large number of ultrahydrophilic group (- COOH), can make the coptis Extract, Herba Patriniae extract, hippophae rhamnoides, angelica extract, fish pelargonium, fermentation Chinese wolfberry fruit liquid, chitosan oligomer and amino Effectively absorption is around its strand in glucose hydrochloride.In addition, big in chitosan oligomer and aminoglucose hydrochloride molecule - the NH of amount3Make it have positive charge, enable chitosan oligomer and aminoglucose hydrochloride effectively with the collagen egg in skin White to wait quick combination, pro-skin performance is very good;Therefore, when laying facial mask, chitosan oligomer and aminoglucose hydrochloride meeting Take the lead in entering in Skin Cell and carry out bactericidal antiphlogistic, then polyglutamic acid can control coptis extract, Herba Patriniae extract, sea-buckthorn Extract, angelica extract, fish pelargonium and the nutritional ingredient in fermentation Chinese wolfberry fruit liquid are slowly extracted into skin, regulation successively again Skin oil and fat, carries out removing toxic substances, toxin expelling, reparation and the cytothesis of acne cell.The sun-proof reparation facial mask of the present invention is effectively controlled Each nutritional ingredient enters the order of Skin Cell, by mutually being cooperateed between each component, collective effect, quick repair cell.
To achieve the above object, the present invention is adopted the following technical scheme that:
A kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, the salubrious oil-control fermentation Chinese wolfberry fruit liquid level film includes spunlace non-woven cloth face The facial mask stoste of film towel and infiltration on spunlace non-woven cloth;The facial mask stoste includes the component of following parts by weight:
The molecular weight of the polyglutamic acid is 91-101 ten thousand.
It is used as preferred technical scheme:
It is preferred that, the molecular weight of the chitosan oligomer is 1300-1600;Fermentation Chinese wolfberry fruit liquid is red fermentation Chinese wolfberry fruit liquid.
It is preferred that, the saccharomycete used during the fermentation Chinese wolfberry fruit liquid fermentation is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:The saccharomycete of 1 mixing.
It is preferred that, the particle diameter of the pearl powder is 100-200nm;The molecular weight of the pulullan polysaccharide is 20-40 ten thousand.
It is preferred that, the facial mask stoste includes the component of following parts by weight:30 parts of pure water, 28 parts of fermentation Chinese wolfberry fruit liquid, 3 parts of polyglutamic acid, 0.4 part of vitamin C, 16 parts of asparagus juice, 12 parts of pearl powder, 0.5 part of propane diols, 3 parts of chitosan oligomer, Huang 8 parts of coptis extract, 5 parts of Flos Pelargonii Hortori, 2 parts of aminoglucose hydrochloride and 5 parts of pulullan polysaccharide, Herba Patriniae extract 4 3 parts of part, 6 parts of hippophae rhamnoides and angelica extract;The molecular weight of the polyglutamic acid is 950,000.
Present invention also offers a kind of preparation method of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, it is characterized in that, including it is following Step:
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, become thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, coptis extract, Flos Pelargonii Hortori, Herba Patriniae extract, hippophae rhamnoides, angelica extract Stirred and evenly mixed with aminoglucose hydrochloride, obtain facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked in facial mask stoste, then vacuum seal Dress, is made matrimony vine facial mask.
It is preferred that, the preparation method of the fermentation Chinese wolfberry fruit liquid is:By dry wolfberry and water in mass ratio 1:8-15 mixing is abundant Mashing, based on liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5-1%, dipotassium hydrogen phosphate 0.03-0.1%, manganese sulfate 0.5-1%, sterilize after fully mixing, inoculation yeast bacterium;It is subsequently placed in 180rpm on shaking table, 30 DEG C, 48h is cultivated, fermentation Chinese wolfberry fruit stoste is obtained;By the fermenation raw liquid filtration sterilization, retain supernatant and be adjusted to the pH value of supernatant Neutrality, obtains fermentation Chinese wolfberry fruit liquid.
It is preferred that, the stir speed (S.S.) used when being stirred in step (1) or step (2) is 80-100r/min;In step (3) The time of immersion is 30-40min.
It is preferred that, Herba Patriniae extract, hippophae rhamnoides, angelica extract, Herba Patriniae extract, hippophae rhamnoides, when The extracting method for returning extract, coptis extract and Flos Pelargonii Hortori is:After the extract that will be prepared is crushed, volume is added Fraction filters for 30%-95% ethanol solution;Then it is placed in after filtered fluid is concentrated on large pore resin absorption column, uses same body After the ethanol solution elution of fraction, dry and obtain the extract.
It is preferred that, the fermentation Chinese wolfberry fruit stoste is handled before filtration sterilization using high-pressure pulse electric and ultrasonic synergistic 15-35 minutes.What the fermentation Chinese wolfberry fruit stoste of the present invention was handled before filtration sterilization using high-pressure pulse electric and ultrasonic synergistic Purpose is in order to by yeast broken wall.Yeast will discharge protein, nucleic acid and vitamin etc. after broken wall, free with removing The effect of base, nourishes rough skin cell, can improve skin metabolism, make skin more delicate smooth.
Inventive principle:
Chitosan oligomer and aminoglucose hydrochloride in the present invention have good inhibiting bacteria and diminishing inflammation and moisturizing effects.It is low Substantial amounts of-NH in chitosan and aminoglucose hydrochloride molecule3Presence it is carried positive charge, can effectively and skin In collagen etc. it is quick combine, pro-skin performance is very good;Therefore, when laying facial mask, chitosan oligomer and aminoglucose Sugared hydrochloride, which can take the lead in entering in Skin Cell, carries out bactericidal antiphlogistic, and then polyglutamic acid can control coptis extract, fish pelargonium Slow with the nutritional ingredient in fermentation Chinese wolfberry fruit liquid is extracted into skin, adjusts skin oil and fat, and carries out the reparation of cell and thin Born of the same parents regenerate.
Due to, containing the ultrahydrophilic group (- COOH) of more than 1000, can fully keep water in polyglutamic acid molecule Point, for improving voidage in matrimony vine facial mask between nutritional ingredient, being carried beneficial to Herba Patriniae extract, hippophae rhamnoides, Radix Angelicae Sinensis The effectively nutritional ingredient such as thing, coptis extract, fish pelargonium, fermentation Chinese wolfberry fruit liquid is taken to absorb, can be in skin surface formation thin film Protect skin to absorb, be the optimal transport platform of nutrient, moisture and Touch skin familiarity in sun-proof facial mask, effectively increase sun-proof Dissolving, storage, conveying in facial mask active ingredient is with absorbing.In addition, polyglutamic acid has hydrophilic radical, carboxyl, ionizable band Negative electrical charge, the adsorbable nutritional ingredient of negative electrical charge;When laying facial mask, adsorb in polyglutamic acid group surrounding nutrient composition, due to Under concentration difference effect and the intermolecular force seen with skin, polyglutamic acid can slowly release above-mentioned nutritional ingredient, in face mask film During, moisture and the uniform dissolution of nutrition can be made so that skin slow-absorbing.Also need to propose, because field pennycress carries The nutritional ingredient in thing, hippophae rhamnoides, angelica extract, coptis extract, fish pelargonium, fermentation Chinese wolfberry fruit liquid is taken to include flavonoids The materials such as material, saponin, beta carotene, alkaloids, forulic acid, Ligustilide, polysaccharose substance, due to them and poly- paddy The active force of propylhomoserin is different, during sustained release, and usually the alkaloids substance with bactericidal action takes the lead in entering intracellular Anti-inflammation and sterilization is carried out again, adjusts skin oil and fat, followed by forulic acid, Flavonoid substances, saponin and polysaccharose substance enter thin Born of the same parents are repaired and cytothesis, are finally that the materials such as beta carotene, Ligustilide enter cell enhancing cell viability, are shone Skin.The sun-proof reparation facial mask of the present invention effectively controls each nutritional ingredient into the order of Skin Cell, by between each component Mutually collaboration, collective effect, quick repair cell.
Therefore, using pure natural polyglutamic acid, this is not merely that instead of collagen, hyaluronic acid, glycerine to the present invention Etc. this moisturizing ingredient, moreover it is possible to Herba Patriniae extract, hippophae rhamnoides, angelica extract, fermentation Chinese wolfberry fruit liquid, the coptis extract Thing and fish pelargonium and chitosan oligomer and aminoglucose hydrochloride etc. act synergistically, and make the using effect of matrimony vine facial mask more preferable.
Beneficial effect:
(1) the salubrious oil control and acne removal facial mask of the present invention is made up of various plants extract, is not stimulated naturally, effectively antibacterial, is relaxed The senses of discomfort such as slow red swelling of the skin, inflammation, more dissolvable pore depths grease soils, dredge blockage hair follicle discharges toxin, salubrious control Oil, and nutrition elite needed for supplement skin in time, promote skin reparation, compact skin, smooth acne hole, reduce acne print, improve skin Matter, while suppressing small pox regeneration.
(2) the salubrious oil control and acne removal facial mask of the present invention is not stimulated gently, easy absorption, non-greasy, safe and efficient, this can be cooperateed with to send out The refreshing oil control and acne removal composition of Ming and Qing quickly penetrates into skin, adjusts skin oil and fat, reaches safe and efficient anti-acne, repairs skin, suppresses The purpose of small pox regeneration;The Deacne pack raw material of the present invention is easy to get simultaneously, and preparation technology is simple, and condition is easily-controllable, can be applicable.
Polyglutamic acid has extremely strong moisture retention, can form layer protecting film on skin to prevent the steaming of skin moisture Hair, it can penetrate into skin deep layer, self moisture-keeping system of recovery skin.With advancing age with the aggravation of physical fatigue, The function of profit certainly of skin can gradually weaken, or even disappear, and the facial mask that with the addition of polyglutamic acid can repair the profit work(certainly of skin Energy.Therefore polyglutamic acid has good beauty protecting effect for the skin of the mankind.
Polyglutamic acid be it is a kind of water-soluble, it is biodegradable, be a kind of to the high-end of the nutritious effect of skin without toxicity Product, is completely suitable for all skins, and provide the lasting moistening effect better than hyaluronic acid and collagen, it is only necessary to Very low concentration, it is possible to reach good effect, therefore cost is very low.Available for skin care item, shampoo, hair-cream, shaving cream In lipstick.Therefore, matrimony vine preparation method of the invention is easy, and feasibility is high, it is easy to promote production, and cost is not high.
The present invention polyglutamic acid this be not merely instead of this moisturizing of collagen, hyaluronic acid, glycerine etc. into Point, polyglutamic acid of the invention not only has extremely strong moisture retention, moreover it is possible to fermentation Chinese wolfberry fruit liquid, coptis extract and fish pelargonium, Synergy, makes the using effect of sun-proof facial mask more preferable.
The present invention uses the fermentation Chinese wolfberry fruit liquid of saccharomycetes to make fermentation, and some skins of farthest degrading are not easy to absorb and easy The material of sensitization, retains the active ingredient in fermentation Chinese wolfberry fruit liquid, and the facial mask of preparation has moisturizing, a whitening, effect of anti-aging, There is certain effect to different crowd.
Active component in the coptis extract coptis extract that the present invention is used can effectively remove that epidermis is damp and hot, and removing toxic substances disappears It is scorching.
Active component in Herba Patriniae extract and sea-buckthorn that the present invention is used can be effectively clearing heat and detoxicating, adjusts skin oil Fat, removes acne print, with cool blood, eliminating dampness, antipruritic effect.
The angelica extract promoting flow of qi and blood circulation that the present invention is used, has effects that cool blood flesh;
The sharp intestines of asparagus juice that the present invention is used purge heat, oil removing skin toner.
The hippophae rhamnoides that the present invention is used can effective repair cell, promoting blood circulation to remove blood stasis accelerates skin Newborn Process, repairs skin The effect of skin scar, with extraordinary bioactivity.
The present invention adapts to various skins using fish pelargonium, can balance sebum secretion and make turgor, can promote blood Liquid is circulated, and accelerates skin Newborn Process, promotes the metabolism of fibrocyte agent epidermal cell, improves skin circulation.
The present invention is using substantial amounts of-NH in oligopolymerization chitosan glycan molecule3With the presence of the highly polar groups of-OH, make itself not Only make chitosan oligomer that there is good moisture-absorbing moisture-keeping function, transepidermal water can be hydrated again, protected so as to play humidification Wet effect.Moreover, the good gas permeability of chitosan oligomer does not disturb excretion of the epidermis to waste and toxin again, skin is not resulted in Acne.The skin-protection product of chitosan oligomer also plays the role of easily to be absorbed by the skin, stimulated circulation.
The present invention uses the structure very phase of aminoglucose hydrochloride and the neural phthalein amine of human epidermal film layer important component Seemingly, product is readily penetrated through, stimulates cell to synthesize, with the antibacterial effect of anti-inflammatory.
The mesh that the fermentation Chinese wolfberry fruit stoste of the present invention is handled before filtration sterilization using high-pressure pulse electric and ultrasonic synergistic Be in order to by yeast broken wall.Yeast will discharge protein, nucleic acid and vitamin etc. after broken wall, with remove free radical, The effect of nourishes rough skin cell, can improve skin metabolism, make skin more delicate smooth.
Matrimony vine, the also known as fruit of Chinese wolfberry, are Solanaceae deciduous plant (Lycium chintnse) or lycium barbarum (Lycium Barbarum ripening fruits), is famous nourishing Chinese medicine, is included in by health ministry《It is both food and the article of medicine List》.Modern pharmacological research result shows that matrimony vine is except having reducing blood lipid known to people, decompression, hypoglycemic, enhancing body to exempt from Epidemic disease function etc. is acted on, moreover it is possible to make erythrocyte sod activity rise.Its polysaccharide Wheat Protein, to safeguarding the normal of human body cell Develop, improve DNA repair ability and promote senile cell to be reversed to young direction and all play beneficial effect.The chemistry of matrimony vine Composition mainly contains LBP-X (LBP), glycine betaine, carotenoid and carotenoid ester, vitamin C, several amino acids and Various trace elements.Because of place of production difference, component content slightly has difference to matrimony vine.By the fermentation process of saccharomycete, Chinese holly can be lifted The absorbability of the nutriment of Qi, converts some compositions to skin sensitivity, reduces allergic reaction.
Embodiment
The invention will be further elucidated with reference to specific embodiments.It should be understood that these embodiments are merely to illustrate this hair Bright rather than limitation the scope of the present invention.In addition, it is to be understood that after the content of the invention lectured has been read, art technology Personnel can make various changes or modifications to the present invention, and these equivalent form of values equally fall within the application appended claims and limited Fixed scope.
Embodiment 1
The present invention salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:
25 parts of pure water;
20 parts of fermentation Chinese wolfberry fruit liquid;
2 parts of polyglutamic acid;Molecular weight is 950,000
0.3 part of vitamin C;
15 parts of asparagus juice;
10 parts of pearl powder;The particle diameter of pearl powder is 100 nanometers;
0.3 part of propane diols;
2 parts of chitosan oligomer;Molecular weight is 1300;
10 parts of coptis extract;
6 parts of Flos Pelargonii Hortori;
1 part of aminoglucose hydrochloride;
2 parts of pulullan polysaccharide;Molecular weight is 200,000;
3 parts of Herba Patriniae extract;
7 parts of hippophae rhamnoides;
6 parts of angelica extract;
The preparation method of the salubrious oil-control fermentation Chinese wolfberry fruit liquid level film of the present invention, comprises the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 80r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, coptis extract, Flos Pelargonii Hortori, Herba Patriniae extract, hippophae rhamnoides, angelica extract Stirred and evenly mixed with aminoglucose hydrochloride, stir speed (S.S.) is 80r/min, obtain facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 30min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
The preparation method of wherein matrimony vine facial mask is as follows:Fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:Dry wolfberry and water are pressed into quality Than 1:8 mixing fully mashing, based on liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, manganese sulfate 0.5% sterilizes after fully mixing, inoculation yeast bacterium.It is placed on shaking table 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C.By the fermenation raw liquid filtration sterilization, reserve rich in Chinese-wolfberry nutritive into The supernatant divided, adjusts pH value to neutrality, saccharomycete is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixes Close, obtain fermentation Chinese wolfberry fruit liquid.
Herba Patriniae extract, hippophae rhamnoides, angelica extract, the extracting method of coptis extract and Flos Pelargonii Hortori For:After the extract that will be prepared is crushed, add volume fraction and filtered for 45% ethanol solution;Then after filtered fluid is concentrated It is placed on large pore resin absorption column, after the ethanol solution elution of same volume fraction, dries and obtain the extract.
Embodiment 2
The present invention salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:
40 parts of pure water;
22 parts of fermentation Chinese wolfberry fruit liquid;
4 parts of polyglutamic acid;Molecular weight is 910,000
0.4 part of vitamin C;
16 parts of asparagus juice;
12 parts of pearl powder;The particle diameter of pearl powder is 200 nanometers;
0.4 part of propane diols;
5 parts of chitosan oligomer;Molecular weight is 1600;
5 parts of coptis extract;
3 parts of Flos Pelargonii Hortori;
3 parts of aminoglucose hydrochloride;
4 parts of pulullan polysaccharide;Molecular weight is 250,000;
5 parts of Herba Patriniae extract;
4 parts of hippophae rhamnoides;
2 parts of angelica extract;
The preparation method of the salubrious oil-control fermentation Chinese wolfberry fruit liquid level film of the present invention, comprises the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 90r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, coptis extract, Flos Pelargonii Hortori, Herba Patriniae extract, hippophae rhamnoides, angelica extract Stirred and evenly mixed with aminoglucose hydrochloride, stir speed (S.S.) is 90r/min, obtain facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 35min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:By dry wolfberry and water in mass ratio 1:10 mixing fully mashing, as Basal liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, sulfuric acid Manganese 0.5%, sterilizes after fully mixing, inoculation yeast bacterium.180rpm on shaking table is placed in, 30 DEG C, 48h is cultivated, obtains fermentation Chinese wolfberry fruit Stoste.Fermentation Chinese wolfberry fruit stoste is handled 25 minutes before filtration sterilization using high-pressure pulse electric and ultrasonic synergistic, then should Fermenation raw liquid filtration sterilization, reserves the supernatant rich in Chinese-wolfberry nutritive composition, adjusts pH value to neutrality.Saccharomycete is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixing, obtains fermentation Chinese wolfberry fruit liquid.
Herba Patriniae extract, hippophae rhamnoides, angelica extract, the extracting method of coptis extract and Flos Pelargonii Hortori For:After the extract that will be prepared is crushed, add volume fraction and filtered for 75% ethanol solution;Then after filtered fluid is concentrated It is placed on large pore resin absorption column, after the ethanol solution elution of same volume fraction, dries and obtain the extract.
Embodiment 3
The present invention salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:It is prepared by matrimony vine facial mask The addition of middle each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
30 parts of pure water;
25 parts of fermentation Chinese wolfberry fruit liquid;
3 parts of polyglutamic acid;Molecular weight is 1,000,000
0.4 part of vitamin C;
17 parts of asparagus juice;
15 parts of pearl powder;The particle diameter of pearl powder is 100 nanometers;
0.8 part of propane diols;
4 parts of chitosan oligomer;Molecular weight is 1400;
6 parts of coptis extract;
4 parts of Flos Pelargonii Hortori;
2 parts of aminoglucose hydrochloride;
5 parts of pulullan polysaccharide;Molecular weight is 300,000;
4 parts of Herba Patriniae extract;
5 parts of hippophae rhamnoides;
4 parts of angelica extract;
The preparation method of the salubrious oil-control fermentation Chinese wolfberry fruit liquid level film of the present invention, comprises the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 100r/min, makes it As thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, coptis extract, Flos Pelargonii Hortori, Herba Patriniae extract, hippophae rhamnoides, angelica extract Stirred and evenly mixed with aminoglucose hydrochloride, stir speed (S.S.) is 100r/min, obtain facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 40min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:By dry wolfberry and water in mass ratio 1:15 mixing fully mashing, as Basal liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, sulfuric acid Manganese 0.5%, sterilizes after fully mixing, inoculation yeast bacterium.180rpm on shaking table is placed in, 30 DEG C, 48h is cultivated, obtains fermentation Chinese wolfberry fruit Stoste.Fermentation Chinese wolfberry fruit stoste is handled 20 minutes before filtration sterilization using high-pressure pulse electric and ultrasonic synergistic, then should Fermenation raw liquid filtration sterilization, reserves the supernatant rich in Chinese-wolfberry nutritive composition, adjusts pH value to neutrality.Saccharomycete is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixing, obtains fermentation Chinese wolfberry fruit liquid.
Herba Patriniae extract, hippophae rhamnoides, angelica extract, the extracting method of coptis extract and Flos Pelargonii Hortori For:After the extract that will be prepared is crushed, add volume fraction and filtered for 60% ethanol solution;Then after filtered fluid is concentrated It is placed on large pore resin absorption column, after the ethanol solution elution of same volume fraction, dries and obtain the extract.
Embodiment 4
The present invention salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:
40 parts of pure water;
35 parts of fermentation Chinese wolfberry fruit liquid;
3 parts of polyglutamic acid;Molecular weight is 1,000,000
0.5 part of vitamin C;
20 parts of asparagus juice;
15 parts of pearl powder;The particle diameter of pearl powder is 100 nanometers;
0.8 part of propane diols;
3 parts of chitosan oligomer;Molecular weight is 1500;
7 parts of coptis extract;
5 parts of Flos Pelargonii Hortori;
2.5 parts of aminoglucose hydrochloride;
3 parts of pulullan polysaccharide;Molecular weight is 200,000;
4.5 parts of Herba Patriniae extract;
6 parts of hippophae rhamnoides;
5 parts of angelica extract;
The preparation method of the salubrious oil-control fermentation Chinese wolfberry fruit liquid level film of the present invention, comprises the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 85r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, coptis extract, Flos Pelargonii Hortori, Herba Patriniae extract, hippophae rhamnoides, angelica extract Stirred and evenly mixed with aminoglucose hydrochloride, stir speed (S.S.) is 85r/min, obtain facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 33min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
The preparation method of wherein matrimony vine facial mask is as follows:Fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:Dry wolfberry and water are pressed into quality Than 1:8 mixing fully mashing, based on liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, manganese sulfate 0.5% sterilizes after fully mixing, inoculation yeast bacterium.It is placed on shaking table 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C.Fermentation Chinese wolfberry fruit stoste uses high-pressure pulse electric before filtration sterilization Handled 15 minutes with ultrasonic synergistic, then by the fermenation raw liquid filtration sterilization, reserve the supernatant rich in Chinese-wolfberry nutritive composition, Adjust pH value to neutrality, saccharomycete is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixing, obtains matrimony vine hair Zymotic fluid.
Herba Patriniae extract, hippophae rhamnoides, angelica extract, the extracting method of coptis extract and Flos Pelargonii Hortori For:After the extract that will be prepared is crushed, add volume fraction and filtered for 30% ethanol solution;Then after filtered fluid is concentrated It is placed on large pore resin absorption column, after the ethanol solution elution of same volume fraction, dries and obtain the extract.
Embodiment 5
The present invention salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:
35 parts of pure water;
30 parts of fermentation Chinese wolfberry fruit liquid;
4 parts of polyglutamic acid;Molecular weight is 1,010,000
0.4 part of vitamin C;
18 parts of asparagus juice;
13 parts of pearl powder;The particle diameter of pearl powder is 100nm;
0.6 part of propane diols;
5 parts of chitosan oligomer;Molecular weight is 1600;
8 parts of coptis extract;
5 parts of Flos Pelargonii Hortori;
2 parts of aminoglucose hydrochloride;
5 parts of pulullan polysaccharide;Molecular weight is 300,000;
5 parts of Herba Patriniae extract;
Hippophae rhamnoides, 6 parts;
4 parts of angelica extract;
The preparation method of the salubrious oil-control fermentation Chinese wolfberry fruit liquid level film of the present invention, comprises the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 95r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, coptis extract, Flos Pelargonii Hortori, Herba Patriniae extract, hippophae rhamnoides, angelica extract Stirred and evenly mixed with aminoglucose hydrochloride, stir speed (S.S.) is 95r/min, obtain facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 38min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
The preparation method of wherein matrimony vine facial mask is as follows:Fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:Dry wolfberry and water are pressed into quality Than 1:8 mixing fully mashing, based on liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, manganese sulfate 0.5% sterilizes after fully mixing, inoculation yeast bacterium.It is placed on shaking table 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C.Fermentation Chinese wolfberry fruit stoste uses high-pressure pulse electric before filtration sterilization Handled 35 minutes with ultrasonic synergistic, then by the fermenation raw liquid filtration sterilization, reserve the supernatant rich in Chinese-wolfberry nutritive composition, Adjust pH value to neutrality, saccharomycete is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixing, obtains matrimony vine hair Zymotic fluid.
Herba Patriniae extract, hippophae rhamnoides, angelica extract, the extracting method of coptis extract and Flos Pelargonii Hortori For:After the extract that will be prepared is crushed, add volume fraction and filtered for 95% ethanol solution;Then after filtered fluid is concentrated It is placed on large pore resin absorption column, after the ethanol solution elution of same volume fraction, dries and obtain the extract.
Embodiment 6
The present invention salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, by weight, including composition it is as follows:
30 parts of pure water;
28 parts of fermentation Chinese wolfberry fruit liquid;
3 parts of polyglutamic acid;The molecular weight of polyglutamic acid is 950,000
0.4 part of vitamin C;
16 parts of asparagus juice;
12 parts of pearl powder;
0.5 part of propane diols;
3 parts of chitosan oligomer;Molecular weight is 1600;
8 parts of coptis extract;
5 parts of Flos Pelargonii Hortori;
2 parts of aminoglucose hydrochloride;
5 parts of pulullan polysaccharide;The molecular weight of pulullan polysaccharide is 300,000;
4 parts of Herba Patriniae extract;
6 parts of hippophae rhamnoides;
3 parts of angelica extract;
The preparation method of the salubrious oil-control fermentation Chinese wolfberry fruit liquid level film of the present invention, comprises the following steps:In prepared by matrimony vine facial mask The addition of each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 95r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, sequentially adds vitamin C, propane diols, pulullan polysaccharide and matrimony vine Zymotic fluid, chitosan oligomer, coptis extract, Flos Pelargonii Hortori, Herba Patriniae extract, hippophae rhamnoides, angelica extract Stirred and evenly mixed with aminoglucose hydrochloride, stir speed (S.S.) is 95r/min, obtain facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 38min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
The preparation method of wherein matrimony vine facial mask is as follows:Fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:Dry wolfberry and water are pressed into quality Than 1:8 mixing fully mashing, based on liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, manganese sulfate 0.5% sterilizes after fully mixing, inoculation yeast bacterium.It is placed on shaking table 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C.Fermentation Chinese wolfberry fruit stoste uses high-pressure pulse electric before filtration sterilization Handled 30 minutes with ultrasonic synergistic, then by the fermenation raw liquid filtration sterilization, reserve the supernatant rich in Chinese-wolfberry nutritive composition, Adjust pH value to neutrality, saccharomycete is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixing, obtains matrimony vine hair Zymotic fluid.
Herba Patriniae extract, hippophae rhamnoides, angelica extract, the extracting method of coptis extract and Flos Pelargonii Hortori For:After the extract that will be prepared is crushed, add volume fraction and filtered for 40% ethanol solution;Then after filtered fluid is concentrated It is placed on large pore resin absorption column, after the ethanol solution elution of same volume fraction, dries and obtain the extract.
Comparative example 1
A kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, its salubrious oil-control fermentation Chinese wolfberry fruit liquid level film prepared with embodiment 6 Difference, which is only that, does not contain chitosan oligomer and aminoglucose hydrochloride.
Comparative example 2
A kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, its salubrious oil-control fermentation Chinese wolfberry fruit liquid level film prepared with embodiment 6 Difference, which is only that, does not contain coptis extract and Flos Pelargonii Hortori.
Comparative example 3
A kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, its salubrious oil-control fermentation Chinese wolfberry fruit liquid level film prepared with embodiment 6 Difference, which is only that, does not contain polyglutamic acid.
Performance detection
Rationally, property is stable for the face pack prescription of the repair function that the present invention is provided, action temperature and, no skin irritation, and By the synergy of various active ingredients, the effects such as with significant repair;
First, human skin patch
With reference to the Ministry of Public Health《Cosmetics health specification》In (version in 2007) related request of " human skin patch " and Method carries out " human body skin enclosed type patch test ".
1st, given the test agent:The facial mask stoste that the embodiment of the present invention 6, comparative example 1-3 are prepared.
2nd, test method:The volunteer that selection 140 meets inclusion criteria participates in experiment, is randomly divided into 4 groups, every group 35 People.From 4 layers of 1cm2The gauze facial mask stoste of size is soaked, and gauze is pasted on into trial volunteer with non-stimulated adhesive tape cloth The bent side of forearm, gently pressed with palm and be allowed to equably be pasted on skin, tested material spot examination device is removed after 24h, respectively at Dermoreaction is observed after 30min, 2h, 4h, 24h and 48h, according to《Skin adverse reaction grade scale table》Record reaction result.
3rd, result of the test:Embodiment 6, the result of the test of all trial volunteers of comparative example 1-3 groups are negative findings, by This can determine that the facial mask of repair function prepared by the embodiment of the present invention 6, comparative example 1-3 is safe without skin adverse reaction.
2nd, salubrious oil-control meter anti-acne effect is evaluated
1st, given the test agent:The facial mask stoste that the embodiment of the present invention 6, comparative example 1-3 are prepared.
2nd, select 140 volunteers for meeting inclusion criteria to participate in experiment, be randomly divided into 4 groups, every group of 35 people, embodiment 6, Each 35 people of comparative example 1-3 groups, during experiment, experiment position disables any external application thing and/or cosmetics, and subject respectively will be tested Sample and the sample of comparative example 1,2,3 are applied to face respectively, daily in the morning, afternoon and evening it is each once, for three days on end, test is red and swollen and shouting pain is disappeared Rate, it is as a result as shown in table 1 below:
(1) refer to《New Chinese medicine guideline of clinical investigations》, Evaluation of Synthetic Effect of Holistic is with skin damaged degree, skin damaged distribution, disease Shape, the total mark of sign calculate curative effect rate.Skin damaged before curative effect=(skin damaged is counted after skin damaged counting-treatment before treatment)/treatment Count * 100%.Cure:Skin damaged regression more than 90%, only a little pigmentation;It is effective:Skin damaged regression 60%~90%, disease Shape mitigates;Effectively:Skin damaged regression 20%~60%, symptom improves;It is invalid:Skin damaged disappears<20%, clinical symptoms do not improve.
(2) fat secretion decrement is tested:Detected respectively with grease measuring instrument using before product and small using product 24 Shi Hou, skin surface fat content calculates the decrement of skin surface fat content, averaged.
(3) lasting fat secretion decrement:It is continuous to use product 1 week, contained with grease measuring instrument detection skin surface grease Amount, disables product, waits after 28 days, then detects skin surface fat content, calculates the lasting fat secretion decrement of skin, makes even Average.
(4) time of acne is cured:Using product, the healing time used is looked into sight, averages.
The salubrious oil control and acne removal effect assessment of the embodiment 6 of table 1 and comparative example 1-3 groups
3rd, sensory evaluation
1st, given the test agent:The facial mask stoste that the embodiment of the present invention 6, comparative example 1-3 are prepared.
2nd, test method:The volunteer that selection 140 meets inclusion criteria participates in experiment, is randomly divided into 4 groups, every group 35 People, each 35 people of embodiment 6, comparative example 1-3 groups.Each group trial volunteer tries out above-mentioned given the test agent respectively, continuous to use one Month, try out after terminating, the using effect such as each trial volunteer this self-assessment moisturizing, whitening, sun-proof, overall assessment is done sense organ and commented Valency, according to using effect in a 0-10/marking, 9-10 points are fine, and 7-8 points are preferable, and 5-6 points are general, and 3-4 points are Poor, 1-2 points are very poor, are averaged.
3rd, result of the test:It is shown in Table 2.
The repairing effect evaluation of the embodiment 6 of table 2 and comparative example 1-3 groups
Group Embodiment 1 Comparative example 1 Comparative example 2 Comparative example 3
Moistening effect 9.0 8.5 8.4 8.0
Whitening effect 8.5 8.3 8.3 8.3
Anti-acne repairing effect 9.2 8.2 8.0 8.1
Clearly without greasy feeling 9.0 8.9 8.9 9.0
Assimilation effect 8.9 8.9 8.9 8.9
Overall assessment 9.0 8.5 8.3 8.2
As can be known from the results of Table 2, the accreditation of the skin care item of salubrious oil control and acne removal repair function prepared by the embodiment of the present invention 6 Degree is high, and using effect is evaluated high.The present invention prepares salubrious oil control and acne removal facial mask and repairs anti-acne effect significantly, after use, flesh Skin is salubrious without greasy feeling, good absorbing effect.After continuously using one month, trial volunteer's dry skin, epidermal pigment calmness etc. Phenomenon is obviously improved.In process of the test, trial volunteer is without allergy or other skin adverse reactions.Contrast 1-3 is prepared The using effect of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film be not so good as the reparation facial mask for preparing of embodiment 6.
Above content is to combine specific preferred embodiment further description made for the present invention, it is impossible to assert The specific implementation of the present invention is confined to these explanations.For general technical staff of the technical field of the invention, On the premise of not departing from present inventive concept, some simple deduction or replace can also be made, should all be considered as belonging to the present invention's Design.

Claims (10)

1. a kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film, it is characterized in that:The salubrious oil-control fermentation Chinese wolfberry fruit liquid level film includes spun lacing The facial mask stoste of non-woven fabrics Face film towel and infiltration on spunlace non-woven cloth;The facial mask stoste includes the group of following parts by weight Point:
25-40 parts of pure water;
20-35 parts of fermentation Chinese wolfberry fruit liquid;
2-4 parts of polyglutamic acid;
0.3-0.5 parts of vitamin C;
15-20 parts of asparagus juice;
10-15 parts of pearl powder;
0.3-0.8 parts of propane diols;
2-5 parts of chitosan oligomer;
5-10 parts of coptis extract;
3-6 parts of Flos Pelargonii Hortori;
1-3 parts of aminoglucose hydrochloride;
3-7 parts of pulullan polysaccharide;
3-5 parts of Herba Patriniae extract
4-7 parts of hippophae rhamnoides
2-6 parts of angelica extract
The molecular weight of the polyglutamic acid is 91-101 ten thousand.
2. salubrious oil-control fermentation Chinese wolfberry fruit liquid level film according to claim 1, it is characterised in that point of the chitosan oligomer Son amount is 1300-1600;Fermentation Chinese wolfberry fruit liquid is red fermentation Chinese wolfberry fruit liquid.
3. salubrious oil-control fermentation Chinese wolfberry fruit liquid level film according to claim 1, it is characterised in that the fermentation Chinese wolfberry fruit liquid fermentation Shi Caiyong saccharomycete is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:The saccharomycete of 1 mixing.
4. salubrious oil-control fermentation Chinese wolfberry fruit liquid level film according to claim 1, it is characterised in that the particle diameter of the pearl powder is 100-200nm;The molecular weight of the pulullan polysaccharide is 20-40 ten thousand.
5. according to any described salubrious oil-control fermentation Chinese wolfberry fruit liquid level film of claim 1, it is characterised in that the facial mask stoste bag Include the component of following parts by weight:30 parts of pure water, 28 parts of fermentation Chinese wolfberry fruit liquid, 3 parts of polyglutamic acid, 0.4 part of vitamin C, aloe 16 parts of juice, 12 parts of pearl powder, 0.5 part of propane diols, 3 parts of chitosan oligomer, 8 parts of coptis extract, 5 parts of Flos Pelargonii Hortori, ammonia 3 parts of 2 parts of base glucosamine salt hydrochlorate, 5 parts of pulullan polysaccharide, 4 parts of Herba Patriniae extract, 6 parts of hippophae rhamnoides and angelica extract; The molecular weight of the polyglutamic acid is 950,000.
6. the preparation method of the salubrious oil-control fermentation Chinese wolfberry fruit liquid level film as described in claim 1-5 is any, it is characterized in that, including with Lower step:
(1)Polyglutamic acid and pearl powder are dissolved in pure water, and stirred, thick liquid is become;
(2)Asparagus juice is added in aforesaid liquid, vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit is sequentially added Liquid, chitosan oligomer, coptis extract, Flos Pelargonii Hortori, Herba Patriniae extract, hippophae rhamnoides, angelica extract and ammonia Base glucosamine salt hydrochlorate is stirred and evenly mixed, and obtains facial mask stoste;
(3)Soaked after the sterilizing of facial mask stoste, then by spunlace non-woven cloth Face film towel in facial mask stoste, then Vacuum Package, system Obtain matrimony vine facial mask.
7. the preparation method of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film according to claim 6, it is characterised in that:The matrimony vine The preparation method of zymotic fluid is:By dry wolfberry and water in mass ratio 1:The abundant mashing of 8-15 mixing, based on liquid, to basal liquid It is middle to add following percentage by weight material:Anhydrous magnesium sulfate 0.5-1%, dipotassium hydrogen phosphate 0.03-0.1%, manganese sulfate 0.5-1%, fill Divide after mixing and sterilize, inoculation yeast bacterium;180rpm on shaking table is subsequently placed in, 30 DEG C, 48h is cultivated, obtains fermentation Chinese wolfberry fruit stoste;Will The fermenation raw liquid filtration sterilization, retains supernatant and the pH value of supernatant is adjusted into neutrality, obtain fermentation Chinese wolfberry fruit liquid.
8. the preparation method of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film according to claim 6, it is characterised in that:Step(1) Or step(2)The stir speed (S.S.) used during middle stirring is 80-100r/min;Step(3)The time of middle immersion is 30-40min.
9. the preparation method of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film according to claim 6, it is characterised in that:Field pennycress carries The extracting method for taking thing, hippophae rhamnoides, angelica extract, coptis extract and Flos Pelargonii Hortori is:What will be prepared carries Take after thing crushing, add volume fraction and filtered for 30%-95% ethanol solution;Then macroporous absorption is placed in after filtered fluid is concentrated On resin column, after the ethanol solution elution of same volume fraction, dry and obtain the extract.
10. the preparation method of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film according to claim 7, it is characterised in that:The Chinese holly Qi fermenation raw liquid is handled 15-35 minutes before filtration sterilization using high-pressure pulse electric and ultrasonic synergistic.
CN201710547637.6A 2017-07-06 2017-07-06 A kind of salubrious oil-control fermentation Chinese wolfberry fruit liquid level film and preparation method thereof Pending CN107308094A (en)

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