CN103263372A - Natural flower petal and cosmetic adopting same - Google Patents

Natural flower petal and cosmetic adopting same Download PDF

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Publication number
CN103263372A
CN103263372A CN2013101992989A CN201310199298A CN103263372A CN 103263372 A CN103263372 A CN 103263372A CN 2013101992989 A CN2013101992989 A CN 2013101992989A CN 201310199298 A CN201310199298 A CN 201310199298A CN 103263372 A CN103263372 A CN 103263372A
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petal
natural
alcohol
solution
cosmetics
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CN103263372B (en
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董义伟
赵仕芝
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Shanghai Yi Chemical Co. Ltd.
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SUZHOU INDUSTRIAL PARK LIZI COSMETIC Co Ltd
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Abstract

The invention relates to a natural flower petal. A preparation method of the natural flower petal comprises the following steps of: (1) pre-treating; (2) boiling by an alcohol; (3) leaching for the first time; (4) boiling by water; and (5) leaching for the second time. According to the preparation method disclosed by the invention, the natural flower petal is subjected to pre-treatment, alcohol boiling, first time of leaching, water boiling and second time of leaching to obtain the natural flower petal finished product; the alcohol boiling takes polyhydric alcohols as an alcohol boiling solution; the alcohol boiling solution has very good viscidity, hygroscopicity, plastifying performance, film-forming property and sterilization so that the natural flower petal subjected to the alcohol boiling has the better toughness and has very high safety and certain corrosion resistance; and when being applied to a cosmetic, the natural flower petal is not easy to crush and is easy to store, so that the natural flower petal can be widely applied into preparations of the cosmetics.

Description

The cosmetics of a kind of natural petal and this natural petal of employing
Technical field
The present invention relates to cosmetic field, be specifically related to the cosmetics of a kind of natural petal and this natural petal of employing.
Background technology
Cosmetics have become the necessary in people's daily life.It not only has the effect of cleaning and beauty treatment skin, and simultaneously, various beautiful outward appearances, fragrance and form also can allow people's body and mind joyful, and this also is a kind of indirect beauty functions in fact.Along with growth in the living standard, people are also more and more higher to the requirement of cosmetics.Various natural skin care theories are rooted in the hearts of the people especially, propagate its belief on a large scale.
The various petals of occurring in nature, as Flos Rosae Rugosae, Flos Chrysanthemi, Paeonia suffruticosa, Flos Camelliae Japonicae, Chimonanthus praecox (L.) Link. etc., not only has beautiful outward appearance, also be rich in simultaneously nutritional labeling, as nutrients such as polysaccharide, flavone, protein, vitamin C, vitamin E, beta-carotene and mineral, polysaccharide wherein and flavone are the important physical active component, and antioxidation and the health care many-sided effect of waiting for a long time is arranged.If it directly can be used in cosmetics, can obtain various natural skin care cosmetics, not only have grace, beautiful outward appearance, also have various physiologically actives, help improve skin.But because natural petal is difficult for storing; and often mix impurity such as a large amount of stones, earth, branch, leaf even insecticide; if directly use water boiling method; can cause its toughness deficiency; broken easily in the Cosmetic Manufacture process, cause it directly to use and in cosmetic formulations, have many difficulties.There is employing that the direct drying back of petal is added the method for using in the cosmetics in the prior art, but it has in the cosmetics preparation process, petal is frangible, can not keep its intrinsic form, and the petal after drying has lost shortcomings such as its original color and luster and active component.
Summary of the invention
For addressing the above problem, the natural petal that the present invention at first provides a kind of and has toughness, intrinsic form is good, safe and has certain anti-corrosive properties.
The technical solution used in the present invention is, a kind of natural petal, and preparation method comprises the steps:
(1) pretreatment: behind the dry flower grass rejecting flower base of a fruit and foreign material with water content≤13%, obtain first petal; Described dry flower grass can be to obtain after the drying processing of flowers after plucking, also can directly buy;
(2) alcohol boils: described first petal and alcohols material are mixed for 1:20~200 by weight, and steaming and decocting is 10 minutes~1 hour under 50 ℃~95 ℃ temperature, obtains second petal and alcohol and boils solution;
(3) dewatering for the first time: will described second petal boil from described alcohol and take out also drop the solution and go out alcohol and boil solution, make the 3rd petal;
(4) decocting in water: described the 3rd petal and deionized water are mixed for 1:20~200 by weight, and steaming and decocting is 5 minutes~0.5 hour under 60 ℃~95 ℃ temperature, makes quatrefoil and decocting in water solution;
(5) dewatering for the second time: will described quatrefoil take out from described decocting in water solution also that drop goes out decocting in water solution, make natural petal.
The weight ratio of first petal and alcohols material is preferably 1:100 in the described step (2), and the form of too many petal can be out of shape, and the form of petal also can't be launched very little.The weight ratio of the 3rd petal and deionized water also is preferably 1:100 in the described step (4).
Preferably, described alcohols material is selected from glycerol, 1, the combination of one or more in 2-propylene glycol, 1,3 butylene glycol, pentanediol and the ethohexadiol.Especially preferably with propylene glycol or butanediol.Adopt the alcohol mode of boiling to be fixed in the petal tissue, make it keep its intrinsic form, in the cosmetics manufacturing process in later stage, also can guarantee form that it is fine and beautiful color and luster and outward appearance, has certain antisepsis simultaneously, and the active component that has better kept in the petal tissue does not run off, and can be fully utilized.
Preferably, described alcohol boils solution and can recycle, and saves cost, cuts the waste, and reduces blowdown.
Preferably, described step (3) is boiled described second petal the solution from described alcohol in the dewatering for the first time and is taken out, and the alcohol that places gauze to leach described second petal boils solution.
Preferably, the drainage mode in described step (5) dewatering second time is selected from one or more in drainage dry in the sun, electricity oven dry and the strainer filtering.
On the basis of the above, the present invention continues to provide a kind of cosmetics, and it comprises above-mentioned natural petal, and the percentage by weight of described natural petal is 0.001-95%.
Preferably, the percentage by weight of described natural petal is 0.01~10%.
Preferred, the percentage by weight of described natural petal is 0.1~2%.
Can also comprise in solvent, emollient, solubilizing agent, antioxidant, PH regulator, penetrating agent, indicator, liposome, wetting agent, thickening agent, nertralizer, chelating agen, surfactant, emulsifying agent, essence, pigment, bright protective agent, antioxidant, active matter and the functional additive one or more in the described cosmetics as required.These materials all can adopt any known used for cosmetic material.
Described cosmetics can be in bath gel, astringent, perfume, floral water, facial film, facial cream, gel, emulsion, elite, makeup removing oil and the transparent soap one or more.
Preferably, the storeroom of natural petal described in the described cosmetics adopts transparent wrapper.Can embody color and luster, the outward appearance of natural petal of the present invention better, if be aided with corresponding fragrance again, can increase the organoleptic attribute of described cosmetics greatly, increase people's desire to buy and use desire.
The present invention adopts above technical scheme, obtained useful effect: among the present invention with natural petal by pretreatment, alcohol boils, dewatering for the first time, decocting in water and and the processing of dewatering for the second time make natural petal, alcohol boils the employing polyalcohols, as glycerol, propylene glycol, butanediol, pentanediol, ethohexadiols etc. boil solution as alcohol, above-mentioned alcohol boils solution and has good viscosity, hygroscopicity, plasticity, film property and bactericidal properties, therefore the natural petal that boils through alcohol has better toughness, and have very high safety and certain anti-corrosive properties, be difficult for broken when being applied in the cosmetics, preserve easily, natural petal can be widely used in the prescription of cosmetics.
The specific embodiment
Below described embodiment only be the present invention part embodiment, rather than whole embodiment.Based on the embodiment among the present invention, those of ordinary skills belong to the scope of protection of the invention not making the every other embodiment that obtains under the creative work prerequisite.
Embodiment 1
Behind the dry flower grass rejecting flower base of a fruit and foreign material with water content≤13%, obtain first petal;
First petal and propylene glycol by weight for 1:100 mixes, are made mixture, and to 70-90 ℃, stirring and evenly mixing boiled 30 minutes, made second petal and propylene glycol solution with this mixture heated;
Pull and place second petal out gauze, the propylene glycol solution drop is gone out and propylene glycol solution is reclaimed, make the 3rd petal;
Petal and deionized water by weight for 1:150 mixes, are made mixture, this mixture heated to 50-90 ℃, was boiled 10 minutes, quatrefoil and deionized water solution are made in stirring while boiling;
Quatrefoil is taken out, the elimination redundant moisture, obtain form natural petal full, bright in colour, the weight of the initial dry petal (first petal) in natural petal Central Plains this moment only accounts for 10-50%, described natural petal can long preservation, at any time take, in order to make various cosmetics or skin care item, as bath gel, astringent, perfume, floral water, facial film, facial cream, gel, emulsion, elite, makeup removing oil and transparent soap etc.
Embodiment 2
Behind the dry flower grass rejecting flower base of a fruit and foreign material with water content≤13%, obtain first petal;
First petal and glycerol by weight for 1:150 mixes, are made mixture, and to 70-90 ℃, stirring and evenly mixing boiled 30 minutes, made second petal and glycerite with this mixture heated;
Pull and place second petal out gauze, the glycerite drop is gone out and glycerite is reclaimed, make the 3rd petal;
Petal and deionized water by weight for 1:100 mixes, are made mixture, this mixture heated to 50-90 ℃, was boiled 10 minutes, quatrefoil and deionized water solution are made in stirring while boiling;
Quatrefoil is taken out, and the elimination redundant moisture obtains form natural petal full, bright in colour, and the weight of the initial dry petal (first petal) in natural petal Central Plains this moment only accounts for 10-50%.
Embodiment 3
Behind the dry flower grass rejecting flower base of a fruit and foreign material with water content≤13%, obtain first petal;
First petal and butanediol by weight for 1:40 mixes, are made mixture, and to 70-90 ℃, stirring and evenly mixing boiled 30 minutes, made second petal and butanediol solution with this mixture heated;
Pull and place second petal out gauze, the butanediol solution drop is gone out and butanediol solution is reclaimed, make the 3rd petal;
Petal and deionized water by weight for 1:40 mixes, are made mixture, this mixture heated to 50-90 ℃, was boiled 10 minutes, quatrefoil and deionized water solution are made in stirring while boiling;
Quatrefoil is taken out, and the elimination redundant moisture obtains form natural petal full, bright in colour, and the weight of the initial dry petal (first petal) in natural petal Central Plains this moment only accounts for 10-50%.
Embodiment 4
Behind the dry flower grass rejecting flower base of a fruit and foreign material with water content≤13%, obtain first petal;
First petal and pentanediol by weight for 1:20 mixes, are made mixture, and to 70-90 ℃, stirring and evenly mixing boiled 30 minutes, made second petal and pentanediol solution with this mixture heated;
Pull and place second petal out gauze, pentanediol solution drop is gone out and pentanediol solution is reclaimed, make the 3rd petal;
Petal and deionized water by weight for 1:20 mixes, are made mixture, this mixture heated to 50-90 ℃, was boiled 10 minutes, quatrefoil and deionized water solution are made in stirring while boiling;
Quatrefoil is taken out, and the elimination redundant moisture obtains form natural petal full, bright in colour, and the weight of the initial dry petal (first petal) in natural petal Central Plains this moment only accounts for 10-50%.
Following examples are the application of resulting natural petal in cosmetics in above-described embodiment, wherein said petal for boil through alcohol with boiled process after the natural petal that makes.The consumption of natural petal is in the weight of initial dry petal (first petal).Each component unit all is weight percentage.
Embodiment 5: the preparation of petal water
Figure BDA00003246443700041
Above-mentioned natural petal is embodiment 1~embodiment 4 arbitrary described natural petals.
Embodiment 6: the preparation of petal bath gel
Figure BDA00003246443700052
Above-mentioned natural petal is embodiment 1~embodiment 4 arbitrary described natural petals.
Embodiment 7: the preparation of petal essence
Figure BDA00003246443700053
Above-mentioned natural petal is embodiment 1~embodiment 4 arbitrary described natural petals.
Embodiment 8: the preparation of petal facial cream
Figure BDA00003246443700062
Above-mentioned natural petal is embodiment 1~embodiment 4 arbitrary described natural petals.
Embodiment 9: the preparation of petals face-mask
Figure BDA00003246443700071
Above-mentioned natural petal is embodiment 1~embodiment 4 arbitrary described natural petals.
Embodiment 10: the preparation of petal gel
Above-mentioned natural petal is embodiment 1~embodiment 4 arbitrary described natural petals.
Embodiment 11: the preparation of petal emulsion
Figure BDA00003246443700081
Above-mentioned natural petal is embodiment 1~embodiment 4 arbitrary described natural petals.
Embodiment 12: the preparation of petal makeup removing oil
Figure BDA00003246443700082
Above-mentioned natural petal is embodiment 1~embodiment 4 arbitrary described natural petals.
Embodiment 1-embodiment 12 is carried out benchmark test, statistical experiment result such as following table 1.
Table 1
Product Petal outward appearance integrity degree Petal toughness (product is deposited the outward appearance integrity degree after 3 months) The petal color and luster
Embodiment 1 Complete Complete Bright-coloured, full
Embodiment 2 Complete Complete Bright-coloured, full
Embodiment 3 Substantially complete Substantially complete Bright-coloured, full
Embodiment 4 Substantially complete Substantially complete Bright-coloured, full
Embodiment 5 Complete Complete Bright-coloured, full
Embodiment 6 Complete Complete Bright-coloured, full
Embodiment 7 Complete Complete Bright-coloured, full
Embodiment 8 Complete Complete Bright-coloured, full
Embodiment 9 Complete Complete Bright-coloured, full
Embodiment 10 Complete Complete Bright-coloured, full
Embodiment 11 Complete Complete Bright-coloured, full
Embodiment 12 Complete Complete Bright-coloured, full
Adopt the beneficial effect of above technical scheme: among the present invention with natural petal by pretreatment, alcohol boils, dewatering for the first time, decocting in water and and the processing of dewatering for the second time make natural petal, alcohol boils the employing polyalcohols, as glycerol, propylene glycol, butanediol, pentanediol, ethohexadiols etc. boil solution as alcohol, above-mentioned alcohol boils solution and has good viscosity, hygroscopicity, plasticity, film property and bactericidal properties, therefore the natural petal that boils through alcohol has better toughness, and have very high safety and certain anti-corrosive properties, be difficult for broken when being applied in the cosmetics, preserve easily, natural petal can be widely used in the prescription of cosmetics.
Above-described embodiment is described preferred implementation of the present invention; be not that scope of the present invention is limited; design under the prerequisite of spirit not breaking away from the present invention; various distortion and improvement that the common engineers and technicians in this area make technical scheme of the present invention all should fall in the definite protection domain of claims of the present invention.

Claims (13)

1. natural petal, it is characterized in that: the preparation method of described natural petal comprises the steps
(1) pretreatment: behind the dry flower grass rejecting flower base of a fruit and foreign material with water content≤13%, obtain first petal;
(2) alcohol boils: described first petal and alcohols material are mixed for 1:20~200 by weight, and steaming and decocting is 10 minutes~1 hour under 50 ℃~95 ℃ temperature, obtains second petal and alcohol and boils solution;
(3) dewatering for the first time: will described second petal boil from described alcohol and take out also drop the solution and go out alcohol and boil solution, make the 3rd petal;
(4) decocting in water: described the 3rd petal and deionized water are mixed for 1:20~200 by weight, and steaming and decocting is 5 minutes~0.5 hour under 60 ℃~95 ℃ temperature, makes quatrefoil and decocting in water solution;
(5) dewatering for the second time: will described quatrefoil take out from described decocting in water solution also that drop goes out decocting in water solution, make natural petal.
2. natural petal according to claim 1, it is characterized in that: the weight ratio of first petal and alcohols material is 1:100 in the described step (2).
3. natural petal according to claim 1 and 2, it is characterized in that: the alcohols material in the described step (2) is selected from glycerol, 1, the combination of one or more in 2-propylene glycol, 1,3 butylene glycol, pentanediol and the ethohexadiol.
4. natural petal according to claim 3, it is characterized in that: described alcohols material is propylene glycol or butanediol.
5. natural petal according to claim 1, it is characterized in that: described alcohol boils solution and recycles.
6. natural petal according to claim 1 is characterized in that: described step (3) is boiled described second petal the solution from described alcohol in the dewatering for the first time and is taken out, and the alcohol that places gauze to leach described second petal boils solution.
7. according to claim 1 or 6 described natural petals, it is characterized in that: the drainage mode in described step (5) dewatering second time is selected from one or more in drainage dry in the sun, electricity oven dry and the strainer filtering.
8. cosmetics, it is characterized in that: comprise each described natural petal of claim 1-7, the percentage by weight of described natural petal is 0.001~95%.
9. cosmetics according to claim 8, it is characterized in that: the percentage by weight of described natural petal is 0.01~10%.
10. cosmetics according to claim 8, it is characterized in that: the percentage by weight of described natural petal is 0.1~2%.
11. each described cosmetics according to Claim 8-10 is characterized in that: also comprise in solvent, emollient, solubilizing agent, antioxidant, PH regulator, penetrating agent, indicator, liposome, wetting agent, thickening agent, nertralizer, chelating agen, surfactant, emulsifying agent, essence, pigment, bright protective agent, antioxidant, active matter and the functional additive one or more in the described cosmetics.
12. each described cosmetics according to Claim 8-10, it is characterized in that: described cosmetics are one or more in bath gel, astringent, perfume, floral water, facial film, facial cream, gel, emulsion, elite, makeup removing oil and the transparent soap.
13. each described cosmetics is characterized in that according to Claim 8-12, the storeroom of described natural petal adopts transparent wrapper.
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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103735457A (en) * 2013-12-25 2014-04-23 金奇集团金奇日化有限公司 Toner containing herbal components and preparation method thereof
CN105853272A (en) * 2016-04-14 2016-08-17 广州丹奇日用化工厂有限公司 Skin-care cleansing water
CN105935343A (en) * 2016-05-30 2016-09-14 哈尔滨源茂达生物技术有限公司 Whitening and spot removing polypeptide essence and preparation method thereof
CN106667838A (en) * 2016-12-30 2017-05-17 广州巧巧生物科技有限公司 Preparation method of flower lotion with persistent color, freshness and shape retaining functions
CN107362057A (en) * 2017-07-12 2017-11-21 熊廷珍 A kind of sea urchin polypeptide tears facial mask and preparation method thereof
CN107362119A (en) * 2017-07-12 2017-11-21 熊廷珍 A kind of sea urchin polypeptide sleep mask and preparation method thereof
CN109820783A (en) * 2019-03-22 2019-05-31 云南省农业科学院花卉研究所 A kind of discoloration method of plant petals
CN111956525A (en) * 2020-09-17 2020-11-20 佛山市南海区桂城埃菲尔化妆品有限公司 Petal shower gel and preparation method thereof
CN112336650A (en) * 2020-11-20 2021-02-09 泉后(广州)生物科技研究院有限公司 Mild and effective single-phase makeup remover
CN115212149A (en) * 2022-07-27 2022-10-21 广州市科能化妆品科研有限公司 Skin-care water dosage form composition for desert muscle and preparation method thereof

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WO1999055152A1 (en) * 1998-04-24 1999-11-04 The University Court Of The University Of St. Andrews Preservation of plant material
KR20080108718A (en) * 2007-06-11 2008-12-16 한국콜마 주식회사 Cosmetic composition for skin massage comprising natural softened plants and manufacturing method thereof

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KR20080108718A (en) * 2007-06-11 2008-12-16 한국콜마 주식회사 Cosmetic composition for skin massage comprising natural softened plants and manufacturing method thereof

Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103735457A (en) * 2013-12-25 2014-04-23 金奇集团金奇日化有限公司 Toner containing herbal components and preparation method thereof
CN103735457B (en) * 2013-12-25 2017-01-11 广东金奇精化股份有限公司 Toner containing herbal components and preparation method thereof
CN105853272A (en) * 2016-04-14 2016-08-17 广州丹奇日用化工厂有限公司 Skin-care cleansing water
CN105935343A (en) * 2016-05-30 2016-09-14 哈尔滨源茂达生物技术有限公司 Whitening and spot removing polypeptide essence and preparation method thereof
CN106667838A (en) * 2016-12-30 2017-05-17 广州巧巧生物科技有限公司 Preparation method of flower lotion with persistent color, freshness and shape retaining functions
CN107362057A (en) * 2017-07-12 2017-11-21 熊廷珍 A kind of sea urchin polypeptide tears facial mask and preparation method thereof
CN107362119A (en) * 2017-07-12 2017-11-21 熊廷珍 A kind of sea urchin polypeptide sleep mask and preparation method thereof
CN109820783A (en) * 2019-03-22 2019-05-31 云南省农业科学院花卉研究所 A kind of discoloration method of plant petals
CN111956525A (en) * 2020-09-17 2020-11-20 佛山市南海区桂城埃菲尔化妆品有限公司 Petal shower gel and preparation method thereof
CN112336650A (en) * 2020-11-20 2021-02-09 泉后(广州)生物科技研究院有限公司 Mild and effective single-phase makeup remover
CN115212149A (en) * 2022-07-27 2022-10-21 广州市科能化妆品科研有限公司 Skin-care water dosage form composition for desert muscle and preparation method thereof

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Patentee before: Suzhou Industrial Park Lizi Cosmetic Co., Ltd.