CN106667838A - Preparation method of flower lotion with persistent color, freshness and shape retaining functions - Google Patents
Preparation method of flower lotion with persistent color, freshness and shape retaining functions Download PDFInfo
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- CN106667838A CN106667838A CN201611261804.2A CN201611261804A CN106667838A CN 106667838 A CN106667838 A CN 106667838A CN 201611261804 A CN201611261804 A CN 201611261804A CN 106667838 A CN106667838 A CN 106667838A
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- petal
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- luster
- suspend
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/41—Amines
- A61K8/416—Quaternary ammonium compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8158—Homopolymers or copolymers of amides or imides, e.g. (meth) acrylamide; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
Abstract
A preparation method of a flower lotion with persistent color, freshness and shape retaining functions comprises following steps: dried petals are pretreated by removing flower stalks and impurities of the dried petals; a quantitative petal immersion liquid is taken, the dried petals are immersed in the petal immersion liquid for 8-24 h at the room temperature, the immersed petals, the immersion liquid and other auxiliaries are jointly added to a lotion, and the flower lotion is prepared through slow stirring. The preparation method has the advantages as follows: the method is simple and easy; active ingredients of the petals can be effectively retained without loss; the petals can keep color, freshness and shape in the lotion persistently without sinking, the guarantee period of the flower lotion can be prolonged, and the grade of the flower lotion is improved.
Description
Technical field
The present invention relates to cosmetic field, specifically refers to a kind of lasting preparation side for protecting the fresh-keeping conformal flowers astringent of color
Method.
Background technology
Commercially available flowers astringent is not rarely seen, and outward appearance is elegant, allows people to have a kind of sensation of back to nature, compares and consumed
Person favor, at present, flowers astringent be typically prepared method be commercially available dry petal is carried out into 10 ~ 30min of decocting in water after be directly added into
In astringent, then the extracting solution for adding this petal toward astringent（Active component）It is and the essence of this petal is obtained, this kind of
Although the preparation method of flowers astringent can make petal absorb moisture extravagance coming, and it is presented in astringent, petal
During decocting in water, the active substance of petal loses a lot, and petal surface does not have anti-corrosion, and easily discoloration is become sour, petal table
Face is relatively thin easily to be sunk by cosmetic water saturates, it is impossible to keep original shape and color and luster, and the shelf-life of flowers astringent is not long, class
It is difficult to improve.Patent CN103263372 discloses a kind of preparation method of natural petal cosmetics, and the patented method is by dry flower
Lobe carries out that alcohol is boiled, first time dewatering, decocting in water, the step such as second dewatering are obtained the flowers being added in cosmetics, and thus spend
Lobe is prepared for various flowers cosmetics, although this kind of method has increased can the petal toughness being added in astringent and anti-corrosive properties
And it is long-term not mention flowers astringent by force, but method is loaded down with trivial details, petal active component is lost during steaming and decocting a lot,
The problem that storage petal sinks.
Patent KR20080072122A discloses a kind of method for preparing flowers astringent, the patented method be with ethanol and
Water is with 1:2~2:1 ratio mixed solution dissolves petal 12 ~ 48 hours at room temperature, then band petalled lysate together
It is added in the base material of astringent, prepares flowers astringent, save the active component of petal well, but the technical scheme is simultaneously
Do not mention and how to keep the color and luster of petal, shape not to change in Storage period.Apply in patent KR20070002718A
The citric acid solution or carbomer solution steaming and decocting dry petal at 70 ~ 90 DEG C, then adds it in astringent, the same technology
Scheme does not mention the problem of the color and luster, shape and the freshness that how to keep petal.
The content of the invention
The present invention provides a kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color.
To achieve these goals, present invention employs following technical scheme：
A kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color, comprises the steps：
S1. dry petal pretreatment：Reject the colored base of a fruit and impurity of dry petal, it is ensured that select the clean without defective products of petal；
S2. take quantitative petal to ooze immersion, make dry petal room temperature in immersion of oozing ooze leaching 8 ~ 24 hours, leaching of oozing places standby after finishing
With dry petal is 1 with the weight ratio of immersion of oozing:50 ~ 150, with 1:80 ~ 120 are advisable, natural petal（In terms of dry petal weight）
0.01% ~ 20%, it is advisable with 0.05% ~ 10%, 0.1% ~ 2% is excellent, and 0.2% ~ 1% is optimum.
S3. the petal that soaked oozing and ooze immersion and other auxiliary agents are added in astringent, be slowly stirred and make
Obtain flowers astringent.
Petal immersion of oozing includes polyhydric alcohol, deionized water and cationic surfactant, wherein, polyhydric alcohol and go
The weight ratio of ionized water is 1:2~2:1；
Cationic surfactant can for polyquaternary ammonium salt, octadecyl trimethyl ammonium chloride, Dodecyl trimethyl ammonium chloride,
Dodecyl dimethyl benzyl ammonium chloride, stearyl dimethyl benzyl ammonium chloride, double dodecyl dimethyl ammonium chloride, sun from
Sub- guar gum etc., accounting 0.01% ~ 2%, is advisable with 0.1% ~ 1%, the effect of cationic surfactant be increase petal into
Film and anti-corrosive properties, in immersion of oozing, the ratio of polyhydric alcohol and deionized water is generally 1:2~2:1, with 1:1.5~1.5:1 is advisable, and 1:
1.2~1.2:1 for excellent, and dry petal oozes in immersion of oozing generally 8 ~ 24 hours leaching time, is advisable with 12 ~ 20 hours, so as to work
With being to make petal sprawl completely to come, the anti-corrosive properties of increase petal, film property, toughness, moisture retention protect color in order to more preferable
It is fresh-keeping conformal.
Polyhydric alcohol is generally 1,3-PD, 1,3 butylene glycol, glycerol, Sorbitol, 1,2- pentanediols, Natrulon H-10,
Polyglycereol -30 etc., effect be increase astringent density and to skin moisture-keeping, make petal be difficult sink, polyhydric alcohol is in formula
In weight ratio generally 10% ~ 40%.It is advisable with 15% ~ 30%.
The weight of polyhydric alcohol and deionized water in immersion of oozing compares 1:1.2~1.2:1, the weight of the cationic surfactant
Amount percentage ratio is 0.1% ~ 1%, and the percentage by weight of polyhydric alcohol is 15% ~ 30%.
Wherein, other auxiliary agents include wetting agent, thickening agent, the essence of corresponding petal, preservative；
The wetting agent includes glycine betaine, hyaluronic acid, hydroxyethyl urea, amino acid humectant, trehalose, the wetting agent
Percentage by weight is 0.01% ~ 5.0%；
Thickening agent：It is acrylic compounds water-soluble polymer, vinyl water-soluble polymer, polyoxyethylene water-soluble polymer, poly-
Glycols water-soluble polymer, hydroxyethyl cellulose, xanthan gum etc., effect are to increase the viscosity of astringent and to skin
Moisturizing, can make petal preferably suspend, thickening agent ratio：0.01% ~ 0.25%, it is advisable with 0.05% ~ 0.15%,
The essence of corresponding petal, to improve the petal fragrance of flowers astringent, odor type must be consistent with the petal type of addition, with
Light perfume (or spice) is advisable, and adding proportion typically constitutes from 0.02 ‰ ~ 0.5 ‰, is advisable with 0.05 ‰ ~ 0.2 ‰；
Preservative, preservative are generally bromo- 2 nitro of Methylisothiazolinone, methylchloroisothiazandnone, phenoxyethanol, 2- third
Alkane -1,3-PD, quaternary ammonium salt -15, imidazolidinyl urea, benzalkonium chloride etc., ratio 0.01% ~ 2.0%, are advisable with 0.05% ~ 1.0%
Further, described other auxiliary agents also include the extract of corresponding petal and proposing for other corresponding petals of animals and plants extract
Thing and other animals and plants extracts are taken, to increase or improve effect of flowers astringent, such as moisturizing, skin softening, convergence, crease-resistant, anti-
Aging, Bearberry Extract.Addition 0.01% ~ 2.0%, is advisable with 0.05% ~ 0.5%.
In addition, can have ethanol can need addition according to astringent function or not add without ethanol in astringent
Plus, addition is such as needed, addition is difficult too much, typically no more than 20%, to be preferred less than 15%, more excellent less than 10%.
The present invention has following advantage：
1st, the inventive method is simple；
2nd, petal active component can be effectively kept not lose；
3rd, the guarantor's color that petal can be made lasting in astringent is fresh-keeping conformal, does not sink, and can increase the shelf-life of flowers astringent,
Improve the class of flowers astringent.
Specific embodiment
Specific the effects are carried out using the method, test case is as follows：
Embodiment one
Water is spent in Flos Matricariae chamomillae reparation
Formula is designed as glycerol 7.0%, 1,3 butylene glycol 10%, glycine betaine 0.5%, reed fragrant plant oil 0.2%, EDTA- disodiums 0.02%, and 1%
Carbopol 941 6%, triethanolamine 0.04%, Flos Matricariae chamomillae extracting solution 0.05%, Herba Portulacae extract 0.1%, PEG-40 hydrogenation castors
Oleum Sesami 0.001%, Flos Matricariae chamomillae essence 0.0004%, Flos Matricariae chamomillae dry petal 0.5%, germall 0.95%, deionized water 81.1%.
1000g when making sample, weighs glycerol 50g, 1,3 butylene glycol 100g, deionized water 120g, octadecyl three first
Ammonio methacrylate 0.6g stirs, and composition petal oozes immersion, weighs Flos Matricariae chamomillae dry petal 5g, ooze be immersed in it is above-mentioned ooze in immersion,
Room temperature is oozed and is soaked 12 hours, standby.Weigh 691g water, glycerol 20g, glycine betaine 5g, EDTA- disodium 0.2g, 1%Carbopol 941
60g, sequentially adds in agitated kettle, is heated to 50 DEG C ~ 70 DEG C, is allowed to dissolving completely, is cooled to 50 DEG C of addition triethanolamine 0.4g,
Stir, be cooled to 45 DEG C, add camomile extract 0.5g, Herba portulacae extract 1g, Cremophor RH40 solubilising
Good Flos Matricariae chamomillae essence, preservative germall 0.5g stirs, and after being completely dissolved, discharging is transferred in storage cylinder, leaching of oozing
Good petal and immersion of oozing together is added to storage cylinder, is slowly stirred.
Embodiment two
Flos persicae liquid distilled from honeysuckle flowers or lotus leaves whitening essence lotion
Formula is designed as glycerol 8.0%, and 1,3-PD 12%, 1% hyaluronic acid matter sodium 1%, EDTA- disodiums 0.05%, ethoxy are fine
Dimension element 15%, Radix Glycyrrhizae extract 0.05%, Folium Vaccinii vitis-idaeae leaf extract 0.05%, vitamin C glucoside 0.1%, Flos persicae extracting solution 0.02%,
Cremophor RH40 0.001%, Flos persicae flavor essence 0.0005%, Flos persicae dry petal 0.3%, phenoxyethanol 0.15%, go from
Sub- water 63.3%.
1000g when making sample, weighs glycerol 60g, 1,3-PD 100g, deionized water 150g, dodecyl two first
Methyl-benzyl ammonium chloride 1.5g stirs, and composition petal oozes immersion, weighs Flos persicae dry petal 3g, oozes and be immersed in above-mentioned immersion of oozing
In, room temperature is oozed and is soaked 18 hours, standby.Weigh 483g water, glycerol 20g, 1% hyaluronic acid matter sodium 10g, EDTA- disodium 0.5g, hydroxyl second
Base cellulose 150g, sequentially adds in agitated kettle, is heated to 50 DEG C ~ 70 DEG C, is allowed to dissolving completely, is cooled to 45 DEG C, adds sweet
Careless extract 0.5g, Folium Vaccinii vitis-idaeae leaf extract 1g, Flos persicae extracting solution 0.2g, the good Flos persicae odor type of Cremophor RH40 solubilising are fragrant
Essence, preservative phenoxyethanol 1.5g, stirs, and after being completely dissolved, discharging is transferred in storage cylinder, the petal soaked oozing
And immersion of oozing together is added to storage cylinder, it is slowly stirred.
Embodiment three
Flos Rosae Rugosae flowers clean skin astringent
Formula is designed as Natrulon H-10 15.0%, Propylene Glycol 10%, glycine betaine 2%, EDTA- disodiums 0.05%, 1% xanthan gum 10%,
Brij92 1%, Flos Rosae Rugosae extracting solution 0.05%, tween 20 0.002%, rose scent essence 0.0005%, Rose Blume Getrocknete
Petal 0.2%, Kazon 0.12%, deionized water 61.5%.
1000g when making sample, weighs Natrulon H-10 100g, Propylene Glycol 100g, deionized water 100g, polyquaternary amine first
- 15 1.2g of salt stirs, and composition petal oozes immersion, weighs Rose Blume Getrocknete petal 2g, ooze be immersed in it is above-mentioned ooze in immersion, room temperature
Ooze and soak 14 hours, it is standby.Weighing 515g water, bis- 0.5g of Natrulon H-10 50g, glycine betaine 20g, EDTA-, 1% xanthan gum 100g,
Sequentially add in agitated kettle, be heated to 50 DEG C ~ 70 DEG C, be allowed to dissolving completely, be cooled to 45 DEG C, add Flos Rosae Rugosae extracting solution 0.5g,
The good Flos persicae flavor essence of tween 20 solubilising, Preservative Kathon CG(Methylchloroisothiazolinone/Methylisothiazolinone combination) 1.2g stirs, and after being completely dissolved, discharging is transferred to storage
Deposit in cylinder, the roseleaf and immersion of oozing soaked oozing together is added to storage cylinder, be slowly stirred
Astringent.
By the three sections of flowers astringent for preparing and commercially available a flowers astringent（Matched group）Respectively room temperature, 45
DEG C, -5 DEG C, long-term and accelerated test is carried out under ultraviolet light, daylight lamp, in investigating flowers astringent, petal protects the fresh-keeping conformal effect of color
Really, it is as a result as follows：
1st, 45 DEG C of result of the tests
| Sample | 1st week | 2nd week | 1st month | 3rd month | 6th month | 8th month | 12nd month |
| Embodiment one | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Outward appearance complete, color and luster substantially It is bright-coloured, suspend intact |
| Embodiment two | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Outward appearance complete, color and luster substantially It is bright-coloured, suspend intact |
| Embodiment three | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Outward appearance complete, color and luster substantially It is bright-coloured, suspend intact |
| Matched group one | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Outward appearance complete, color and luster substantially There is loss, suspend intact | Outward appearance complete, color and luster substantially There is loss, suspend intact | Outward appearance has damage, color and luster portion more than 1/3 Divide obscure, part petal sinks | Cosmetic injury surpasses 2/3, color Pool is obscure, and petal sinks |
2nd, -5 DEG C of result of the tests
| Sample | 1st week | 2nd week | 1st month | 3rd month | 6th month | 8th month | 12nd month |
| Embodiment one | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Embodiment two | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Embodiment three | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Matched group one | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Outward appearance complete, color and luster substantially There is loss, suspend intact | Outward appearance complete, color and luster substantially has loss, Suspend intact | Outward appearance is damaged more than 1/3 Wound, color and luster part are obscure, Part petal sinks |
Ultraviolet optical tests：
| Sample | 1st week | 2nd week | 1st month | 3rd month | 6th month | 8th month | 12nd month |
| Embodiment one | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Embodiment two | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Embodiment three | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Matched group one | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Outward appearance complete, color and luster substantially There is loss, suspend intact | Outward appearance complete, color and luster substantially There is loss, suspend intact | Outward appearance has damage, color and luster portion more than 1/3 Divide obscure, part petal sinks | Cosmetic injury surpasses 2/3, color Pool is obscure, and petal sinks |
Daylight lamp test
| Sample | 1st week | 2nd week | 1st month | 3rd month | 6th month | 8th month | 12nd month |
| Embodiment one | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Embodiment two | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Embodiment three | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Matched group one | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Outward appearance complete, color and luster substantially It is bright-coloured, suspend intact | Outward appearance complete, color and luster substantially has loss, Suspend intact | Outward appearance is damaged more than 1/3 Wound, color and luster part are obscure, Part petal sinks |
Long term test：
| Sample | 1st week | 2nd week | 1st month | 3rd month | 6th month | 8th month | 12nd month |
| Embodiment one | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Embodiment two | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Embodiment three | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, lovely luster, have suspended It is good | Complete appearance, color and luster are fresh It is gorgeous, suspend intact |
| Matched group one | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Complete appearance, color and luster are fresh It is gorgeous, suspend intact | Outward appearance complete, color and luster substantially It is bright-coloured, suspend intact | Outward appearance complete, color and luster substantially has loss, Suspend intact | Outward appearance is damaged more than 1/3 Wound, color and luster part are obscure, Part petal sinks |
From upper figure, technical scheme has obvious advantage.
Embodiment described above is only that the preferred embodiment of the present invention is described, not the model to the present invention
Enclose and be defined, on the premise of without departing from design spirit of the present invention, skill of this area ordinary skill technical staff to the present invention
Various modifications and improvement that art scheme is made, all should fall within the protection domain of claims of the present invention determination.
Claims (9)
1. a kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color, it is characterised in that comprise the steps：
S1. dry petal pretreatment：Reject the colored base of a fruit and impurity of dry petal, it is ensured that select the clean without defective products of petal；
S2. take quantitative petal to ooze immersion, make dry petal room temperature in immersion of oozing ooze leaching 8 ~ 24 hours, leaching of oozing places standby after finishing
With dry petal is 1 with the weight ratio of immersion of oozing:50 ~ 150, the percentage by weight of dry petal is 0.01% ~ 20%；
S3. the petal that soaked oozing and ooze immersion and other auxiliary agents are added in astringent, be slowly stirred
Grass astringent.
2. a kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color according to claim 1, which is special
Levy and be, petal immersion of oozing includes polyhydric alcohol, deionized water and cationic surfactant, wherein, polyhydric alcohol and go
The weight ratio of ionized water is 1:2~2:1；
The percentage by weight of the cationic surfactant is 0.01% ~ 2%, including polyquaternary ammonium salt, octadecyl trimethyl chlorine
Change ammonium, Dodecyl trimethyl ammonium chloride, dodecyl dimethyl benzyl ammonium chloride, stearyl dimethyl benzyl ammonium chloride,
Double dodecyl dimethyl ammonium chloride, cation guar gum；
The percentage by weight of polyhydric alcohol be 10% ~ 40%, including 1,3-PD, 1,3 butylene glycol, glycerol, Sorbitol, 1,2-
Pentanediol, Natrulon H-10, polyglycereol -30.
3. a kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color according to claim 2, which is special
Levy and be, the weight of polyhydric alcohol and deionized water compares 1 in immersion of oozing:1.2~1.2:1, the weight of the cationic surfactant
Percentage ratio is 0.1% ~ 1%, and the percentage by weight of polyhydric alcohol is 15% ~ 30%.
4. a kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color according to claim 3, which is special
Levy and be, dry petal is 1 with the weight ratio of immersion of oozing:80 ~ 120, the percentage by weight of dry petal is 0.05% ~ 10%, dry petal
The leaching time is oozed in immersion of oozing for 12 ~ 20 hours.
5. a kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color according to claim 4, which is special
Levy and be, the percentage by weight of dry petal is 0.1% ~ 2%.
6. a kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color according to claim 4 or 5, its
It is characterised by, other auxiliary agents include wetting agent, thickening agent, the essence of corresponding petal, preservative；
The wetting agent includes glycine betaine, hyaluronic acid, hydroxyethyl urea, amino acid humectant, trehalose, the wetting agent
Percentage by weight is 0.01% ~ 5.0%；
Thickening agent include acrylic compounds water-soluble polymer, vinyl water-soluble polymer, polyoxyethylene water-soluble polymer,
Polyethylene glycols water-soluble polymer, hydroxyethyl cellulose, xanthan gum, the percentage by weight of the thickening agent is 0.01% ~
0.25%；
The essence of corresponding petal, odor type are consistent with the petal type of addition, and adding proportion typically constitutes from 0.02 ‰ ~ 0.5 ‰,
Preservative includes the bromo- 2 nitropropane -1,3- of Methylisothiazolinone, methylchloroisothiazandnone, phenoxyethanol, 2- third
Glycol, quaternary ammonium salt -15, imidazolidinyl urea, benzalkonium chloride, the percentage by weight of the preservative is 0.01% ~ 2.0%.
7. a kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color according to claim 6, which is special
Levy and be, in described other auxiliary agents, the percentage by weight of thickening agent is 0.05% ~ 0.15%, the quality hundred of the essence of corresponding petal
It is 0.05% ~ 1.0% to divide than the percentage by weight for 0.05 ‰ ~ 0.2 ‰, the preservative.
8. a kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color according to claim 6, which is special
Levy and be, described other auxiliary agents also including corresponding petal extract and other animals and plants extracts, addition be 0.01% ~
2.0%。
9. a kind of preparation method that can persistently protect the fresh-keeping conformal flowers astringent of color according to claim 8, which is special
Levy and be, the addition of the extract of petal and other animals and plants extracts is 0.05% ~ 0.5%.
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| CN201611261804.2A CN106667838B (en) | 2016-12-30 | 2016-12-30 | Preparation method of flower toning lotion capable of keeping color, fresh and shape for a long time |
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| CN201611261804.2A CN106667838B (en) | 2016-12-30 | 2016-12-30 | Preparation method of flower toning lotion capable of keeping color, fresh and shape for a long time |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107737058A (en) * | 2017-12-01 | 2018-02-27 | 绿馨颜（惠州）生物科技有限公司 | A kind of gold moisture retention water of biological carbohydrate gum 1 and preparation method thereof |
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| CN103263372A (en) * | 2013-05-24 | 2013-08-28 | 苏州工业园区黎姿化妆品有限公司 | Natural flower petal and cosmetic adopting same |
| KR20160020968A (en) * | 2014-08-15 | 2016-02-24 | 김서희 | flower bady cosmetics |
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2016
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103263372A (en) * | 2013-05-24 | 2013-08-28 | 苏州工业园区黎姿化妆品有限公司 | Natural flower petal and cosmetic adopting same |
| KR20160020968A (en) * | 2014-08-15 | 2016-02-24 | 김서희 | flower bady cosmetics |
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| 黄洪周等: "《中国表面活性剂总览》", 31 August 2003, 化学工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107737058A (en) * | 2017-12-01 | 2018-02-27 | 绿馨颜（惠州）生物科技有限公司 | A kind of gold moisture retention water of biological carbohydrate gum 1 and preparation method thereof |
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