CN109820783A - A kind of discoloration method of plant petals - Google Patents
A kind of discoloration method of plant petals Download PDFInfo
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- CN109820783A CN109820783A CN201910222394.8A CN201910222394A CN109820783A CN 109820783 A CN109820783 A CN 109820783A CN 201910222394 A CN201910222394 A CN 201910222394A CN 109820783 A CN109820783 A CN 109820783A
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Abstract
The invention discloses a kind of discoloration methods for toner plant petals, belong to cosmetic field.It include: that plant petals, water, solvent are sequentially added into container by predetermined ratio;It is stirred and heated to the first preset temperature, and temperature-rise period is greater than or equal to 20 minutes;It is filtered after heat preservation decoloration under the conditions of the first preset temperature, respectively obtains plant petals and the filtrate of decoloration, and collect plant petals and the filtrate of decoloration respectively;It repeats decolorization at least once, obtains decoloration petal.The plant petals that more completely decolourize can be obtained using discoloration method of the invention, better appearance can be obtained by being added in product.The filtrate that the present invention obtains also can be carried out recycling, save the cost.
Description
Technical field
The present invention relates to cosmetic field, in particular to the discoloration method of the plant petals added in a kind of cosmetics.
Background technique
Prior art introduction
There are a kind of addition plant petals, and the cosmetics for making it suspend on the market.Since appearance is elegant, novel, this kind ofization
Cosmetic is more popular with consumers.But the pigment in petal will be slow dissolution, cause the change of product characteristics, influence product matter
Amount.And natural pigment in petal and unstable, oxidation or illumination can make its discoloration, and product appearance and quality is made to be deteriorated.Cause
The plant petals of this addition, which generally require, first carries out decolorization.At present generally using certain density ethyl alcohol to plant petals into
Row heating decoloration, makes the pigment in petal dissolve out and achieve the purpose that decoloration.
The technical problems existing in the prior art
Decoloration generally is carried out to plant to need to carry out break process to plant, cannot keep the integrality of plant petals, shadow
It rings beautiful.And heating decoloration is carried out to plant petals using certain density ethyl alcohol, certain ethyl alcohol residual is had, skin is made
At stimulation.
Summary of the invention
(1) goal of the invention
The object of the present invention is to provide a kind of discoloration method of plant petals, to solve plant petals decoloration, to have ethyl alcohol residual
It stays and skin is damaged, is difficult to obtain the problem of complete plant petals.By the present invention in that replacing ethyl alcohol with solvent and adding
To make plant petals decolourize, there is no the residuals of ethyl alcohol therefore will not damage to skin for heat and stirring, controls heating temperature
And mixing speed keeps the petal of decoloration more complete, better appearance can be obtained by being added in product.
(2) technical solution
To solve the above problems, the first aspect of the present invention provides a kind of decoloration side for toner plant petals
Method, comprising:
S1: plant petals, water, solvent are sequentially added into container by predetermined ratio;
S2: it is stirred and heated to the first preset temperature, and temperature-rise period is greater than or equal to 20 minutes;
S3: filtering after heat preservation decoloration under the conditions of the first preset temperature, respectively obtain plant petals and the filtrate of decoloration, and
Plant petals and the filtrate of decoloration are collected respectively;
S4: repeating step S1-S3 at least once, obtains decoloration petal.
Further, the step S1 is specifically included:
S11: the plant petals that parts by weight are 0.1~0.5 part are taken to be added in container;
S12: the water that parts by weight are 80~90 parts is taken to be added in container;
S13: it takes the solvent that parts by weight are 3~10 parts to be added in container, is uniformly mixed.
Further, the container is the water phase pot of homogenizer.
Further, the plant petals include roseleaf, safflower petal, pot marigold petal, one in sweet osmanthus petal
Kind is a variety of.
Further, the solvent includes glycerol, propylene glycol and/or butanediol.
Further, the S1 step specifically includes:
S11 ': taking parts by weight is 0.1~0.5 part of roseleaf, 0.1~0.5 part of safflower petal, 0.1~0.5 part of golden small cup
One of flower petal, 0.1~0.5 part of sweet osmanthus petal or a variety of addition containers;
S12 ': take the water that parts by weight are 80~90 parts that container is added;
S13 ': taking parts by weight is that stirring appearance is added in 3~8 parts of glycerol, 4~10 parts of propylene glycol and/or 4~10 parts of butanediols
Device is uniformly mixed.
Further, the S2 step specifically includes:
80~90 DEG C are stirred and heated to the revolving speed of 10~15r/min, and temperature-rise period is greater than or equal to 20 minutes.
Further, the S3 step specifically includes:
Heat preservation decoloration is filtered after 10~120 minutes under the conditions of 80~90 DEG C of temperature, respectively obtains the plant flowers of decoloration
Valve and filtrate, and plant petals and the filtrate of decoloration are collected respectively.
Further, in the S4, step S1-S3 is repeated twice to four times.
Another aspect of the present invention provides a kind of plant petals of decoloration, using plant flowers described in any of the above embodiments
The discoloration method of valve is prepared.
Another aspect of the present invention provides a kind of toner of plant petals containing decoloration, including above-mentioned decoloration
Plant petals.
Another aspect of the present invention provides a kind of filtrate, using the decoloration side of plant petals described in any of the above embodiments
Method is prepared.
Plant petals are picked, the beauty of final products can be guaranteed by removing impurity and damaged petal;Use plant
Petal, water, solvent lower temperature stir at low speed it is lower repeatedly decolourized, can not only plant petals decoloration thoroughly can also be maximum
The integrality of the guarantee plant petals of degree.
(3) beneficial effect
Above-mentioned technical proposal of the invention has following beneficial technical effect: method of the invention can make plant petals
Therefore decoloration will not damage skin without using ethyl alcohol, can obtain more complete plant petals, be added in product
It can obtain better appearance.
Specific embodiment
In order to make the objectives, technical solutions and advantages of the present invention clearer, With reference to embodiment, to this
Invention is further described.It should be understood that these descriptions are merely illustrative, and it is not intended to limit the scope of the invention.This
Outside, in the following description, descriptions of well-known structures and technologies are omitted, so as not to unnecessarily obscure the concept of the present invention.
According to the application embodiment, a kind of discoloration method for toner plant petals, including following step
It is rapid:
S1: plant petals, water, solvent are sequentially added into container by predetermined ratio.Wherein, water can be pure water, deionization
Water or cosmetics dedicated water, but be not limited to it is above-mentioned enumerate, preferably deionized water.
S2: it is stirred and heated to the first preset temperature, and temperature-rise period is greater than or equal to 20 minutes;Wherein heating time is excellent
Choosing is 20~60 minutes, is further preferably 25~45 minutes;In the present embodiment, heating can more than or equal to 20 minutes
Think 20 minutes, 21 minutes, 22 minutes, 23 minutes, 25 minutes, 28 minutes, 32 minutes, 37 minutes, 44 minutes, 48 minutes, 50
Minute, 55 minutes, 60 minutes etc. but be not limited to it is above-mentioned enumerate, can be appropriate according to the degree of the effect and dissolution that actually mix
Adjustment heating duration.
S3: filtering after heat preservation decoloration under the conditions of the first preset temperature, respectively obtain plant petals and the filtrate of decoloration, and
Plant petals and the filtrate of decoloration are collected respectively.Select suitable filter method that the complete of decoloration petal can be improved when wherein filtering
Whole degree, such as uses cartridge filter, and the control of the rate of filtration can also play same effect.
S4: repeating step S1-S3 at least once, obtains decoloration petal.
In an alternative embodiment, step S1 is specifically included:
S11: the plant petals that parts by weight are 0.1~0.5 part are taken to be added in container.
Wherein plant petals weight fraction can for 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1.0 parts, 1.1 parts,
1.2 parts, 1.3 parts, 1.4 parts, 1.5 parts etc. but be not limited to it is above-mentioned enumerate, can according to the actual situation it is appropriate adjustment petal weight
Amount number parts by weight, preferably 0.8~1.2 part.
S12: the water that parts by weight are 80~90 parts is taken to be added in container.In the present embodiment, the parts by weight weight of water
Number can be 80 parts, 81 parts, 82 parts, 83 parts, 84 parts, 85 parts, 86 parts, 87 parts, 88 parts, 89 parts, 90 parts etc. but be not limited to
It states and enumerates, it can be according to the parts by weight parts by weight of the content adjustment water appropriate of the effect and other materials that actually mix
Number, such as 75~95 parts, 65~88 parts.
S13: it takes the solvent that parts by weight are 3~10 parts to be added in container, is uniformly mixed.
In an alternative embodiment, container is the water phase pot of homogenizer.In the present embodiment, container can also have for other
The container of heating function.The utilization rate that equipment can be improved using the decoloration that water phase pot carries out plant petals, has saved cost.
In an alternative embodiment, plant petals include roseleaf, safflower petal, pot marigold petal, in sweet osmanthus petal
It is one or more.In the present embodiment, plant petals can also be plant petals such as lotus, chrysanthemum of other appearance looks elegants etc..
The cosmetics containing petal sold on the market generally only add a kind of plant petals, and in an embodiment of the present invention
It it is added to various plants petal, achieves unexpected progress in appearance, obtained more beautiful containing plant petals
Product.
In an alternative embodiment, solvent includes glycerol, propylene glycol and/or butanediol.Using glycerol, propylene glycol and/or
Butanediol this kind, which replaces ethyl alcohol as solvent in the solvent that makeup kind largely uses, can reduce stimulation of the ethyl alcohol to skin,
The cosmetics for making to add decoloration petal in the present embodiment do not stimulate mildly more.And use glycerol, propylene glycol and/or butanediol same
Sample can adjust the polarity of aqueous solution, dissolve out the pigment in plant petals and reach good decolorizing effect.
In an alternative embodiment, S1 step is specifically included:
S11 ': taking parts by weight is 0.1~0.5 part of roseleaf, 0.1~0.5 part of safflower petal, 0.1~0.5 part of golden small cup
One of flower petal, 0.1~0.5 part of sweet osmanthus petal or a variety of addition containers.
Wherein rose weight fraction can be 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1.0 parts, 1.1 parts, 1.2
Part, 1.3 parts, 1.4 parts, 1.5 parts etc. but be not limited to it is above-mentioned enumerate, can adjustment petal appropriate according to the actual situation parts by weight
Number parts by weight, preferably 0.8~1.2 part.
Wherein sweet osmanthus weight fraction can be 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1.0 parts, 1.1 parts, 1.2
Part, 1.3 parts, 1.4 parts, 1.5 parts etc. but be not limited to it is above-mentioned enumerate, can adjustment petal appropriate according to the actual situation parts by weight
Number parts by weight, preferably 0.8~1.0 part.
Wherein pot marigold weight fraction can be 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1.0 parts, 1.1 parts, 1.2
Part, 1.3 parts, 1.4 parts, 1.5 parts etc. but be not limited to it is above-mentioned enumerate, can adjustment petal appropriate according to the actual situation parts by weight
Number parts by weight, preferably 0.8~1.3 part.
Wherein safflower weight fraction can be 0.5 part, 0.6 part, 0.7 part, 0.8 part, 0.9 part, 1.0 parts, 1.1 parts, 1.2
Part, 1.3 parts, 1.4 parts, 1.5 parts etc. but be not limited to it is above-mentioned enumerate, can adjustment petal appropriate according to the actual situation parts by weight
Number parts by weight, preferably 0.9~1.2 part.
S12 ': take the water that parts by weight are 80~90 parts that container is added.
S13 ': taking parts by weight is that stirring appearance is added in 3~8 parts of glycerol, 4~10 parts of propylene glycol and/or 4~10 parts of butanediols
Device is uniformly mixed.
The parts by weight parts by weight of glycerol can be 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts etc. but be not limited to above-mentioned column
It lifts, can be according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~10 parts etc..
The weight fraction of propylene glycol can for 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts etc. but be not limited to it is above-mentioned enumerate,
Can be according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~15 parts etc..
The weight fraction of butanediol can for 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts etc. but be not limited to it is above-mentioned enumerate,
Can be according to the effect actually mixed adjustment appropriate, such as can be 2~6 parts, 5~15 parts etc..
In an alternative embodiment, S2 step is specifically included:
80~90 DEG C are stirred and heated to the revolving speed of 10~15r/min, and temperature-rise period is greater than or equal to 20 minutes.Its
Middle r/min be stirring revolving speed, for rpm, revolving speed can be 10r/min, 11r/min, 12r/min, 13r/min, 14r/
Min, 15r/min etc. but be not limited to it is above-mentioned enumerate, can according to the effect actually mixed adjustment appropriate, such as can for 5~
12r/min, 8~20r/min etc..
Wherein heating temperature can also be 80 DEG C, 81 DEG C, 82 DEG C, 83 DEG C, 84 DEG C, 85 DEG C, 86 DEG C, 87 DEG C, 88 DEG C, 89
DEG C, 90 DEG C but be not limited to above-mentioned enumerate.For example, can be increased or decreased according to environmental condition is appropriate to the first preset temperature,
It such as can be 80~100 DEG C, or be 70~85 DEG C.
In an alternative embodiment, S3 step is specifically included:
Heat preservation decoloration is filtered after 10~120 minutes under the conditions of 80~90 DEG C of temperature, respectively obtains the plant flowers of decoloration
Valve and filtrate, and plant petals and the filtrate of decoloration are collected respectively.
Wherein bleaching time is preferably 20~100 minutes, is further preferably 30~80 minutes, still more preferably
It is 40~60 minutes.Can for 40 minutes, 41 minutes, 42 minutes, 43 minutes, 44 minutes, 45 minutes, 46 minutes, 47 minutes,
48 minutes, 49 minutes, 50 minutes, 51 minutes, 52 minutes, 53 minutes, 54 minutes, 55 minutes, 56 minutes, 57 minutes, 58 minutes,
It 59 minutes, 60 minutes can also be for such as 21 minutes, 22 minutes, 23 minutes, 24 minutes, 25 minutes, 36 minutes, 37 minutes, 38 points
Clock, 39 minutes, 70 minutes, 71 minutes, 72 minutes, 73 minutes, 84 minutes, 85 minutes, 86 minutes, 87 minutes, 98 minutes, 99 points
Clock, 100 minutes etc. but be not limited to it is above-mentioned enumerate, can according to the degree adjustment appropriate of the effect and dissolution that actually mix plus
The duration of heat.
The filtrate after fading can also wherein be reused.The investment of equipment can be reduced.Promote the function of product
Effect and appearance further reduce the cost, and reduce environmental pressure.Filtrate collect after enter the comprehensive utilization stage, carry out flavones, pigment,
The effective components such as saponin(e, these ingredients can do the raw material of other cosmetics, if pigment can do the coloring of other things, saponin(e,
Flavones is common Effect raw material in cosmetics, this process is related to the concentration and purification of filtrate.
In an alternative embodiment, in S4, step S1-S3 is repeated twice to four times.
Carrying out repeatedly decoloration can be such that pigment in plant petals sloughs more thoroughly, wherein decoloration number can be according to petal
Difference and increased or decreased, can for 1 time, 2 times, 3 times, 4 it is inferior but be not limited to it is above-mentioned enumerate, can be according to practical de-
The adjustment appropriate of the effect of color, such as 2~3 times, 5~6 times.
Embodiment 1
Taking parts by weight is that container is added in 0.1 part of roseleaf;Take the water that parts by weight are 80 parts that container is added;Take weight
Number is 3 parts of glycerol, 4 parts of propylene glycol addition stirring containers, is uniformly mixed.
80 DEG C are stirred and heated to the revolving speed of 10r/min, and temperature-rise period is 20 minutes.Under the conditions of 80 DEG C of temperature
Heat preservation decoloration is filtered after ten minutes, respectively obtains roseleaf and the filtrate of decoloration, and collect the plant rose of decoloration respectively
Valve and filtrate.
It repeats step above-mentioned steps twice, obtains the complete roseleaf that decolourizes.
Embodiment 2
Taking parts by weight is that container is added in 0.3 part of roseleaf;Take the water that parts by weight are 85 parts that container is added;Take weight
Number is 6 parts of glycerol, 8 parts of propylene glycol addition stirring containers, is uniformly mixed.
85 DEG C are stirred and heated to the revolving speed of 13r/min, and temperature-rise period is 25 minutes.Under the conditions of 85 DEG C of temperature
Heat preservation decoloration filter after sixty minutes, respectively obtain roseleaf and the filtrate of decoloration, and collect respectively decoloration roseleaf and
Filtrate.
It repeats step above-mentioned steps 3 times, obtains the complete roseleaf that decolourizes.
Embodiment 3
Taking parts by weight is that container is added in 0.5 part of safflower petal;Take the water that parts by weight are 90 parts that container is added;Take weight
Number is 8 parts of glycerol, 10 parts of propylene glycol addition stirring containers, is uniformly mixed.
90 DEG C are stirred and heated to the revolving speed of 15r/min, and temperature-rise period is 30 minutes.Under the conditions of 90 DEG C of temperature
Heat preservation decoloration 120 minutes after filter, respectively obtain safflower petal and the filtrate of decoloration, and collect respectively decoloration safflower petal and
Filtrate.
It repeats step above-mentioned steps four times, obtains the complete safflower petal that decolourizes.
Embodiment 4
Parts by weight are taken to be 0.4 part of roseleaf, the water phase pot that homogenizer is added in 0.2 part of sweet osmanthus petal;Take parts by weight
The water phase pot of homogenizer is added for 82 parts of water;Taking parts by weight is that 6 parts of glycerol, 6 parts of propylene glycol and 10 parts of butanediols additions are even
The water phase pot of matter machine is uniformly mixed.
88 DEG C are stirred and heated to the revolving speed of 14r/min, and temperature-rise period is 35 minutes.Under the conditions of 88 DEG C of temperature
Heat preservation decoloration 90 minutes after filter, respectively obtain plant petals and the filtrate of decoloration, and collect respectively decoloration plant petals and
Filtrate.
It repeats step above-mentioned steps 3 times, the plant petals to be decolourized completely.
Embodiment 5
Parts by weight are taken to be 0.2 part of safflower petal, the water phase pot that homogenizer is added in 0.4 part of pot marigold petal;Take parts by weight
The water phase pot of homogenizer is added in the water that number is 87 parts;Parts by weight are taken to be 7 parts of glycerol, the water phase that homogenizer is added in 4 parts of butanediols
Pot is uniformly mixed.
83 DEG C are stirred and heated to the revolving speed of 11r/min, and temperature-rise period is 28 minutes.Under the conditions of 87 DEG C of temperature
Heat preservation decoloration 35 minutes after filter, respectively obtain plant petals and the filtrate of decoloration, and collect respectively decoloration plant petals and
Filtrate.
It repeats step above-mentioned steps 2 times, the plant petals to be decolourized completely.
The test of user's use feeling Contrast on effect
(1) test specimen: the toner of decoloration roseleaf prepared by addition embodiment 2;Certain commercially available roseleaf
Adornment water.
(2) subject: 60 healthy males and women (each 30), the age was at 20~40 years old.Male and female respectively with
Machine is divided into two groups, is named as A group and B group (respectively containing male 15, women 15).
(3) application method: before sleeping at night and after morning warm water face cleaning, appropriate test specimen is taken to be applied to the centre of the palm, later gently
It pats and beats cheek 1 minute, to promote the absorption of test specimen effective component;Subject does not use other changes during the test
Cosmetic.
(4) judgment criteria: test two months by a definite date is tested subject after expiring and is commented the trial target that oneself is used
Valence is divided into sensory evaluation scores and whether is interested in continuing with use, is respectively divided into three grades.
(5) test structure is shown in Table 1
1 user's use feeling Contrast on effect measuring unit of table: people
As seen from the above table, after 30 subjects, being comfortable on is 25 people, satisfaction 83%;It is interested in continuing with and uses
26 people, account for 86.6%.And using the subject of certain commercially available roseleaf suspension toner is 56.6% to its satisfaction, only
There is 50% subject to be interested in continuing with use.From the foregoing, it will be observed that the toner of the decoloration roseleaf prepared using addition embodiment 2
Use feeling is good, does not stimulate, and receives subject and likes.
Decoloration plant petals integrated degree comparison
(1) test specimen: the decoloration petal prepared by 1-5 of the embodiment of the present invention.
(2) contrast sample: certain commercially available petal toner 1 (roseleaf), certain commercially available petal toner 2 (safflower petal).
(3) test method: the percentage of head rice of the decoloration petal of Statistics Implementation example 1-5 preparation, it will be in certain commercially available petal toner
Petal take out, count its percentage of head rice.Wherein percentage of head rice is the ratio between integral petal number and whole petal numbers, wherein statistics is every
The petal weight of a sample is identical.Record is as shown in table 2.
The decoloration plant petals integrated degree comparison of table 2
The petal of the decoloration obtained as seen from the above table by discoloration method of the invention is than the plant in commercially available petal toner
Object petal is more complete thus more beautiful.
Claims (10)
1. a kind of discoloration method for toner plant petals characterized by comprising
S1: plant petals, water, solvent are sequentially added into container by predetermined ratio;
S2: it is stirred and heated to the first preset temperature, and temperature-rise period is greater than or equal to 20 minutes;
S3: filtering after heat preservation decoloration under the conditions of the first preset temperature, respectively obtains plant petals and the filtrate of decoloration, and respectively
Collect plant petals and the filtrate of decoloration;
S4: repeating step S1-S3 at least once, obtains decoloration petal.
2. the discoloration method of plant petals according to claim 1, which is characterized in that the step S1 is specifically included:
S11: the plant petals that parts by weight are 0.1~0.5 part are taken to be added in container;
S12: the water that parts by weight are 80~90 parts is taken to be added in container;
S13: it takes the solvent that parts by weight are 3~10 parts to be added in container, is uniformly mixed.
3. the discoloration method of plant petals according to claim 1, which is characterized in that the plant petals include rose
One of valve, safflower petal, pot marigold petal, sweet osmanthus petal are a variety of;
The solvent includes glycerol, propylene glycol and/or butanediol.
4. the discoloration method of plant petals according to claim 2, which is characterized in that the S1 step specifically includes:
S11 ': taking parts by weight is 0.1~0.5 part of roseleaf, 0.1~0.5 part of safflower petal, 0.1~0.5 portion of pot marigold
One of valve, 0.1~0.5 part of sweet osmanthus petal or a variety of addition containers;
S12 ': take the water that parts by weight are 80~90 parts that container is added;
S13 ': taking parts by weight is that stirring container is added in 3~8 parts of glycerol, 4~10 parts of propylene glycol and/or 4~10 parts of butanediols,
It is uniformly mixed.
5. the discoloration method of plant petals according to claim 1, which is characterized in that the S2 step specifically includes:
80~90 DEG C are stirred and heated to the revolving speed of 10~15r/min, and temperature-rise period is greater than or equal to 20 minutes.
6. the discoloration method of plant petals according to claim 1, which is characterized in that the S3 step specifically includes:
Under the conditions of 80~90 DEG C of temperature heat preservation decoloration 10~120 minutes after filter, respectively obtain decoloration plant petals and
Filtrate, and plant petals and the filtrate of decoloration are collected respectively.
7. the discoloration method of plant petals according to claim 1, which is characterized in that in the S4, repeat step S1-S3
Twice to four times.
8. a kind of plant petals of decoloration, which is characterized in that using the decoloration of the described in any item plant petals of claim 1-7
Method is prepared.
9. a kind of toner of the plant petals containing decoloration, which is characterized in that planted including decolourizing as claimed in claim 10
Object petal.
10. a kind of filtrate, which is characterized in that prepared using the discoloration method of the described in any item plant petals of claim 1-7
It forms.
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CN111956525A (en) * | 2020-09-17 | 2020-11-20 | 佛山市南海区桂城埃菲尔化妆品有限公司 | Petal shower gel and preparation method thereof |
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