CN109350595A - A kind of cosmetics and its preparation method and application containing bird's nest active extract - Google Patents
A kind of cosmetics and its preparation method and application containing bird's nest active extract Download PDFInfo
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- CN109350595A CN109350595A CN201811555086.9A CN201811555086A CN109350595A CN 109350595 A CN109350595 A CN 109350595A CN 201811555086 A CN201811555086 A CN 201811555086A CN 109350595 A CN109350595 A CN 109350595A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The present invention provides a kind of cosmetics and its preparation method and application containing bird's nest active extract.The preparation method of bird's nest active extract, by bird's nest and water by 1:(19-199) mass ratio be soaked 1-3h, 5-30min is sheared at room temperature, it is sheared again after being heated to 50-100 DEG C, keep 5-30min, yarn filters out swallow hair and impurity before cooling, and bird's nest active extract then is made through ultrafiltration.The extraction process for the bird's nest extracting solution being added in cosmetics is simplified, while simplifying the preparation process that bird's nest active extract is compounded with cosmetic base homogeneous.By bird's nest extracting solution (aqueous solution of bird's nest active component content 0.45%-4.5%) it is not spray-dried or freeze-drying directly with cosmetic base homogeneous, reduce drying process bring energy consumption.Bird's nest extracting solution Sialic acid rich in, amino acid, active peptide and microelement have significant cosmetology effect, just because of these effects, further simplify its technique for cooperateing with compounding with other active materials.
Description
Technical field
The invention belongs to cosmetic technical field, more particularly to a kind of cosmetics containing bird's nest active extract, with
And the preparation method of the cosmetics, also change the application of cosmetics.
Background technique
Skin is the outermost layer tissue of human body, and in general keratoderma water content can just make between 10%-20%
Skin surface is wet, smooth, high resilience.Maintain the normal moisture content of cuticula for keeping skin health, moisturizing, pre-
Anti- skin aging plays an important role.In addition, free radical is also the major reason for leading to skin aging.With people's living standard
It improves, there are anti-oxidant and moisture-keeping functions cosmetics to have become wherein indispensable a part.Therefore, there is an urgent need to develop
It is a kind of to use natural active matter as raw material and with anti-oxidant and moisture-keeping functions skin-protection product.
Bird's nest is that the saliva of esculent swift (Apodidae) secretion and its down mixing bond built up nest.Bird's nest mainly contains
There are the nutriments such as sialic acid, glycoprotein, minerals.Research shows that the polysaccharide in bird's nest, can be improved the immunity of Skin Cell,
The self-regulating function for protecting skin prevents water loss, resists ultraviolet damage, eliminates skin surface free radical, increases skin
The synthesis of skin collagen, cutin-softening layer promote blood circulation and skin regeneration, can play wrinkle resistant, sun-proof, anti-radiation, beautiful
The effect of white, nti-freckle, delay skin aging.The amino acid that obtains after protein hydrolysis in bird's nest, peptides, Sialic acid is to body
Growth and development, metabolism, disease and aging play most crucial effect, had been demonstrated apparent moisturizing oil-control,
Exfoliating, the activity for inhibiting tyrosinase, the effect for enhancing skin immune function controlling, delay skin aging.Therefore, important in bird's nest
Active matter Quality Research, exploitation, using with tempting bright prospects.
Summary of the invention
It is rare for the cosmetics of active extract containing bird's nest present in existing cosmetics category, it has a single function or does not show
It writes, has effects that the problems such as component of beauty and skin care is not discovered and used sufficiently in bird's nest, the present invention is using bird's nest as natural activity
Substance prepares cosmetics, has good anti-aging, moisturizing and anti-oxidation function.And provide a kind of preparation of technique it is simple,
Active component is abundant, obvious effect, the category multiplicity cosmetics containing bird's nest active extract.
The preparation method of bird's nest active extract, by bird's nest and water by 1:(19-199) mass ratio be soaked 1-3h, room temperature
Lower shearing 5-30min, revolving speed 10000-40000r/min are sheared again after being heated to 50-100 DEG C, revolving speed 10000-
40000r/min, keeps 5-30min, and cooling preceding yarn filters out swallow hair and impurity, bird's nest active extract then is made through ultrafiltration.
The bird's nest active extract as made from above-mentioned preparation method, the admittedly solidifying content of freeze-drying is 0.45wt%-4.5wt%,
It is removed other than moisture, mainly contains Sialic acid, active glycopeptide, free amino acid and microelement.
Cosmetics are made in above-mentioned bird's nest active extract, the bird's nest active extract accounts for the 0.5wt%- of total weight
1wt%.
It further, further include Sodium Hyaluronate 0.05wt%-1wt%, vitamin C 1wt%-10wt% in the cosmetics,
Surplus is cosmetic base.The dosage form of cosmetics can be cream, lotion, aqua, gel, aerosol or facial mask.
Cosmetics containing bird's nest active extract can be applied to the clean of face, eye circumference, lip, neck, trunk or four limbs
Skin, skin care.
Sialic acid and free amino acid rich in, Sialic acid energy in bird's nest active extract disclosed in the technical program
Delaying human body caducity promotes epidermal growth, promotes cell division, antiviral and other effects.It include leucine, silk in free amino acid
Propylhomoserin, threonine, glycine, alanine, proline, arginine, glutamic acid, tyrosine, phenylalanine etc..Leucine can add
The metabolism of fast Skin Cell promotes skin tissue regeneration and healing;Serine can increase epidermal cell vigor and moisturizing, prolong
Slow skin aging, prevents scurf from generating.Serine, threonine, glycine and alanine are the natural moisturizing factors of skin.Sweet ammonia
Acid, alanine and proline are the constituents of collagen;Arginine can promote blood flow, vasodilator, promote new old
Metabolism.Glutamic acid has antioxidant activity, can promote the differentiation and proliferation of cell, promotes the life of wound healing and collagen
At.In addition, tyrosine, phenylalanine, arginine, proline are ultraviolet absorbers, there is the ability for absorbing ultraviolet light.
The cosmetics of the active extract containing bird's nest have better moisture-keeping efficacy in the present invention, and can be reduced scattering and disappearing for moisture
Amount.After continuous use 2 months, the elasticity of skin, crease-resistant, compactness, drying, roughness, itch, skin blemishes and skin
Color has apparent improvement, and cosmetology effect is comprehensive, suitable for water shortage, the skin quality that elasticity is insufficient, wrinkle is more.
Raw materials used China's correlation bird's nest that meets is using standard, and quality guarantee is safe and non-toxic, and source is sufficient.Extracting work
Using being soaked in skill, high speed shear is heated, and high speed shear goes out the substances quick release such as Sialic acid, amino acid and microelement
Come.Ultrafiltration technology is simple, and active matter loss is few, and yield is 90% or more.
Simplify the extraction process for the bird's nest extracting solution being added in cosmetics, at the same simplify bird's nest active extract with
The preparation process of cosmetic base homogeneous compounding.By bird's nest extracting solution, (bird's nest active component content 0.45%-4.5%'s is water-soluble
Liquid) it is not spray-dried or freeze-drying directly with cosmetic base homogeneous, reduce drying process bring energy consumption.Swallow
Nest extracting solution Sialic acid rich in, amino acid, active peptide and microelement have significant cosmetology effect, just because of
These effects further simplify its technique that compounding is cooperateed with other active materials.
After the cosmetics of the active extract containing bird's nest cooperate with compounding with Sodium Hyaluronate and vitamin C, it is significantly enhanced
Cosmetology effect substantially increases it and is going wrinkle, moisturizing, improving the function such as the colour of skin, improvement skin elasticity, removal face's flaw
Effect.
Specific embodiment
In the examples where no specific technique or condition is specified, according to the literature in the art described technology or conditions or
Person carries out according to product description.Reagents or instruments used without specified manufacturer, being can be by the normal of commercially available acquisition
Advise product.
Embodiment 1:
It takes and meets China's correlation bird's nest in right amount using the edible bird's nest of standard, add the water of 19 times of quality, be soaked 1h, room temperature
Lower high speed shear 5min, revolving speed 40000r/min are heated to 50 DEG C, at the same time high speed shear, revolving speed 40000r/min,
5min is kept, yarn filters out swallow hair and impurity while hot, bird's nest active extract (aqueous solution) is made after ultrafiltration, bird's nest active component
Content is 4.5%, for use.
The preparation of oily phase: raw material according to the mass fraction, cetostearyl alcohol 3, monoglyceride 2, shea butter 3, poly dimethyl silicon
Oxygen alkane 2, glycerol three (thylhexoic acid) ester 10.By the above material mixing, it is stirred and heated to 75-80 DEG C, dissolution obtains oily phase, to
With.
The preparation of water phase: raw material according to the mass fraction, bird's nest active extract 22, deionized water 46.5, glycerol 3, the third two
Alcohol 5, laruyl alcohol sodium phosphate 2, laruyl alcohol sodium sulfovinate 0.1, carbomer 0.2.By bird's nest active extract, propylene glycol and glycerol
It is add to deionized water, is stirred and heated to 80-90 DEG C, keep 20min sterilizing, be cooled to 75-80 DEG C, water phase is added, and remaining is former
Material, stirring and dissolving uniformly obtain water phase, for use.
Two-phase mixtures: raw material according to the mass fraction, oily phase 20, water phase 78.8, preservative 0.8, triethanolamine 0.2, essence
0.2.The oil prepared is added to water phase to mix, is cooled to room temperature after homogeneous stirring, three ethyl alcohol of neutralizer is added at the same time
The cream containing 1% bird's nest active component is made in amine, preservative, essence.
Homogeneous fine and smooth, glossy, the stable, grease of cream of present embodiment configuration does not separate.Coated in face, lip
The positions such as week, trunk and four limbs, are easy to be absorbed, and after continuous use one month, dry, cracking skin becomes water profit light
It is sliding.
Embodiment 2:
It takes and meets China's correlation bird's nest in right amount using the edible bird's nest of standard, add the water of 99 times of quality, be soaked 2h, room temperature
Lower high speed shear 20min, revolving speed 25000r/min are heated to 75 DEG C, at the same time high speed shear, revolving speed 25000r/
Min keeps 20min, and yarn filters out swallow hair and impurity while hot, and bird's nest active extract (aqueous solution) is made after ultrafiltration, and bird's nest is living
Property constituent content be 0.9%, for use.
The preparation of oily phase: raw material according to the mass fraction, cetostearyl alcohol 1.5, monoglyceride 1, dimethyl silicone polymer 2, carbon
Dioctyl phthalate 3, glycerol three (thylhexoic acid) ester 5.By the above material mixing, it is stirred and heated to 75-80 DEG C, dissolution obtains oily phase,
For use.
The preparation of water phase: according to the mass fraction, bird's nest active extract 55.6, glycerol 5, is gone Sodium Hyaluronate 0.1 raw material
Ionized water 23.2, xanthan gum 0.1, laruyl alcohol sodium phosphate 2, laruyl alcohol sodium sulfovinate 0.1, carbomer 0.2.Bird's nest activity is mentioned
It takes liquid, glycerol to be add to deionized water, is stirred and heated to 80-90 DEG C, keep 20min sterilizing, be cooled to 75-80 DEG C, be added
Remaining raw material of water phase, stirring and dissolving uniformly obtain water phase, for use.
Two-phase mixtures: raw material is according to the mass fraction, oily phase 12.5, water phase 86.3, preservative 0.8, triethanolamine 0.2, fragrant
Essence 0.2.At 75-80 DEG C, the oil phase is added to the aqueous phase mixing homogeneous 20min, homogeneous stirring after be cooled to room temperature, at the same time plus
Enter preservative and neutralizer triethanolamine, essence, the lotion containing 0.5% bird's nest active component is made.
The lotion feel of present embodiment configuration is fine and smooth, whom has do not separate, is coated with uniform, easily absorption.Be applied to face,
Neck, after eye circumference one month, skin lines shoal, expression line disappear.
Embodiment 3
It takes and meets China's correlation bird's nest in right amount using the edible bird's nest of standard, add the water of 199 times of quality, be soaked 3h, room
Temperature lower high speed shear 30min, revolving speed 10000r/min, are heated to 100 DEG C, at the same time high speed shear, revolving speed 10000r/
Min keeps 30min, and yarn filters out swallow hair and impurity while hot, and bird's nest active extract (aqueous solution) is made after ultrafiltration, and bird's nest is living
Property constituent content be 0.45%, for use.
Preparation method: raw material according to the mass fraction, bird's nest active extract 11, Sodium Hyaluronate 0.1, butanediol 3, glycerol
3, deionized water 79.03, propylene glycol 3, Chlorphenesin 0.2, methyl esters 0.1, Phenoxyethanol 0.25, solubilizer 0.3, essence 0.02.
Bird's nest active extract, glycerol are add to deionized water, are stirred and heated to 80-90 DEG C, 20min sterilizing is kept, is cooled to
It 75-80 DEG C, is added after Sodium Hyaluronate is dispersed with butanediol, stirring and dissolving, is cooled to 50 DEG C hereinafter, for A phase, for use.
By propylene glycol, Chlorphenesin, methyl esters, Phenoxyethanol be heated to 60-65 DEG C be uniformly dissolved after, be cooled to 50 DEG C with
Under, it is B phase, for use.
Solubilizer, essence are uniformly mixed under room temperature state, are C phase, for use.
A, B, C are mixed: being stirred evenly, is aged, is made and containsBird's nest active component, 0.1% Sodium Hyaluronate
Aqua.
The aqua transparency of present embodiment configuration is high, without precipitating, non-stimulated.After being applied to face and neck one month, skin
Skin moistens flexible, and skin line shoals, and spot disappears, pale bright.
Embodiment 4
According to the method for preparing bird's nest active extract in embodiment 3, bird's nest active component content, which is prepared, is
0.45%, for use.
Raw material according to the mass fraction, bird's nest active extract 22, Sodium Hyaluronate 0.1, allantoin 0.1, glycerol 2, the third two
Alcohol 5, preservative 0.55, deionized water 69.1, ammonium acryloyl taurate/VP copolymer 0.8, solubilizer 0.3, essence
0.05。
Deionized water is added in vacuum emulsification pot, ammonium acryloyl taurate/VP copolymer is heated with stirring to 80
DEG C dissolution, will then be added after propylene glycol dispersed transparent matter acid sodium, sequentially adds glycerol, allantoin, 20min is stirred, to temperature
When dropping to 45 DEG C, bird's nest active extract is added, stirs 10min, sequentially adds preservative, solubilizer and essence, stirring is taken out true
The gel containing 0.1% bird's nest active component is made in sky.
Embodiment 5
According to the method for preparing bird's nest active extract in embodiment 3, bird's nest active component content, which is prepared, is
0.45%, for use.
Raw material according to the mass fraction, bird's nest active extract 2.2, Sodium Hyaluronate 0.01, Vc1,75% ethyl alcohol 10, go from
Sub- water 86.24, essence 0.05, preservative 0.5.Bird's nest active extract is added in deionized water under room temperature, is sequentially added
Bright matter acid sodium, Vc, 75% ethyl alcohol, essence and preservative are madeBird's nest active component, 0.01% Sodium Hyaluronate, 1%Vc's
Aerosol.
Embodiment 6
According to the method for preparing bird's nest active extract in embodiment 3, bird's nest active component content, which is prepared, is
0.45%, for use.
Raw material according to the mass fraction, bird's nest active extract 1.1, Sodium Hyaluronate 0.1, Vc1, hydroxyethyl cellulose 0.1,
Glycerol 1, propylene glycol 3, butanediol 3, carbomer 0.1, triethanolamine 0.1, deionized water 90, preservative 0.5.By bird's nest under room temperature
Active extract is added in deionized water, sequentially adds Sodium Hyaluronate, hydroxyethyl cellulose, and it is equal to be heated to 75-80 DEG C of stirring
Matter dissolution, stirs 10min, is cooled to 45 DEG C hereinafter, sequentially add Vc, 75% ethyl alcohol, essence and preservative, is madeSwallow
Nest active component, 0.1% Sodium Hyaluronate, 1%Vc facial mask.
After freeze-dried to bird's nest active extract of the invention, constituent analysis is carried out, the results are shown in Table 1.
Principle components analysis after the freeze-drying of 1 bird's nest active extract of table
Antioxidant activity is analyzed after freeze-dried to bird's nest active extract of the invention, the results are shown in Table 2.
2 bird's nest active extract antioxidant activity of table
Free radical scavenging activity is measured under conditions of 5mg/mL.
The present invention prepares the cosmetics of the active extract containing bird's nest as follows: being containing for 0.45%-4.5% by concentration
Directly cream, lotion, aqua, gel, aerosol or facial mask is made with cosmetic base homogeneous in bird's nest active extract.The present invention
Cosmetics it is homogeneous, glossy, spreadability is good, stability is good, skin easily absorbs, not allergy.
Choose 80 healthy volunteers, each half of men and women, the age between 20-60 years old, no immune deficiency or immune
Property disease, without serious systemic disease, without anaphylactia, to cosmetics without allergy history, non-long-term steroid class drug in nearly January
Or immunosuppressor, other clinical trials are not participated in, do not smear other cosmetics.It is mentioned to produced by the present invention containing only bird's nest activity
Take the cosmetics of liquid, containing only the cosmetics of bird's nest active extract and hyalomitome sodium, containing only bird's nest active extract and hyalomitome
Sour sodium and ascorbic cosmetics carry out moisturizing and skin effect evaluation.
After smearing 1,2,4,6,8 hour, using the hydration status of moisture of skin measuring instrument test skin, skin water is used
Decentralized measure instrument tests the water windage of skin, the results are shown in Table 3.After continuous use 2 months, compare the improvement feelings to skin
Condition the results are shown in Table 4.
Moistening effect of the table 3 to skin
To the improvement situation of skin after the use of table 42 months
Compared with cosmetic base, the cosmetics of the active extract containing bird's nest have better moisture-keeping efficacy in the present invention, and
It can be reduced the windage of moisture.Continuous use 2 months after, the elasticity of skin, crease-resistant, compactness, drying, roughness,
Itch, skin blemishes and the colour of skin have apparent improvement, and cosmetology effect is comprehensive, are suitable for water shortage, elasticity deficiency, wrinkle
More skin quality.
The cosmetics of active extract containing bird's nest and Sodium Hyaluronate in the present invention increase the elasticity and compact journey of skin
Degree, the itch and drying regime of skin are all significantly improved, other skin effects are also improved, and are suitable for more water shortage, scabies
Itch, the skin quality more than not compact and flaw.
Active extract containing bird's nest, Sodium Hyaluronate and ascorbic cosmetics, not only increase skin in the present invention
Elasticity and compactness, improve the itch and drying of skin, simultaneously because the antioxidation of Vc, the colour of skin and flaw of skin
Have and significantly increase, is suitable for colour of skin dimness, coarse, many skin quality of flaw.
Claims (9)
1. the preparation method of bird's nest active extract, which is characterized in that by bird's nest with water by 1:(19-199) mass ratio be soaked
1-3h shears 5-30min, revolving speed 10000-40000r/min at room temperature, shears again after being heated to 50-100 DEG C, and revolving speed is
10000-40000r/min, keeps 5-30min, and cooling preceding yarn filters out swallow hair and impurity, bird's nest activity then is made through ultrafiltration
Extracting solution.
2. a kind of bird's nest active extract, which is characterized in that be made, be lyophilized solid solidifying by preparation method described in claim 1
Content is 0.45wt%-4.5wt%.
3. bird's nest active extract according to claim 2, which is characterized in that contain Sialic acid, active glycopeptide, free ammonia
Base acid, microelement and water.
4. the cosmetics containing bird's nest active extract, which is characterized in that containing by bird's nest activity described in claim 2 or 3
Extracting solution, the bird's nest active extract account for the 0.5wt%-1wt% of total weight.
5. the cosmetics according to claim 4 containing bird's nest active extract, which is characterized in that further include hyaluronic acid
Sodium 0.05wt%-1wt%.
6. the cosmetics according to claim 5 containing bird's nest active extract, which is characterized in that further include vitamin C
1wt%-10wt%.
7. the cosmetics according to any one of claim 4 to 6 containing bird's nest active extract, which is characterized in that surplus
For cosmetic base.
8. the cosmetics according to claim 7 containing bird's nest active extract, which is characterized in that the agent of the cosmetics
Type is cream, lotion, aqua, gel, aerosol or facial mask.
9. the described in any item cosmetics containing bird's nest active extract of claim 4~8 are in face, eye circumference, lip, neck
The application of the cleaning and caring skin of neck, trunk or four limbs.
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WO2022032803A1 (en) * | 2020-08-10 | 2022-02-17 | 广西自贸区燕握生物科技有限公司 | Extraction method for edible bird's nest, and extract and product thereof |
CN114306192A (en) * | 2020-10-10 | 2022-04-12 | 香港科技大学 | Application of cannabidiol and combination of cannabidiol and cubilose extract in skin moisturizing |
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