CN109010130A - A kind of polyethylene glycol oxide skin care mask carriers substrate and preparation method thereof - Google Patents

A kind of polyethylene glycol oxide skin care mask carriers substrate and preparation method thereof Download PDF

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Publication number
CN109010130A
CN109010130A CN201811063864.2A CN201811063864A CN109010130A CN 109010130 A CN109010130 A CN 109010130A CN 201811063864 A CN201811063864 A CN 201811063864A CN 109010130 A CN109010130 A CN 109010130A
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polyethylene glycol
glycol oxide
preparation
facial mask
water
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崔跃飞
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South China University of Technology SCUT
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South China University of Technology SCUT
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55Phosphorus compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/604Alkylpolyglycosides; Derivatives thereof, e.g. esters
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

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  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
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  • Cosmetics (AREA)

Abstract

A kind of polyethylene glycol oxide skin care facial mask liquid base and preparation method thereof of disclosure of the invention.The preparation method includes following component (parts by weight meter): polyethylene glycol oxide (PEO) 5-15;Pulullan polysaccharide 3-10;Ethoxy urea 5-10;Glycerol 3-10;Propylene glycol 3-8;Sucrose ester 0.5-2.0;Imidazolidinyl urea 0.1-0.3;P-hydroxybenzoate 0.1-0.3;Essence 0.1-0.3;Distilled water 300-500.After being uniformly mixed after each component metering, phytic acid is added and carries out PH adjusting, adjusting aqueous ph value is 7.0.As polyethylene glycol oxide (PEO) skin care facial mask liquid base.The facial mask liquid base good film-forming property, docile and obedient property is good, fissility is good;Transparent dense, ventilative, soft comfortable after film forming;And it can be to the lasting moisturizing of human skin.

Description

A kind of polyethylene glycol oxide skin care mask carriers substrate and preparation method thereof
Technical field
The present invention relates to the preparations and application field of mask carriers material in skin care, cosmetics, and in particular to a kind of polyoxy Change ethylene (PEO) skin care facial mask liquid base and preparation method thereof.
Background technique
With social progress and improvement of living standard, using the functions such as beauty, health care, comfortable, leisure as the beauty of representative Hold face-mask material and the powerful market demand occur, the face-mask material in skin care field is rapidly developed to be substituted with new technology. While beauty, moisturizing and other effects are provided, the special efficacies such as facial mask product also has elimination fatigue, relieves stress.
Facial mask becomes the deep skin-protection product welcome by people seeking beauty because of the advantages such as its is easy to carry, effect is obvious.Facial mask is made With mechanism including the following three aspects: 1. facial mask passes through the contact obstructed skin with air, inhibits evaporation of perspiration, keeps facial skin The sufficient nutrition of skin and moisture enhance the elasticity and vigor of skin;2. large quantity of moisture can sufficiently moisturize the skin cutin in facial mask Layer, enhances the penetration of cuticula, so that the nutriment in facial mask is effectively infiltered skin, promote Epithelial cell Metabolism;3. facial mask has adhesion, when throwing off facial mask, skin dirt is (epidermal cell metabolin, extra sebum, residual Adornment etc.) with facial mask sticky removing, keep skin follicle unobstructed, sebum is smoothly discharged.Therefore, as long as scientific and reasonable use facial mask, just Skin water shortage and low and deep can be effectively improved, microgroove is reduced and generate, delay skin aging, and play to a certain extent dispel spot and The effect of acne.
There are many classification methods of facial mask, can be classified as moisture saver mask, facial masks for whitening faces and removing spots, crease-resistant according to facial mask effect Facial mask, Deacne pack, cleaning pack, compact pore facial mask etc.;There are many patent report in terms of in relation to facial mask effect, such as CN203915533U, CN104337735A, CN106580719A, CN105919916A, CN106074233A, CN105748302A, CN106309282A, CN105596281A, CN106511207A, CN105616326A, CN106265445A, CN106265453A, CN105943482A, CN106309320A, CN106511240A, CN105963227A, CN106726632A, CN106309321A, CN106344484A, CN106265454A, CN106265446A, CN105055293A, CN105534770A, CN104856912A, CN104958238A, CN104856909A, CN105147576A, CN104069052A, CN104688615A, CN104652039A, CN103405374A, CN102232913A etc. concentrate on the various function that facial mask is realized by peculiar preparation and nutrient solution etc. Energy;Peel off pack, cream pack, powder face pack and wet cloth shape facial mask can be divided into according to the dosage form classification of facial mask;According to facial mask Carrier medium can be divided into mounted wet cloth shape facial mask and non-mounted facial mask;Mantle and dura mater can be divided into according to physicochemical property.
Mask carriers material can be divided into two major classes according to usage mode: non-mounted facial mask and mounted facial mask, non-mounted facial mask Be mainly water-soluble thickener at membrane material, mounted facial mask at membrane material include non-woven fabrics, silk, biological fiber, tencel and Bamboo charcoal fiber etc.;Related patent report such as CN105287354A, CN105287354A, CN104337736A, CN101491486、CN101332158、CN101386877、CN101361700、CN104337736A、CN105437667A、 CN106265322A、CN106038407A、CN105496906A、CN105726354A、CN105560071A、 CN106551806A、CN105232354A、CN104490626A、CN104958223A、CN104840407A、 CN105088543A、CN104762756A、CN105088532A、CN206183677U、CN104562440A、 CN204379815U、CN105616170A、CN103976897A、CN203496359U、CN104812374A、 CN103126909A、CN203354927U、CN105228488A、CN103041440A、CN102988197A、 CN202682388U、CN102670415A、CN102940583A、CN102505183A、CN105401337A、CN104593945A Deng being all the preparation for belonging to mask carriers substrate.
1 mounted mask carriers material
At present on the market common mounted mask carriers material include non-woven fabrics, silk, concept stealth silk, hydrogel, Pure cotton fiber, biological fiber, viscose rayon, tencel and bamboo charcoal fiber.Non-woven fabrics and skin affinity are bad, and water imbibition is bad, Gas permeability is general, and such as white mask when use, visual impression is poor.A large amount of petroleum resources can be consumed in production process, be not belonging to Environmentally friendly product.Pure cotton fiber is raw material by cotton, and the spun lacing nonwoven fabric structure made of cross lapping method has and inhales The advantages that aqueous good, drawing force is strong, patch skin is good, but cotton-wool easily causes skin allergy.Silk mask base fabric is light, saturating, soft, thin, Therefore patch skin is good, and stealthy effect is good;Meanwhile silk is porous fiber, water imbibition is strong, and penetration is good, and moisturizing degree is common 5-10 times of facial mask.But silk mask base fabric draftability is poor, fragile, molding is bad and at high cost, using being subject to certain restrictions. Concept stealth silk mask is the material of all natural pure silk floss, is the upgrades of non-woven fabrics, has suction as silk mask base fabric It is aqueous it is strong, penetration is good, patch skin is good, and stealthy effect is good;And draftability is strong, can be stretched and be adjusted according to different shapes of face, made The every nook and cranny for covering skin, with silk gloss and silk smooth felling, so referred to as silk mask, is most to be disappeared at present One of favorite facial mask material of the person of expense.Hydrogel facial mask is, the inside non-stimulated to skin using hydrophilic gel as mask matrix Various both effectiveness ingredients (such as arbutin, vitamin E, niacinamide, glutathione ingredient) can be injected and functional face is made Film, while it is strong to paste skin, is not easy to evaporate, dries, the effect releived of bringing down a fever is to acute skin injury (such as allergy, long acne, wiping Wound) there is good result, and one of facial mask more salable at present.Made of biology cellulose facial mask is fermented gluconacetobacter Bacteria cellulose is a kind of natural macromolecular material for having both biodegradability and biocompatibility, has extremely strong water suction Property, patch skin and toughness, wrinkle and skin mound depths can be pasted into, therefore more general cloth surface of second order film has more promotion and skin tightening effect.By In having the characteristic that do not repelled by human body, cardiovascular reparation is used as in medical field and artificial skin uses.But it is raw at present The disadvantages of there are complex process, at high cost, requirements for the production of fibres mask substrate strictly, facial mask filling process is difficult.Bamboo charcoal is fine Tieing up facial mask is to use pure oxygen high temperature and nitrogen barrier delay calcining moso bamboo, then again by its calcined product and with honeycomb micropore The polyester modification slice melt spinning of structure and be made, thus bamboo charcoal fiber facial mask has preferable hygroscopicity, gas permeability and clear Deep layer cleaning effect.Tencel is the upgrade version of viscose rayon, is produced using wood pulp as raw material through solvent spinning process a kind of brand-new Fiber, with cotton " comfort, terylene " intensity ", wool fabric " luxurious aesthetic feeling " and silk " unique sense of touch " and " it is soft Soft vertical pendant ", no matter in the state of dry or wet, great toughness.Although there are many mask substrate type on the market, people also exist Constantly look for the mask substrate raw material and production technology of modern.
2 non-mounted mask carriers materials
Non- mounted facial mask is the key that facial mask is successfully prepared at the selection of membrane material, at present on the market commonly at membrane material It mainly include 4 major class water-soluble thickeners: organic natural water-soluble copolymer, organic semi-synthetic water-soluble polymer, You Jihe At water-soluble polymer, inorganic water-soluble polymer.Organic natural water-soluble copolymer includes vegetalitas colloid class and animality Colloid class, wherein vegetalitas colloid class has starch, tragacanth gum, gum arabic, xanthan gum, pectin, antler glue, agar, brown Mosanom, bletilla striata rubber cement and guar gum etc., animality colloid class include gelatin, chitosan, collagen etc..It is organic semi-synthetic Water-soluble polymer have modified cellulose class (such as carboxymethyl cellulose, hydroxypropyl cellulose, microcrystalline cellulose), guar gum and its Derivative, modified starch series (such as octyl starch butanedioic acid aluminium).Organic synthesis water-soluble polymer includes vinyl (such as polyethylene Alcohol, polyvinylpyrrolidone, polyvinyl methyl ethermaleic anhydride and its copolymer), polyoxyethylene, polyethylene glycol.Inorganic water-soluble polymer Including colloidality aluminium-magnesium silicate, colloidality silica, sodium magnesium silicate, bentonite etc..These water-soluble thickeners be facial mask it is both effectiveness at The good carrier divided reduces moisture of skin evaporation by filming function to promote skin hydration to act on, while non-stimulated to skin, Without allergy, non-toxic reaction, therefore liked deeply by cosmetic formulations teacher and consumer.
The present invention is that primary raw material is prepared for a kind of liquid-type mask carriers substrate, the liquid using polyethylene glycol oxide (PEO) Body carrier substrate has good film-forming property, takes water as a solvent, Environmental Safety, and film strength is high after film forming, and soft comfortable is aided with various Effect component, which can be prepared into, has effects that various cosmetology facial masks.
The mask carriers substrate is a kind of water-soluble viscous solution, has certain mobility, can use when in use Hand is uniformly applied on skin (human skins such as face skin, skin of hand), because having certain flowing levelling before film forming Property, so energy all standing coat, there is no coating dead angles;Naturally, film forming after having coated, be after film forming it is transparent, ventilative, The facial treatment mask of soft comfortable;Coating film is transparent after film forming, has polarity adhesiveness, can be naturally docile and obedient in human skin On, the normal life and work of people are not influenced, and in the case where not needing moisturizing, moisture retention is lasting, can provide for a long time to skin Skin-moisturizing, skin;It easily can completely strip from skin after use, the mask carriers stripped down can be water-soluble, institute It is rinsed with water completely with can directly throw into sewer, there is no rear waste is used, has more environment protection significance.
Summary of the invention
The purpose of the present invention is to provide a kind of (PEO) skin care of polyethylene glycol oxide facial mask liquid base and its preparation sides Method belongs to a kind of liquid-carrier substrate, not only easy to use, can also be directly water-soluble without generating waste after use.
The purpose of the present invention is achieved through the following technical solutions.
A kind of polyethylene glycol oxide (PEO) skin care facial mask liquid base, based on parts by weight, including following component:
Preparation method includes: that will measure in above-mentioned each component, and polyethylene glycol oxide (PEO) is 1. added to >=95 DEG C of distillation In water and stir, while stirring Temperature fall, until polyethylene glycol oxide (PEO) be completely dissolved in water it is transparent;2. then proceeding to Other each components (in addition to phytic acid) are added, stirring and dissolving is uniform;3. measure the pH value of uniformly mixed aqueous solution, be added phytic acid into Row pH is adjusted, and adjusting pH value of water solution is 7.0.As polyethylene glycol oxide (PEO) skin care facial mask liquid base.
Further, the polyethylene glycol oxide (PEO) is molecular weight 1 × 105—1×106Polyethylene glycol oxide;Particular type Number for U.S. combinating carbide company production WSR-N-10, WSR-N-80, WSR-N-750, WSR-N-3000, WSR-N-12k, One of WSR-205, WSR-N-1105 etc..
Further, the pulullan polysaccharide is the stable microbial polysaccharide of a kind of nonionic, irreducibility.Because of it It can be degraded by microorganisms utilization in nature, environmental pollution will not be caused, therefore be known as nuisanceless polysaccharide.Pulullan polysaccharide has Excellent film forming, plasticity, film forming rear film is transparent, colourless, odorless, nontoxic, has toughness, high grease resistance, can eat;And Soluble easily in water, nontoxic, colorless and odorless, and have many characteristics, such as blocking oxygen, pulullan polysaccharide used in the present invention is point Son amount is 200,000 or so commodity.
Further, the ethoxy urea is a kind of moisturizer, and efficient moisture-retention effect can be provided to skin care item simultaneously again Moisturizer without sticky feel, ethoxy urea can penetrate into cuticula, increase the aquation of skin, alleviate drying, fill out Microgroove is mended, increases skin elasticity, and there is very moist skin sense.Simultaneously due to containing amide in ethoxy urea molecule structure Group can form with polyethylene glycol oxide (PEO) be complexed in water, enhance the compatibility to each component.
Further, the glycerol and propylene glycol are added as polyethylene glycol oxide (PEO) stabilized aqueous solution agent, can be pressed down Polyethylene glycol oxide (PEO) processed is in water due to viscosity change caused by degrading.
Further, the sucrose ester refers to C >=8 in fatty acid carbon chain, average esterification degree 1.20-1.55, and monoesters contains The sucrose ester of amount >=60%;S-1570, S-1670, P-1570, P-1670, SW-1570, PW- are produced including Japanese Ling Tang company One of 1570 etc..
Further, the phytic acid is a kind of natural chelators, antioxidant.It can promote oxyhemoglobin in human body The release of middle oxygen improves erythrocyte function, extends the life cycle of erythrocyte;Its hydrolysate be inositol and phosphatide, the former With anti-aging effects, the latter is human body cell important component.
Further, the imidazolidinyl urea and p-hydroxybenzoate are efficient composite anti-corrosives used in the present invention Agent.
Further, the essence is food grade water-soluble essence.
Further, each component raw material selects food grade or pharmaceutical grade.
Compared with prior art, the invention has the advantages that and technical effect:
A kind of polyethylene glycol oxide (PEO) skin care of the present invention has the feature that 1 with facial mask liquid carrier substrate) completely with Water is decentralized medium, environmental protection, safety;2) it can form a film within 15-30 minutes after being coated under natural environment;It can also continue to grow after film forming Time moisturizing;3) because being liquid-carrier, spreadability is good when coating on the skin, can accomplish all standing, naturally docile and obedient in human body On skin, facial mask is transparent dense not to influence appearance;4) transparent dense, ventilative, soft comfortable after forming a film;5) liquid-carrier substrate at Film property is good, and fissility is good;Easily removing after having nursed, because being complete water solubility, even if having a small amount of residual in removing, It can be rinsed well with clear water;6) after liquid-carrier (facial mask) substrate film forming, film layer has complete water soluble characteristic, after use may be used Sewer is water-soluble to drain directly to throw into, and does not pollute the environment, will not remain waste.7) various nutrient solutions and preparation are added Skin care (facial mask) product of various effects can be prepared afterwards.
Specific embodiment
Further specific detailed description, but reality of the invention is made to technical solution of the present invention below in conjunction with specific embodiment It applies mode and protection scope is without being limited thereto.
Embodiment 1
A kind of polyethylene glycol oxide (PEO) skin care facial mask liquid base and preparation method thereof, based on parts by weight (such as it is single Position g), including following component:
It will measure, 1. polyethylene glycol oxide (PEO) is added in >=95 DEG C of distilled water and stirs, side in above-mentioned each component Stir side Temperature fall, until polyethylene glycol oxide (PEO) be completely dissolved in water it is transparent;2. then proceeding to that other each components are added (in addition to phytic acid), stirring and dissolving is uniform;3. measuring the pH value of uniformly mixed aqueous solution, phytic acid is added and carries out pH adjusting, adjusts PH value of water solution is 7.0.As polyethylene glycol oxide (PEO) skin care facial mask liquid base is tested real after forming a film under natural environment It tests such as table 1.
1. embodiment of table, 1 facial mask liquid base test experiments:
From above-mentioned experimental data it is found that the moistening effect of embodiment 1 is clearly in dry environments;And the face after removing Film film layer is completely dissolved time≤60S in water.Use test equipment are as follows: the fine jade that rubs (MOQI) high-definition intelligent skin detection instrument SH- 608。
Embodiment 2
A kind of polyethylene glycol oxide (PEO) skin care facial mask liquid base and preparation method thereof, based on parts by weight, including such as Lower component:
It will measure, 1. polyethylene glycol oxide (PEO) is added in >=95 DEG C of distilled water and stirs, side in above-mentioned each component Stir side Temperature fall, until polyethylene glycol oxide (PEO) be completely dissolved in water it is transparent;2. then proceeding to that other each components are added (in addition to phytic acid), stirring and dissolving is uniform;3. measuring the pH value of uniformly mixed aqueous solution, phytic acid is added and carries out pH adjusting, adjusts PH value of water solution is 7.0.As polyethylene glycol oxide (PEO) skin care facial mask liquid base is tested real after forming a film under natural environment It tests such as table 2.
2. embodiment of table, 2 facial mask liquid base test experiments:
From above-mentioned experimental data it is found that the moistening effect of embodiment 2 is clearly in dry environments;And the face after removing Film film layer is completely dissolved time≤60S in water.Use test equipment are as follows: the fine jade that rubs (MOQI) high-definition intelligent skin detection instrument SH- 608。
Embodiment 3
A kind of polyethylene glycol oxide (PEO) skin care facial mask liquid base and preparation method thereof, based on parts by weight, including such as Lower component:
It will measure, 1. polyethylene glycol oxide (PEO) is added in >=95 DEG C of distilled water and stirs, side in above-mentioned each component Stir side Temperature fall, until polyethylene glycol oxide (PEO) be completely dissolved in water it is transparent;2. then proceeding to that other each components are added (in addition to phytic acid), stirring and dissolving is uniform;3. measuring the pH value of uniformly mixed aqueous solution, phytic acid is added and carries out pH adjusting, adjusts PH value of water solution is 7.0.As polyethylene glycol oxide (PEO) skin care facial mask liquid base is tested real after forming a film under natural environment It tests such as table 3.
3. embodiment of table, 3 facial mask liquid base test experiments:
From above-mentioned experimental data it is found that the moistening effect of embodiment 3 is clearly in dry environments;And the face after removing Film film layer is completely dissolved time≤60S in water.Use test equipment are as follows: the fine jade that rubs (MOQI) high-definition intelligent skin detection instrument SH- 608。
Embodiment 4
A kind of polyethylene glycol oxide (PEO) skin care facial mask liquid base and preparation method thereof, based on parts by weight, including such as Lower component:
It will measure, 1. polyethylene glycol oxide (PEO) is added in >=95 DEG C of distilled water and stirs, side in above-mentioned each component Stir side Temperature fall, until polyethylene glycol oxide (PEO) be completely dissolved in water it is transparent;2. then proceeding to that other each components are added (in addition to phytic acid), stirring and dissolving is uniform;3. measuring the pH value of uniformly mixed aqueous solution, phytic acid is added and carries out pH adjusting, adjusts PH value of water solution is 7.0.As polyethylene glycol oxide (PEO) skin care facial mask liquid base is tested real after forming a film under natural environment It tests such as table 4.
4. embodiment of table, 4 facial mask liquid base test experiments:
From above-mentioned experimental data it is found that the moistening effect of embodiment 4 is clearly in dry environments;And the face after removing Film film layer is completely dissolved time≤60S in water.Use test equipment are as follows: the fine jade that rubs (MOQI) high-definition intelligent skin detection instrument SH- 608。
Embodiment 5
A kind of polyethylene glycol oxide (PEO) skin care facial mask liquid base and preparation method thereof, based on parts by weight, including such as Lower component:
It will measure, 1. polyethylene glycol oxide (PEO) is added in >=95 DEG C of distilled water and stirs, side in above-mentioned each component Stir side Temperature fall, until polyethylene glycol oxide (PEO) be completely dissolved in water it is transparent;2. then proceeding to that other each components are added (in addition to phytic acid), stirring and dissolving is uniform;3. measuring the pH value of uniformly mixed aqueous solution, phytic acid is added and carries out pH adjusting, adjusts PH value of water solution is 7.0.As polyethylene glycol oxide (PEO) skin care facial mask liquid base is tested real after forming a film under natural environment It tests such as table 5.
Table 5,5 facial mask liquid base test experiments of embodiment:
From above-mentioned experimental data it is found that the moistening effect of embodiment 5 is clearly in dry environments;And the face after removing Film film layer is completely dissolved time≤60S in water.Use test equipment are as follows: the fine jade that rubs (MOQI) high-definition intelligent skin detection instrument SH- 608。
The above embodiment is a preferred embodiment of the present invention, but embodiments of the present invention are not by above-described embodiment Limitation, other any changes, modifications, substitutions, combinations, simplifications made without departing from the spirit and principles of the present invention, It should be equivalent substitute mode, be included within the scope of the present invention.

Claims (9)

1. a kind of polyethylene glycol oxide skin care facial mask liquid base, it is characterised in that based on parts by weight, including following component:
Polyethylene glycol oxide 5-15
Pulullan polysaccharide 3-10
Ethoxy urea 5-10
Glycerol 3-10
Propylene glycol 3-8
Sucrose ester 0.5-2.0
Appropriate phytic acid
Imidazolidinyl urea 0.1-0.3
P-hydroxybenzoate 0.1-0.3
Essence 0.1-0.3
Distilled water 300-500.
2. preparing a kind of polyethylene glycol oxide skin care facial mask liquid base described in claim 1, which is characterized in that will be above-mentioned each It measures, 1. polyethylene glycol oxide is added in >=95 DEG C of distilled water and stirs in component, while stirring Temperature fall, until poly- Ethylene oxide is completely dissolved transparent in water;2. then proceeding to other each components being added in addition to phytic acid, stirring and dissolving is uniform;③ The pH value of the uniformly mixed aqueous solution of measurement is added phytic acid and carries out pH adjusting, and adjusting pH value of water solution is 7.0;As polyoxygenated Ethylene skin care facial mask liquid base.
3. preparation method according to claim 2, which is characterized in that the polyethylene glycol oxide is molecular weight 1 × 105 — 1 ×106Polyethylene glycol oxide.
4. preparation method according to claim 2, which is characterized in that the molecular weight of the pulullan polysaccharide is 200,000 left It is right.
5. preparation method according to claim 2, which is characterized in that the glycerol and propylene glycol are as polyethylene glycol oxide Stabilized aqueous solution agent and be added, for inhibit polyethylene glycol oxide in water due to degradation caused by viscosity change.
6. preparation method according to claim 2, which is characterized in that the sucrose ester refers to C >=8 in fatty acid carbon chain, Average esterification degree is 1.20-1.55, the sucrose ester of monoester content >=60%.
7. preparation method according to claim 2, which is characterized in that the imidazolidinyl urea and p-hydroxybenzoate are made For high-efficiency compound preservative.
8. preparation method according to claim 2, which is characterized in that the essence is food grade water-soluble essence.
9. preparation method according to claim 2, which is characterized in that each component raw material selects food grade or medicine Grade.
CN201811063864.2A 2018-09-12 2018-09-12 A kind of polyethylene glycol oxide skin care mask carriers substrate and preparation method thereof Pending CN109010130A (en)

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